Makmal KKM List

Skim Akreditasi Makmal Malaysia (SAMM) No.
Any details on food matrix of sampel (materials/products) tested by the laboratories, please
refer to website http://www.jsm.gov.my/cab-directories
BIL. LABORATORY SAMM NO.

1 MKKM Perlis 203 0203
2 MKKM Kedah 327
3 MKKM Pulau Pinang 337
4 MKKM Selangor 159
5 MKKM Kelantan 339
6 MKKM Terengganu 340
7 MKKM Pahang 344
8 MKKM Sarawak 239
9 MKKM Miri 334
10 MKKM Sandakan 348
11 MKA Kebangsaan, Sg. Buloh 267
12 MKA Ipoh 345
13 MKA Johor Bahru 208
14 MKA Kota Bharu 797
15 MKA Kota Kinabalu 349
MKKM - Makmal Keselamatan dan Kualiti Makanan

MKA - Makmal Kesihatan Awam
M) No.
tories, please
VETERINARY DRUG RESIDUES AND SCHEDULED POISONS
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
DOC. NO TEST METHOD REFERENCE PARAMETER FOOD MATRIX
MIRI
(µg/kg)
MOH D03-001 Determination of Anthelmintics in Muscle by Leo M.L. Nollet. 2000. Second Edition. Food Thiabendazole Meat & Meat 5
HPLC Analysis by HPLC Products, Fish & Fish A
Flubendazole Products 10
A
MOH D03-002 Determination of Antibacterial Residues in Leo M.L. Nollet. 2000. Second Edition. Food Sulfamerazine Meat & Meat 20
muscle by High Performance Liquid Analysis by HPLC Products, Fish & Fish A NA A A A A A A A
Chromatography Products
Sulfadimidine 40-50
A NA A NA NA A A A A
Pyrimethamine 50
NA A NA NA
Sulfamonomethoxine 30
A NA A NA A A A A A
Oxolinic acid 40-50

A NA A A A A A A NA
Sulfadimethoxine 40
A NA A A A A A A NA
Difurazone 100
A
Sulfaquinoxaline 40-50
A NA A NA A A A A NA
Nicarbazine 20
A NA A A A A A A
Sulfadiazine 40
A NA A A A A A A NA
Sulfathiazole 40
A NA A A NA A A A NA
MOH D03-003 Determination of Tetracyclines in Muscle by Modification AOAC 995.05, 2000 Oxytetracycline Meat & Meat 40
High Performance Liquid Chromatography Products, Fish & Fish A NA NA A A A
Products
Tetracycline 40
A NA NA A A A
Chlortetracycline 60
A NA NA A A A
Doxycycline 40
A NA NA A A A
MOH D03-004 Determination of Enrofloxacin in Muscle by Leo M.L. Nollet. 2000. Second Edition. Food Enrofloxacin Meat and Meat 30
High Performance Liquid Chromatography Analysis by HPLC Products A
MOH D03-005 Determination Of Lasalocid Sodium in Leo M.L. Nollet. 2000. Second Edition. Food Lasalocid Sodium Meat and Meat 30
Muscle by High Performance Liquid Analysis by HPLC Products NA
Chromatography
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-006 Determination Of Nitrofuran Metabolite Journal of Chromatography A, 939 (2001) Furazolidone metabolite : AOZ Meat & Meat 1
Residues in Muscle by Liquid Products, Fish & Fish A NA A A A A
Chromatography Tandem Mass Furaltadone metabolite : AMOZ Products 1
Spectrometry A NA A A A A
SEL- muslce, honey
Nitrofurantoin metabolite : AHD and egg 1
NA A NA A NA
Nitrofurazone metabolite : SEM 1

NA NA A A A NA
MOH D03-007 Determination of Chloramphenicol in Muscle Journal of Chromatography A, 994 (2003) Chloramphenicol (CAP) Meat & Meat 0.2
by Liquid Chromatography Tandem Mass Products, Fish & Fish
Spectrometry Products A A
MOH D03-008 Determination of Antibacterial Residues in Journal of Chromatography B, 774 (2002) Sulfadiazine Egg 40
NA NA NA NA NA A NA
Eggs by High Performance Liquid
Chromatography Sulfathiazole 40
NA NA NA NA NA A NA
Sulfapyridine 40
NA NA NA NA A NA
Sulfamerazine 40
NA NA NA NA NA A NA
Sulfadimidine 20
NA NA NA NA NA A NA
NA NA NA NA NA A NA
Sulfadimethoxine 20
NA NA NA NA NA A NA
Sulfaquinoxaline 40
NA NA NA NA NA A NA
MOH D03-009 Determination of Chloramphenicol in Honey Poster B105, 5th International Symposium Chloramphenicol (CAP) Honey 0.05-0.2
by Liquid Chromatography Tandem Mass on Hormone and Veterinary Drug Residue
Spectrometry Analysis, Antwerp, Belgium, May 16-19, A A A A A A
2006
MOH D03-010 Screening analysis of Beta-Agonist Kit Instruction Manual Clenbuterol Meat and Meat 1
(Clenbuterol) in Animal Tissue using Bioo Products and Fish NA
Scientific Test Kit and Fish Products
MOH D03-011 Screening analysis of Beta Agonist using Kit Instruction Manual Salbutamol Meat & Meat 1
Romerlabs test Kit Products, Fish & Fish NA
Products
MOH D03-012 Screening analysis of Chloramphenicol Kit Instruction Manual Chloramphenicol (CAP) Meat & Meat 0.3-1
using Romerlabs test Kit Products, Fish & Fish A NA
Products
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-013 Determination of Multi-residue Veterinary Journal of Chromatography A, 1205 (2008) Albendazole Milk 10
Drugs in Milk and Milk Products by Liquid A NA
Chromatography Mass Spectrometry and Chloramphenicol (CAP) 0.2
Tandem Mass Spectrometry A NA
Florfenicol 0.5
A NA
Oxfendazole 10
A NA
Sulphadimidine 10
A NA
Sulphadimethoxine 5
A NA
Thiabendazole 10
A NA
Thiamphenicol 0.5
A NA
Sulphadiazine 5
NA
Sulphathiazole 5
NA
Sulphamerazine 5
NA
Sulphamonomethoxine 5
NA
Sulphaquinoxaline 5
NA
Sulphapyridine 5
NA
2-amino-albendazole sulfone 10
NA
Albendazole Sulfoxide 10
NA
Albendazole sulfone 10
NA
Flubendazole 10
NA
Mebendazole 10
NA
Febantel 10
NA
Fenbendazole 10
NA
Oxibendazole 10
NA
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-014 Determination of Beta-agonists in Muscle by SOP ARO/480 (2005), National Public Clenbuterol Meat & Meat 0.1
Liquid Chromatography Tandem Mass Health and Environment, Netherlands, Products NA
Spectrometry after Molecular Imprinted Cimaterol 0.1
Polymers clean-up NA
Mabuterol 0.1
NA
Terbutaline 0.1
NA
Ractopamine 0.1
NA
Salbutamol 0.1
NA
MOH D03-015 Determination of Triphenylmethane Dyes in (a) Analytica Chimica Acta 586 (2007) Malachite Green Fish & Fish Products 0.5
Fish and Fish Products by Liquid A A
Chromatography Tandem Mass (b) J. Agric Food Chemistry Leucomalachite Green 1
Spectrometry A A
Crystal Violet 1
NA NA
Leucrystal Violet 1
NA NA
MOH D03-016 Screening Analysis of Nitrofuran (AMOZ & Kit Instruction Manual Furazolidone metabolite : AOZ Fish, shrimp, meat, 0.5
AOZ) using Bioo Scientific Test Kit egg, honey and milk NA
Furaltadone metabolite : AMOZ 0.5

NA
MOH D03-017 Determination of Benzimidazole Residues in (a) Leo M.L. Nollet. 2000. Second Edition. 2-amino-albendazole sulfone Meat & Meat 1
Muscle by Liquid Chromatography Tandem Food Analysis by HPLC Products, Fish & Fish A A A A A
Mass Spectrometry Albendazole sulfone Products 1
(b) Journal of Chromatography, A A A A A
498 (1990)
Fenbendazole 1
A A A A A
Oxfendazole 1
A A A A A
Thiabendazole 1
A A A A A
Albendazole 1
A NA A A A
Flubendazole 1
A A A A A
Mebendazole 1
A A A A A
Albendazole Sulfoxide 1
A A A A A
Febantel 1
A A A A A
Oxibendazole 1
NA
Triclabendazole 1
NA
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-018 Determination of Nitroimidazole Residues in Journal of Chromatography A, 882 (2000) Dimetridazole metabolites Fish and Fish 1
Muscle by Liquid Chromatography Tandem Products and meat A A A NA
Mass Spectrometry Metronidazole and meat product 0.5
A A A NA
Ronidazole 0.2
A A A NA
Metronidazole Hydroxy
A
MOH D03-019 Determination of synthetic Peng Zou et.al.2006. Journal of Tadalafil Herbal dietary 1mg/kg
phosphodiesterase- 5 (PDE-5) inhibitors in Chromatography A, 1104(2006) 113-112. supplement A NA A NA
Food using Liquid Chromatography vardenafil 1mg/kg
A NA A NA
sildenafil 1mg/kg
A NA A NA
Analog PDE5 20
NA NA
20
Analog Sibutramine NA NA
MOH D03-020 Determination of Quinolones and Master Thesis of Marni Sapar UM 2010 Ciprofloxacin Meat & Meat 5
Fluoroquinolones Residues In Muscle and Products, Fish & Fish NA NA A A NA
Egg by Liquid Chromatography Tandem Enrofloxacin Products 5
Mass Spectrometry NA NA A A NA
Difloxacin 5
NA NA NA A NA
Sarafloxacin 5
NA NA A A NA
Danofloxacin 10
NA NA A A NA
Marbofloxacin 2
NA NA A A NA
Norfloxacin 5
NA NA A A NA
Oxolinic acid 5
NA NA A NA
MOH D03-021 Determination of Phenicol Residues in Journal of Chromatography B, 875 (2008) Chloramphenicol (CAP) Meat and Meat 0.2
MUscle by Liquid Chromatography Tandem Products and Fish A A A A A
Mass Spectrometry Florfenicol and Fish Products 0.5
A A A A A
Thiamphenicol 0.5
A A A A A
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-022 Determination of Antibacterial Residue in Acta Chromatographica (2006) 17, page Sulfadiazine Honey 5
Honey by High Performance Liquid 320-327 QuEChERS Method, LCMSMS A
Chromatography Sulfathiazole 10
A
Sulfapyridine 10
A
Sulfamerazine 10
A
Sulfadimidine 10
A
A
Sulfadimethoxine 1
A
Sulfaquinoxaline 5
A
MOH D03-023 Determination of Amphenicol in Muscle and Nollet, L.M.L; Toldora, F. 2009. Handbook of Chloramphenicol (CAP) Honey, Meat and 0.2
Honey by Ultra Performance Liquid Muscle Food Analysis Meat Products A
Chromatography Tandem Mass Florfenicol 0.2
Spectrometry A
Thiamphenicol 0.2
A
MOH D03-024 Determination of Macrolides In Meat and Journal Agric. Food Chem. 56, (2008) Erythromycin Meat and Meat 10
Meat Products by Liquid Chromatography Products A
Tandem Mass Spectrometry Lincomycin 10
A
Tylosin 10
A
MOH D03-025 Determination of Tetracycline In Milk and Journal of Chromatography A, 987 (2003) Oxytetracycline Milk and Muscle 60
Muscle by High Performance Liquid (MKAI - 10) NA NA NA
Chromatography Tetracycline 610
(MKAI - 10) NA NA NA
Chlortetracycline 80
Doxycycline 80
MOH D03-026 Determination of Macrolides in Honey by Agilent Technologies Application Note 5991- Erythromycin Honey 3
Liquid Chromatography Tandem Mass 3190 (2013) A
Spectrometry Tylosin 3
A
Lincomycin 3
A
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-027 Determination of β-agonists in Meat and Modification AFRL for VDR Workshop 2013: Clenbuterol Meat and Meat 0.5
Meat Products with SPE purification by Analytical Method for beta-Agonist, 13th - Products A NA NA A A
Liquid Chromatography Tandem Mass 16th August 2013; Cimaterol 0.5
Spectrometry A NA A A
Mabuterol 0.5
A NA A A
Terbutaline 1
A NA NA A A
Ractopamine 0.5
A NA NA A A
Salbutamol 1
A NA NA A A
MOH D03-028 Determination of Anthelmintic Avermectin In Kinsella, B., et al (2009). Analytica Chimica Emamectin Fish and Fish Product 1
Fish and fish product by Liquid Acta, 637(1-2), 196-207 A
Chromatography Tandem Mass
Spectrometry Doramectin NA
Ivermectin NA
MOH D03-029 Determination of Triphenylmethane Dyes by Hurtaud-Pessel,D., Couëdor,P., Verdon, Malachite Green Fish and Fish Product 0.5
Solvent Extraction in Fish and Fish products P.E. (2011). Journal of Chromatography A, (MKAI - 0.2) NA A NA
by Liquid Chromatography Tandem Mass 1218 (2011) 1632–1645
Leucomalachite Green 0.5
Spectrometry NA A NA
(MKAI - 0.2)
Crystal Violet 0.5
(MKAI - 0.2) NA A NA
Leucrystal Violet 0.5

(MKAI - 0.2) NA A NA
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-030 Determination of Multi residue Antibacterial S., George & B., Timothy. (2009). Analytica Danofloxacin Fish and Fish 10
in muscle using dispersive solid phase Chimica Acta 637 (2009) 68-78. Product, Meat and A NA A NA
extraction by Liquid Chromatography Meat Products
Tilmicosin 10
Tandem Mass Spectrometry A A NA
Oxolinic acid 10
NA A NA
Difloxacin 5
A NA A NA
Trimetoprim 5
A A NA
(MKAI - 10)
Sulfadiazine 2
(MKAI - 10) NA A NA
(MKAI - 10) NA A NA
Sulfadimidine 4
(MKAI - 10) NA A NA
Ormetoprim 1
(MKAI - 10) A NA
Sulfathiazole 2
(MKAI - 10) NA A NA
Sulfadimethoxine 3
(MKAI - 10) NA A NA
Sulfaquinoxaline 4
(MKAI - 10) NA A NA
Sulfapyridine 5
(MKAI - 10) A NA
Sulfamerazine 6
(MKAI - 10) NA A NA
MOH D03-031 Determination of Multi residue Antibacterial Marilena E. Dasenaki and Nikolaos S. Sulphadiazine Meat and Meat 1
in muscle using solvent extraction by Liquid Thomaidis, . 2010. Analytica Chimica Acta. Products, Fish and NA
Chromatography Tandem Mass 672 (2010) 93-102 Fish Product
Sulphathiazole 1
Spectrometry NA
Sulphamerazine 0.5
NA
Sulphadimidine 1
NA
Sulphamonomethoxine 1
NA
Pyrimethamine 1
NA
Oxolinic Acid 1
NA
Sulphaquinoxaline 1
NA
Sulphadimethoxine 1
NA
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
IPOH
MIRI
(µg/kg)
MOH D03-032 Determination of Aminoglycoside Residues J. B. Arsand, L. Jank, M. T. Martins, R. B. Streptomycin Milk and Muscle Milk:40
in Milk and Muscle by Liquid Hoff, F. Barreto, T. M. Pizzolato and C. Muscle:50 NA
Chromatography Tandem Mass Sirtori, Talanta, 2016, 154, 38-45.
Dihydrostreptomycin Milk:40
Spectrometry NA
Muscle:50
Spectinomycin Milk:40
Muscle:30 NA
Gentamycin Milk:20 Muscle:5

NA
Kanamycin Milk:30
Muscle:10 NA
Neomycin Milk:200
Muscle:50 NA
Apramycin Milk:10
Muscle:100 NA
Paromomycin Milk:10
Muscle:50 NA
MOH D03-33 Determination of Colistin In Muscle by Liquid Qin F., Xiaowei L., Kangni Z., Yuebin K., Colistin A Meat 50
Chromatography Tandem Mass Yingxu W., Lina W., Fugen Y., and Xi X.,
Spectrometry (2018) Determination of Colistin In Animal NA
Tissues, Egg, Milk, And Feed by Ultra High-
Performance Liquid Chromatography
Tandem Mass Spectrometry. J. Food Chem Colistin B 50
248, 166 - 172. NA
NA Capable but not accredited ISO/IEC 17025

A Capable and accredited ISO/IEC 17025
FOOD ADDITIVES
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
DOC. NO TEST METHOD REFERENCE PARAMETER FOOD MATRIX LOQ
MIRI
MOH E03-001 Qualitative Test of Boric Acid AOAC , Vol. II (1995), Chapter 47 Boric Acid Noodle / Kuey teow / 10-40 mg/kg,
and Borates in Food Fish ball / Fish 20 mg/kg (MKAK)
cake/Other foods 20 mg/kg (MKKM PS) A A A A A A A A A A A A
MOH E03-002 The Determination of Benzoic Food J. Assoc. Off. Anal. Chem. Benzoic & Sorbic acid All types of food 20 - 100 mg/kg
Acid and Sorbic Acid in Food 70 (5) 50 mg/kg (MKKM PS) A A A A A A A NA A A A
Using Liquid Chromatography
Bread, flour, Coconut 5 - 20 mg/kg
milk, cream NA A NA NA
Cheese 30 mg/kg
NA NA A
Bread, flour, sauce, 20 mg/kg

juice A
Coconut Milk, cream 5 mg/kg

A
Sauce, juice, chilly 30 mg/kg

slurry, soft drink, pasta,
preserved dried fruit,
A
fish and fish product
Fish and Fish Products 30 mg/kg

NA
Other types of food 30 mg/kg

NA
The Determination of Water AOAC (19750). Selected types of

Permitted Colour
MOH E03-003 Allura Red AC 50 - 500 mg/kg

Soluble Synthetic Food Colour 12th edition. Chapter 34 food** A A NA A A NA A A A
in Food by Chromatography
Paper and UV/VIS Amaranth
Spectrophotometer A A NA A A NA A A NA
Brilliant Black
PN A A A NA A A NA
Brilliant Blue
FCF NA A NA A A NA A A A
Carmoisine
NA A NA A A A A A A
Chocolate
Brown HT A NA A A NA
Erythrosine BS
A A NA A NA NA A A NA
Fast Green
FCF A NA NA A NA A A NA
Green S
A A NA A NA A A NA
Indigotine
A A NA NA NA NA A A NA
Ponceau 4R
NA A NA A A NA A A NA
Sunset Yellow
FCF A A NA A A A A A A
Tartrazine
A A NA A A A A A A
Quinoline
Yellow A A NA A A NA A A NA
Ponceau 6R
A
Non-Permitted Colour
Auromine o
NA NA NA A A NA
Orange 11
A NA NA A A NA
Fast Yellow AB
A A NA
Naphtol Yellow
S NA NA A A NA
Red 2G
NA NA NA A A NA
Rhodamine B
A A NA NA NA NA A A NA
Patent Blue V
A NA NA NA A A A
MOH E03-004 The Determination of Synthetic (a) AOAC Official Method 983.15, Butylated hydroxyanisol Edible Fat and Edible 4 - 10 mg/kg
Antioxidants (BHA & BHT) in Ch.47 (BHA) Oil NA A A
Fats, Oils, and Butter Oil by
Liquid Chromatography (b) AOAC International,
16th Edition, Butylated hydroxytoulene 4 - 20 mg/kg
Volume II, 1996 (BHT) NA A A
Oil Soluble Colour (Prohibited Colour)
MOH E03-005 Determination of Synthetic (a) ASTA (American Spice Trade Para Red Selected types of 3 - 15 mg/kg
Colours in Food Using Liquid Association) 2005 food** NA NA A NA
Chromatography
(b) Yoshioka (2008) - Talanta. Vol. Dimethyl 6 mg/kg
74 Yellow NA A NA
(c ) Katerina S. M., Christina. F. Sudan 1 3-6 mg/kg

NA NA A NA
S., Nikolaos. S. T., 2007. Analytica
Chimica Act.Vol. 583, page 103 – Sudan 2 3 mg/kg
110. NA NA A NA
Sudan 3 6 mg/kg
NA NA A NA
Sudan 4 15 mg/kg
NA NA A NA
Water Soluble Colour (Permitted Colour)
Allura Red AC Liquid/ Semi Solid:

3 - 20 mg/kg NA NA A A A NA NA A NA A
Amaranth Solid:
10-20 mg/kg NA NA A A A NA NA A NA A
Brilliant Black
PN NA NA NA NA NA NA A NA A
Brilliant Blue
FCF NA NA A A A NA NA A NA A
Solid:
Water Soluble Colour (Permitted

10-20 mg/kg
Chocolate
Brown HT NA NA NA NA A NA
Carmoisine
NA NA A NA A NA NA A NA A
Erythrosine BS
NA NA NA A NA NA A NA
Fast Green
FCF NA NA A NA NA NA NA A NA A
Green S
NA NA NA A NA NA A NA A
Indigotine
NA NA NA NA NA NA NA A NA A
Ponceau 4R
NA A A A NA NA A NA A
Sunset Yellow
FCF NA NA A A A NA NA A NA A
Tartrazine
NA NA A A A NA NA A NA A
Quinoline
Yellow NA NA A NA NA NA A NA
Ponceau 6R
NA
Water Soluble Colour

(Non-Permitted Colour)
Red 2G
NA NA NA
Orange 11
NA NA NA NA A
Patent Blue V
NA NA A NA NA NA NA A
MOH E03-006 The Determination of JAOAC (Lawrence et al) Vol. 71, 20mg/kg
Saccharin and Cyclamate in No 5, 1988 Soft Drink 80mg/kg (MKKM PS) A A A
Food using Liquid
Chromatography 20 mg/kg
Saccharin Preserved fruit 80 mg/kg (MKKM PS) A A NA
Other types of food** 20 mg/kg

80 mg/kg (MKKM PS) A A A A A A A NA NA A A NA
Cyclamate 120 mg/kg

Soft Drink 80 mg/kg (MKKM PS) A A A
100 mg/kg
Preserved fruit 80 mg/kg (MKKM PS) A A NA
Other types of food** 120 mg/kg

80 mg/kg (MKKM PS) A A A A A A A NA NA A A NA
MOH E03-007 The Determination of Sulphites AOAC Official Method 961.09. Sulfur Dioxide Pasta 10 mg/kg
calculated as Sulphur Dioxide 17th edition. (qualitative) A A NA A NA A A A A NA
in Food by Titration Vol. II. Chapter 47
Sulfur Dioxide Fish and Fish Products 10 mg/kg
(quantitative) 10 mg/kg (MKKM PS) A A A NA A NA A A A A NA
MOH E03-008 Determination of Aspartame (a) Journal of Food Hygiene Aspartame Soft Drink 100 mg/kg, 50 mg/L (PS)
and Phenylalanine in Soft Society of Japan, Vol. 33: , 1992.
Drink by High Performance A A A NA
Liquid Chromatography (b) Rapid Analysis Methods for
Pesticide Residues, Hygiene and
Chemistry, No. 48, April 8,1997. Phenylalanine 10 mg/L (MKKM PS)
A A A NA
MOH E03-009 Determination of Acesulfame K European Standard Acesulfame Potassium Beverages 2.5 - 10.0 mg/L
using by High Performance EN 12865 10 mg/L (MKKM Ps)
Liquid Chromatography A A NA NA NA A A NA
MOH E03-010 The Determination of Sulphites (a) Egan,H et al.(1981) Pearson's Sulfur Dioxide Selected types of 30 mg/kg
calculated as Sulphur Dioxide Chemical Analysis of Food food**
in Food using Monier- Williams (8th.Ed)
Method
(b) AOAC 16th Ed . Vol .II (1995), A A
AOAC Official Method 932.16,
Chap.47
MOH E03-011 The Determination of Propionic Isshiki et al : assoc off anal Chem Propionic Acid Bread and Flour 400 mg/kg (MKKM PS)
Acid In Bread and Flour Vol 64, No 2 1981. Pages 280 – Confectionery
Confection by Gas 281.
A A A NA
Chromatography Using
Internal Standard
MOH E03-012 The Determination of Synthetic Magda Rafecas, Francesc Synthetic Antioxidant Edible Oil 10 -75 mg/kg
Antioxidants (PG, TBHQ, Guardiola, Miquei Illera, Rafael
BHA , BHT, LG and OG) in Codony & Joseph Boatella.
Edible Oil by High (1998). Liquid Chromatographic
Performance Liquid Determination of Phenolic
Chromatography Antioxidants in Bakery Product. A NA
Journal of Chromatography A
MOH E03-013 Determination of Nitrite and US Environmental Protection Nitrate & Nitrite Meat & Meat Products 50 mg/kg
Nitrate in Meat Products using Agency. Determination of
Ion Chromatography Inorganic Anions By Ion
Chromatography. Method 9056A. NA
Revision 1 November 2000.
MOH E03-014 Determination of Benjakul et.al. Food Hydrocolloids Formaldehyde Fish and Fish Products 0.1 - 8.5 mg/kg
Formaldehyde in Fish & Fish 19(2005) Effect of Frozen Storage 1 mg/kg (MKKM PS)
Products and Pasta using on Chemical & Gel-Forming
Nash's Method Properties of Fish Commonly A A A NA NA NA A A
Used For Surimi Production in
Thailand
MOH E03-015 Determination of Jianrong. L., Junli. Z., Lifang. Ye., Formaldehyde Pasta (spagetthi) 2.5 mg/kg
Formaldehyde in Food using 2007. Determination of
High Performance Liquid formaldehyde in squid by high A A A
Chromatography performance liquid
chromatography. Asia Pacific
Fish and Fish Products 20 mg/kg
Journal of Clinical Nutrition. Vol.
16, page 127 – 130. NA
MOH E03-016 Determination of Citrate in Fish US Environmental Protection Citrate Fish and Fish Products 25 mg/kg
and Fish Products using Ion Agency
Chromatography (EPA Method 9056A), NA
Rev. , 1 Nov. 2000
MOH E03-017 The Determination Of Afidah A. Rahim, Bahruddin Saad, DEGME, DEG, Coumarin Selected types of 10 mg/kg
Diethylene Glycol Monoethyl Hasnah Osman, Noorhasani food**
Ether (DEGME), Diethylene Hashim, Solhan Yahya,
Glycol (DEG) and Coumarin in Khairuddin Md Talib,
Food by Gas Chromatography Simaltaneous determination of
Using Internal Standard diethylene glycol, diethylene glycol
monoethyl ether, coumarin and
A
caffeine in food items by gas
chromatography, Food Chemistry
126 (2011) page 1412-1416
MOH E03-018 Determination of US Environmental Protection Polyphosphate Fish and Fish Products 375 mg/kg
Polyphosphate in Fish and Agency (EPA Method 9056A),
Fish Products using Ion Rev. 1, Nov. 2000 A
Chromatography
Monophosphate 125 mg/kg

A
Diphosphate 125 mg/kg

A
Triphosphate 125 mg/kg

A
MOH E03-019 The Determination of Journal of Chromatography A, Methylparaben Selected types of 3 - 20 mg/kg
Parabens in Food using Liquid 1073 (2005) food** 4 mg/kg (MKKM PS) A A A A NA A A A A
Chromatography
Ethylparaben
A A A A NA A A A A
Propylparaben
A A A A NA A A A A
Butylparaben
A A A A NA A A A A
MOH E03-020 Determination of Formadehyde Takashi.H. ,et al., 1987. Formaldehyde Shrimp 20 mg/kg
using liquid chromatography Determination of Hydrogen
Peroxide in Beverages by High
Performance Liquid
Chromatography with A
Fluorescence Detection. Journal
of Chromatography. 411 (1987),
423-429.
MOH E03-021 The Determination of Di(2- A.K.Chaudhary,S.Ankushrao Di(2-ethylhexyl)phthalate Beverages 2 mg/kg

ethylhexyl)phthalate (DEHP) in Waske, S.Yadav.T.G (DEHP)
Food By Using High Chandrashekhar and Vandana
Performance Liquid Sigh Validated Reverse Phase
Chromatography HPLC Method for the
Determination of DEHP Content in
Reconstituting Diluents and NA
Reconstituted Solutions of
Imipenem and Cilastatin for
Injection. E-Journal of Chemistry
2010,7(2),501-513
MOH E03-022 Determination of Citrate and US Environmental Protection Monophosphate, Fish and Fish Products Polyphosphates 1000
Polyphosphate in Fish and Agency. Determination of Diphosphate, mg/kg
Fish Products using Ion Inorganic Anions by Ion Triphosphate, Citrate
Chromatography (Metrohm) Chromatography. Method 9056A. Citrates 500mg/kg A
MOH E03-023 Determination of Maleic Acid In Pelin Gunc Ergonul and Cevdet Maleic acid Starch and Starch 4 -8 mg/kg
Starch and Starch Products by Nergiz. 2010. Determination of Products 8 mg/kg (MKKM PS)
High Performance Liquid Organic acids in olive fruit by
Chromatography with DAD HPLC. Czech. J. Food Sci. Vol. A A NA NA A NA NA NA
28, 2010, No 3: 202-205
MOH E03-024 The Determination of Benzoyl Yukiko Abe-Onishi, Chikako Benzoyl Peroxide Flour 1 - 20 mg/kg
Peroxide in Flour by Liquid Yomoto, Naoki Sugimoto, Hiroki 5 mg/kg (MKKM PS)
Chromatography Kubota, Kenichi Tanamoto, 2004.
Determination of benzoyl peroxide
and benzoic acid in wheat flour by
high-performance liquid
chromatography and its
identification by high- performance
liquid chromatography-mass A A NA A A A A
spectrometry in Journal of
Chromatography A, 1040 (2004),
page 209 -214.
MOH E03-025 Determination of Ethoxyquin in 1. Schreier & Greene: Journal of Ethoxyquin Meat 0.006mg/kg
Foods by Liquid AOAC International, Vol. 80, No.
Chromatography 4, 1997,pg.725 -731.
2. AOAC Official Method 996.13,

Ethoxyquin in Feeds, Liquid A NA
Chromatographic Method, First
Action 1996, Final Action 1997.
MOH E03-026 Determination of Nitrite and US Environmental Protection Nirite Raw & Edible Bird's 2 - 7mg/kg
Nitrate in Raw & Edible Bird's Agency Nest A A
Nest Using Ion (EPA Method 9056A),
Chromatography (METROHM) Rev. 1, Nov. 2000 Nitrate 27 - 42 mg/kg
A A
MOH E03-027 Determination of Nitrite and US Environmental Protection Nitrate & Nitrite Meat & Meat Products 50 mg/kg
Nitrate in Meat using Ion Agency. Determination of
Chromatography (Methrohm) Inorganic Anions By Ion
Chromatography. Method 9056A. A
MOH E03-028 Determination of 1)Determination of formaldehyde Formaldehyde Flour 75 mg/kg

Formaldehyde in Flour using in squid by high performance
Liquid Chromatography liquid chromatography, 2007, Asia
Pacific Journal of Clinical
Nutrition. Vol. 16, page 127 – 130.
2) Determination of Formaldehyde NA
in Flour Samples, 2011, Final
Report, USM.
MOH E03-029 The Determination of Agata Zygler, Andrzej Wasik, Acesulfame-K Selected types of 0.2 mg/kg
Sweeteners in Food using Agata Kot-Wasik, Jacek food** NA
Liquid Chromatography Mass Namieśnik, 2011. Determination of
Spectrometry (LC-MS) nine high –intensity sweeteners in Aspartame 0.2 mg/kg
NA
various foods by high-
performance liquid Neotame 0.2 mg/kg
chromatography with mass NA
spectrometric detection. Anal
Bioanal Chem, 400: page. 2159- Sucralose 0.2 mg/kg
2172. NA
Saccharin 0.2 mg/kg

NA
Cyclamate 0.2 mg/kg

NA
MOH E03-030 The Determination of Boric United State Environmental Boric Acid (as Boron) Flour and Flour Not Available
Acid in Flour and Flour Protection Agency. 1996. 2nd Products
Products using Inductively Revision. Method Acid Digestion
Coupled Plasma-Optical of Sediment, Sludge and Solid.
Emission Spectrophotometry Method 3050B.
(ICP-OES)
MOH E03-031 Determination of Neotame in Agilent Application Solution. Neotame Soft Drink 5 mg/L (MKKM PS)
Soft Drink using Liquid Quantification of artificial
Chromatography with Diode sweeteners in diet colas using an
Array Detector Agilent 1260 Infinity Binary LC A NA
system with UV detection.
MOH E03-032 Determination of MERCK, Merkoquant® 10036 Formaldehyde Fish and Fish Products Not Available
Formaldehyde using Test Kit Formaldehyde Test Kit’s NA
(Merkoquant) Instruction Manual.
A Capable and accredited to ISO/IEC 17025

** Refer sheet SAMM NO.
PESTICIDE RESIDUES
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
MOH F03-001 Multiple Simultaneous Method for Journal of Food Hygiene Society of Azinphos ethyl Fresh Fruits & Vegetables 0.025,
Organophosporus
Pesticide Residues in Fruits and Japan, Vol. 44, No. 5 NA A NA NA A
Vegetables
Carbofenothion 0.1
NA NA A NA A
Chlorpyriphos 0.5 (MKAJB), 0.025 (ALL), 0.3

(SEL) A NA A A NA A A
Chlorpyrifos methyl 0.6 (MKAJB) 0.025 (ALL), 0.3

Cyanofenphos 0.025
A NA NA A NA A A
Diazinon 0.4 (MKAJB) 0.01 (ALL), 0.3

Dichlorvos 0.025
NA NA A NA A
Dimethoate 0.025
NA NA
Ethion 0.5 (MKAJB), 0.025 (ALL)

A NA NA A NA A A
Fenitrothion 0.5 (MKAJB),

0.025 (ALL) NA A NA A A
Fensulfothion 0.01
NA
Fenthion 0.9 (MKAJB) 0.025 (ALL), 0.3

(SEL) A NA NA NA
Formothion 0.9 (MKAJB) 0.025 (ALL)

A NA A NA NA
Malathion 0.5 (MKAJB), 0.02 (ALL)

A NA NA A NA A A
Methamidophos 0.025
NA
Methidathion 0.9 (MKAJB)

0.01 (ALL) 0.3 (SEL) A A A NA NA A
Parathion ethyl 0.05

NA NA A NA A A
Parathion methyl 0.8 (MKAJB), 0.05 (ALL)

NA A NA A A
Phosalone 2 (MKAJB) 0.05 (ALL)

A NA A NA NA A
Pirimiphos methyl 0.4 (MKAJB) 0.01 (ALL)

A NA NA A NA A A
Profenophos 0.025
A NA NA A NA A A
Prothiophos 0.025, 0.3 (SEL)

NA A A NA A A
Quinalphos 0.02, 0.3 (SEL)

A NA A A NA A A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Tolclophos methyl 0.6 (MKAJB) 0.025 (ALL)

A NA NA A NA A A
2,4-DDT 0.025
Organochlorine
NA A
4,4-DDD 0.025
NA NA NA A
4,4-DDE 0.025, 0.03 (SEL)

NA A NA A
4,4-DDT 0.025
NA NA NA A
Aldrin 0.025, 0.03 (SEL)

NA A NA NA A
Captafol 0.25
NA NA A
Captan 0.25
NA NA NA A
Chlordane 0.005
NA NA NA NA
Dichloran 0.015, 0.03 (SEL)

NA A NA NA A
Dieldrin 0.01, 0.03 (SEL)

NA A NA NA A
Endrin 0.01
NA NA NA NA A NA
Endosulfan 0.03
Endosulfan (alpha) 0.03, 0.03 (SEL)

A NA
Endosulfan (beta) 0.03, 0.03 (SEL)

A NA
Gamma-HCH / 0.05, 0.03 (SEL)

Lindane NA A NA NA A
Heptachlor 0.005, 0.03 (SEL)

NA A NA NA A
Quintozene 0.005, 0.03 (SEL)

NA A NA A
Triademefon 0.05, 0.03 (SEL)

NA A NA A NA
Triflumuron 0.5
NA NA NA A NA
Cyfluthrin 0.25, 0.3 (SEL)

S.Pyrethroid
NA A NA A NA
Cypermethrin 0.25, 0.3 (SEL)

NA A NA A NA
Fenvalerate 0.25, 0.3 (SEL)

NA A NA A NA
Deltamethrin 0.05
NA
Permethrin 0.25, 0.3 (SEL)

A NA A NA
MOH F03-002 Multiple Simultaneous Method for Journal of Food Hygiene Society of Azinphos ethyl Onion, Garlic & Shallot 0.025
Organophosporus
Pesticide Residues in Vegetables Japan, Vol.33, No.6 NA NA NA

(Frozen Method)
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
MOH F03-002 Multiple Simultaneous Method for Journal of Food Hygiene Society of Onion, Garlic & Shallot
Organophosporus
Pesticide Residues in Vegetables Japan, Vol.33, No.6
(Frozen Method)
Carbofenothion 0.1
NA NA
Chlorpyriphos 0.5 (MKAJB), 0.025 (ALL)

NA NA NA
Chlorpyrifos methyl 0.6 (MKAJB) 0.025 (ALL)

NA NA NA
Cyanofenphos 0.025
NA NA NA
Diazinon 0.4 (MKAJB) 0.01 (ALL)

NA NA NA
Dichlorvos 0.025
NA NA
Dimethoate 0.025
NA
Ethion 0.5 (MKAJB), 0.025 (ALL)

NA NA NA
Fenitrothion 0.5 (MKAJB), 0.025 (ALL)

NA NA NA
Fensulfothion 0.01
Fenthion 0.9 (MKAJB) 0.025 (ALL)

NA NA

NA NA

NA NA NA
Methamidophos 0.025
NA
Methidathion 0.9 (MKAJB) 0.01 (ALL)

NA NA NA
Parathion ethyl 0.05

NA NA NA
Parathion methyl 0.8 (MKAJB), 0.05 (ALL)

NA NA NA
Phosalone 2 (MKAJB) 0.05 (ALL)

NA NA NA

NA NA NA
Profenophos 0.025
NA NA NA
Prothiophos 0.025
NA NA NA
Quinalphos 0.02
NA NA NA

NA NA NA
2,4-DDT 0.025
Organochlorine
NA NA
4,4-DDD 0.025
NA NA
4,4-DDE 0.025
NA NA
KOTA KINABALU
Organochlorine
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
4,4-DDT 0.025
NA NA
Aldrin 0.025
NA NA
Captafol 0.25
NA NA
Captan 0.25
NA
Dichloran 0.015
NA NA
Dieldrin 0.01
NA NA
Endrin 0.01
NA NA NA
γ-HCH/Lindane 0.05
NA NA
Heptachlor 0.005
NA NA
Quintozene 0.005
NA NA
Triademefon 0.05
NA NA NA
Triflumuron 0.5
NA NA NA
Chlordane
NA
Cyfluthrin 0.25
S.Pyrethroid
NA NA NA
Cypermethrin 0.05
NA NA NA
Fenvalerate 0.05
NA NA NA
Deltamethrin 0.01
NA NA
Permethrin 0.025
NA NA NA
MOH F03-003 Multiple Simultaneous Method for Journal of Food Hygiene Society of Azinphos ethyl Cereal, Seeds & Beans 0.200
Organophosporus
Pesticide Residues in Cereal, Bean Japan, Vol. 44, No. 5 NA NA NA NA NA

and Seeds
Carbofenothion 0.150
NA NA NA NA NA
Chlorpyriphos 0.5 (MKAJB),

0.025 (ALL)
A NA NA NA NA NA NA
Chlorpyrifos methyl 0.6 (MKAJB) 0.025 (ALL)

A NA NA NA NA NA NA
Cyanofenphos 0.05 (ALL)

A NA NA NA NA NA NA
Diazinon 0.4 (MKAJB)

0.01 (ALL) A NA NA NA NA NA NA
Dichlorvos 0.025 (ALL)

NA NA NA NA NA
Or
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Dimethoate 0.025
NA NA
Ethion 0.5 (MKAJB),

0.025 (ALL) A NA NA NA NA NA NA
Fenitrothion 0.5 (MKAJB), 0.025 (ALL)

NA NA NA NA NA
Fensulfothion 0.100
NA
Fenthion 0.025
NA NA NA NA

A NA NA NA NA

A NA NA NA NA NA NA
Methamidophos 0.025
NA
Methidathion 0.9 (MKAJB) 0.01 (ALL)

A NA NA NA NA NA
Parathion ethyl 0.005 (ALL)

NA NA NA NA NA NA
Parathion methyl 0.05 (ALL), 0.8 (MKAJB)

NA NA NA NA NA
Phentoate 0.025
NA
Phosalone 0.05 (ALL), 2 (MKAJB)

A NA NA NA NA NA

A NA NA NA NA NA NA
Profenophos 0.025
A NA NA NA NA NA NA
Quinalphos 0.2 (ALL)

A NA NA NA NA NA NA
Prothiophos 0.025 (ALL)

NA NA NA NA NA

A NA NA NA NA NA NA
2,4-DDT 0.0125 (ALL)

Organochlorine
NA NA NA
4,4-DDD 0.0125 (ALL)

NA NA NA NA
4,4-DDE 0.0125 (ALL)

NA NA NA NA
4,4-DDT 0.0125 (ALL)

NA NA NA NA NA
Aldrin 0.010
NA NA NA NA NA
Chlordane 0.005
NA NA NA NA NA NA
Dichloran 0.005 (ALL)

NA NA NA NA NA
Or
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Dieldrin 0.010
NA NA NA NA NA
Endrin 0.010
NA NA NA NA NA NA
Triflumuron 0.05
NA NA NA NA NA
Captan 0.01
NA NA NA NA
Captafol 0.15
NA NA
γ-HCH/Lindane 0.05 (ALL)

NA NA NA NA NA
Heptachlor 0.010
NA NA NA NA NA
Quintozene 0.005 (ALL)

NA NA NA NA
Triademefon 0.05 (ALL)

NA NA NA NA NA
Cyfluthrin 0.025
S. Pyrethroid
NA NA NA NA NA
Cypermethrin 0.050
NA NA NA NA NA
Deltamethrin 0.050
NA NA NA
Fenvalerate 0.050
NA NA NA NA NA
Permethrin 0.025
NA NA NA NA
MOH F03-004 Analysis of Chlorinated Pesticide in Guideline for Residue Monitoring in DDT Water 0.003 mg/L (MKAK)
Organochlorine
Water the Eropean Union, Second Edition NA

(1999/2000). Quality Control for
Pesticide Residue Analysis Aldrin 0.003 mg/L (MKAK)
NA
Chlordane (mix 0.003 mg/L (MKAK)

isomers) NA
Dieldrin 0.003 mg/L (MKAK)

NA
γ-HCH/Lindane 0.003 mg/L (MKAK)

NA
Heptachlor 0.003 mg/L (MKAK)

NA
Hexachlorobenzene 0.003 mg/L (MKAK)

NA
Metoxychlor 0.003 mg/L (MKAK)

NA
MOH F03-005 Determination of Dithiocarbamate in Journal of AOAC International, 83 Fresh Fruits & Vegetables
CS2
Dithiocarbamate (express 0.05

Vegetable by Gas Chromatography- (3) as CS2) 0.15 (MKKM Perlis)
Mass Spectrometry A NA A NA NA A A A
MOH F03-006 Determination of Organochlorine 4,4-DDD Meat, Prawn, Squid & Fish 0.10
Organochlorine
Standard Methods of Analysis of the

Pesticides in Muscle using Gas Association of Official Analytical NA NA A
Chromatography Chemists, 17th ed. Vol
1. 4,4-DDE 0.05
NA NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
DOC.
MOH NO
F03-006 TESTofMETHOD REFERENCE PARAMETER Meat,FOOD
Prawn,MATRIX
Squid & Fish
Organochlorine
Determination Organochlorine Standard Methods of Analysis of the
IPOH
MIRI
(µg/kg) / (mg/kg)
Pesticides in Muscle using Gas Association of Official Analytical
Chromatography Chemists, 17th ed. Vol
1.
4,4-DDT 0.10
NA NA A
Alpha-BHC/alpha-HCH 0.05
NA NA A
Beta-BHC/beta-HCH 0.05
NA NA A
Gamma-BHC/gamma-HCH 0.05
NA NA A
Delta-BHC/Delta-HCH 0.05
NA NA A
Aldrin 0.10
NA NA A
Alpha-chlordane 0.05
NA NA A
Gamma-chlordane 0.05
NA NA A
Dieldrin 0.05
NA NA A
Endrin 0.05
NA NA A
Heptachlor 0.05
NA NA A
Heptachlor epoxide 0.10

NA NA A
MOH F03-007 Determination of Pesticide Journal of AOAC International Trichlorfon Fruit and Vegetables 0.3
Organophosporus
Residues in Low-Fat Products using Vol. 86, No. 2 NA

QuEChERS Method
Acephate 0.3
NA NA
Omethoate 0.2
NA
Demeton (o+s) 0.05
Demeton-s methyl 0.05
Dicrotophos
Ethioprophos 0.05
NA
Monocrotophos 0.05
Phorate 0.2
Etrimphos 0.05
Diclofenthion 0.05
0.005 (MKKM Perlis) NA NA
Fenchlorphos 0.05
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Bromophos
Pirimiphos ethyl 0.05

NA NA
Chlorfenvinphos 0.2
Prothiophos
Fenamiphos 0.05
0.02 (MKKM Perlis) NA
Triazophos 0.05
NA
Phosmet 0.05
0.02 (MKKM Perlis) NA
Azinphos methyl 0.1

NA NA
Coumaphos 0.05
Methamidophos 0.05
NA NA
Dimethoate 0.05
0.005 (MKKM Perlis) NA NA NA NA
Dichlorvos 0.01
NA NA NA A
Diazinon 0.01 (SEL-0.3)

NA NA NA NA A
Formothion 0.01
0.025 (MKKM Perlis) NA NA NA A
Parathion Methyl 0.01

NA NA A
Chlorpyrifos Methyl 0.01 (SEL-0.3)

NA NA NA NA A
Tolclophos Methyl 0.01 (SEL-0.3)

NA NA NA NA A
Pirimiphos Methyl 0.01 (SEL-0.3)

NA NA NA NA A
Fenitrothion 0.01 (SEL-0.3)

NA NA NA A
Malathion 0.01
NA NA NA A
Chlorpyrifos NA NA
Parathion 0.01
NA A
Phenthoate 0.01
0.005 (MKKM Perlis) NA NA A
Quinalphos 0.01 (SEL-0.3)

NA NA NA NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Methidathion 0.01
NA NA NA A
Bromophos-ethyl 0.01
NA A
Profenophos 0.01
0.015 (MKKM Perlis) NA NA NA NA A
Fensulfothion 0.01
0.005 (MKKM Perlis) NA NA A
Ethion 0.01 (SEL-0.3)

NA NA NA NA A
Carbofenothion 0.01
NA NA NA A
Cyanofenphos 0.01
NA NA NA A
Phosalone 0.01
NA NA A
Azinphos Ethyl 0.01

NA NA A
Fenthion sulfoxide 10ppb

NA
Sulfotep 10ppb
NA
carbofuran 10ppb
Organonitrogen
NA
fenobucarb 10ppb
NA
carbosulfan 10ppb
NA
methiocarb 10ppb
NA
Chlorfenapyr 10ppb
NA
Acetamiprid 10ppb
NA
Cyromazine 10ppb
NA
Chlorothalonil 10ppb
NA
Hexaconazole 10ppb
NA
Fipronil 10ppb
NA
Myclobutanil 10ppb
NA
Pecycuron 10ppb
NA
Tolfenpyrad 10ppb
NA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Difenoconazole 10ppb
NA
Metalaxyl 10ppb
NA
Tebuconazole 10ppb
NA
Fenazaquin 10ppb
NA
Iprodione 10ppb
NA
Paclobutrazole 10ppb
NA
Flusilazole 10ppb
NA
Propamocarb 10ppb
NA
Propiconazole 10ppb
NA
Indoxacarb 10ppb
NA
Pyriproxyfen 10ppb
NA
Pyrimethanil 10ppb
NA
Procymidone 10ppb
NA
Procloraz 10ppb
NA
Pendimethanil 10ppb
NA
Dimethomorph 10ppb
NA
Trifloxystrobin 10ppb
NA
Azoxystrobin 10ppb
NA
Pyraclostrobin 10ppb
NA
Kresoxim-methyl 10ppb
NA
Hexachlorobenzene 0.01
Organochlorine
NA A
0.01 (MKKM Perlis),

Alpha-BHC (SEL-0.03) A NA
Beta-BHC 0.01
NA NA A
Delta-BHC 0.01
A NA NA A
Organochlorine
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Propanil 0.01
A
Triadimefon 0.01 (SEL-0.03)

A NA NA NA A
Heptachlor endo-epoxide 0.01

NA NA A
Chlordane-trans (gamma) 0.01

A NA NA A
Alpha-endosulfan 0.01 (SEL-0.03)

NA NA A
Chlordane-cis (alpha) 0.01

A NA NA A
2,4-DDD 0.01
NA A
Endrin 0.01
A NA NA A
0.01 (SEL-0.03)
Beta-endosulfan NA
4,4-DDD 0.01
A NA NA A
2,4-DDT
Endosulfan sulfate 0.01

NA A
Methoxychlor 0.10
A
Tetradifon 0.01
A
Mirex 0.01
A
Gamma HCH 0.01

A NA
Dichloran 0.01 (SEL-0.03)

A NA NA
0.03
Gamma-BHC NA
Quintozene 0.01 (SEL-0.03)

A NA NA
Heptachlor 0.01 (SEL-0.03)

A NA NA
Aldrin 0.01 (SEL-0.03)

A NA NA
4,4-DDE 0.01 (SEL-0.03)

A NA NA
Dieldrin 0.01 (SEL-0.03)

A NA NA
Permethrin 0.01 (SEL-0.3)

S.Pyrethroid
A NA NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
S.Pyrethroid GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Cyfluthrin 0.01
0.05(MKKM Perlis), (SEL-0.3) A NA NA NA A
Cypermethrin 0.02
0.05(MKKM Perlis), (SEL-0.3) A NA NA NA A
Fenvalerate 0.01
0.05(MKKM Perlis), (SEL-0.3) A NA NA A
Deltamethrin 0.01
NA A
Fipronil 0.005
Others
Imidacloprid 0.01
NA
Cereal and Cereal
Organophosporus
Metamidophos Products 0.02 A
Omethoate 0.01 A
Demeton-S-Methyl 0.04 A
Dicrotophos 0.01 A
Monocrotophos 0.01 A
Dimethoate 0.01 A
Dichlofenthion 0.01 A
Fenclorphos 0.01 A
Bromophos 0.01 A
Pirimiphos-ethyl 0.01 A
Chlorfenvinphos 0.01 A
Prothiophos 0.01 A
Triazophos 0.01 A
Phosmet 0.01 A
Azinphos-methyl 0.04 A
Coumaphos 0.01 A
Diazinon 0.005 A
Formothion 0.01 A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Parathion-methyl 0.01 A
Chlorpyrifos-methyl 0.01 A
Tolclofos-methyl 0.01 A
Pirimiphos-methyl 0.01 A
Fenitrothion 0.01 A
Malathion 0.005 A
Chlorpyrifos 0.01 A
Parathion 0.01 A
Phenthoate 0.005 A
Quinalphos 0.005 A
Methidathion 0.01 A
Bromophos-ethyl 0.01 A
Profenofos 0.01 A
Fensulfothion 0.01 A
Ethion 0.01 A
Carbophenothion 0.01 A
Cyanofenphos 0.005 A
Phosalone 0.01 A
Azinphos-ethyl 0.01 A
Organochlorine
0.01 A
Alpha-BHC
Beta-BHC 0.005 A
Delta-BHC 0.01 A
Hexachlorobenzene 0.01 A
Dicloran 0.01 A
Organochlorin
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Gamma-BHC 0.01 A
Quintozene 0.01 A
Propanil 0.01 A
Heptachlor 0.005 A
Aldrin 0.005 A
Triadimefon 0.01 A
Heptachlor endo-epoxide 0.005 A
Chlordane-trans (gamma) 0.005 A
Chlordane-cis (alpha) 0.005 A
2,4-DDD 0.005 A
4,4-DDE 0.01 A
Dieldrin 0.005 A
Endrin 0.01 A
Beta-endosulfan 0.01 A
4,4-DDD 0.01 A
2,4-DDT 0.01 A
Endosulfan sulfate 0.01 A
Methoxychlor 0.01 A
Tetradifon 0.005 A
Mirex 0.005 A
S.Pyrethroid
Permethrin 0.01 A
Cyfluthrin 0.01 A
Cypermethrin 0.01 A
Fenvelerate 0.01 A
S.Pyrethroid
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Deltamethrin 0.01 A
Organophosp
Malathion Garam dan rempah 0.4 NA
orus
Kekeras dan Hasil
Methamidophos 0.03 NA
kekeras
MOH F03-008 Determination of Pesticide Alpha-endosulfan Tea
Organochlorine
Journal of AOAC International Vol. 0.05 (SARAWAK),
Residues in Tea using QuEChERS 86, No. 2 : 412-431 1.0 (MKAK) NA A
Method
Beta-endosulfan 0.05 (SARAWAK),
1.0 (MKAK) NA A
Endosulfan sulfate 0.1 (SARAWAK),

1.0 (MKAK) NA A
Dichloran 0.4 (SARAWAK),

0.05 (MKAK) NA NA A
Dieldrin 0.2 (SARAWAK),

0.05 (MKAK) NA NA A
Hexachlorobenzene 0.2 (SARAWAK),

0.05 (MKAK) NA A
Gamma-HCH 0.1 (SARAWAK),

0.05 (MKAK) NA NA A
4,4'-DDE 0.05
NA NA A
4,4'-DDD 0.05
A
4,4'-DDT 0.1
NA NA
Cypermethrin 0.1 (SARAWAK), 1.0 (MKAK)

S.Pyrethroid
NA NA A
Deltamethrin 0.4 (SARAWAK), 1.0 (MKAK)

NA A
Fenvalerate 0.2 (SARAWAK),

0.5 (MKAK) NA NA A
MOH F03-009 4,4-DDD 0.01

Organochlorine
Determination of Pesticide Norazlina, O., Jamilah, B., and Fish, Meat and Its
Residues in Fish, Meat and Its Kharidah, M. (2013). Determination Products A A NA A A
Products Using QuEChERS Method of organochlorine pesticides in
by Gas Chromatography shrimp by gas chromatography– 4,4-DDE 0.01
mass spectrometry using a modified A A NA A A
QuEChERS approach. Food Control,
34(2), 318-322. 4,4-DDT 0.01
A NA A A
Alpha -BHC 0.01

0.02(MKKM Perlis) A A A A
Beta-BHC 0.01
A A A
Gamma-BHC 0.01
A A NA A A
Delta-BHC 0.01
A A A A
Aldrin 0.01
A A NA A A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Dichloran 0.01
A A NA
Dieldrin 0.01
A A NA A A
Endrin 0.01
A A NA A A
Heptachlor 0.01
A A NA A A
Heptachlor-exo-epoxide 0.01
A A A
Gamma-chlordane 0.01
A A NA A A
Alpha-chlordane 0.01
A A NA A A
Triadimefon 0.01
A NA
Cyfluthrin 0.03
S.Pyrethroid
A NA
Cypermethrin 0.03
A NA
Fenvalerate 0.02
A NA
Permethrin 0.03
A
Fipronil 0.005
Others
Milk
Organophosphorus
Dichlorvos 0.010 NA
Dimethoate 0.010 NA
Diazinon 0.010 NA
Parathion methyl 0.010 NA
Malathion 0.010 NA
Fenthion 0.010 NA
Chlorpyrifos 0.010 NA
Ethion 0.010 NA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Organochlorine
Alpha-HCH 0.010 NA
Beta-HCH 0.010 NA
Gamma-HCH 0.010 NA
Heptachlor 0.010 NA
Aldrin 0.010 NA
2,4'-DDT 0.010 NA
4,4'-DDE 0.010 NA
Dieldrin 0.010 NA
Endrin 0.010 NA
4,4'-DDD 0.010 NA
4,4'-DDT 0.010 NA
Organophosphorus phospor
Organo
Methidathion Egg 0.01 NA

us
MOH F03-010 Determination of Pesticide Lian-Kuet Chai, Nur-Dzaina Zaidel Acephate Fruit and Vegetables 0.40
Residues in Fruits and Vegetables and Hans Christian Brunn Hansen, A
using QuEChERS Technique 2011. A rapid multi-residue method
for determination of pesticide Azinphos Ethyl 0.01
residues in choi sum, yardlong A A
beans and aubergines. Journal of
Food Chemistry, 131 (2012) : 611- Azinphos-methyl 0.60
A
616.
Bromophos-methyl 0.03
A
Carbofenothion 0.01
NA A A
Cyanofenphos 0.01
A NA A
Chlorfenvinphos 0.20
A
Coumaphos 0.40
A
Demeton-s-methyl 1.00
NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Dichlorvos 0.02
NA A A
Diazinon 0.01
A NA A A
Dimethoate 0.03
NA A
Dichlofenthion 0.02
A
Ethion 0.01
0.02(MKKM Perlis) A NA A A
Ethoprophos 0.02
NA A
Fenamiphos 0.05
A
Fenchlorphos 0.02
A
Methamidophos 0.06
NA A
Monocrotophos 1.00
A
Omethoate 0.40
A
Phorate 0.02
A
Phosmet 0.30
A
Triazophos 0.10
A
Trichlorfon 0.04
A A
Formothion 0.01
A
Parathion Methyl 0.04

A A
Tolclophos Methyl 0.02

A NA A A
Fenitrothion 0.01
A A
Pirimiphos Methyl 0.01

A NA A
0.04
Pirimiphos-ethyl A
Malathion 0.01
0.06(MKKM Perlis) A NA A A
Fenthion 0.02
0.01(MKKM Perlis) A A
Parathion Ethyl 0.03

0.04(MKKM Perlis) A NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Chlorpyrifos 0.02
A NA A A
0.01
Chlorpyrifos Methyl 0.03 (MKKM Perlis) A A
Quinalphos 0.01
A NA A A
Phentoate 0.02
A
Methidathion 0.01
A
Prothiophos 0.01
0.03(MKKM Perlis) A A
Profenophos 0.01
NA NA A
Fensulfothion 0.01
A
Phosalone 0.03
NA A
Dicloran 0.10
Organochlorine
NA A
Triflumuron 0.21
NA A
Gamma-HCH 0.03
NA A
Quintozene 0.08
NA A
Heptachlor 0.05
NA A
Dieldrin 0.06
NA A
Aldrin 0.03
NA A
4,4'-DDE 0.07
NA A
Endrin 0.07
NA A
2,4'-DDT 0.06
A
4,4'-DDT 0.05
NA A
Permethrin 0.1, 0.14 (MKAK)

S.Pyrethroid
Cyfluthrin 0.07, 0.08 (MKAK)

NA A
Cypermethrin 0.09
NA A
Fenvalerate 0.20
NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
MOH F03-011 Determination of Pesticides Propamocarb Fruit and Vegetables 0.010
Organonitrogen
Maurice Hiemstra and Andre' de
Organonitrogen in Food by Kok, 2002. Determination of NA A
Liquid Chromatography Tandem propamocarb in vegetables using
Mass Spectrometry polymer-based high-performance Oxamyl 0.002
liquid chromatography coupled with NA
electrospray mass spectrometry.
Journal of Chromatography A, 972 Carbendazim 0.002
NA A
(2002) : 231-239.
Aldicarb 0.002
NA
Bendiocarb 0.002
NA A
Pirimicarb 0.002
NA A
Propoxur 0.002
NA
Carbofuran 0.002
NA
Carbaryl 0.002
NA A
Fenobucarb 0.010
NA A
Benomyl (express as 0.020

Carbendazim)
Thiobencarb 0.020
NA
Methomyl 0.002
NA
MOH F03-012 Determination of Highly Polar Ethephon Durian 0.050

Ethephon
Quick Method for the Analysis of

Pesticides in Food Of Plant Origin numerous Highly Polar Pesticides in
by Liquid Chromatography-Tandem Foods of Plant Origin via LC-MS/MS
Mass Spectrometry involving Simultaneous Extraction
with Methanol (QuPPe-Method) -
Version 9.2 (October 2016,
Document History, see page 65)
Authors: M. Anastassiades; D. I. A
Kolberg; A. Benkenstein; E.
Eichhorn; S. Zechmann; D. Mack; C.
Wildgrube; I. Sigalov; D. Dörk; A.
Barth.
MOH F03-013 Determination of Organochlorine 4,4-DDD Fish 0.03

Organochlorine
Method from Application Notes

NA
Pesticides in Muscle using (Agilent Technologies) for
QuEChERS method by Gas Organochlorine analysis 4,4-DDE 0.03
NA
Chromatography
4,4-DDT 0.03
NA
Aldrin 0.03
NA
Alpha-BHC 0.03
NA
Beta-BHC 0.03
NA
Delta-BHC 0.03
Dieldrin 0.03
NA
Chromatography
Organo
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
GROUP
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg) / (mg/kg)
Gamma-BHC 0.03
NA
Heptachlor 0.03
NA
MOH F03-014 Determination of Pesticides Validation Data of 127 Pesticides Azinphos-ethyl Cooking Oil 0.060
Organophosphorus
NA
Residues in Edible Oil by Gas Using a Multiresidue Method by LC-
Chromatography MS/MS and GC-MS/MS in Olive Oil. Chlorfenvinphos 0.060
NA
European Union Reference
Laboratory.2012. Diazinon 0.060
NA
Methidathion 0.060
NA
Parathion-ethyl 0.060
NA
Parathion-methyl 0.060
NA
Pirimiphos-methyl 0.060
NA
Profenofos 0.060
NA
Triazophos 0.060
NA
4,4'-DDE 0.060
Organochlorine
NA
4,4'-DDT 0.060
Aldrin 0.060
NA
Alpha-endosulfan 0.060
NA
Beta-endosulfan 0.060
NA
Dieldrin 0.060
NA
Endosulfan sulfate 0.060
NA
Endrin 0.060
NA
Gamma-HCH 0.060
NA
Heptachlor 0.060
NA
Hexachlorobenzene 0.060
NA
FOOD BIOTECHNOLOGY
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
DOC. NO TEST METHOD REFERENCE PARAMETER TECHNIQUE FOOD MATRIX LOD
IPOH
MIRI
MOH G03-111 (1) DNA Extraction Using QIAGEN DNeasy® Plant Mini Kit Handbook Extraction raw material Not Applicable Unprocessed food (cereal, NA
DNeasy® Plant Mini Kit vegetables and vegetable (MKKM Perlis)
product, fruit and fruit 1.0 ng/µl
product) (MKKM Selangor)
1.0 x 10-1 ng/µl
(MKKM Miri)
Raw Plant 0.1
ng/ul, Semi NA NA NA A
processed 1.0 ng/µl
(MKAK)
MOH G03-121 (1) Detection of Plant DNA (Universal Ref: MS ISO 21569:2005(E) Annex Plant gene Detection Food (cereal & cereal 1.0 x 10-5 ng/µl
Plant) by Gel Electrophoresis A.2 product, vegetables & (MKAK)
vegetables product and fruit A
& fruit product)
MOH G03-121(2) Detection of Plant DNA (Universal MS ISO 21569:2005, 2007. Plant gene Detection Food (cereal & cereal NA
Plant) by Real-Time PCR (qPCR) - Foodstuffs – Method of Analysis for product, vegetables & (MKKM Perlis)
SYBR Green the Detection of Genetically vegetables product and fruit 1.0 x 10-5 ng/µl
Modified Organisms and Derived & fruit product) (MKKM Selangor)
Products – Qualitative Nucleic Acid 1.0 x 10-4 ng/ul
Based Methods. (MKKM Miri)
Bioline SensiFAST™ SYBR® Hi-

ROX Kit. 2016. NA NA NA
Standard Operating Procedure for

CFX96 Real-Time PCR System
(bran: Bio-Rad)
MOH G03-122(1) Detection of Lectin in Soybean by MS ISO 21569:2005(E) Annex A.1 Lectin gene Detection Soybean kernel and 1.0 x 10-1 ng/µl
Gel Electrophoresis soybean product (MKAK) A
MOH G03-122 (2) Detection of Lectin in Soybean by MS ISO 21569:2005, 2007. Lectin gene Detection Soybean kernel and 1.0 x 10-4 ng/µl
Real-Time PCR (qPCR) - SYBR Foodstuffs – Method of Analysis for soybean product (MKKM Selangor)
Green the Detection of Genetically
Modified Organisms and Derived
Products – Qualitative Nucleic Acid
Based Methods.

ROX Kit. 2016. NA NA

(brand: Bio-Rad)
MOH G03-123 (1) Detection of Maize in Corn by Gel MS ISO 21569:2005 (E) Annex A.4 Maize gene Detection Corn Kernel and corn 1.0 x 10-1 ng/µl
Electrophoresis product (MKAK) A
MOH G03-124 (1) Detection of Polygalacturonase in MS ISO 21569:2005(E) Annex A.3 Polygalacturonase Detection Raw Tomato 1.0 x 10-1 ng/µl
Tomato by Gel Electrophoresis gene (MKAK)
A
MOH G03-124 (2) Detection of Polygalacturonase in MS ISO 21569:2005(E) Annex A.3 Polygalacturonase Detection Tomato 1.0 x 10-2 ng/µl
Tomato by Real-Time PCR (qPCR) gene (MKKM Selangor)
– SYBR Green NA NA
MOH G03-126 (1) Detection of Patatain in Potato by In house method based on Testing Patatain gene Detection Potato and potato product 1.0 x 10-1 ng/µl
Gel Electrophoresis for Food Produced by Recombinant (MKAK)
DNA Techniques; Provisional
Translation by MHLW; Page 3-19 A
MOH G03-127(1) Detection of Triticum aestivum in M. Arlorio et. al. (2002) Polymerase Triticum aestivum Detection Wheat and wheat product
Wheat by Gel Electrophoresis Chain Reaction (PCR) of gene
puroindoline b and
ribosomal/puroindoline b multiplex
PCR for the detection of common
wheat (Triticum aestivum) in Italian
Pasta
MOH G03-131 (1) Screening of Genetically Modified MS ISO 21569:2005(E) Annex B.1 CaMV 35S Promoter Detection Food (cereal & cereal
Food (CaMV 35S Promoter) by Gel gene product, vegetables & 0.01 ng/ul (MKAK)
Electrophoresis vegetables product and fruit
& fruit product)
A
MOH G03-131 (2) Screening of Genetically Modified MS ISO 21569:2005(E) Annex B.3 nos 3’ Terminator gene Detection Food (cereal & cereal 0.1%
Food (Agrobacterium tumefaciens product, vegetables & (MKAK)
nos 3' Terminator) by Gel vegetables product and fruit A
Electrophoresis & fruit product)
MOH G03-131 (3) Screening of Genetically Modified MS ISO 21569:2005(E) Annex B.4 npt II gene Detection Food (cereal & cereal 0.1%
Food (npt ll gene) by Gel product, vegetables & (MKAK)
Electrophoresis vegetables product and fruit A
& fruit product)
MOH G03-131 (4) Screening of Genetically Modified JRC Compedium of Reference Phosphinothricin Detection Food (cereal & cereal
Food (phosphinothricin Method for GMO Analysis, acetyltransferase (pat) product, vegetables &
acetyltransferase gene) by Real- Qualitative PCR method for gene vegetables product and fruit
Time PCR (qPCR) - SYBR Green detection of Phosphinothricin N- & fruit product)
acetyltransferase (pat) gene NA
(Barbau-Piaednoir et al.). (2014)
MOH G03-131 (5) Screening of Genetically Modified MS ISO 21569:2005, 2007. CaMV 35S Promoter Detection Food (cereal & cereal NA
Food (CaMV 35S Promoter) by Foodstuffs – Method of Analysis for gene product, vegetables & (MKKM Perlis)
Real-Time PCR (qPCR) - SYBR the Detection of Genetically vegetables product and fruit 1.0 x 10-2 ng/µl
Green Modified Organisms and Derived & fruit product) (MKKM Selangor)
Products – Qualitative Nucleic Acid 1.0 ng/µl

(brand: Bio-Rad)
MOH G03-131 (6) Screening of Genetically Modified MS ISO 21569:2005, 2007. nos 3’ Terminator gene Detection Food (cereal & cereal NA
Food (Agrobacterium tumefaciens Foodstuffs – Method of Analysis for product, vegetables & (MKKM Perlis)
nos 3' Terminator) by Real-Time the Detection of Genetically vegetables product and fruit 1.0 x 10-1 ng/µl
PCR (qPCR) - SYBR Green Modified Organisms and Derived & fruit product) (MKKM Selangor)

(brand: Bio-Rad)
MOH G03-131 (7) Screening of Genetically Modified MS ISO 21569:2005, 2007. npt II gene Detection Food (cereal & cereal NA
Food (npt II gene) by Real-Time Foodstuffs – Method of Analysis for product, vegetables & (MKKM Perlis)
PCR (qPCR) - SYBR Green the Detection of Genetically vegetables product and fruit 1.0 x 10-1 ng/µl
Modified Organisms and Derived & fruit product) (MKKM Selangor)


(brand: Bio-Rad)
MOH G03-131 (8) Screening of Genetically Modified JRC Compendium of Reference bar-gene Detection Food (cereal & cereal
Food (bar-gene) by Real-Time PCR Methods for GMO Analysis, 2014. product, vegetables & 1.0 x 10-1 ng/µl
(qPCR) - SYBR Green vegetables product and fruit (MKKM Selangor) NA
& fruit product)
MOH G03-131 (9) Screening of Genetically Modified JRC Compendium of Reference CTP2 & CP4 epsps Detection Food (cereal & cereal
Food (CTP2 & CP4 epsps gene) by Methods for GMO Analysis, 2017. gene product, vegetables & 1.0 x 10-1 ng/µl
Real-Time PCR (qPCR) - SYBR vegetables product and fruit (MKKM Selangor) NA
Green & fruit product)
MOH G03-131 (10) Screening of Genetically Modified JRC Compendium of Reference Cry 1Ab/Ac gene Detection Food (cereal & cereal
Food (Cry 1Ab/Ac gene) by Real- Methods for GMO Analysis, 2017. product, vegetables & 1.0 x 10-1 ng/µl
Time PCR (qPCR) - SYBR Green vegetables product and fruit (MKKM Selangor) NA
& fruit product)
MOH G03-142(1) Detection of Event-Specific MS ISO 21569:2005(E) Annex C.1 RRS gene Detection Soybean Kernel and 0.1%
Roundup Ready® Soybean (RRS) soybean product (MKAK)
A
by Gel Electrophoresis
MOH G03-142 (2) Detection of Event-Specific JRC Compedium of Reference MON 89788 Detection Soybean Kernel and 1.0 x 10-3 ng/µl
Soybean MON 89788 by Real-Time Method for GMO Analysis, QT-EVE- soybean product (MKAK)
PCR (qPCR) - Probe Based GM-Quantitative PCR Method for NA
Detection of Soybean Event MON
89788 2011.
MOH G03-142(3) Detection of Event-Specific JRC Compendium of Reference Soybean GTS Detection Soybean kernel and 0.01%
Soybean GTS Methods for GMO Analysis, QT- 40-3-2 soybean product (MKKM Selangor)
40-3-2 by Real-Time PCR (qPCR) – EVE-GM-005, 2011. NA
Probe Based
MOH G03-142(4) Detection of Event-Specific JRC Compendium of Reference Soybean DP-305423-1 Detection Soybean kernel and 0.1%
Soybean DP-305423-1 by Real- Methods for GMO Analysis, QT- soybean product (MKKM Selangor)
Time PCR (qPCR) – Probe Based EVE-GM-008, 2011. NA
MOH G03-142(5) Detection of Event-Specific JRC Compendium of Reference Soybean DP-356043-5 Detection Soybean kernel and 0.01%
Soybean DP-356043-5 by Real- Methods for GMO Analysis, QT- soybean product (MKKM Selangor)
Time PCR (qPCR) – Probe Based EVE-GM-008, 2011. NA
MOH G03-143 (1) Detection of Event-Specific Maize MS ISO 21569:2005(E) Annex C.3 Maize Bt 11 gene Detection Corn Kernel and corn 0.1%
A
Bt 11 by Gel Electrophoresis product (MKAK)
MOH G03-143 (2) Detection of Event-Specific Maize MS ISO 21569:2005(E) Annex C.4 Maize Bt 176 gene Detection Corn Kernel and corn 0.1%
A
Bt 176 by Gel Electrophoresis product (MKAK)
MOH G03-143 (3) Detection of Event-Specific Maize MS ISO 21569:2005(E) Annex D.1 Maize MON 810 gene Detection Corn Kernel and corn 0.1%
A
MON 810 by Gel Electrophoresis product (MKAK)
MOH G03-143 (4) Detection of Event-Specific Maize T MS ISO 21569:2005(E) Annex C.5 Maize T 25 gene Detection Corn Kernel and corn 0.1%
A
25 by Gel Electrophoresis product (MKAK)
MOH G03-143 (5) Detection of Event-Specific Maize Heller K.J. 2003. Genetically Maize GA 21 gene Detection Corn Kernel and corn 0.1%
GA 21 by Gel Electrophoresis Engineered Food; Methods and product (MKAK)
Detection. Germany. Wiley-VSH A
GmbH & Co. KGaA.
MOH G03-144(1) Detection of Event-Specific Tomato MS ISO 21569:2005(E) Annex C.2 Zeneca® F282 gene Detection Tomato and tomato product NA
Zeneca® F282 by Gel (MKAK) NA
Electrophoresis
MOH G03-146 (1) Detection of Event-Specific Potato Testing for Food Produced by New Leaf Plus gene Detection Potato and potato product NA
New Leaf Plus by Gel Recombinant DNA Techniques; (MKAK)
Electrophoresis Provisional Translation by MHLV;
NA
Page 3 – 19.
MOH G03-146 (2) Detection of Event-Specific Potato Testing for Food Produced by New Leaf Y gene Detection Potato and potato product NA
New Leaf Y by Gel Electrophoresis Recombinant DNA Techniques; (MKAK)
Provisional Translation by MHLV;
Page 3 – 19. NA
MOH G03-211 (1) DNA Extraction Using QIAGEN QIAGEN DNeasy® Tissue Kit Extraction meat Not Applicable All animal tissues and its 1.0 x 10 ng/µl
-1
DNeasy® Tissue Kit DNeasy® Tissue Handbook product (raw meat/poultry, (MKKM Miri)
burger, minced 1.0 ng/µl
meat/poiultry, sausage, (MKAK) NA A
meatball)
MOHG03-211 (3) DNA Extraction using DNeasy® QIAGEN Dneasy® mericonTM Food Raw, semi-processed Not Applicable Raw, semi-processed and NA
mericonTM Food Kit Kit Handbook and processed food processed food (cereal & (MKKM Perlis)
cereal product, vegetables 1.0 x 10-1 ng/µl
& vegetables product, fruit (MKKM Selangor)
& fruit product and meat & 1.0 x 10-1 ng/µl
meat product) (MKKM Miri) NA A NA A
1.0 ng/µl
(MKAK)
MOH G03-221(1) Detection of Mammalian DNA by Rodriguez, M.A. et al., 2004. Mammalian DNA Detection Meat and meat product 1.0 x 10-6 ng/µl
Real-Time PCR (qPCR) - SYBR TaqMan Real-Time PCR for the (MKKM Selangor)
Green Detection and Quatification of Pork
in Meat Mixtures. Meat Science 70 NA
(2005) 113 – 120.
MOH G03-242(1) Detection of Porcine DNA using Rodriguez M.A et al (2004) TaqMan Pork DNA Detection Meat and meat product
Real-Time PCR (Light Cycler® real-time PCR for the detection and
Taqman® Master) quantification of pork in meat
mixtures
MOH G03-243(1) Detection of Bubalus bubalis DNA in Use of duplex polymerase chain Water Buffalo DNA Detection Meat and meat product
Animal Tissue/Meat Products by reaction (duplex-PCR) technique to
Gel Electrophoresis identify bovine and water buffalo
milk in making mozzarella cheese
by Stefano Rea, Koichi Chikuni,
Raffaella Branciari, Ram Sukasi
Sangamaya, David Ranucci and
Paolo Avellini
MOH G03-243 (2) Detection of Bubalus Bubalis DNA Buffalo bulletin, Identification and Water Buffalo DNA Detection Meat and meat product 1.0 x 101 ng/µl
using Real Time PCR differentiation of Cattle and Buffalo (MKAK)
processed meat by duplex PCR
(Rohita Gupta, D.N.Rank & C.G. NA
Joshi). Vol 31 No 1 March 2012
MOH G03-243 (3) Detection of Water Buffalo (Bubalus Gorban, E.Z. et al., 2011. Molecular Water Buffalo DNA Detection Meat and meat product 1.0 x 10-5 ng/µl
bubalis) DNA by Real-Time PCR Traceability of the Species Origin of (MKKM Selangor)
(qPCR) - SYBR Green Meats using Multiplex PCR. African
Journal of Biotechnology Vol. 10(73) NA
pp.15461-16465.
MOH G03-244 (1) Detection of Gallus gallus Goren, A.C., 2013. Halal Food and Chicken DNA Detection Raw meat, semi prcesses, 3.55 x 10-2 ng/µl
domesticus (Chicken) DNA in Metrology; International 2nd Halal processed & highly (MKAK)
Animal Tissue/Meat Products by and Healthy Food Congress; 97-107 processed food A
Gel Electrophoresis
MOH G03-245 (1) Detection of Bovine DNA using Real Soichi Tanabe, Makiko Hase, Takeo Bovine (Cattle and Detection Meat and meat product 1.0 x 10-4 ng/µl
Time PCR Yano, Masahiko Sato, tatsuya Water Buffalo) DNA (MKAK)
Fujimura, Hiroshi Akiyama (7
December 2007); Biosci.
Biotechnol. Biochem, 71 (12) Pg.
3131-3135; A Real-Time A
Quantitative PCR Detection Method
for Pork, Chicken, Beef, Mutton and
Horseflesh in Food
MOH G03-247(1) Detection of Cattle (Bos taurus) Gorban, E.Z. et al., 2011. Molecular Cattle DNA Detection Meat and meat product 1.0 x 10-1 ng/µl
DNA by Real-Time PCR (qPCR) - Traceability of the Species Origin of (MKKM Selangor)
SYBR Green Meats using Multiplex PCR. African
Journal of Biotechnology Vol. 10(73) NA
pp.15461-16465
MOH G03-248(1) Detection of Goat (Capri hircus) African Journal of Biotechnology, Goat DNA Detection Meat and meat product 1.0 x 10-4 ng/µl
DNA by Real-Time PCR (qPCR) - Vol. 10 (73), pg 15461-16465. (MKKM Selangor)
SYBR Green NA
MOH G03-249(1) Detection of Sheep (Ovis aries) Biochem., 71(12) pg 3131-3135. Sheep DNA Detection Meat and meat product 1.0 x 10 ng/µl
-5
DNA by Real-Time PCR (qPCR) - (MKKM Selangor)

SYBR Green NA

FOOD INDUSTRIAL & ENVIRONMENTAL POLLUTION (HEAVY METALS)
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
DOC. NO TEST METHOD REFERENCE PARAMETER FOOD MATRIX LOQ (mg/kg)
IPOH
MIRI
MOH H03-001 The Determination of Total Mercury in Food by MS 954 : Part 13, 1989 Total Mercury Perishable and non- 0.04 (MKAK)
Using Atomic Absorption Spectrometer- Flow perishable food** A
Injection Analysis System (AAS- FIAS)
MOH H03-002 The Determination of Heavy Metal in Food by AOAC 999.10, 2000 Plumbum Perishable and non- 0.4 (MKKMKEL) A
Using Inductively Coupled Plasma- Optical perishable food (except salt 0.5 (MKKM Perlis) A
Emission Spectrometer (ICP-EOS) and sugar)**
Cadmium 0.07 (MKAK)
0.2 (MKKMKEL) A
A A
0.5 (MKKM Perlis)
Total Arsenic 0.8 (MKKMKEL) NA
NA
2.5 (MKKM Perlis)
Antimony 0.75 (MKKM Perlis) A
Stanum 10 (MKAK) A
25 (MKKM Perlis) A
MOH H03-003 The Determination of Lead, Cadmium and AOAC 25.107, 1984 Plumbum Perishable and non- 0.1 (MKA JB)
Arsenic in Food by Graphite Furnace Atomic perishable food ** 0.03 (MKAK)
Absorption Spectrometer (GFAAS) 0.1 (MKKM Phg) A NA A
0.2 (MKKM Tganu)
Total Arsenic 0.10 (MKA JB)

A
Cadmium 0.05 (MKKM Phg)

0.04 (MKA JB) NA A A
0.02 (MKKM Tganu)
MOH H03-004 The Determination of Metals (Plumbum, AOAC 25.107, 1984 Plumbum All type of food (except salt, 2.5 (Terengganu)
Cadmium, Antimoni) in Food by Atomic oil & fat)** 0.4 (MKAKB) NA
Absorption Spectrometry AAS-Flame
Cadmium 0.75 (Terengganu)
0.1 (MKAKB) NA
MOH H03-006 The Determination of Heavy Metals In Food AOAC 999.10, 2000 Total Arsenic All type of Food except salt** 0.05
Using Inductively Coupled Plasma-Mass (MKKM Selangor & MKKM
Spectrometry (ICP-MS) Srwk) NA NA NA
0.01 (MKAK)
Plumbum 0.05
(MKKM Selangor & MKKM NA NA
Srwk)
Antimony 0.05
(MKKM Selangor) NA
Total Mercury 0.01

(MKKM Selangor & MKKM NA NA
Srwk)
Stanum 0.05
NA
(MKKM Selangor)
Cadmium Fish and Fish Products 0.05
(MKKM Selangor)
0.01 (MKKM Srwk) NA NA A
0.01 (MKAK)
MOH H03-007 The Determination of Heavy Metals In Edible AOAC 999.10, 2000 Total Arsenic Edible Bird's Nest 0.01
Bird's Nest Using Inductively Coupled Plasma- A
Mass Spectrometry (ICP-MS)
Plumbum
A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
DOC. NO TEST METHOD REFERENCE PARAMETER FOOD MATRIX LOQ (mg/kg)
IPOH
MIRI
MOH H03-007 The Determination of Heavy Metals In Edible AOAC 999.10, 2000 Edible Bird's Nest 0.01
Bird's Nest Using Inductively Coupled Plasma-
Mass Spectrometry (ICP-MS)
Antimony
A
Total Mercury
A
Cadmium
A
MOH H03-008 The Determination of Methyl Mercury In Fish by In-House Method, Based on Atomic Methyl Mercury Fish & Fish Products 0.1 (MKAK)
Using High Performance Liquid Chromatography Spectroscopy , Vol. 32(3), May/June
- Inductively Coupled Plasma-Mass 2011 A
Spectrometry (HPLC-ICP-MS)
MOH H03-009 The Determination of Arsenic Speciation In Fish MKAK - Not offered to client yet Arsenic (III) & Arsenic (V) Fish & Fish Products
by Using High Performance Liquid
Chromatography - Inductively Coupled Plasma-
Mass Spectrometry (HPLC-ICP-MS)
MOH H03-010 The Determination of Arsenic Speciation In Rice Journal of Chemosphere 75 (2009) Arsenic (III) & Arsenic (V) Rice and Seaweed
by Using High Performance Liquid 1065–1073.
Chromatography - Inductively Coupled Plasma-
Mass Spectrometry (HPLC-ICP-MS)
MOH H03-011 The Determination of Antimony In Food by Using AOAC 999.10, 2000 Antimony (Sb) Soft Drink 0.05 (MKAK)
Inductively Coupled Plasma-Mass Spectrometry A
(ICP-MS)
MOH H03-012 The Determination of Tin (Sn) in food by using Journal of Microchemical, 94 (2010) Tin (Sn) Fish 10 (MKAK)
Inductively Coupled Plasma-Optical Emission 171-174 A
Spectrometer (ICP-EOS)
MOH H03-013 The Determination of Arsenic Speciation In Fish Journal of AOAC International, Vol. 97, Arsenic (III) & Arsenic (V) Fish Arsenic (III) 0.005 Arsenic
& Seaweed by Using Liquid-Liquid Extraction No. 3, 946 – 955. (V) 0.005
and High Performance Liquid Chromatography - (MKAK)
Inductively Coupled Plasma-Mass Spectrometry NA A
(HPLC-ICP-MS)
MOH H03-015 The Determination of Heavy Metals In Food Total Arsenic FOOD** 0.01
(Post-spiked ISTD) Using Inductively Coupled NA
Plasma-Mass Spectrometry (ICP-MS)
Plumbum
NA
Antimony
NA
Total Mercury
NA
Cadmium
NA

STANDARD AND NUTRITIONAL LABELLING
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
TERENGGANU
KEBANGSAAN,
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
DOC. NO TEST METHOD REFERENCE PARAMETER FOOD MATRIX LOQ
MIRI
MOH J03-001 Determination of Moisture in Food Based On Training Material Provided Moisture All type of foods Not Applicable
using Drying Technique (Conventional by JICA's Expert (2004) extracted from
and Vacuum Oven) Analytical Manual for Standard Tables
of Food Composition in Japan, 5th
Revised Edition (2000)
A A NA NA A NA
MOH J03-002 Detemination of Ash in Food Muffle Based On Training Material Provided Ash All type of foods Not Applicable
Furnace by JICA's Expert (2004) extracted from
Analytical Manual for Standard Tables
A NA A NA
MOH J03-003 Determination of Protein in Food Based On Training Material Provided Protein All type of foods Not Applicable
Using Kjeldahl Technique by JICA's Expert (2004) extracted from
of Food Composition in Japan, 5th A
MOH J03-004 Determination of Fat in Food Using Based On Training Material Provided Fat All type of foods Not Applicable
Acid Hydrolysis Technique by JICA's Expert (2004) extracted from
MOH J03-005 Determination of Fat in Milk and Milk Based On Training Material Provided Fat Milk and Milk Products Not Applicable
Products Using Roese Gotlieb Method by JICA's Expert (2004) extracted from
MOH J03-006 Determination of Fat in Dry Food using Based On Training Material Provided Fat Dry Food Not Applicable
Soxhlet Technique by JICA's Expert (2004) extracted from
Revised Edition (2000) A A
MOH J03-007 Determination of Fat in Wet Food Based On Training Material Provided Fat Wet Food Not Applicable
using Soxhlet Technique by JICA's Expert (2004) extracted from
MOH J03-008 Overall Calculation and Interpretation Analytical Manual for Standard Tables Carbohydrate, Energy All type of foods Not Applicable
of Proximate Analysis in Food of Food Composition in Japan, 5th A
Samples Revised Edition, 2000
MOH J03-009 Determination Total Dietary Fibre in AOAC International, 16th Edition, Total Dietary Fiber All type of foods Not Applicable
Food Volume II, Section 45.4.07, Method NA
985.29 (1997)
MOH J04-010 The Determination of Alcohol (Ethyl In House method based on Ethanol Alcoholic Beverages and soft drinks Not Available
Alcohol) in beverages by Gas Instrumental Methods Of Food NA
Chromatography Analysis.
MOH J03-011 The Determination of Amino Acid in 1) AOAC Official Method 983.15, Ch. Amino Acid Bird Nest In progress
Food by Using High Performance 47, page 2-5, AOAC International,
Liquid Chromatography 16th Edition, Volume II, 1996.
2) Waters AccQ Tag Chemistry
Package, Instruction Manual, Manual
number WAT052874,Rev 0 April 1993.
MOH J03-012 The Determination of Total Alkalinity in USDAIAR, 2008 - Stuttgart National Total Alkalinity Waters samples Not Available
Water by Titration Aquaculture Research Center, SOP
WQJlNC 202.1; Date: 10/15/2008
MOH J03-013 Measurement of pH for Water AOAC International, 16th Edition, pH Water and Packaged Drinking Water Not Applicable
Volume I, Section 11.1.03, Method NA NA NA NA NA NA
973.41 (1995)
MOH J03-014 Determination of Fat in Meat and Meat Official Methods of Analysis of AOAC Fat Meat and Meat Products Not Applicable
Products Using Soxhlet Technique International,17th Edition, Volume II,
Section 39.1.08,Method 991.36. A
MOH J03-015 Determination of Minerals (Sodium, 1) Test Method The Determination of Sodium,Phosphorus,M Infant Formula and Follow up Formula Not Available
Phosphorus, Magnesium, Calcium, Sodium (Na) and Phosporus (P) In agnesium,Calcium,Pot
Potassium, Zink, Ferum) in Infant Food by Using Inductively Coupled assium,Zink,Ferum
Formula and Follow up Formula Using Plasma-Optical Emission
ICP-OES Spectrometer (ICP-OES), J04-017.
2) Charles B. Book and Kenneth J.

Fredeen. 1999. 2nd Edition. Concepts,
Instrumentation and Techniques in
Inductively Coupled Plasma Optical
Emission Spectrometry, ICP-OES
Methodology, p.4-14. Perkin Elmer
Corporation.
MOH J03-016 The Determination of Caffeine in Journal of Chemical Education, 1985, Caffeine Coffee and instant coffee 0.125% (Perlis),
Foods by Liquid Chromatography Vol. 62 ,No 5 0.01% (Kelantan),
Fd. Chem Toxicology 0.02%(MKAK), A NA NA A A A A NA
Vol. 27, No. 1 0.08% (MKAKK)
Flavoured drink 20 mg/L (MKAKK),

50mg/L (Perlis),
10 mg/L (P.Pinang),
10 mg/L (Kelantan),
0.8mg/L ( Sarawak),
A A A A A A NA A A A
2mg/L (MKAK)
5mg/l (Pahang),
100mg/L (MKAI),
0.42 mg/L (Sel)
MOH J03-017 The Determination of Sodium Chloride Eugene A. and R. F. Muraca. 1959. Sodium Chloride Salted Foods 1% (MKAK),
in Salted Foods by Using Volhard Determination of Small Amounts of 2%( Sandakan)
Method Chloride by Volhard Titration;
Evaluation of Operator Determinate A
NA A NA
end-point Error. Anal. Chim. Acta,
23(1960) 136-144.
MOH J03-018 The Determination of Percentage A) International Temperature Total Soluble Solid All types of food Not Applicable
Soluble Solid in Food by Correction Table, 1936. Int. Sugar J.
Refractometry 39, 24s, 1937.
B) Manual Instructions for Hand NA NA NA NA
Refractometer N Type Series.
MOH J03-019 The Determination of Percentage of Lawrence , J.F., JAOAC, Vol 71, No 5, Net Content Canned Fish Not Applicable
Fish in Canned Product by Drained 1988
Weight Method A NA
MOH J03-020 The Determination of Iodine Content in De Maeyer EM, Lowenstein FW and Iodine Iodised Salt 6mg/kg (Pahang),
Iodised Salt using Iodometric Titration Thilly CH – “The Control of Endemic 10mg/kg (Perlis),
by IMR Method Goiter” WHO, Geneva, 1979 15 mg/kg (Kelantan) A A A
MOH J03-021 The Determination of Iodine Content in The Chemical Analysis of Foods, Iodine Content Salt 2mg/kg ( Sarawak),
Iodised Salt Using Iodometric Titration 8th Edition 2mg/kg (P.Pinang), NA A NA A A A
(Pearson) 2mg/kg (MKAKK)
MOH J03-022 The Determination Of Acid Value In Oil MPOB Test Method p2:3:2004 - PV Edible oil Not Available
And Fat Using Titration Method Peroxide value
MOH J03-023 The Determination Of Peroxide Value MPOB Test Method p2:3:2004 - PV Edible oil Not Applicable
In Oil And Fat Using Titration Method Peroxide value NA NA
MOH J03-024 The Determination of Total Acidity in Harold Egan et al., Pearson's Total Acidity All types of food 0.2% -Sauce (MKAKB &
Food by Titration Chemical Analysis of Foods. 1981 8th Perlis)
Edition 0.6% - Sauce (Sandakan) NA NA
6.21% - Venegar
(Sandakan)
MOH J03-025 Determination of Melamine in Foods USDA/CFSAN. 2007. Laboratory Melamine Selected types of food** 0.025mg/kg (MKAJB),
by Liquid Chromatography Tandem Information Bulletin No. 4396, 0.01mg/kg (MKAK, MKAI &
Mass Spectrometry Volume 23 Kedah)
A A A NA
MOH J03-026 Reductase Test in Milk 1)Atherton, H.V. And Newlander, J.A. Reductase Test Pasteurized milk Not Applicable
Chemistry and Testing of Dairy
Products. 4th Edn. AVI, Wetsport, CT.
2) Martin R. Adams, Maurice O.2008
Food Microbiology. Moss Royal A
Society of Chemistry. United Kingdom
MOH J03-027 Determination of Protein in Food Based on Method J04-004 Protein Prepared cereal food bread , milk , Not Available
Using Kjeldahl Technique cultured milk, flour confection,
canned meat, canned meat with other
food, canned fish , canned vegetables,
canned fruits , fruit juice, salad
dressing, mayonnaise, soft drinks
A
MOH J03-028 Determination of Fat Soluble Vitamin Everlyn Goh, Tarang Nema, Antonietta Fat Soluble Vitamin Infant Formula 10mg/L
(A, E and K1) In Infant Formula Using Gledhill. Extraction and Analysis of (A,E and K1)
High Pressure Liquid Chromatography Fat-Soluble Vitamins In Fortified Food
Products and Infant Formula. Waters
Pacific Pte Ltd, Singapore; Waters NA
Corporation, Manchester, UK.
MOH J03-029 Determination of Acidity in Honey by Method for Acidity in Honey, MAFF Content of acid Honey Not Applicable
Titration Validated Method V19, April 1992 Acidity A
MOH J03-030 Determination of Water Soluble AOAC International, 18th Edition, B1, B2, B3, and B6 Infant Formula Dalam proses MV
Vitamin (B1, B2, B3 and B6) In Infant 2005 (Current through revision 2,
Formula Using Ultra High 2007), Section 50.1.08, Method NA
Performance Liquid Chromatography 986.27
(UHPLC)
MOH J03-031 Determination of Cholesterols 2008. K.Madzlan. Determination of Cholesterol content Egg 0.002g/100g
contents in Eggs using Liquid Cholesterol in several types of eggs by
Chromatography Tandem Mass gas chromatography NA
Spectrometry
MOH J03-032 Determination of Methanol In Alcoholic Fat and oils derivatives – Fatty Acid Methanol Alcoholic Beverages 0.6mg/L
Beverages Using Gas Methyl Esters (FAME) - Determination
Chromatography Flame Ionization of Methanol Content. European
Detector with Headspace Technique Standard EN14110:2003, NA A
ICS67.200.10, April 2003.
MOH J03-033 The Determination of Fruit Content in Official Method of Analysis of AOAC Fruit Content Jam Not Applicable
Jam (Fruit-Sugar Mixture) by International, 17th Edition NA NA
Refractometry
MOH J03-034 Determination of Caffeine and Coffee 1) Malaysian Standard MS 1360, Caffeine & coffee Coffee & coffee mixtures Caffeine 0.0001%; Coffee
Content in Coffee and Coffee Mixtures 1994. Penentuan Untuk Kopi content 0.01% (Perlis),
by Reflux Method and Liquid Campuran. Standards & Industrial Caffeine 0.06%, Coffee
Chromatography Research Institute of Malaysia. (2) Content 0.07% (MKAK),
Test Method J04-027: The Caffeine 0.0001%; Coffee A NA NA A
Determination of Caffeine in Food by 0.01% (MKAI)
Liquid Chromatography.
MOH J03-035 Determination of Sugars in Honey 13.1 AOAC Official Method 977.20, Fructose, Honey Fructose 0.01%,
using High Performance Liquid 2006 Glucose Glucose 0.03%,
Chromatography with Refractive Index Sucrose Sucrose 0.02%, A
Detector Maltose Maltose 0.06%
MOH J03-036 Determination of Diameter of a Raghavendra, N.V & Krishnamurthy, Diameter Jelly Not Applicable
sherical product by vernier caliper L. (2013). Engineering Metrology and
Measurement. Chapter 4 limear NA NA NA
measurement (pg.80).
MOH J03-037 Quantitative Test of Osmolarity In 11.2 Mettler S.,Rusch C.,Colombani Osmolarity Isotonic Electrolite Drink In progress
Electrolyte Drink P.C.: Osmolarity and pH of sport and
other drinks available in
Switzerland.SchwezerischeZeitschriff
furSportmedizin und Sporttraumatologi NA
54(3),92-95,2006
MOH J03-038 The Determination of Ethyl Alcohol in Application Note: Analysis of Distilled Ethyl Alcohol Alcoholic Beverages 0.3% (MKKM Sarawak)
Beverages Using Gas Spirits using an Agilent J&W DB-Wax
Chromatography Flame Ionization Ultra Inert Capillary GC Column NA
Detector with Headspace Technique
MOH J03-039 Determination of Sulfated Ash Using Official Methods of Analysis of AOAC Sulfated ash Sugar, Brown sugar and Glucose Not Applicable
Muffle Furnace International, 2006.17th Edition,
Volume II, Section 44.1.05, Method NA
900.02
MOH J03-040 Determination of Vitamin C @ Analysis of ascorbic acid, citric acid Vitamin C soft drink 2mg/L (MKKM Kelantan)
Ascorbic Acid in Soft Drink By Liquid and benzoic acid in orange juice,
Chromatography Application Note, Agilent Application NA
Solution
MOH J03-041 Determination of Ash Insoluble in Acid Official Methods of Analysis of AOAC Ash Insoluble in Acid spice Not Applicable
Using Muffle Furnace International,17th Edition, Volume
II,Section 43.1.05,Method 941.12 NA
MOH J03-042 Determination of Moisture in Honey AOAC Official Method 969.38, Moisture Honey LOD=13%
using Refractrometer Moisture in Honey, 2000 NA
MOH J03-043 Determination of Alcohol (Methanol & Chromatography 2015, 2, 691-708; Methanol & Ethyl Alcoholic Beverages LOQ: 0.025%
Ethyl alcohol) in Beverages by Gas Journal alcohol
Chromatography Flame Ionization of Food and Drug Analysis NA
Dectector with Headspace Technique 11(11):133-140
MOH J03-044 Determination of Total Milk Solids in Official Methods of Analysis of AOAC Total Milk Solids Milk and Milk Products Not Applicable
Milk and Milk Products Using Forced International,17th Edition, Volume
Air Oven Drying II,Section 33.2.44,Method 990.20 NA
MOH J03-046 Phosphatase Test in Pasteurized Milk R.Aschaffenburg and J.E.C Mullen. 1948. Phosphatase Pasteurized milk In progress
381. A Rapid and Simple Phosphatase
Test for Milk; Journal of Dairy Research
pg 58-67
MOH J03-048 Proximate Analysis by Using TGA TGA701 Thermogravimetric Analyzer Moisture All types of food Not Applicable
Instruction Manual (2003), LECO Ash NA
Corporation, Software Version 1.05.

FOOD MICROBIOLOGY
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
DOC. NO TEST METHOD PARAMETER TECHNIQUE LOD
IPOH
MIRI
MOH K03-101(1) ISO 4833-1:2013(E) Microbiology of the food chain — Horizontal Standard Plate Count Enumeration 10 CFU/g
method for the enumeration of microorganisms — Part 1: Colony NA NA NA A NA
count at 30 °C by the pour plate technique
MOH K03-101(2) ISO 4833-2:2013(E ) Microbiology of the food chain — Horizontal Standard Plate Count Enumeration 100 CFU/g
method for the enumeration of microorganisms — Part 2: Colony NA NA NA
count at 30 °C by the surface plating technique
MOH K03-102 (2) ISO 21527:2008(E) Microbiology of food and animal feeding stuffs – Yeast & mould Enumeration 100 CFU/g
Horizontal method for the enumeration of yeast and moulds – Part 2:
Colony count technique in product with water activity less than or NA
equal to 0.95
MOH K03-103 (1) ISO 9308-1:2014(E) Water Quality - Enumeration of Escherichia coli Escherichia coli / coliform Enumeration 1 CFU/100ml
and coliform bacteria Part 1- Membrane Filtration Method for waters (Water) A A A NA NA A A NA A A A A
with low bacterial background flora
MOH K03-105 (1) ISO 6888-1:1999(E) / Amd.1:2003 (E )Microbiology of food and Coagulase Positive Enumeration 100 CFU/g
animal feeding stuffs - Horizontal method for the enumeration of Staphylococci
Coagulase-positive staphylococci (Staphylococcus aureus and other A A A A A A A A A A A A A
species) Part 1: Technique using Baird-Parker agar medium
MOH K03-106(2) ISO 7899-2 : 2000(E )Water quality - Detection and enumeration of Enterococci Enumeration 1 CFU/100 ml (water)
intestinal enterococci - Part 2 : Membrane filtration method (Water)
A A A A
MOH K03-107 (1) ISO 7932:2004(E) Microbiology of food and animal feeding stuffs - Bacillus cereus Enumeration 100 CFU/g
Horizontal method for the enumeration of presumptive Bacillus A A A A A A A A A A A A A A
cereus - Colony-count technique at 30°C
MOH K04-107(2) ISO 21871:2006(E) Microbiology of food and animal feeding stuffs - Horizontal Bacillus cereus Enumeration &
method for determination of low numbers of presumptive Bacillus cereus - Most Detection
probable number technique and detection method NA
MOH K03-108 (1) ISO 6579 : 2002 (E) Microbiology of food and animal feeding stuffs - Salmonella Detection 0.04 CFU/g
Horizontal method for the detection of Salmonella spp 0.12 CFU/g (MKAJB)
A A A A A A A A A A A A A
MOH K03-108 (1) -i ISO 6579 : 2017 (E) Microbiology of the food chain - Horizontal Salmonella Detection 0.04 CFU/g
method for the detection, enumeration and serotyping of Salmonella
- Part 1: Detection of Salmonella spp. NA A NA NA A
MOH K03-108 (2) ISO 19250:2010 (E )Water Quality - Detection of Salmonella Salmonella Detection 1 CFU/100 ml (water)
(Water)
NA NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
MIRI
MOH K03-111 (1) ISO 21872-1:2007(E) Microbiology of food and animal feeding Vibrio parahaemolyticus & Detection 0.04 cfu/g
stuffs - Horizontal method for the detection of potentially Vibrio cholerae
enteropathogenic Vibrio spp — Part 1: Detection of Vibrio (MKAJB)
parahaemolyticus and Vibrio cholerae V.cholerae: 0.20
cfu/g A A A A A A A A A A A A A
V.parahaemolyticus:
0.12 cfu/g
MOH K03-111 (1)-i ISO 21872-1:2017(E) Microbiology of the food chain - Horizontal Vibrio parahaemolyticus, Vibrio Detection 0.04 CFU/g
method for the determination of Vibrio spp — Part 1: Detection of cholerae and Vibrio vulnificus
potentially enteropathogenic Vibrio parahaemolyticus, Vibrio NA A NA A
cholerae and Vibrio vulnificus
MOH K03-111 (2) ISO 21872-2:2007 Microbiology of food and animal feeding stuffs - Other than Vibrio Detection 0.04 CFU/g
Horizontal method for the detection of potentially enteropathogenic parahaemolyticus & Vibrio
Vibrio spp - Part 2 : Detection of species other than Vibrio cholerae A A A A A
parahaemolyticus and Vibrio cholerae
MOH K03-112 ISO 16654:2001(E) Microbiology of food and animal feeding stuffs - Escherichia coli 0157 Detection 0.04 CFU/g
Horizontal method for the detection of Escherichia coli 0157 0.20 CFU/g (MKAJB) NA NA A A A A A A
MOH K03-113 (1) ISO 11290-1:1996 /Amd.1:2004(E) Microbiology of food and animal Listeria monocytogenes Detection 0.04 CFU/g
feeding stuffs - Horizontal method for the detection and enumeration 0.38 CFU/g (MKAJB)
of Listeria monocytogenes- Part 1: Detection Method A A A A A A A A A A A A A
MOH K03-113 (1)-i ISO 11290-1:2017(E) Microbiology of food and animal feeding stuffs Listeria monocytogenes Detection 0.04 CFU/g
- Horizontal method for the detection and enumeration of Listeria
monocytogenes and of Listeria spp.- Part 1: Detection Method NA NA A
MOH K03-113 (2) ISO 11290-2:1998/Amd.1:2004(E) Horizontal Method for The Listeria monocytogenes Enumeration 100 CFU/g
Detection and Enumeration of Listeria monocytogenes- Part 2: A A A NA NA A A A
Enumeration Method
MOH K03-113 (2)-i ISO 11290-2:2017 (E) Microbiology of food and animal feeding stuffs Listeria monocytogenes Enumeration 100 CFU/g
- Horizontal method for the detection and enumeration of Listeria
monocytogenes and of Listeria spp.- Part 2: Enumeration Method NA
MOH K03-114 (1) ISO 10272-1:2006(E) Microbiology of food and animal feeding stuffs Campylobacter spp. Detection LOD : 0.04 cfu/g
- Horizontal method for detection and enumeration of Campylobacter
spp - Part 1: Detection Method NA A A A A A A
MOH K03-114 (2) ISO 10272-2:2006 (E ) Microbiology of food and animal feeding Campylobacter spp. Enumeration 100 CFU/g
stuffs - Horizontal method for detection and enumeration of
Campylobacter spp. - Part 2 : Colony count-techniques
MOH K03-115 ISO/TS 22964:2006(E) IDF/RM 210 :2006(E) Milk and milk products Enterobacter sakazakii Detection 0.04 CFU/g
- Detection of Enterobacter sakazakii 0.26 CFU/g (MKAJB)
A A A A A NA A A A A A A
MOH K03-116 (1) ISO 15214:1998(E ) Microbiology of food and animal feeding stuffs- Lactic Acid Bacteria Enumeration 10 CFU/g
Horizontal method for the Enumeration of Mesophilic Lactic acid 100CFU/g (P.Pinang) A NA NA A NA A NA
bacteria- Colony Count Technique at 30°C
MOH K03-117 (1) ISO 7937:2004(E) Microbiology of food and animal feeding stuffs – Clostridium perfringens Enumeration 100 CFU/g
Horizontal method for the enumeration of Clostridium perfringens-
A A A A
Colony Count Technique
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
MIRI
MOH K03-117(2) ISO 14189: 2013 (E ) Water quality- Enumeration of Clostridium Clostridium perfringens Enumeration 1 CFU/100 ml (water)
perfringens- Method using membrane filtration (Water) A A
MOH K03-119 ISO 21567:2004 (E) Microbiology of food and animal feeding stuffs- Shigella spp. Detection 0.04 CFU/g
Horizontal methods for the detection of Shigella spp. NA A A A A A A A
MOH K03-121 (1) ISO 4831:2006(E) Microbiology of food and animal feeding stuffs - Coliform Enumeration 0.1MPN/g
Horizontal method for the detection and enumeration of coliforms -
A NA A A A A A A A A A
Most probable number technique
MOH K03-122 (1) ISO 7251:2005(E) Microbiology of food and animal feeding stuffs- Escherichia coli Enumeration 0.1MPN/g
Horizontal method for detection and enumeration of presumptive A A A A A A A A A A A
Esherichia coli - Most probable number technique
MOH K03-122 (2) ISO 16649-1:2001 (E )Microbiology of food and animal feeding stuffs Escherichia coli Enumeration 100 CFU/g
– Horizontal method for the enumeration of ß-glucuronidase-positive
Escherichia coli Part 1: Colony count technique at 44˚C using
membranes and 5-bromo-4-chloro-3-indoyl ß-D-glucuronide
MOH K03-122 (3) ISO 16649-2:2001 (E )Microbiology of food and animal feeding stuffs Escherichia coli Enumeration 100 CFU/g
– Horizontal method for the enumeration of ß-glucuronidase-positive
Escherichia coli. Part 2: Colony count technique at 44°C using 5-
bromo-4-chloro-3-indoyl ß-D-glucuronide
MOH K03-122 (4) ISO 16649-3:2015 (E ) Microbiology of food and animal feeding Escherichia coli Enumeration 0.1MPN/g
stuffs – Horizontal method for the enumeration of ß-glucuronidase-
positive Escherichia coli Part 3 : Detection and most probable
number technique using membranes and 5-bromo-4-chloro-3-indoyl
ß-D-glucuronide
MOH K03-125 (1) ISO 21528-1:2004 (E) Microbiology of food and animal feeding stuffs Enterobacteriaceae Detection 0.04 CFU/g
-- Horizontal method for the detection and enumeration of
Enterobacteriaceae -- Part 1: Detection and Enumeration by MPN NA NA
Technique with pre-enrichment
MOH K03-125(2) ISO 21528-2:2004 (E) Microbiology of food and animal feeding stuffs Enterobacteriaceae Enumeration 100 CFU/g
Enterobacteriaceae -- Part 2: Colony Count Method NA
MOH K03-125(2) ISO 21528-2:2004 (E) Microbiology of food and animal feeding stuffs Enterobacteriaceae Enumeration 100 CFU/g
Enterobacteriaceae -- Part 2: Colony Count Method NA NA A
MOH K03-126(1) ISO 20128:2006(E) IDF 192:2006(E) - Milk products - Enumeration Lactobacillus acidophilus Enumeration 100 CFU/g
of presumptive Lactobacillus acidophilus on a selective medium -
Colony count technique at 37̊C A NA A A NA
MOH K03-127 ISO13720:2010(E ) Meat and meat products - Enumeration of Pseudomonas spp Enumeration 100 CFU/g
presumptive Pseudomonas spp
NA NA NA NA
MOH K03-128 ISO 16266:2006(E) Water quality - Detection and enumeration of Pseudomonas aeruginosa Enumeration 1 CFU/100 ml (water)
Pseudomonas aeruginosa - Method by membrane filtration (Water)
A A A NA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
MIRI
MOH K03-129 ISO 10273:2003(E) Microbiology of food and animal feeding stuffs - Yersinia enterocolitica Detection 0.04 CFU/g
Horizontal method for the detection of presumptive pathogenic A NA
Yersinia enterocolitica
MOH K03-130(1) ISO 15213: 2003 (E 0 Microbiology of food animal feeding stuffs - Sulfite Reducing Anaerobes Enumeration 100 CFU/g
Horizontal method for the enumeration of sulfite-reducing bacteria NA
growing under anaerobic conditions.
MOH K03-130(2) ISO 6461-2: 1986 (E ) Water quality - Detection and enumeration of Sulfite Reducing Anaerobes Enumeration 1 CFU/100 ml (water)
the spores of sulfite reducing anaerobes (Clostridia) (Water)
Part 2 : Method by membrane filtration NA A A
MOH K03-136 (1) ISO 7889:2003 (E ) /IDF 117:2003 (E ) Yogurt - Enumeration of Lactobacillus delbrueckii subsp. Enumeration 100 CFU/g
characteristic microorganisms - Colony-count technique at 37°C bulgaricus and Streptococcus
thermophilus (Yogurt) A
MOH K03-136 (2) ISO 9232: 2003 (E ) / IDF 146: 2003 (E ) Yogurt - Identification of Detection 0.04 CFU/g
characteristic microorganisms (Lactobacillus delbrueckii subsp.
bulgaricus and Streptococcus thermophilus) A
MOH K03-201 AOAC Official Method 990.12 Aerobic Plate Count in Foods - 3MTM Aerobic Count Plates Enumeration 10 CFU/g
PetrifilmTM A A A A A A A A A A A NA A A
MOH K03-202(1) AOAC Official Method 997.02 Yeast and Mould - 3M™ Petrifilm™ Yeast & mould Enumeration 10 CFU/g
NA NA A A A A NA A
MOH K03-202(2) AOAC Official Method 2014.05 Enumeration of Yeast and Mould in Yeast & mould Enumeration 10 CFU/g
Food -3M™ Petrifilm™ Rapid Yeast and Mould Count Plate A
MOH K03-203 AOAC Official Method 991.14 Coliform and Escherichia coli counts in Escherichia coli / coliform Enumeration 10 CFU/g
Foods - 3MTM PetrifilmTM A A A A A A A A A A A A A A
MOH K03-205 AOAC Official Method 2003.07 Enumeration of staphylococcus Staphylococcus aureus Enumeration 10 CFU/g
aureus in selected types of processed and prepared foods - 3M™
A A A A A A A A A A A A A A
Petrifilm™
AOAC 2003.08 Enumeration of staphylococcus aureus in selected Staphylococcus aureus Enumeration 10 CFU/g
dairy foods - 3M™ Petrifilm™ A A NA A A A A A A A A A A
AOAC 2003.11 Enumeration of staphylococcus aureus in selected Staphylococcus aureus Enumeration 10 CFU/g
meat, seafood and poultry - 3M™ Petrifilm™ A A NA A A A A A A A A A A
MOH K03-225 AOAC Official Method 2003.01 Enumeration of Enterobacteriaceae Enterobacteriaceae Enumeration 10 CFU/g
in selected foods A NA NA A NA A
MOH K03-301 (2) AS 1766.2.1-1991 Examination for specific organisms - Standard Standard Plate Count Enumeration 100 CFU/g
Plate Count A
MOH K03-303 AS 1766.2.3 – 1992 Examination for specific organisms – Coliforms Coliform & Escherichia coli Enumeration 3 MPN/g (food)
and Escherichia coli A A A A A A A
MOH K03-303 AS 1766.2.3 – 1992 Examination of Coliforms and Escherichia coli - Coliform & Escherichia coli Enumeration 1 MPN/100 ml (water)
MPN Technique (Water samples) A A A A A A A NA
MOH K03-310 AS 1766.2.9 – 1997 Examination for specific organisms – Vibrio Vibrio parahaemolyticus Enumeration 3 MPN/g (food)
parahaemolyticus NA NA NA A NA
MOH K03-401 MMEF Part 4 Sect.1 Enumeration of Mesophilic Aerobes (Total Plate Standard Plate Count Enumeration 100 CFU/g
Count) A NA A A A A A A A NA A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
MIRI
MOH K03-421 MMEF Part 4 Section 2 Enumeration of Fecal Coliform -MPN Feacal Coliforms Enumeration 3 MPN/g (food)
Technique NA NA NA
MOH K03-602 Method for the enumeration of Yeast and Mold Count in Foods - Yeast & mould Enumeration 100 CFU/g
using Compact Dry Nissui Kit A A
MOH K03-607 Method : Determination of the Emetic Toxin Cereulide by Liquid Bacillus emetic toxin Enumeration 50ug/kg
Chromatography Mass Spectrometry (LCMS)
MOH K03-624 KKM In house: Detection of Brucella spp. in Milk Brucella spp. Detection 0.04 CFU/g
A
MOH K03-706 APHA 9230 C Standard Methods for the Examination of Water and Enterococcus Detection 1 CFU/100 ml (water)
Wastewater. Faecal Streptococcus and Enterococcus Groups- A
Membrane Filtration Techniques.
MOH T03-001 Antimicrobial Susceptibility Testing Using Salmonella & Escherichia coli Enumeration
Disk Diffusion Method NA NA NA
MOH T03-001 Antimicrobial Susceptibility Testing Using Salmonella & Escherichia coli Enumeration
Minimum Inhibitory Concentrations (MICs) Method By Sensititre® NA NA NA
Plate
MOH Bacterial identification by MALDITOF Salmonella & Escherichia coli Detection

NA
MOH K04-117 Water Quality -Enumeration Of Clostridium perfringens-Method Clostridium perfringens Membrane 10 CFU/100 ml
NA
Using Membrane Filtration Filtration
MOH K04-128 Water Quality -Detection and enumeration of Pseudomonas Pseudomonas aeruginosa Membrane 10 CFU/100 ml
NA
aeruginosa -Method by membrane filtration Filtration

MYCOTOXIN
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg)
MOH L03-001 Determination of Aflatoxin B1, AOAC Official Method 991.31 Aflatoxin B1 Peanuts, Treenuts 0.8
A A A A NA A A A A
B2, G1 and G2 in Nuts, Cereal, and VICAM AflaTest Instruction (e.g almond,
Fish and their products by using Manual Method Number 5.4 and Aflatoxin B2 hazel & pistachio), 0.4
Immunoaffinity Column Clean 5.12 Rice, Cereal & A A A A NA A A A A
Up and PHRED Fish Products
Aflatoxin G1 0.8
A A A A NA A A A A
Aflatoxin G2 0.4
A A A A NA A A A A
MOH L03-002 Determination of Aflatoxin B1, VICAM AflaTest Instruction Aflatoxins B1 Chillies and Chilli 0.8
A A A A NA A A
B2, G1 and G2 in Spices By Manual Method Number 5.10 Powder
Using Immunoaffinity Column and 5.13 Aflatoxins B2 0.4
and PHRED A A A A NA A A
Aflatoxins G1 0.8
A A A A NA A A
Aflatoxins G2 0.4
A A A A NA A A
MOH L03-003 Determination of Aflatoxin B1, AOAC Official Method 991.31 Aflatoxin B1 Peanuts 0.8
A
B2, G1 and G2 in Peanuts by and VICAM AflaTest Instruction
using Immunoaffinity Column Manual Method Number 4.3 and Aflatoxin B2 0.25
Clean Up and TFA 5.3 A
Aflatoxin G1 0.8
A
Aflatoxin G2 0.25
A
MOH L03-004 Determination of Zearalenone in VICAM ZearalaTest Instruction Zearalenone Cereal Flour, Rice, 18
Cereal and Cereal Products by Manual Method Number 5.3 Wheat and Wheat
using Immunoaffinity Column Products NA A A A A
Clean Up
MOH L03-005 Determination of Ochratoxin A in VICAM OchraTest Instruction Ochratoxin A Rice, Wheat, 0.5
Cereal and Cereal Products by Manual Method Number 5.8 Cereals
using Immunoaffinity Column NA A NA A NA A A A
Clean Up and HPLC
MOH L03-006 Determination of Ochratoxin A in VICAM OchraTest Instruction Ochratoxin A Coffee 0.8
Coffee by using Immunoaffinity Manual Method Number 5.4
Column Clean Up NA NA NA NA A A A
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg)
MOH L03-007 Determination of Aflatoxin M1 in VICAM AflaTest Instruction Aflatoxin M1 Milk and Milk 0.05
Liquid Milk by using Manual Method Number 5.6 Product ( ready to
Immunoaffinity Column Clean drink- not including
Up Infant Formula, A A A A A A A A
powdered milk and
canned milk)
MOH L03-008 Determination of Deoxynivalenol VICAM DONTest HPLC Deoxynivalenol Cereal Flour, Rice, 100,
in Cereal and Cereal Products Instruction Manual Method Wheat and Wheat 75 (MKAK)
by using Immonuaffinity Column Number 4.1 Products, NA A
Clean Up breakfast cereal
MOH L03-009 Determination of Ochratoxin A in VICAM OchraTest Instruction Ochratoxin A Chilli and chilli 0.5
Spices by Using Immunoaffinity Manual Method products
Column Clean Up NA
MOH L03-010 Determination of Ochratoxin A in VICAM OchraTest Instruction Ochratoxin A Fruits & its product 0.7
fruits by using immunoaffinity Manual Method NA
column clean up
MOH L03-011 The Determination of Aflatoxin Kit Instruction Manual Total Aflatoxin Peanuts, Treenuts 4.00 / 10.00
By Using Agrastrip test Kit (e.g almond,
hazel & pistachio),
Cereal NA A A NA A
MOH L03-012 Determination of Fumonisin B1 Agilent Technologies Fumonisin B1 Maize and maize 80
and B2 in Maize and Maize Application Note. Publication products A
Product By Using no.5990-6560 LC-MS/MS
Immunoaffinity Column Clean Fumonisin B2 85
Up A
MOH L03-013 The Determination of Patulin in Journal of AOAC, Vol.90, Patulin Apple Juice 20
Apple Juice by Multifunctional No.1,2007
Column Clean Up NA A
MOH L03-014 Determination of Aflatoxin M1 in Journal of Food Control, 50 Aflatoxin M1 Milk powder for 0.25
Milk Powder By Using (2015), page 467-471 regular
Immunoaffinity Column Clean consumption (not
Up for infant, children NA A
and special need)
MOH L03-015 Determination of Citrinin in VICAM CitriTest Instruction Citrinin Cereal Flour 100
Cereal and Cereal Products By Manual, Method 5.3
Using Immunoaffinity Column NA
Clean Up and UHPLC
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
IPOH
MIRI
(µg/kg)
MOH L03-016 Determination of Aflatoxin M1 in Journal of Food Chemistry, 126 Aflatoxin M1 Milk Powder for 0.01
Milk Powder for Infants Formula (2011), page 737-744 Infants Formula
and Follow-up Formula By and Follow-up
Using Immunoaffinity Column Formula NA NA
Clean Up
MOH L03-017 Determination of Aflatoxin B1 in Journal of Food Chemistry, 126 Aflatoxin B1 Cereal-based 0.05
Cereal-based Food for Infants (2011), page 737-744 Food for Infants
and Young Children By Using and Young
Immunoaffinity Column Clean Children NA
Up
MOH L03-011 Qualitative Determination of Kit Instruction Manual Total Aflatoxin Peanut, Treenuts LOD
Aflatoxin By Using Agrastrip (e.g almond, hazel 4.00 / 10.00
Test Kit & Pistachio), A
cereal

FOOD CONTACT MATERIALS
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
DOC. NO TEST METHOD REFERENCE PARAMETER MATRIX
IPOH
MIRI
(mg/kg)
MOH M03-001 Identification of Packaging Material Manual Thermo Nicolet 5700 FTIR Material Identification All type of plastic NA
Using Fourier Transform Infrared packaging, seaweed &
Spectroscopy (FT-IR) dried bean curd sheets NA A
(fucuk)
MOH M03-002 Spectrum Identification of Rice Using Manual Thermo Nicolet 5700 FTIR Fake Rice Raw Rice NA
Fourier Transform Infrared
Spectrometer (FTIR) NA NA
MOH M03-003 Detection of Plastic Residue in Cooking In house developed method with no Plastic Residue in Oil Cooking oil used for frying LOD (PE) : 100 mg/L
Oil reference 1) Polyethylene (PE) NA A
2) Polypropylene (PP) LOD (PP): 80 mg/L

NA A
MOH M03-004 Determination of Residual Styrene The Pharmaceutical Society of Japan 1. Toluene Any containers, packaging LOQ : 10 mg/kg
Monomer and Other Volatile Organic (Hygiene Test Method Note) materials, kitchenware and A
Compounds (VOCs) in Food Contact 2. Ethylbenzene tableware made of LOQ : 10 mg/kg
Materials using Gas Chromatography POLYSTYRENE (PS) A
(Material Test) plastic materials
3. iso-Propylbenzene LOQ : 10 mg/kg
A
4. n-Propylbenzene LOQ : 10 mg/kg
A
5. Styrene LOQ : 10 mg/kg
A
MOH M03-005 Determination of Residual Bisphenol A, Specification and Standards for foods, 1. Phenol Feeding bottle LOQ : 8 mg/kg, SEL 10mg/kg
Phenol, 4-tert-butylphenol and their containers and packages etc. made from NA A
Diphenylcarbonate in Food Contact (Based on the Food Sanitation Law), 2. Bisphenol A POLYCARBONATE (PC) LOQ : 6 mg/kg, SEL 10mg/kg
Materials using High Performance Japan Food Hygiene Association, plastic NA A
Liquid Chromatography (Material Test) 1992
3. 4-tert-butylphenol LOQ : 4 mg/kg, SEL 10mg/kg
NA A
4. Diphenylcarbonate SEL 10mg/kg
NA NA
MOH M03-006 Determination of Plasticizers in Food Specification and Standards for foods, 1. Diethyl phthalate (DEP) Any containers, packaging 70.0 mg/kg
Contact Materials using Gas their containers and packages etc. materials, kitchenware and A
Chromatography (Material Test) (Based on the Food Sanitation Law), 2. Di-iso-propyl phthalate (DiPP) tableware made of 65.8 mg/kg
Japan Food Hygiene Association, POLYSTYRENE (PS) / A
1992 POLYCARBONATE (PC) /
3. Di-n-propyl phthalate (DPP) POLYVINYL CHLORIDE 56.4 mg/kg
A
(PVC) / POLYVINYLIDINE
4. Di-iso butyl phthalate (DiBP) CHLORIDE (PVdC) plastic 38.0 mg/kg
A
materials
5. Di-n-butyl sebacate (DBS) 94.4 mg/kg
A
6. Butyl phthalyl butyl glycolate (BPBG) 157.6 mg/kg
A
7. Di-hexyl phthalate (DHxP) 42.6 mg/kg
A
8. Di-cylohexyl phthalate (DCHP) 41.0 mg/kg
A
9. Tri-n-butyl trimellitate (TBTM) 74.8 mg/kg
A
10. Di-2-ethylhexyl azelate (DEHA8) 37.2 mg/kg
A
11. Dimethyl phthalate (DMP) 84.2 mg/kg
A
12. Di-n-butyl phthalate (DnBP) 47.2 mg/kg
A
13. Dipentyl phthalate (DPeP) 49.4 mg/kg
A
14. Acetyl-tri-n-butyl citrate (ATBC) 100.0 mg/kg
A
15. Butyl benzyl phthalate (BBP) 46.4 mg/kg
A
16. Di-2-ethyl hexyl adipate (DEHA) 43.2 mg/kg
A
17. Tri-2-ethylhexyl phthalate (TOP) 61.6 mg/kg
A
18. Di-2-ethylhexyl phthalate (DEHP) 30.0 mg/kg
A
19. Di-n-octyl phthalate (DnOP) 27.6 mg/kg
A
20. Tri-2-ethylhexyl trimellitate (TOTM) 157.6 mg/kg
A
MOH M03-007 The Determination of Plumbum and AOAC 999.10, 2000 1) Plumbum Plastic Food Contact 25 mg/kg
Cadmium In Plastic Food Contact Materials NA NA
material by Using Inductively Coupled
Plasma-Optical Emission Spectrometer 2) Cadmium
(Material Test) NA NA
MOH M03-008 Determination of Chromium in Food Corrosion-induced release of Chromium Stainless Steel 0.006 mg/kg
Simulants using Inductively Coupled chromium and iron from ferritic
Plasma-Optical Emission Spectrometer stainless steel grade AISI 430 in
(ICP-OES) (Migration Test) simulated food contact, Journal of
Food Engineering, 87 (2008) 291-300. NA
G. Herting, I. Odnevall Wallinder, C.
Leygraf.
Simulant 10% Ethanol

Determination of Melamine (2,4,6- A
LOQ : 0.5 mg/kg @ 0.08 mg/dm2
triamino-1,3,5-triazine) in Food
MOH M03-009 Simulants Using High Performance DD CEN/TS 13130-27:2005 Melamine Melamine-ware
Liquid Chromatography (Migration
Test) Simulant 3% Acetic Acid
NA
LOQ : 0.5 mg/kg @ 0.08 mg/dm2
MOH M03-010 Ceramic ware, glass-ceramic ware and MS ISO 6486-1:2003, MOD 1. Lead (Pb) Ceramic ware Simulant 4% Acetic Acid
glass dinnerware in contact with food – 1) LOQ Lead (Pb) : 0.01 mg/L @ A A A
Release of lead and cadmium (based 0.002 mg/dm2
on MS ISO 6486-1:2003)
2. Cadmium (Cd) 2) LOQ Cadmium (Cd) : 0.001 mg/L @
0.0002 mg/dm2 NA A A NA A
MOH M03-011 Determination of Phenol Compounds in DD CEN/TS 13130-13:2005 Phenol Compounds Any containers, packaging Simulant 10% Ethanol
Food Simulants using High 1) Bisphenol A materials, kitchenware and 1) Bisphenol A : 0.05 mg/kg @ 0.008
Performance Liquid Chromatography 2) Phenol tableware made of mg/dm²
(Migration Test) 3) 4-tert-butylphenol POLYCARBONATE (PC) 2) Phenol : 0.1 mg/kg @ 0.017
plastic materials except mg/dm²
feeding bottle 3) 4-tert-butylphenol : 0.05 mg/kg @
0.008 mg/dm²
Simulant 3 % Acetic Acid

1) Bisphenol A : 0.05 mg/kg @ 0.008
mg/dm²
2) Phenol : 0.1 mg/kg @ 0.017
mg/dm²
3) 4-tert-butylphenol : 0.05 mg/kg @
0.008 mg/dm²
NA
MOH M03-012 Determination of Acrylonitrile in Food The Pharmaceutical Society of Japan Acrylonitrile Acrylonitrile Butadine 50µg/L
Simulants Using Gas Chromatography (Hygiene Test Method Note) Styrene (ABS) or Styrene
with Headspace (Migration Test) Acrylonitrile (SAN)
MOH M03-013 Determination of Styrene and α- Iranian Journal of Chemical 1. Styrene Any containers, packaging Styrene: 0.5mg/kg @ 0.08 mg/dm²
methylstyrene in food simulant using Enginering Vol 8,No4 (Autumn),2011, materials, kitchenware and NA
Gas Chromatography Mass IAChe tableware made of
Spectrometry with Headspace POLYSTYRENE (PS)
(Migration Test) 2.α-methylstyrene plastic materials α-methylstyrene: 0.05mg/kg @ 0.008
mg/dm² NA
MOH M03-014 Determination of Halogenated Solvents Analytica Chimica Acta, 552, 60-66 1. Bromodichloromethane Food stored in glass jars NA
Content in Olive using Headspace Gas with metal closures
Chromatography Mass Spectrometry containing PVC gasket
MOH M03-014 Determination of Halogenated Solvents Analytica Chimica Acta, 552, 60-66 Food stored in glass jars NA
Content in Olive using Headspace Gas with metal closures
Chromatography Mass Spectrometry containing PVC gasket
2. Dibromochloromethane
3. Chloroform
4. Bromoform
5. Tetrachloroethene
6. Trichloroethene
MOH M03-015 Determination of Bisphenol A In Milk by Journal of Chromatography A, 1216 Bisphenol A Milk 5 ug/kg
Liquid Chromatography Tandem Mass (2009) 449-470
Spectrometry
MOH M03-016 Determination of Maleic Acid and EN13130-24:2005 Determination of Maleic Acid Any containers, packaging 3 mg/kg
Maleic Anhydride in Food Simulants Maleic Acid and Maleic Anhydride in materials, kitchenware and
(Migration Test) Food Simulants tableware made of
POLYSTYRENE (PS) /
POLYCARBONATE (PC) /
POLYVINYL CHLORIDE
(PVC) / POLYVINYLIDINE
CHLORIDE (PVdC) plastic
materials
MOH M03-017 Determination of Plasticizers in Food Wenzl T. (2009). Methods for the 1. Bis(2-ethylhexyl)phthalate (DEHP) Commercially packed food 1. Bis(2-ethylhexyl)phthalate (DEHP) :
using Gas Chromatography Mass determination of phthalates in food: 1 mg/kg A
Spectrometry Outcome of a survey conducted
among European food control 2. Diisononyl phthalates (DINP) 2. Diisononyl phthalates (DINP) : 3
laboratories. JRC Scientific and mg/kg A
Technical Reports, European
Communities, Luxembourg. 3. Di-2-ethylhexyl adipate (DEHA) 3. Di-2-ethylhexyl adipate (DEHA) : 1
mg/kg A
4. Butylbenzyl phthalate (BBP) 4. Butylbenzyl phthalate (BBP) : 1

mg/kg A
5. Acetyl-tri-n-butyl citrate (ATBC) 5. Acetyl-tri-n-butyl citrate (ATBC) : 1

mg/kg A
6. Diisodecyl phthalate (DIDP) 6. Diisodecyl phthalate (DIDP) : 3

mg/kg A
7. Di-n-butyl phthalate (DnBP) 7. Di-n-butyl phthalate (DnBP) : 1

mg/kg A
8. Di-n-butyl sebacate (DBS) 8. Di-n-butyl sebacate (DBS) : 1 mg/kg

A
MOH M03-018 Determination of Bisphenol A In Journal of Chromatography A, 1216 Bisphenol A Canned Fish 5 ug/kg
Canned Fish by Liquid (2009) 449-469
Spectrometry
MOH M03-019 Determination of Bisphenol A In Journal of Chromatography A, 1216 Bisphenol A Canned Food 5 ug/kg
Canned Food (Vegetables, Fruits, (2009) 449-469 (Vegetables, Fruits, Sauce
Sauce and Carbonated Drink) by Liquid and Carbonated Drink)
Spectrometry
MOH M03-020 Determination of Epoxidized Soybean European Food Research and Epoxidized Soybean Oil (ESBO) Food stored in glass jars Oil : 70 mg/kg Sauce : 23 mg/kg
Oil in Foods Stored in Glass Jars with Technology with metal closures Infant Food : 14 mg/kg
Metal Lids Using Gas Chromatography containing PVC gasket
(Migration Test)
Determination of Formaldehyden in Eur Food Res Technol (2016) Formaldehyden Melamine ware 15 mg/kg
Melamine ware 242:1187-1199
NA

NATURAL CONTAMINANT AND ALLERGEN
MKKM MKA
PULAU PINANG
KEBANGSAAN,
TERENGGANU
SANDAKAN
SELANGOR
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
LOQ
MIRI
(mg/kg)
MOH N03-001 Determination of Nitrate and Nitrite in US Environmental Protection Agency Nitrite Vegetables 5 (All)
Vegetables using Ion (EPA) Method 9056A Revision 1 Feb 50 (P.Pinang) NA NA
Chromatography 2007
Nitrate
NA NA
MOH N03-002 Determination of Chloride and US Environmental Protection Agency Chloride Rice 10
Bromide in Rice using Ion (EPA) Method 9056A Revision 1 Feb
Chromatography 2007
Bromide
MOH N03-003 Determination of Peanut Allergen In Kit Instruction Manual Peanut Allergen Various products 2.5
Food By Veratox® Peanut Allergen except peanut and its A
Test products
MOH N03-004 Determination of Milk Allergen In Kit Instruction Manual Milk Allergen Various products 2.5
Food by Veratox® Total Milk Allergen except milk and its A
Test Kit products
MOH N03-005 Determination of Egg Allergen In Kit Instruction Manual Egg Allergen Various products 2.5
Food by Veratox® Egg Allergen Test except egg and its A
products
MOH N03-006 Determination Of Gliadin In Food by Kit Instruction Manual Gliadin Allergen Various products 5
Veratox® Gliadin Test except oat, barley, A
wheat & its products
MOH N03-007 Determination of Biogenic Amines In Journal of Chromatography B, 693 Putrescine Fish and Fish 50
Fish & Fish Product by High (1997) Products, Seafood and A
Performance Liquid Chromatography Fermented Food
(HPLC) Cadaverine
A
Spermidine
A
Spermine
A
Tyrptamine
A
Histamine
A
2-phenylethylamine
A
MOH N03-008 The Detection of Soy Allergen in Food Kit Instruction Manual Soy Allergen Various products 2.5
By Using Veratox® Soy Allergen except soy and its NA
Quantitative Test Kit product
MOH N03-009 Determination of 4-methylimidazole in Journal of Separation Science, 29, 4-methyl imidazole Dark colored drinks 0.06
Carbonated Beverages by Liquid 378-384 (2006)
Chromatography Tandem Mass A
Spectrometry
MOH N03-010 Determination of 7 Anions In Drinking US Environmental Protection Agency Fluoride Water ( as per 25th, 0.5
Water By Ion Chromatography (EPA) Method 300.1 25th A and 26th NA
Schedule of Food
Chloride Regulations 1985) 12.5
NA
Bromide 5
NA
Nitrite 0.5
NA
Nitrate 5
NA
Sulphite 12.5
NA
Phosphate 5
NA
MOH N03-011 Determination of A) International Honey Commission, Hydroxymethyl- Honey and Sugar 0.5,
Hydroxymethylfurfural by Liquid 2002., page 25-26. furfural Containing Food MKKM Perlis
Chromatography B) Identification and Quantification of Products (50 mg/kg)
%-Hydroxymethyl Furfual HMF in
Some Sugar-containing Food NA A
products by HPLC, 2009, Pakistan
Journal of Nutrition 8 (9), page 1391-
1396.
MOH N03-012 The Determination of Biogenic

Amines In Fish and Fish Product by
High Performance Liquid A
Chromatography (HPLC) using
Internal Standard
MOH N03-013 Determination of 3MCPD in soy Jabatan Kimia 3MCPD soy sauce MKKM Perlis
sauce USM (0.5 mg/kg) NA
The Determination of Tetradotoxin In Training material by Biosekuriti Tetradotoxin Fish and fish product 3
Fish and Fish Product by LCMSMS perikanan NA

IPOH
KOTA BHARU
NA
MKA
JOHOR BAHRU
A
A
A
A
A
A
A
KOTA KINABALU
DIOXIN
MKKM
PULAU PINANG
TERENGGANU
SELANGOR
KELANTAN
SARAWAK
PAHANG
LOQ
PERLIS
KEDAH
MIRI
(ng/kg)
MOH P03-001 Determination of PCDD/FS and SARAF Method, WHO- Toxic DIOXIN Hen eggs and egg 0.2
Dioxin-Like PCBs in Hen Eggs and Equivalency factors 2005, EPA 1613, products NA
egg products by Isotope Dilution EPA 8290
HRGC/ HRMS DIOXIN LIKE PCBs
NA
MOH P03-002 Determination of PCDD/FS and SARAF Method, WHO- Toxic DIOXIN Milk powder 0.2
Dioxin-Like PCBs in Milk Powder for Equivalency factors 2005, EPA 1613, NA
infants and young childrens by EPA 8290
Isotope Dilution HRGC/ HRMS DIOXIN LIKE PCBs
NA
MOH P03-003 Determination of PCDD/FS and SARAF Method, WHO- Toxic DIOXIN Marine oil for human 0.2
Dioxin-Like PCBs in Marine oil by Equivalency factors 2005, EPA 1613, consumption NA
Isotope Dilution HRGC/ HRMS EPA 8290
DIOXIN LIKE PCBs
NA

SANDAKAN
KEBANGSAAN,
SG. BULOH
IPOH
KOTA BHARU
MKA
JOHOR BAHRU
KOTA KINABALU
FOOD MOLECULAR
MKKM MKA
KOTA KINABALU
PULAU PINANG
JOHOR BAHRU
KEBANGSAAN,
TERENGGANU
KOTA BHARU
SELANGOR
SANDAKAN
SG. BULOH
KELANTAN
SARAWAK
PAHANG
PERLIS
KEDAH
IPOH
DOC. NO TEST METHOD REFERENCE PARAMETER FOOD MATRIX LOD
MIRI
MOH R03-101 DNA Extraction Using Boiling Cell International Standard. 2006. Bacteria DNA extraction Ready-to-eat food NA
Method Microbiology of food and animal (MKAK)
feeding stuffs – Polymerase chain
reaction (PCR) for the detection of
food-borne pathogens –
Requirements for sample NA A
preparation for qualitative methods.
Reference number ISO
20837:2006E
MOH R03-102 DNA Extraction Using QIAGEN QIAGEN Mericon DNA Bacteria Bacteria DNA extraction Ready-to-eat food 1.0 ng/µl
Mericon™ Bacteria Kit Handbook.September 2010 (MKKM Selangor)
10 ng/µl A NA A
(MKAK)
MOH R03-103 DNA Extraction using QIAGEN QIAGEN Mericon DNA Bacteria Bacteria gram positive Ready-to-eat food 1.0 ng/µl
mericon™ Bacteria Plus Kit Handbook.September 2010 DNA extraction (MKKM Selangor) A NA NA
MOH R03-201 RNA Extraction Using QIAGEN RNeasy® Mini Kit Handbook Virus extraction Water, Soft Fruits and NA
RNeasy® Mini Kit Salad (ulam) (MKAK) A
MOH R03-202 RNA Extraction Using QIAGEN RNeasy® Plus Mini Kit Handbook Virus extraction Bivalve Molluscan NA
RNeasy® Plus Mini Kit Shellfish (MKAK) A
MOH R03-203 RNA and DNA Extraction Using Nucleospin® Virus Kit Handbook Virus extraction Water, Soft Fruits, 5.0 ng/µl
Nucleospin® Virus Kit Salad (ulam) and (MKAK)
Bivalve Molluscan A NA
Shellfish
MOH R03-301 Detection of Salmonella spp. by Miyamoto, T., Trevanich,S., Honjoh, Salmonella spp. Ready-to-eat food 1.0 ng/µl
Gel Electrophoresis K. and Hatano, S., 1999. Rapid (MKKM Selangor)
Detection of Salmonella spp. By 4.0 x 10-2 CFU/g
PCR amplification of Salmonella (MKAK) A NA A
Specific region in gatD gene. Jpn. J.
Food Microbiol., 16(2), 99-109
MOH R03-302 Detection of Vibrio cholerae toxin Fukushima, H., Tsunomori, Y. and Vibrio cholerae Ready-to-eat food 5.0 x 10-1 ng/µl
by Gel Electrophoresis Seki, R., 2003. Duplex Real Time (MKAK)
SYBR Green PCR Assays for
Detection of 17 Species of Food or NA
waterborne Pathogens in stools.
J.Clin. Microbiology. 2003, p.5134-
5146
MOH R03-303 Detection of Brucella spp. by Patel, T.J., 2007, Serological, Brucella spp. Meat, milk and milk 1.0 x 10-2 ng/µl
Real-Time PCR (qPCR) – SYBR Culture and Molecular Detection of products (MKKM Selangor)
Green Brucella Infection in Bovines NA
Including quantification in Milk by
Real Time PCR
MOH R03-304 Detection of Brucella spp. by Gel Sanjay, G., Ashish R., D.N. Rank Brucella spp. Milk and milk products 1.0 ng/µl
Electrophoresis and Bharat B.B., 2010. Identification (MKKM Selangor)
of Brucella spp. from Animals with 1.0 x 10-3 ng/µl
Reproductive Disorders by (MKAK)
Polymerase Chain Reaction Assay.
B. B., 2010. Identification of Brucella
spp. from Animals with Reproductive NA A
Disorders by Polymerase Chain
reaction Assay. B. Bulletin Vol. 29
No. 2
MOH R03-305 Detection of Listeria Journal of Microbiology, Vol;. 44. Listeria monocytogenes Ready-to-eat food 1.0 ng/µl
monocytogenes by Gel p.92-97 (MKKM Selangor)
Electrophoresis 4.0 x 10-2 CFU/g A A
(MKAK)
MOH R03-306 Detection of Escherichia coli Multiplex PCR for Detection of Trait Escherichia coli O157:H7 Ready-to-eat food NA
O157:H7 by Gel Electrophoresis and Virulence Factors in (MKAK)
Enterochemorrhagic E.coli NA
Serptypes. Molecular and Cellular
Probes, Vol 14 333-337
MOH R03-307 Detection of Listeria Yeon, S.P., Sang, R.L. and Young, Listeria monocytogenes Ready-to-eat food 1.0 x 10-4 ng/µl
monocytogenes by Real-Time G.K. 2005. Detection of Escherichia (MKKM Selangor)
PCR (qPCR) - SYBR Green coli O157:H7, Salmonella spp.,
Staphylococcus aureus and Listeria
monocytogenes in Kimchi by NA
Multiplex Polymerase Chain
Reaction (mPCR)
MOH R03-308 Detection of Enteroinvasive Vilchez, S., Reyes, D., Paniagua, M., Enteroinvasive Ready-to-eat food NA
Escherichia coli (EIEC) by Gel Bucardo, F., Möllby, R. and Escherichia coli (EIEC) (MKAK)
Electrophoresis Weintraub, A., 2009. Prevalence of
Diarrhoeagenic Escherichia coli in
NA
Children from León, Nicaragua. J.
Med Microbiology (2009), 58, 630 -
637
MOH R03-311 Detection of Enterotoxigenic Vilchez, S., Reyes, D., Paniagua, M., Enterotoxigenic Ready-to-eat food NA
Escherichia coli (ETEC) by Gel Bucardo, F., Möllby, R. and Escherichia coli (ETEC) (MKAK)
Electrophoresis Weintraub, A., 2009. Prevalence of
Diarrhoeagenic Escherichia coli in
Children from León, Nicaragua. J. NA
Med Microbiology (2009), 58, 630 -
637.
MOH R03-312 Detection of Vibrio Based on thesis submitted to the Vibrio parahaemolyticus Ready-to-eat food NA
parahaemolyticus toxR by Gel School of Graduate Studies,UPM- toxR gene (MKAK)
Electrophoresis Prevalence and molecular
characterization of Vibrio
parahaemolyticus isolated from NA
cultured tiger prawns (Penaeus
monodon) from Malacca.
Zainazor.T.C. 2006
MOH R03-313 Detection of Vibrio Fukushima, H., Tsunomori, Y. and Vibrio parahaemolyticus Ready-to-eat food NA
parahaemolyticus tdh and trh by Seki, R., 2003. Duplex Real-Time tdh and trh gene (MKAK)
Gel Electrophoresis SYBR Green PCR Assays for
Detection of 17 Species of Food- or NA
Waterborne Pathogens in Stools. J.
Clin. Microbiol. 2003, p. 5134 - 5146
MOH R03-314 Detection of Escherichia coli Molecular and Cellular Probes, Vol. Escherichia coli O157:H7 Meat, milk and milk stx 1 gene: 1 x 10-2
O157:H7 by Real-Time PCR 14 p. 333 - 337. products ng/µl
(qPCR) – SYBR Green stx 2 gene: 1 x 10-5
ng/µl
eaeA gene: 1 x 10-5
ng/µl
ehxA gene: 1 x 10-5
ng/µl NA
uidA gene: 1 x 10-5
ng/µl
(MKKM Selangor)
MOH R03-315 Detection of Campylobacter jejuni Persson,S.& Olsen, K.E.P. 2005. Campylobacter jejuni Ready-to-eat food NA
by Gel Electrophoresis Multiplex PCR for identification of (MKAK)
Campylobacter jejuni from pure
cultures and directly on stool NA
samples. Journal of Medical
Microbiology (2005), 54, 1043-1047
MOH R03-316 Detection of Vibrio vulnificus by Fukushima, H., Tsunomori, Y. and Vibrio vulnificus Ready-to-eat food
Gel Electrophoresis Seki, R., 2003. Duplex Real-Time
SYBR Green PCR Assays for
Detection of 17 Species of Food- or
Waterborne Pathogens in Stools. J.
Clin. Microbiol. 2003, p. 5134 - 5146
MOH R03-317 Detection of Staphylococcus Hirotaki, S., sasaki, T.,Kuwahara- Staphylococcus aureus Ready-to-eat food NA
aureus by Gel Electrophoresis Arai, K. and Hiramatsu,K.,2011. (MKAK)
Rapid and accurate Identification of
Human-Associated Staphylococcus
NA
aureus by use of Multiplex PCR. J.
Clin.Microbiol. 2011, 49 (10):3627
MOH R03-318 Detection of Yersinia Wannet, W.J.B., Reessink, M., Yersinia enterocolitica Ready-to-eat food
enterocolitica by Gel Brunings, H.A. and Maas, H.M.E.,
Electrophoresis 2001. Detection of Pathogenic
Yersinia enterocolitica by a Rapid
and Sensitive Duplex PCR Assay. J.
Clin. Microbiol. 2001, p. 4483 - 4486
MOH R03-319 Detection of Cronobacter Xiang Yan,Joshua Gurtler, Pina Cronobacter sakazakii Ready-to-eat food NA
sakazakii by Gel Electrophoresis Fratamico,Jing Hu,Nereus W. (MKAK)
Gunther IV, Vijay Juneja and Lihan
Huang. Comprehensive Approaches
to Molecular Biomarker Discovery for
Detection and Identification of NA
Cronobacter spp. (Enterobacter
sakazakii) and Salmonella spp.
MOH R03-320 Detection of Clostridium Villamizar-Rodriguez, G., Javier- Clostridium perfringens Ready-to-eat food 1 x 10-4 ng/µl
perfringens by Real-Time PCR Fernandez, Marin, L., Muniz, J., (MKKM Selangor)
(qPCR) – SYBR Green Gonzalez, I. and Lombo. F., 2015.
Multiplex Detection of Nine Food-
borne Pathogens by mPCR and
Capillary Eletrophoresis after using a NA
Universal Pre-enrichment Medium.
Frontiers in Microbiology, 2015.
MOH R03-321 Detection of Salmonella by qPCR iQ-Check Salmonella II Kit (Bio-RAD) Salmonella spp. Food and Drinks, Swab NA
from Environmental (MKKM Perlis)
Samples (Food 1.0 x 10-1 ng/µl
A NA
Production/Handling) (MKKM Miri)
MOH R03-322 Detection of Salmonella typhi by Chai, F.P., et al, 2011. Multiplex Salmonella typhi Ready-to-eat food 1.0 x 10-1 ng/µl
Gel Electrophoresis PCR for the Concurrent Detection (MKAK)
and Differentiation of Salmonella
spp., Salmonella typhi and A
Salmonella typhimurium. T. Med and
Health Vol. 39 No.1, 2011 pp 9 - 15.
MOH R03-323 Detection of Salmonella Chai, F.P., et al, 2011. Multiplex Salmonella typhimurium Ready-to-eat food 3.0 x 10-1 ng/µl
typhimurium by Gel PCR for the Concurrent Detection (MKAK)
Electrophoresis and Differentiation of Salmonella
spp., Salmonella typhi and A
Salmonella typhimurium. T. Med and
Health Vol. 39 No.1, 2011 pp 9 - 15.
MOH R03-324 Detection of Salmonella spp. by Miyamoto, T., Trevanich, S., Honjoh, Salmonella spp. Ready-to-eat food
Gel Electrophoresis K., and Hatano, S. 1999. Rapid
(Conventional) Detection of Salmonella Specific
Region in gatD gene. Jpn. J. Food
Microbiol., 16(2), 99-109
MOH R03-325 Detection of Vibrio cholerae toxin Hiroshi, F., Tsunomori, Y. and Seki, Vibrio cholerae Ready-to-eat food
by Gel Electrophoresis R. 2003. Duplex Real-Time SYBR
(Conventional) Green PCR Assays for Detection of
17 Species of Food- or Waterborne
Pathogens in stools. Journal of
Clinical Microbiology
MOH R03-326 Detection of Listeria Hiroshi, F., Tsunomori, Y. and Seki, Listeria monocytogenes Ready-to-eat food
monocytogenes by Gel R. 2003. Duplex Real-Time SYBR
Electrophoresis (Conventional) Green PCR Assays for Detection of
MOH R03-327 Detection of Escherichia coli Hiroshi, F., Tsunomori, Y. and Seki, Escherichia coli O157:H7 Ready-to-eat food
O157:H7 by Gel Electrophoresis R. 2003. Duplex Real-Time SYBR
MOH R03-328 Detection of Vibrio Zainazor .T. C. 2006. Prevalence Vibrio parahaemolyticus Ready-to-eat food
parahaemolyticus by Gel and molecular characterization of
Electrophoresis (Conventional) Vibrio parahaemolyticus isolated
from cultured tiger prawns (Penaeus
monodon) from Malacca. Thesis
Submitted to the School of Graduate
Studies, Universiti Putra Malaysia
MOH R03-329 Detection of Campylobacter jejuni Hiroshi, F., Tsunomori, Y. and Seki, Campylobacter jejuni Ready-to-eat food
by Gel Electrophoresis R. 2003. Duplex Real-Time SYBR
MOH R03-330 Detection of Vibrio vulnificus by Kim, M. S. and Jeong, H. D., 2001. Vibrio vulnificus Ready-to-eat food
Gel Electrophoresis Development of 16S rRNA targeted
(Conventional) PCR methods for the detection and
differentiation of Vibrio vulnificus in
marine environments. Aquaculture
193 (2001) 199-211
MOH R03-332 Detection of Escherichia coli Journal of Hong Kong Institute of Escherichia coli O111 Ready-to-eat food 1 x 10-5 ng/µl
O111 by Real-Time PCR (qPCR) Medical Laboratory Sciences, 2011-
– SYBR Green 2012 Volume 13 No 1 & 2.
NA
MOH R03-333 Detection of Escherichia coli O26 Journal of Hong Kong Institute of Escherichia coli O26 Ready-to-eat food 1 x 10-5 ng/µl
by Real-Time PCR (qPCR) – Medical Laboratory Sciences, 2011-
SYBR Green 2012 Volume 13 No 1 & 2.
NA
MOH R03-334 Detection of Escherichia coli J. Clin Microbiol. 50:3485 – 3492. Escherichia coli O104:H4 Ready-to-eat food 1 x 10-7 ng/µl
O104:H4 by
Real-Time PCR (qPCR) – SYBR
Green
NA
MOH R03-335 Detection of Clostridium ISO/TS 17919 Technical Clostridium botulinum Ready-to-eat food NA
botulinum Type A, B, E & F by Specification, 2013. Type A, B, E & F
Real-Time PCR (qPCR) – Probe
Based
NA
MOH R03-402 Detection of Hepatitis A Virus by Wan Norhana, M.N., Masazurah, Hepatitis A Virus Water, Soft Fruits, 100 RT-PCR unit/µl
Gel Electrophoresis A.R., Nor Ainy, M. and Ismail,I. 2011. Salad (ulam) and (MKAK)
Reverse Transcriptase PCR Bivalve Molluscan
detection of Hepatitis A Virus (HAV) Shellfish
in cultured and wild shellfish from A
Peninsular Malaysia. International
Food Research Journal 18:411-415
MOH R03-403 Detection of Adenovirus by Real S.A. Feeney, V.J. Armstrong, S.J. Adenovirus Water, Soft Fruits, 6.0 x 10-7 ng/µl
time Polymerase Chain Reaction Mitchell, L.Crawford, C.McCaughey Salad (ulam) and (MKAK)l
(qPCR) and P.V. Coyle. Development and Bivalve Molluscan
Clinical Validation of Multiplex Shellfish
TaqMan R Assays for Rapid
Diagnosis of Viral Gastroenteritis. A
Journal of Medical Virology 83:
1650-1656 (2011)
MOH R03-404 Detection of Rotavirus A by Real Andi Y., Elisabeth DH., Pramita GD. Rotavirus A Water, Soft Fruits, 1.0 x 102 copies/µl
time Polymerase Chain Reaction And Beti ED. Detection of Human Salad (ulam) and (MKAK)
(qPCR) Group A and C Rotaviruses in Bivalve Molluscan
Pediatric Patients with Acute Shellfish
Gastroenteritis by Real Time RT-
PCR Assay: A Preliminary Study. A
Makara Kesehatan, Vol. 14, No. 2
(2010).
MOH R03-501 Protocol for Molecular Subtyping Protocol for Molecular Subtyping of E. coli 0157:H7, DNA NA
of E. coli 0157:H7, Salmonella E. coli 0157:H7, Salmonella Salmonella serotypes, (MKKM Perlis)
serotypes, Shigella sonnei and serotypes, Shigella sonnei and Shigella sonnei and 10 ng/µl
Shigella flexneri by Pulsed Field Shigella flexneri by Pulsed Field Gel Shigella flexneri (MKKM Miri)
Gel Electrophoresis Electrophoresis A NA
MOH R03-204 RNA Extraction Using QIAamp® QIAamp® Viral RNA Mini Handbook Virus extraction Food and food contact 5.0 ng/µl
Viral RNA Mini Kit surfaces (KKM Selangor)
NA
MOH R03-405 Detection of SARS-CoV2 by SuperScript™ III Platinum™ One- SARS-CoV2 (COVID-19) Food and food contact 1.0 x 10-3 ng/µl
Real-Time PCR (qPCR) - Probe Step qRT-PCR Kit, Pub. No. surfaces (MKM Selangor)
Based MAN0001006 Rev. C.O.
NA
MOH R03-331 Detection of Vibrio cholerae toxin J.Clin. Microbiol. 2003, p. 5134 - Vibrio cholerae toxin Ready-to-eat food 1.0 x 10-4 ng/µl
by Real-Time PCR (qPCR) - 5146. (MKKM Selangor)
SYBR Green
NA

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Skim Akreditasi Makmal Malaysia (SAMM) No.

BIL. LABORATORY SAMM NO.

MKKM - Makmal Keselamatan dan Kualiti Makanan

Oxolinic acid 40-50

Nitrofurazone metabolite : SEM 1

Furaltadone metabolite : AMOZ 0.5

Leucrystal Violet 0.5

Gentamycin Milk:20 Muscle:5

NA Capable but not accredited ISO/IEC 17025

Bread, flour, sauce, 20 mg/kg

Coconut Milk, cream 5 mg/kg

Sauce, juice, chilly 30 mg/kg

Fish and Fish Products 30 mg/kg

Other types of food 30 mg/kg

The Determination of Water AOAC (19750). Selected types of

MOH E03-003 Allura Red AC 50 - 500 mg/kg

(c ) Katerina S. M., Christina. F. Sudan 1 3-6 mg/kg

Allura Red AC Liquid/ Semi Solid:

Water Soluble Colour (Permitted

Water Soluble Colour

Other types of food** 20 mg/kg

Cyclamate 120 mg/kg

Other types of food** 120 mg/kg

Monophosphate 125 mg/kg

Diphosphate 125 mg/kg

Triphosphate 125 mg/kg

MOH E03-021 The Determination of Di(2- A.K.Chaudhary,S.Ankushrao Di(2-ethylhexyl)phthalate Beverages 2 mg/kg

2. AOAC Official Method 996.13,

MOH E03-028 Determination of 1)Determination of formaldehyde Formaldehyde Flour 75 mg/kg

Saccharin 0.2 mg/kg

Cyclamate 0.2 mg/kg

NA Capable but not accredited ISO/IEC 17025

A Capable and accredited to ISO/IEC 17025

Chlorpyriphos 0.5 (MKAJB), 0.025 (ALL), 0.3

Chlorpyrifos methyl 0.6 (MKAJB) 0.025 (ALL), 0.3

Diazinon 0.4 (MKAJB) 0.01 (ALL), 0.3

Ethion 0.5 (MKAJB), 0.025 (ALL)

Fenitrothion 0.5 (MKAJB),

Fenthion 0.9 (MKAJB) 0.025 (ALL), 0.3

Formothion 0.9 (MKAJB) 0.025 (ALL)

Malathion 0.5 (MKAJB), 0.02 (ALL)

Methidathion 0.9 (MKAJB)

Parathion ethyl 0.05

Parathion methyl 0.8 (MKAJB), 0.05 (ALL)

Phosalone 2 (MKAJB) 0.05 (ALL)

Pirimiphos methyl 0.4 (MKAJB) 0.01 (ALL)

Prothiophos 0.025, 0.3 (SEL)

Quinalphos 0.02, 0.3 (SEL)

Tolclophos methyl 0.6 (MKAJB) 0.025 (ALL)

4,4-DDE 0.025, 0.03 (SEL)

Aldrin 0.025, 0.03 (SEL)

Dichloran 0.015, 0.03 (SEL)

Dieldrin 0.01, 0.03 (SEL)

Endosulfan (alpha) 0.03, 0.03 (SEL)

Endosulfan (beta) 0.03, 0.03 (SEL)

Gamma-HCH / 0.05, 0.03 (SEL)

Heptachlor 0.005, 0.03 (SEL)

Quintozene 0.005, 0.03 (SEL)

Triademefon 0.05, 0.03 (SEL)

Cyfluthrin 0.25, 0.3 (SEL)

Cypermethrin 0.25, 0.3 (SEL)

Fenvalerate 0.25, 0.3 (SEL)