OREAS 623 Datapack

Table 1.
Abbreviations used for OREAS 623
Abbreviation
<
IND
NR
PDM3
Rel.Std.Dev.
Std.Dev.
Method Codes:
3A*AAS
3A*OES
4A*AAS
4A*MS
4A*OES
4A*OES/MS
AR*AAS
AR*GFAAS
AR*MS
AR*OES
AR*OES/AAS
AR*OES/MS
FA*AAS
FA*OES
INAA
IRC
PF*MS
PF*OES
PF*OES/MS
Legend:-
Individual
Batch & Limits

Table 1. Abbreviations used for OREAS 623
Explanation
‘less than’
indeterminate
not reported
percent deviation of lab mean from corrected mean of means
one sigma relative standard deviation
one sigma standard deviation
3-acid (HNO3-HCIO4-HCI) digest with AAS finish

3-acid (HNO3-HCIO4-HCI) digest with OES finish
4-acid (HF-HNO3-HClO4-HCl) digest with AAS finish
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-MS finish
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES finish
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES or ICP-MS finish as appropriate
aqua regia digest with AAS finish
aqua regia digest with graphite furnace AAS finish
aqua regia digest with ICP-MS finish
aqua regia digest with ICP-OES finish
ore grade aqua regia digest with either AAS or ICP-OES finish as appropriate
aqua regia digest with ICP-OES or ICP-MS finish as appropriate
fire assay with AAS finish
fire assay with ICP-OES finish
INAA using a charge weight as deemed appropriate
infrared combustion furnace
sodium peroxide fusion with ICP-MS finish
sodium peroxide fusion with ICP-OES finish
sodium peroxide fusion with OES or MS finish as appropriate
(for Method Group Tabulated Results omitted in the determination of Certified Values)
- Outlying individual values
- Outlying laboratory batch data sets and superfluous limit values

Table 5. Participating Laboratory List used for OREAS 623
Lab Slot
Legend:-
Individual
Batch & Limits

Table 5. Participating Laboratory List used for OREAS 623
Laboratory Name and Location
Acme (BV), Santiago, Chile

Actlabs, Ancaster, Ontario, Canada
ALS, Brisbane, QLD, Australia
ALS, Johannesburg, South Africa
ALS, Lima, Peru
ALS, Loughrea, Galway, Ireland
ALS, Orange, NSW, Australia
ALS, Perth, WA, Australia
ALS, Vancouver, BC, Canada
Bureau Veritas Commodities Canada Ltd, Vancouver, BC, Canada
Bureau Veritas Geoanalytical, Adelaide, SA, Australia
Bureau Veritas Geoanalytical, Perth, WA, Australia
Intertek Genalysis, Adelaide, SA, Australia
Intertek Genalysis, Perth, WA, Australia
Intertek Minerals (IMI), Jakarta, Indonesia
Intertek Testing Services, Cupang, Muntinlupa, Philippines
PT Geoservices Ltd, Cikarang, Jakarta Raya, Indonesia
SGS Australia Mineral Services, Perth (Newburn), WA, Australia
SGS Canada Inc., Vancouver, BC, Canada
SGS del Peru, Lima, Peru
SGS Geosol Laboratorios Ltda, Vespasiano, Minas Gerais, Brazil
SGS Lakefield Research Ltd, Lakefield, Ontario, Canada
SGS Mineral Services, Townsville, QLD, Australia
(for Method Group Tabulated Results omitted in the determination of Certified Values)
- Outlying individual values
- Outlying laboratory batch data sets and superfluous limit values

Table 2. Certified Values, SD's, 95% Confidence and Tolerance Limits for OREAS 623
95% Confidence 95% Tolerance
Certified
Constituent SD Limits Limits
Value Low High Low High
Fire Assay
Au, Gold (ppm) 0.827 0.039 0.811 0.842 0.814 0.839
Infrared Combustion
S, Sulphur (wt.%) 9.07 0.180 9.00 9.14 8.93 9.20
Peroxide Fusion ICP
Ag, Silver (ppm) 22.7 3.5 19.4 25.9 IND IND
Al, Aluminium (wt.%) 5.25 0.152 5.15 5.35 5.13 5.36
As, Arsenic (ppm) 86 9 80 92 80 92
Ba, Barium (ppm) 1395 64 1342 1447 1348 1441
Bi, Bismuth (ppm) 17.7 0.90 16.8 18.6 16.8 18.6
Ca, Calcium (wt.%) 1.37 0.072 1.33 1.41 1.32 1.42
Cd, Cadmium (ppm) 55 4.6 51 58 52 57
Ce, Cerium (ppm) 49.9 4.21 44.4 55.4 47.3 52.5
Co, Cobalt (ppm) 225 10 220 231 216 235
Cr, Chromium (ppm) 30.0 5.9 24.1 35.8 IND IND
Cs, Cesium (ppm) 3.00 0.37 2.59 3.41 2.80 3.21
Cu, Copper (wt.%) 1.73 0.092 1.68 1.77 1.64 1.81
Fe, Iron (wt.%) 13.45 0.379 13.25 13.64 13.05 13.84
Ga, Gallium (ppm) 23.7 2.4 21.1 26.3 21.9 25.5
In, Indium (ppm) 2.04 0.177 1.93 2.16 1.83 2.26
K, Potassium (wt.%) 1.53 0.114 1.46 1.59 1.45 1.60
La, Lanthanum (ppm) 24.9 4.4 20.5 29.3 23.5 26.3
Li, Lithium (ppm) 18.0 2.1 16.3 19.6 IND IND
Mg, Magnesium (wt.%) 1.23 0.026 1.22 1.24 1.20 1.26
Mn, Manganese (wt.%) 0.060 0.003 0.058 0.063 0.058 0.063
Mo, Molybdenum (ppm) 10.2 0.55 9.5 10.9 IND IND
Nb, Niobium (ppm) 10.4 0.89 9.6 11.3 IND IND
Nd, Neodymium (ppm) 24.9 2.37 21.9 27.8 23.2 26.5
Ni, Nickel (ppm) < 50 IND IND IND IND IND
Pb, Lead (wt.%) 0.247 0.010 0.242 0.253 0.240 0.254
Pr, Praseodymium (ppm) 6.53 0.573 5.82 7.24 5.89 7.17
Rb, Rubidium (ppm) 67 3.8 63 70 64 69
S, Sulphur (wt.%) 8.83 0.365 8.57 9.10 8.57 9.10
Sb, Antimony (ppm) 28.0 2.56 25.1 30.8 25.1 30.8
Sc, Scandium (ppm) < 10 IND IND IND IND IND
Si, Silicon (wt.%) 24.45 0.958 23.68 25.22 23.80 25.11
Sr, Strontium (ppm) 90 10 84 95 84 96
Th, Thorium (ppm) 7.29 0.423 6.93 7.65 6.74 7.84
Ti, Titanium (wt.%) 0.150 0.008 0.146 0.154 0.135 0.166
Tl, Thallium (ppm) 0.71 0.10 0.61 0.81 IND IND
U, Uranium (ppm) 2.78 0.191 2.60 2.96 2.54 3.02
W, Tungsten (ppm) 4.22 0.401 3.80 4.64 IND IND
Y, Yttrium (ppm) 19.1 1.42 17.8 20.5 18.3 20.0
Yb, Ytterbium (ppm) 1.76 0.143 1.67 1.85 IND IND
Zn, Zinc (wt.%) 1.03 0.040 1.01 1.06 1.01 1.06
4-Acid Digestion
Ag, Silver (ppm) 20.4 1.06 19.9 20.9 19.6 21.2
Al, Aluminium (wt.%) 5.04 0.329 4.89 5.19 4.88 5.20
As, Arsenic (ppm) 77 5.3 75 80 75 80
Be, Beryllium (ppm) 1.39 0.24 1.30 1.48 IND IND
Bi, Bismuth (ppm) 17.7 1.77 16.7 18.8 17.1 18.4
Ca, Calcium (wt.%) 1.38 0.074 1.34 1.41 1.33 1.42
Cd, Cadmium (ppm) 54 3.9 52 56 52 55
Ce, Cerium (ppm) 45.6 5.4 41.6 49.6 43.8 47.5
Co, Cobalt (ppm) 222 10 217 226 215 228
Cr, Chromium (ppm) 24.8 4.8 22.9 26.8 23.0 26.6
Cs, Cesium (ppm) 2.85 0.109 2.78 2.92 2.74 2.97
Cu, Copper (wt.%) 1.73 0.064 1.72 1.75 1.67 1.80
Fe, Iron (wt.%) 13.42 0.778 13.09 13.76 13.11 13.73
Ga, Gallium (ppm) 21.7 1.40 20.7 22.7 21.0 22.4
Hf, Hafnium (ppm) 3.97 0.247 3.80 4.15 3.81 4.14
In, Indium (ppm) 2.10 0.093 2.06 2.14 1.98 2.21
K, Potassium (wt.%) 1.45 0.117 1.40 1.50 1.41 1.49
La, Lanthanum (ppm) 21.6 3.7 19.1 24.0 20.9 22.2
Li, Lithium (ppm) 15.7 1.35 14.9 16.6 15.1 16.3
Lu, Lutetium (ppm) 0.24 0.03 0.22 0.26 0.21 0.27
Mg, Magnesium (wt.%) 1.20 0.091 1.16 1.24 1.17 1.23
Mn, Manganese (wt.%) 0.060 0.004 0.058 0.062 0.059 0.061
Mo, Molybdenum (ppm) 9.55 0.696 9.23 9.87 9.00 10.10
Na, Sodium (wt.%) 1.12 0.070 1.09 1.15 1.09 1.15
Nb, Niobium (ppm) 8.58 0.729 8.14 9.02 8.35 8.81
Ni, Nickel (ppm) 16.8 3.2 15.6 18.0 16.0 17.6
P, Phosphorus (wt.%) 0.043 0.005 0.041 0.045 0.041 0.045
Pb, Lead (wt.%) 0.250 0.007 0.247 0.252 0.243 0.256
Rb, Rubidium (ppm) 62 3.7 60 65 60 64
S, Sulphur (wt.%) 9.06 0.321 8.88 9.23 8.86 9.25
Sb, Antimony (ppm) 27.6 1.91 26.4 28.9 26.6 28.7
Sc, Scandium (ppm) 8.32 1.35 7.69 8.95 7.99 8.65
Se, Selenium (ppm) 18.7 1.86 17.7 19.7 16.6 20.7
Sn, Tin (ppm) 5.94 0.264 5.80 6.07 5.63 6.24
Sr, Strontium (ppm) 80 7.7 76 83 77 83
Ta, Tantalum (ppm) <1 IND IND IND IND IND
Tb, Terbium (ppm) 0.53 0.05 0.48 0.58 0.49 0.57
Te, Tellurium (ppm) 0.58 0.08 0.54 0.62 0.50 0.67
Th, Thorium (ppm) 6.40 0.87 5.82 6.99 6.13 6.67
Ti, Titanium (wt.%) 0.139 0.012 0.134 0.145 0.132 0.147
Tl, Thallium (ppm) 0.74 0.08 0.68 0.79 0.71 0.77
U, Uranium (ppm) 2.63 0.118 2.55 2.71 2.58 2.68
V, Vanadium (ppm) 26.0 3.5 24.7 27.3 25.1 26.9
W, Tungsten (ppm) 4.28 0.365 4.02 4.54 4.03 4.52
Y, Yttrium (ppm) 13.3 1.25 12.6 14.1 12.9 13.8
Zn, Zinc (wt.%) 1.03 0.030 1.02 1.04 1.00 1.05
Zr, Zirconium (ppm) 150 6 146 153 146 154
3-Acid Digestion (no HF)
Ag, Silver (ppm) 20.6 0.67 20.2 21.0 19.6 21.6
As, Arsenic (ppm) 79 10 71 86 75 82
Cu, Copper (wt.%) 1.74 0.042 1.73 1.75 1.68 1.80
Fe, Iron (wt.%) 13.41 0.400 13.18 13.64 13.06 13.76
Pb, Lead (wt.%) 0.251 0.007 0.247 0.255 0.245 0.257
Zn, Zinc (wt.%) 1.02 0.043 0.99 1.05 0.99 1.05
Aqua Regia Digestion
Ag, Silver (ppm) 20.4 1.15 20.0 20.9 19.8 21.0
Al, Aluminium (wt.%) 1.80 0.091 1.76 1.84 1.75 1.85
As, Arsenic (ppm) 76 6.8 73 78 73 78
Au, Gold (ppm) 0.797 0.038 0.778 0.816 0.783 0.810
B, Boron (ppm) < 10 IND IND IND IND IND
Bi, Bismuth (ppm) 16.9 2.4 16.0 17.7 16.1 17.6
Ca, Calcium (wt.%) 1.09 0.060 1.06 1.12 1.07 1.11
Cd, Cadmium (ppm) 52 3.7 51 54 51 54
Ce, Cerium (ppm) 36.4 5.2 32.8 40.0 35.3 37.5
Co, Cobalt (ppm) 216 11 211 221 211 221
Cr, Chromium (ppm) 19.4 2.1 18.7 20.1 18.4 20.4
Cs, Cesium (ppm) 0.75 0.13 0.65 0.86 0.72 0.79
Cu, Copper (wt.%) 1.72 0.066 1.70 1.75 1.68 1.77
Fe, Iron (wt.%) 13.01 0.546 12.78 13.25 12.75 13.28
Ga, Gallium (ppm) 11.9 1.03 11.2 12.6 11.5 12.3
Hf, Hafnium (ppm) 1.32 0.21 1.15 1.48 1.24 1.40
Hg, Mercury (ppm) 0.83 0.08 0.77 0.89 0.79 0.87
In, Indium (ppm) 1.94 0.107 1.85 2.03 1.84 2.04
K, Potassium (wt.%) 0.175 0.027 0.163 0.188 0.170 0.181
La, Lanthanum (ppm) 17.9 2.4 16.5 19.2 17.1 18.6
Li, Lithium (ppm) 10.0 1.1 9.2 10.9 9.5 10.5
Lu, Lutetium (ppm) 0.12 0.010 0.11 0.13 IND IND
Mg, Magnesium (wt.%) 1.11 0.070 1.08 1.14 1.08 1.14
Mn, Manganese (wt.%) 0.057 0.003 0.056 0.058 0.055 0.058
Na, Sodium (wt.%) 0.068 0.011 0.063 0.073 0.066 0.070
Nb, Niobium (ppm) <1 IND IND IND IND IND
Ni, Nickel (ppm) 15.6 1.7 14.9 16.3 14.9 16.3
P, Phosphorus (wt.%) 0.040 0.002 0.039 0.041 0.038 0.042
Pb, Lead (wt.%) 0.252 0.010 0.247 0.256 0.246 0.257
S, Sulphur (wt.%) 8.75 0.630 8.33 9.16 8.47 9.03
Sb, Antimony (ppm) 20.2 4.1 18.1 22.2 19.3 21.0
Sc, Scandium (ppm) 4.63 0.53 4.38 4.88 4.46 4.80
Se, Selenium (ppm) 18.6 1.9 17.3 19.8 16.9 20.2
Sn, Tin (ppm) 4.07 0.213 3.92 4.22 3.78 4.36
Sr, Strontium (ppm) 14.2 1.5 13.6 14.8 13.7 14.6
Ta, Tantalum (ppm) < 0.05 IND IND IND IND IND
Tb, Terbium (ppm) 0.34 0.032 0.31 0.37 0.32 0.36
Te, Tellurium (ppm) 0.57 0.08 0.53 0.61 0.51 0.63
Th, Thorium (ppm) 4.72 0.325 4.49 4.95 4.53 4.90
Ti, Titanium (wt.%) < 0.06 IND IND IND IND IND
Tl, Thallium (ppm) 0.26 0.04 0.23 0.28 0.24 0.27
U, Uranium (ppm) 1.43 0.104 1.36 1.51 1.37 1.50
V, Vanadium (ppm) 15.8 1.52 15.1 16.5 IND IND
W, Tungsten (ppm) 2.62 0.30 2.40 2.84 2.49 2.75
Y, Yttrium (ppm) 7.43 1.01 6.69 8.17 7.18 7.67
Zn, Zinc (wt.%) 1.01 0.038 1.00 1.03 1.00 1.03
Zr, Zirconium (ppm) 50 3.4 48 53 49 52
Table 3. Indicative Values for OREAS 623
Constituent Unit Value Constituent Unit Value Constituent Unit Value
Fire Assay
Pd ppb <5 Pt ppb <5
Infrared Combustion
C wt.% 0.427
Peroxide Fusion ICP
B ppm < 50 Hf ppm 4.51 Sn ppm 9.40
Be ppm 1.61 Ho ppm 0.61 Ta ppm 0.87
Dy ppm 3.46 Lu ppm 0.28 Tb ppm 0.62
Er ppm 1.88 P wt.% 0.050 Te ppm <1
Eu ppm 1.60 Re ppm < 0.1 Tm ppm 0.24
Gd ppm 4.39 Se ppm 15.6 V ppm 34.1
Ge ppm 1.65 Sm ppm 5.26 Zr ppm 167
4-Acid Digestion
B ppm 0.75 Gd ppm 4.00 Pr ppm 5.79
Ba ppm 1198 Ge ppm 0.66 Re ppm < 0.05
Dy ppm 3.09 Hg ppm 0.56 Sm ppm 4.86
Er ppm 1.63 Ho ppm 0.56 Tm ppm 0.24
Eu ppm 1.36 Nd ppm 22.3
Bi ppm 9.17 Co ppm 218 Ni ppm 15.0
Ba ppm 241 Ge ppm 0.22 Pt ppb <5
Dy ppm 1.78 Ho ppm 0.32 Rb ppm 8.08
Er ppm 0.88 Nd ppm 16.0 Re ppm < 0.05
Eu ppm 0.92 Pd ppb < 10 Sm ppm 3.35
Gd ppm 2.75 Pr ppm 4.33 Tm ppm 0.14
Table 4. Pooled-Lab Performance Gates for OREAS 623
Certified Absolute Standard Deviations Relative Standard Deviations 5% window

Constituent
Value 1SD 2SD Low 2SD High 3SD Low 3SD High 1RSD 2RSD 3RSD Low
Fire Assay
Au, ppm 0.827 0.039 0.749 0.904 0.710 0.943 4.71% 9.41% 14.12% 0.785
Infrared Combustion
S, wt.% 9.07 0.180 8.71 9.43 8.53 9.61 1.98% 3.97% 5.95% 8.61
Peroxide Fusion ICP
Ag, ppm 22.7 3.5 15.6 29.7 12.1 33.2 15.55% 31.10% 46.65% 21.5
Al, wt.% 5.25 0.152 4.95 5.55 4.79 5.71 2.90% 5.79% 8.69% 4.99
As, ppm 86 9 67 105 58 114 10.88% 21.76% 32.63% 82
Ba, ppm 1395 64 1268 1522 1204 1585 4.55% 9.11% 13.66% 1325
Bi, ppm 17.7 0.90 15.9 19.5 15.0 20.4 5.11% 10.22% 15.33% 16.8
Ca, wt.% 1.37 0.072 1.23 1.51 1.15 1.59 5.27% 10.55% 15.82% 1.30
Cd, ppm 55 4.6 45 64 41 69 8.51% 17.02% 25.53% 52
Ce, ppm 49.9 4.21 41.5 58.3 37.3 62.5 8.44% 16.88% 25.32% 47.4
Co, ppm 225 10 205 245 195 255 4.45% 8.90% 13.35% 214
Cr, ppm 30.0 5.9 18.1 41.8 12.2 47.8 19.81% 39.62% 59.43% 28.5
Cs, ppm 3.00 0.37 2.26 3.74 1.89 4.11 12.32% 24.65% 36.97% 2.85
Cu, wt.% 1.73 0.092 1.54 1.91 1.45 2.00 5.31% 10.62% 15.93% 1.64
Fe, wt.% 13.45 0.379 12.69 14.20 12.31 14.58 2.82% 5.64% 8.45% 12.77
Ga, ppm 23.7 2.4 18.9 28.5 16.5 30.9 10.19% 20.37% 30.56% 22.5
In, ppm 2.04 0.177 1.69 2.40 1.51 2.57 8.64% 17.29% 25.93% 1.94
K, wt.% 1.53 0.114 1.30 1.75 1.18 1.87 7.47% 14.93% 22.40% 1.45
La, ppm 24.9 4.4 16.0 33.8 11.5 38.2 17.90% 35.80% 53.70% 23.6
Li, ppm 18.0 2.1 13.8 22.2 11.7 24.2 11.63% 23.26% 34.88% 17.1
Mg, wt.% 1.23 0.026 1.18 1.28 1.15 1.31 2.11% 4.22% 6.32% 1.17
Mn, wt.% 0.060 0.003 0.054 0.067 0.050 0.071 5.67% 11.34% 17.01% 0.057
Mo, ppm 10.2 0.55 9.1 11.3 8.6 11.8 5.34% 10.68% 16.03% 9.7
Nb, ppm 10.4 0.89 8.7 12.2 7.8 13.1 8.52% 17.03% 25.55% 9.9
Nd, ppm 24.9 2.37 20.2 29.6 17.8 32.0 9.52% 19.04% 28.55% 23.6
Ni, ppm < 50 IND IND IND IND IND IND IND IND IND
Pb, wt.% 0.247 0.010 0.227 0.267 0.217 0.277 4.06% 8.12% 12.19% 0.235
Pr, ppm 6.53 0.573 5.38 7.68 4.81 8.25 8.77% 17.54% 26.31% 6.20
Rb, ppm 67 3.8 59 74 55 78 5.69% 11.37% 17.06% 63
S, wt.% 8.83 0.365 8.10 9.56 7.74 9.93 4.13% 8.26% 12.39% 8.39
Sb, ppm 28.0 2.56 22.8 33.1 20.3 35.7 9.16% 18.33% 27.49% 26.6
Sc, ppm < 10 IND IND IND IND IND IND IND IND IND
Si, wt.% 24.45 0.958 22.54 26.37 21.58 27.33 3.92% 7.83% 11.75% 23.23
Sr, ppm 90 10 70 110 60 120 11.24% 22.48% 33.72% 85
Th, ppm 7.29 0.423 6.44 8.14 6.02 8.56 5.81% 11.62% 17.43% 6.93
Ti, wt.% 0.150 0.008 0.134 0.166 0.126 0.174 5.25% 10.50% 15.75% 0.143
Tl, ppm 0.71 0.10 0.51 0.91 0.41 1.00 13.92% 27.85% 41.77% 0.67
U, ppm 2.78 0.191 2.40 3.16 2.21 3.35 6.88% 13.76% 20.64% 2.64
W, ppm 4.22 0.401 3.42 5.02 3.02 5.43 9.49% 18.99% 28.48% 4.01
Y, ppm 19.1 1.42 16.3 22.0 14.9 23.4 7.44% 14.88% 22.32% 18.2
Yb, ppm 1.76 0.143 1.47 2.04 1.33 2.18 8.14% 16.28% 24.42% 1.67
Zn, wt.% 1.03 0.040 0.96 1.11 0.92 1.15 3.85% 7.70% 11.55% 0.98
4-Acid Digestion
Ag, ppm 20.4 1.06 18.3 22.5 17.2 23.6 5.19% 10.38% 15.56% 19.4
Al, wt.% 5.04 0.329 4.38 5.70 4.05 6.03 6.54% 13.08% 19.61% 4.79
As, ppm 77 5.3 67 88 62 93 6.86% 13.72% 20.59% 74
Be, ppm 1.39 0.24 0.91 1.86 0.68 2.09 17.03% 34.06% 51.09% 1.32
Bi, ppm 17.7 1.77 14.2 21.3 12.4 23.0 9.98% 19.96% 29.94% 16.8
Ca, wt.% 1.38 0.074 1.23 1.52 1.15 1.60 5.35% 10.69% 16.04% 1.31
Cd, ppm 54 3.9 46 62 42 66 7.25% 14.50% 21.75% 51
Ce, ppm 45.6 5.4 34.7 56.5 29.3 61.9 11.92% 23.84% 35.76% 43.3
Co, ppm 222 10 203 241 193 250 4.30% 8.59% 12.89% 210
Cr, ppm 24.8 4.8 15.2 34.5 10.4 39.3 19.37% 38.75% 58.12% 23.6
Cs, ppm 2.85 0.109 2.63 3.07 2.53 3.18 3.82% 7.65% 11.47% 2.71
Cu, wt.% 1.73 0.064 1.61 1.86 1.54 1.93 3.68% 7.36% 11.04% 1.65
Fe, wt.% 13.42 0.778 11.87 14.98 11.09 15.76 5.80% 11.59% 17.39% 12.75
Ga, ppm 21.7 1.40 18.9 24.5 17.5 25.9 6.45% 12.90% 19.35% 20.6
Hf, ppm 3.97 0.247 3.48 4.47 3.24 4.71 6.20% 12.41% 18.61% 3.78
In, ppm 2.10 0.093 1.91 2.28 1.82 2.38 4.44% 8.88% 13.32% 1.99
K, wt.% 1.45 0.117 1.22 1.69 1.10 1.80 8.07% 16.14% 24.21% 1.38
La, ppm 21.6 3.7 14.1 29.0 10.4 32.7 17.18% 34.36% 51.53% 20.5
Li, ppm 15.7 1.35 13.0 18.4 11.7 19.8 8.62% 17.23% 25.85% 14.9
Lu, ppm 0.24 0.03 0.18 0.30 0.15 0.33 12.25% 24.49% 36.74% 0.23
Mg, wt.% 1.20 0.091 1.02 1.38 0.93 1.47 7.54% 15.09% 22.63% 1.14
Mn, wt.% 0.060 0.004 0.052 0.068 0.048 0.072 6.44% 12.88% 19.33% 0.057
Mo, ppm 9.55 0.696 8.16 10.94 7.46 11.64 7.29% 14.57% 21.86% 9.07
Na, wt.% 1.12 0.070 0.98 1.26 0.91 1.33 6.24% 12.48% 18.72% 1.07
Nb, ppm 8.58 0.729 7.12 10.04 6.39 10.77 8.50% 16.99% 25.49% 8.15
Ni, ppm 16.8 3.2 10.3 23.3 7.1 26.5 19.27% 38.54% 57.80% 16.0
P, wt.% 0.043 0.005 0.033 0.053 0.029 0.058 11.32% 22.64% 33.95% 0.041
Pb, wt.% 0.250 0.007 0.235 0.265 0.228 0.272 2.97% 5.93% 8.90% 0.237
Rb, ppm 62 3.7 55 70 51 73 5.87% 11.74% 17.61% 59
S, wt.% 9.06 0.321 8.42 9.70 8.10 10.02 3.54% 7.09% 10.63% 8.61
Sb, ppm 27.6 1.91 23.8 31.4 21.9 33.3 6.91% 13.82% 20.73% 26.2
Sc, ppm 8.32 1.35 5.62 11.02 4.27 12.37 16.22% 32.43% 48.65% 7.90
Se, ppm 18.7 1.86 14.9 22.4 13.1 24.2 9.97% 19.94% 29.90% 17.7
Sn, ppm 5.94 0.264 5.41 6.46 5.15 6.73 4.44% 8.88% 13.32% 5.64
Sr, ppm 80 7.7 64 95 57 103 9.66% 19.32% 28.98% 76
Ta, ppm <1 IND IND IND IND IND IND IND IND IND
Tb, ppm 0.53 0.05 0.42 0.63 0.37 0.69 10.05% 20.09% 30.14% 0.50
Te, ppm 0.58 0.08 0.43 0.73 0.35 0.81 13.03% 26.06% 39.09% 0.55
Th, ppm 6.40 0.87 4.67 8.13 3.80 9.00 13.53% 27.07% 40.60% 6.08
Ti, wt.% 0.139 0.012 0.116 0.163 0.105 0.174 8.34% 16.68% 25.02% 0.132
Tl, ppm 0.74 0.08 0.57 0.90 0.49 0.98 11.09% 22.17% 33.26% 0.70
U, ppm 2.63 0.118 2.39 2.86 2.28 2.98 4.49% 8.97% 13.46% 2.50
V, ppm 26.0 3.5 19.1 32.9 15.6 36.4 13.31% 26.62% 39.92% 24.7
W, ppm 4.28 0.365 3.55 5.01 3.18 5.37 8.53% 17.06% 25.59% 4.06
Y, ppm 13.3 1.25 10.8 15.8 9.6 17.1 9.38% 18.76% 28.15% 12.7
Yb, ppm 1.47 0.077 1.32 1.63 1.24 1.70 5.24% 10.47% 15.71% 1.40
Zn, wt.% 1.03 0.030 0.97 1.09 0.94 1.12 2.96% 5.93% 8.89% 0.98
Zr, ppm 150 6 137 162 131 169 4.19% 8.38% 12.57% 142
Ag, ppm 20.6 0.67 19.3 22.0 18.6 22.6 3.24% 6.49% 9.73% 19.6
As, ppm 79 10 58 99 48 109 12.82% 25.64% 38.47% 75
Cu, wt.% 1.74 0.042 1.66 1.82 1.61 1.87 2.43% 4.85% 7.28% 1.65
Fe, wt.% 13.41 0.400 12.61 14.21 12.21 14.61 2.99% 5.97% 8.96% 12.74
Mo, ppm 8.42 1.64 5.14 11.71 3.50 13.35 19.49% 38.99% 58.48% 8.00
Pb, wt.% 0.251 0.007 0.238 0.264 0.231 0.271 2.63% 5.26% 7.88% 0.238
Zn, wt.% 1.02 0.043 0.93 1.10 0.89 1.15 4.22% 8.44% 12.66% 0.97
Ag, ppm 20.4 1.15 18.1 22.7 17.0 23.9 5.62% 11.24% 16.86% 19.4
Al, wt.% 1.80 0.091 1.62 1.98 1.53 2.07 5.03% 10.06% 15.09% 1.71
As, ppm 76 6.8 62 89 55 96 8.99% 17.99% 26.98% 72
Au, ppm 0.797 0.038 0.720 0.873 0.682 0.911 4.80% 9.60% 14.40% 0.757
B, ppm < 10 IND IND IND IND IND IND IND IND IND
Be, ppm 0.37 0.07 0.22 0.52 0.15 0.59 20.15% 40.31% 60.46% 0.35
Bi, ppm 16.9 2.4 12.0 21.7 9.6 24.1 14.33% 28.66% 42.99% 16.0
Ca, wt.% 1.09 0.060 0.97 1.21 0.91 1.27 5.51% 11.01% 16.52% 1.03
Cd, ppm 52 3.7 45 60 41 64 7.08% 14.15% 21.23% 50
Ce, ppm 36.4 5.2 26.1 46.7 20.9 51.8 14.16% 28.32% 42.48% 34.6
Co, ppm 216 11 194 237 184 248 4.97% 9.94% 14.91% 205
Cr, ppm 19.4 2.1 15.3 23.5 13.3 25.6 10.58% 21.16% 31.74% 18.4
Cs, ppm 0.75 0.13 0.49 1.02 0.36 1.15 17.53% 35.06% 52.58% 0.71
Cu, wt.% 1.72 0.066 1.59 1.86 1.53 1.92 3.83% 7.66% 11.49% 1.64
Fe, wt.% 13.01 0.546 11.92 14.10 11.37 14.65 4.19% 8.39% 12.58% 12.36
Ga, ppm 11.9 1.03 9.8 14.0 8.8 15.0 8.66% 17.32% 25.98% 11.3
Hf, ppm 1.32 0.21 0.90 1.74 0.69 1.94 15.86% 31.72% 47.58% 1.25
Hg, ppm 0.83 0.08 0.66 1.00 0.57 1.08 10.24% 20.48% 30.72% 0.79
In, ppm 1.94 0.107 1.72 2.15 1.62 2.26 5.52% 11.04% 16.57% 1.84
K, wt.% 0.175 0.027 0.121 0.230 0.094 0.257 15.54% 31.07% 46.61% 0.166
La, ppm 17.9 2.4 13.0 22.7 10.6 25.1 13.56% 27.13% 40.69% 17.0
Li, ppm 10.0 1.1 7.8 12.3 6.7 13.4 11.13% 22.25% 33.38% 9.5
Lu, ppm 0.12 0.010 0.10 0.14 0.09 0.15 8.41% 16.82% 25.23% 0.11
Mg, wt.% 1.11 0.070 0.97 1.25 0.90 1.32 6.34% 12.68% 19.02% 1.05
Mn, wt.% 0.057 0.003 0.051 0.063 0.048 0.066 5.06% 10.12% 15.19% 0.054
Mo, ppm 8.38 1.29 5.79 10.96 4.50 12.25 15.44% 30.88% 46.32% 7.96
Na, wt.% 0.068 0.011 0.046 0.090 0.036 0.101 15.92% 31.84% 47.76% 0.065
Nb, ppm <1 IND IND IND IND IND IND IND IND IND
Ni, ppm 15.6 1.7 12.2 19.0 10.5 20.7 10.85% 21.71% 32.56% 14.8
P, wt.% 0.040 0.002 0.035 0.044 0.033 0.047 5.78% 11.57% 17.35% 0.038
Pb, wt.% 0.252 0.010 0.232 0.271 0.223 0.281 3.83% 7.67% 11.50% 0.239
S, wt.% 8.75 0.630 7.49 10.01 6.86 10.64 7.20% 14.40% 21.59% 8.31
Sb, ppm 20.2 4.1 12.0 28.4 7.9 32.5 20.37% 40.73% 61.10% 19.2
Sc, ppm 4.63 0.53 3.56 5.70 3.03 6.23 11.52% 23.03% 34.55% 4.40
Se, ppm 18.6 1.9 14.7 22.4 12.8 24.4 10.41% 20.82% 31.22% 17.6
Sn, ppm 4.07 0.213 3.64 4.49 3.43 4.71 5.24% 10.48% 15.72% 3.86
Sr, ppm 14.2 1.5 11.2 17.1 9.8 18.6 10.38% 20.76% 31.14% 13.5
Ta, ppm < 0.05 IND IND IND IND IND IND IND IND IND
Tb, ppm 0.34 0.032 0.28 0.41 0.25 0.44 9.31% 18.62% 27.93% 0.32
Te, ppm 0.57 0.08 0.41 0.72 0.33 0.80 13.69% 27.39% 41.08% 0.54
Th, ppm 4.72 0.325 4.07 5.37 3.74 5.69 6.89% 13.79% 20.68% 4.48
Ti, wt.% < 0.06 IND IND IND IND IND IND IND IND IND
Tl, ppm 0.26 0.04 0.18 0.33 0.15 0.37 14.31% 28.63% 42.94% 0.24
U, ppm 1.43 0.104 1.23 1.64 1.12 1.75 7.23% 14.45% 21.68% 1.36
V, ppm 15.8 1.52 12.8 18.8 11.2 20.4 9.61% 19.22% 28.83% 15.0
W, ppm 2.62 0.30 2.01 3.23 1.71 3.53 11.62% 23.23% 34.85% 2.49
Y, ppm 7.43 1.01 5.40 9.46 4.39 10.47 13.65% 27.30% 40.95% 7.06
Yb, ppm 0.80 0.021 0.76 0.84 0.74 0.86 2.65% 5.30% 7.96% 0.76
Zn, wt.% 1.01 0.038 0.94 1.09 0.90 1.13 3.76% 7.52% 11.28% 0.96
Zr, ppm 50 3.4 44 57 40 61 6.77% 13.53% 20.30% 48
5% window
High
0.868
9.52
23.8
5.51
90
1464
18.6
1.44
57
52.4
236
31.5
3.15
1.81
14.12
24.9
2.15
1.60
26.1
18.9
1.29
0.064
10.7
11.0
26.1
IND
0.260
6.86
70
9.27
29.4
IND
25.68
94
7.65
0.158
0.74
2.92
4.43
20.1
1.84
1.09
21.4
5.29
81
1.46
18.6
1.44
57
47.9
233
26.1
3.00
1.82
14.09
22.8
4.17
2.20
1.52
22.6
16.5
0.26
1.26
0.063
10.03
1.18
9.01
17.7
0.045
0.262
65
9.51
29.0
8.74
19.6
6.23
84
IND
0.55
0.61
6.72
0.146
0.77
2.76
27.3
4.49
14.0
1.55
1.08
157
21.7
83
1.83
14.08
8.84
0.264
1.07
21.4
1.89
80
0.837
IND
0.39
17.7
1.14
55
38.2
227
20.4
0.79
1.81
13.66
12.5
1.38
0.87
2.03
0.184
18.8
10.5
0.12
1.16
0.060
8.79
0.071
IND
16.4
0.042
0.264
9.18
21.2
4.86
19.5
4.27
14.9
IND
0.36
0.60
4.95
IND
0.27
1.51
16.6
2.75
7.80
0.84
1.07
53
Analytical results for Au in OREAS 623 (Certified Value 0.827 ppm)
Au Round Replicate Lab Lab Lab Lab Lab Lab
No No 00 01 02 04 05 06
INAA FA*AAS FA*AAS FA*OES FA*AAS FA*AAS
1.0g 30g 30g 30g 30g 30g
1 1 0.829 0.792 0.854 0.800 0.824 0.740
1 2 0.836 0.763 0.849 0.721 0.821 0.690
1 3 0.866 0.778 0.862 0.747 0.819 0.780
1 4 0.828 0.792 0.832 0.736 0.822 0.830
1 5 0.873 0.792 0.865 0.756 0.812 0.810
1 6 0.866 0.809 0.865 0.795 0.810 0.770
7 0.853
8 0.846
9 0.796
10 0.822
11 0.813
12 0.838
13 0.802
14 0.846
15 0.838
16 0.852
17 0.874
18 0.857
19 0.842
20 0.840
Mean 0.841 0.788 0.855 0.759 0.818 0.770
Median 0.841 0.792 0.858 0.752 0.820 0.775
Std Dev. 0.022 0.016 0.013 0.032 0.006 0.050
Rel.Std.Dev. 2.59% 1.98% 1.52% 4.21% 0.70% 6.52%
PDM3 1.72% -4.71% 3.38% -8.16% -1.04% -6.85%
Z-Score (Absolute) NA 1.28 0.47 2.02 0.49 1.32
Analytical results for Pd in OREAS 623 (Indicative Value < 5 ppb)

Pd Round Replicate Lab
No No 22
FA*OES
40g
1 1 <5
1 2 <5
1 3 <5
1 4 <5
1 5 <5
1 6 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA
Analytical results for Pt in OREAS 623 (Indicative Value < 5 ppb)

Pt Round Replicate Lab
No No 22
FA*OES
40g
1 1 <5
1 2 <5
1 3 <5
1 4 <5
1 5 <5
1 6 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Lab Lab Lab Lab Lab Lab Lab Lab Lab
07 08 09 10 11 12 13 14 15
FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*OES FA*AAS
30g 30g 30g 25g 30g 20g 30g 25g 40g
0.849 0.847 0.860 0.880 0.840 0.880 0.817 0.830 0.887
0.868 0.844 0.840 0.860 0.863 0.860 0.820 0.800 0.876
0.858 0.850 0.870 0.870 0.901 0.840 0.813 0.860 0.864
0.857 0.845 0.860 0.860 0.863 0.860 0.814 0.840 0.850
0.864 0.857 0.860 0.870 0.890 0.840 0.820 0.830 0.876
0.870 0.810 0.870 0.870 0.880 0.860 0.807 0.860 0.880
0.861 0.842 0.860 0.868 0.873 0.857 0.815 0.837 0.872

0.861 0.846 0.860 0.870 0.871 0.860 0.816 0.835 0.876
0.008 0.016 0.011 0.008 0.022 0.015 0.005 0.023 0.013
0.91% 1.95% 1.27% 0.87% 2.52% 1.76% 0.62% 2.69% 1.51%
4.16% 1.88% 4.04% 5.05% 5.59% 3.64% -1.37% 1.22% 5.51%
0.64 0.31 0.61 0.83 0.94 0.52 0.56 0.00 0.93
16 17 19 20 21 22 23 24 25
FA*AAS FA*AAS FA*AAS FA*AAS FA*AAS FA*OES FA*AAS FA*AAS FA*AAS
30g 30g 30g 30g 30g 40g 30g 30g 30g
0.850 0.832 0.809 0.831 0.740 0.823 0.832 0.753 0.827
0.890 0.850 0.791 0.805 0.760 0.857 0.813 0.796 0.824
0.860 0.858 0.805 0.785 0.760 0.844 0.794 0.751 0.814
0.870 0.825 0.808 0.811 0.700 0.859 0.770 0.772 0.826
0.860 0.819 0.798 0.771 0.770 0.837 0.837 0.782 0.822
0.850 0.844 0.801 0.829 0.760 0.858 0.819 0.765 0.814
0.863 0.838 0.802 0.805 0.748 0.846 0.811 0.770 0.821

0.860 0.838 0.803 0.808 0.760 0.851 0.816 0.769 0.823
0.015 0.015 0.007 0.024 0.026 0.014 0.025 0.017 0.006
1.74% 1.81% 0.85% 2.96% 3.42% 1.71% 3.10% 2.25% 0.71%
4.44% 1.38% -2.98% -2.57% -9.47% 2.39% -1.91% -6.87% -0.66%
0.70 0.03 0.90 0.82 2.05 0.25 0.67 1.74 0.40
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.827
7.000
Indicative
1.00
ppb
0.00
0.00
1
1
16
<5
7
Indicative
1.00
ppb
0.00
0.00
1
1
16
<5
7
Analytical results for C in OREAS 623 (Indicative Value 0.427 wt.%)
C Round Replicate Lab
No No 02
IRC
1 1 0.424
1 2 0.428
1 3 0.424
1 4 0.428
1 5 0.429
1 6 0.428
Mean 0.427
Median 0.428
Std Dev. 0.002
Rel.Std.Dev. 0.52%
PDM3 0.00%
Analytical results for S in OREAS 623 (Certified Value 9.07 wt.%)

S Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 04 05 06 08
IRC IRC IRC IRC IRC IRC
1 1 9.27 9.21 9.27 8.73 8.03 9.33

1 2 9.38 8.82 9.05 8.91 8.95 9.36
1 3 9.35 8.94 9.09 9.10 8.82 9.40
1 4 9.34 9.13 9.10 8.98 8.88 9.38
1 5 9.44 8.84 9.00 9.34 8.72 9.38
1 6 9.31 9.07 9.02 8.87 8.75 9.37
Mean 9.35 9.00 9.09 8.99 8.69 9.37
Median 9.34 9.00 9.07 8.95 8.79 9.38
Std Dev. 0.058 0.160 0.097 0.211 0.335 0.024
Rel.Std.Dev. 0.63% 1.77% 1.07% 2.35% 3.85% 0.25%
PDM3 3.10% -0.72% 0.24% -0.87% -4.14% 3.34%
Z-Score (Absolute) 2.31 0.10 0.50 0.20 1.34 2.46
09 10 11 12 13 14 15 16 17
IRC IRC IRC IRC IRC IRC IRC IRC IRC
9.15 9.06 8.89 8.50 9.03 8.92 9.04 9.23 8.82

9.23 9.06 8.91 8.41 8.94 8.78 8.79 9.12 9.34
9.37 9.14 9.06 8.51 9.12 8.96 8.87 9.21 9.01
9.16 8.92 8.95 8.31 8.92 8.90 9.00 9.22 8.97
9.05 9.26 8.50 8.66 8.87 8.95 9.08 9.23 8.64
9.13 10.30 9.02 9.24 9.06 8.91 9.11 9.16 9.24
9.18 9.29 8.89 8.61 8.99 8.90 8.98 9.20 9.00
9.16 9.10 8.93 8.50 8.98 8.92 9.02 9.22 8.99
0.109 0.507 0.201 0.332 0.096 0.065 0.128 0.045 0.259
1.19% 5.46% 2.26% 3.86% 1.07% 0.73% 1.42% 0.49% 2.88%
1.27% 2.46% -1.97% -5.09% -0.85% -1.80% -0.95% 1.41% -0.70%
1.15 0.50 0.35 3.76 0.19 0.79 0.25 1.24 0.09
Lab Lab Lab Lab Lab Lab
19 21 22 23 24 25
IRC IRC IRC IRC IRC IRC
9.00 8.82 9.27 9.04 9.10 8.98

9.06 8.96 9.55 9.14 9.03 9.21
9.06 8.88 9.44 9.35 9.11 9.10
8.98 9.20 9.57 9.31 9.09 9.24
8.98 8.90 9.44 9.01 9.01 9.69
9.02 8.78 9.52 9.10 9.34 9.13
9.02 8.92 9.46 9.16 9.11 9.23
9.01 8.89 9.48 9.12 9.09 9.17
0.037 0.149 0.110 0.141 0.118 0.245
0.41% 1.67% 1.16% 1.54% 1.30% 2.66%
-0.55% -1.58% 4.39% 1.01% 0.51% 1.74%
0.00 0.65 3.13 0.99 0.67 0.80
Indicative
1.00
wt.%
3.00
3.00
1.000
3.000
16.000
0.427
9.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
9.07
9.00
Analytical results for Ag in OREAS 623 (Certified Value 22.7 ppm)
Ag Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 12 21 22
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*MS PF*MS
1 1 24.4 18.0 20.0 < 20 20.0 25.0

1 2 23.9 16.0 30.0 < 20 20.0 20.0
1 3 23.4 19.0 30.0 < 20 25.0 25.0
1 4 21.8 19.0 30.0 < 20 20.0 25.0
1 5 24.3 19.0 20.0 < 20 20.0 25.0
1 6 23.0 19.0 50.0 20.0 25.0 20.0
Mean 23.5 18.3 30.0 20.0 21.7 23.3
Median 23.6 19.0 30.0 20.0 20.0 25.0
Std Dev. 1.0 1.2 11.0 2.6 2.6
Rel.Std.Dev. 4.19% 6.61% 36.51% 11.92% 11.07%
PDM3 3.55% -19.06% 32.44% -11.70% -4.35% 3.01%
Z-Score (Absolute) 0.29 1.12 1.06 3.28 0.25 0.25
Analytical results for Al in OREAS 623 (Certified Value 5.25 wt.%)

Al Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
PF*OES/MSPF*OES/MS PF*OES PF*OES PF*OES PF*OES
1 1 5.25 5.02 5.09 4.61 5.17 5.27

1 2 5.27 5.01 5.13 4.30 5.36 5.32
1 3 5.29 4.96 5.16 4.68 5.21 5.19
1 4 5.06 5.04 5.22 4.68 5.31 5.04
1 5 5.38 5.00 5.17 4.62 5.39 5.15
1 6 5.30 5.03 5.12 4.50 5.90 5.27
Mean 5.26 5.01 5.15 4.57 5.39 5.21
Median 5.28 5.02 5.15 4.62 5.34 5.23
Std Dev. 0.107 0.028 0.045 0.146 0.264 0.103
Rel.Std.Dev. 2.04% 0.56% 0.88% 3.19% 4.90% 1.97%
PDM3 0.13% -4.57% -1.93% -13.04% 2.67% -0.82%
Z-Score (Absolute) 0.05 1.76 0.74 4.63 0.28 0.31
Analytical results for As in OREAS 623 (Certified Value 86 ppm)

As Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
PF*OES/MSPF*OES/MS PF*MS PF*MS PF*OES PF*OES
1 1 85 83 80 80 181 200
1 2 86 84 80 100 213 200
1 3 85 87 70 100 161 < 100
1 4 82 86 80 100 226 < 100
1 5 85 86 80 90 191 100
1 6 82 89 80 140 212 100
Mean 84 86 78 102 197 150
Median 85 86 80 100 202 150
Std Dev. 2 2 4 20 24 58
Rel.Std.Dev. 2.10% 2.49% 5.21% 20.08% 12.22% 38.49%
PDM3 -2.14% -0.20% -8.92% 18.21% 129.44% 74.41%
Z-Score (Absolute) 0.14 0.00 0.62 0.67 9.21 5.30
Analytical results for B in OREAS 623 (Indicative Value < 50 ppm)

B Round Replicate Lab Lab Lab Lab
No No 13 14 21 22
PF*OES/MS PF*OES PF*OES PF*OES
1 1 < 50 < 50 < 20 20

1 2 < 50 < 50 < 20 20
1 3 < 50 < 50 < 20 20
1 4 < 50 < 50 < 20 20
1 5 < 50 < 50 < 20 20
1 6 < 50 < 50 < 20 20
Mean 20
Median 20
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3
Z-Score (Absolute) NA NA NA NA
Analytical results for Ba in OREAS 623 (Certified Value 1395 ppm)

Ba Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 12 13
PF*OES/MSPF*OES/MS PF*OES PF*OES PF*OES PF*OES/MS
1 1 1356 1400 1300 1277 1620 1408

1 2 1410 1370 1220 1571 1540 1401
1 3 1399 1400 1330 1415 1640 1372
1 4 1325 1390 1350 1461 1430 1389
1 5 1395 1400 1320 1474 1490 1396
1 6 1403 1440 1300 1411 1580 1390
Mean 1382 1400 1303 1435 1550 1393
Median 1397 1400 1310 1438 1560 1393
Std Dev. 33 23 45 97 80 12
Rel.Std.Dev. 2.41% 1.63% 3.45% 6.73% 5.16% 0.88%
PDM3 -0.94% 0.39% -6.54% 2.89% 11.14% -0.14%
Z-Score (Absolute) 0.06 0.06 1.46 0.60 2.41 0.06
Analytical results for Be in OREAS 623 (Indicative Value 1.61 ppm)

Be Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
PF*OES/MSPF*OES/MS PF*OES PF*MS PF*OES PF*OES/MS
1 1 <5 <5 < 10 1.70 11.00 1.52

1 2 <5 <5 < 10 1.70 5.00 1.36
1 3 <5 <5 < 10 1.70 <5 1.34
1 4 <5 <5 < 10 1.80 <5 1.51
1 5 <5 <5 < 10 1.60 <5 1.56
1 6 <5 <5 < 10 0.90 11.00 1.65
Mean 1.57 9.00 1.49
Median 1.70 11.00 1.51
Std Dev. 0.333 3.464 0.119
Rel.Std.Dev. 21.23% 38.49% 7.98%
PDM3 -2.75% 458.68% -7.63%
Z-Score (Absolute) NA NA NA 0.11 27.42 1.32
Analytical results for Bi in OREAS 623 (Certified Value 17.7 ppm)

Bi Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
PF*OES/MSPF*OES/MS PF*MS PF*MS PF*OES/MS PF*MS
1 1 18.1 17.0 20.0 10.1 15.8 18.6

1 2 17.9 17.4 20.0 11.1 16.5 19.4
1 3 17.8 17.6 20.0 10.8 16.0 18.2
1 4 17.0 17.8 20.0 11.4 16.1 18.5
1 5 18.0 17.6 20.0 10.6 16.0 18.5
1 6 17.8 17.7 20.0 13.8 16.2 18.0
Mean 17.8 17.5 20.0 11.3 16.1 18.5
Median 17.9 17.6 20.0 11.0 16.1 18.5
Std Dev. 0.403 0.286 0.000 1.302 0.236 0.480
Rel.Std.Dev. 2.27% 1.63% 0.00% 11.52% 1.47% 2.59%
PDM3 0.34% -1.02% 13.01% -36.15% -9.07% 4.73%
Z-Score (Absolute) 0.15 0.46 2.70 9.01 2.27 0.83
Analytical results for Ca in OREAS 623 (Certified Value 1.37 wt.%)

Ca Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 1.38 1.40 1.38 1.94 1.31 1.37

1 2 1.37 1.40 1.37 1.82 1.43 1.35
1 3 1.36 1.40 1.41 1.96 1.36 1.33
1 4 1.32 1.40 1.42 1.95 1.39 1.28
1 5 1.39 1.40 1.41 1.95 1.43 1.33
1 6 1.39 1.40 1.39 1.92 1.73 1.35
Mean 1.37 1.40 1.40 1.92 1.44 1.34
Median 1.38 1.40 1.40 1.94 1.41 1.34
Std Dev. 0.026 0.000 0.020 0.052 0.148 0.032
Rel.Std.Dev. 1.89% 0.00% 1.41% 2.72% 10.29% 2.39%
PDM3 0.04% 2.20% 1.95% 40.40% 5.24% -2.54%
Z-Score (Absolute) 0.33 0.02 0.02 6.42 0.17 0.74
Analytical results for Cd in OREAS 623 (Certified Value 55 ppm)
Cd Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 13 14
PF*OES/MSPF*OES/MS PF*OES PF*OES PF*OES/MS PF*MS
1 1 60 54 50 73 55 56
1 2 61 53 50 46 53 54
1 3 60 54 50 47 53 53
1 4 57 54 50 49 52 54
1 5 59 54 50 50 54 57
1 6 60 55 50 47 53 54
Mean 60 54 50 52 53 55
Median 60 54 50 48 53 54
Std Dev. 1.3 0.7 0.0 10.4 1.1 1.5
Rel.Std.Dev. 2.11% 1.22% 0.00% 19.99% 1.97% 2.75%
PDM3 9.23% -1.13% -8.42% -4.76% -2.35% 0.13%
Z-Score (Absolute) 1.07 0.07 0.87 1.32 0.20 0.07
Analytical results for Ce in OREAS 623 (Certified Value 49.9 ppm)

Ce Round Replicate Lab Lab Lab Lab Lab
No No 02 04 06 21 22
PF*OES/MSPF*OES/MS PF*MS PF*MS PF*MS
1 1 50.0 51.1 39.2 50.2 52.0

1 2 49.3 51.1 43.4 48.1 51.5
1 3 49.8 52.9 42.3 51.9 53.0
1 4 49.0 53.3 43.6 51.7 52.0
1 5 52.6 53.8 41.5 54.7 52.0
1 6 55.3 52.3 29.1 55.2 52.0
Mean 51.0 52.4 39.9 52.0 52.1
Median 49.9 52.6 41.9 51.8 52.0
Std Dev. 2.471 1.132 5.502 2.686 0.492
Rel.Std.Dev. 4.85% 2.16% 13.81% 5.17% 0.94%
PDM3 2.20% 5.06% -20.13% 4.16% 4.39%
Z-Score (Absolute) 1.47 0.67 14.93 0.00 0.17
Analytical results for Co in OREAS 623 (Certified Value 225 ppm)

Co Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*OES PF*OES
1 1 240 245 230 190 206 230

1 2 239 247 220 180 222 180
1 3 236 256 220 200 218 220
1 4 224 254 230 200 212 200
1 5 226 255 230 200 221 210
1 6 220 263 220 200 218 240
Mean 231 253 225 195 216 213
Median 231 255 225 200 218 215
Std Dev. 8 7 5 8 6 22
Rel.Std.Dev. 3.67% 2.58% 2.43% 4.29% 2.81% 10.13%
PDM3 2.50% 12.53% -0.06% -13.38% -3.98% -5.24%
Z-Score (Absolute) 1.44 5.81 0.32 5.48 1.39 0.65
Analytical results for Cr in OREAS 623 (Certified Value 30 ppm)

Cr Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 12
1 1 32.1 20.0 < 100 30.0 46.0 30.0

1 2 27.3 30.0 < 100 30.0 33.0 30.0
1 3 28.7 20.0 < 100 30.0 23.0 30.0
1 4 29.2 20.0 < 100 30.0 31.0 30.0
1 5 31.2 20.0 < 100 30.0 28.0 30.0
1 6 31.1 20.0 < 100 30.0 38.0 30.0
Mean 29.9 21.7 30.0 33.2 30.0
Median 30.1 20.0 30.0 32.0 30.0
Std Dev. 1.8 4.1 0.0 8.0 0.0
Rel.Std.Dev. 6.08% 18.84% 0.00% 24.23% 0.00%
PDM3 -0.17% -27.67% 0.14% 10.72% 0.14%
Z-Score (Absolute) 0.04 4.14 NA 0.00 1.31 0.00
Analytical results for Cs in OREAS 623 (Certified Value 3 ppm)

Cs Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 2.88 2.60 < 10 3.40 2.73 2.90

1 2 2.83 2.50 < 10 3.50 2.64 2.90
1 3 2.75 2.60 < 10 3.50 2.68 3.00
1 4 2.64 2.60 < 10 3.60 2.73 3.10
1 5 2.72 2.60 < 10 3.40 2.76 2.80
1 6 2.75 2.70 < 10 1.60 2.78 3.10
Mean 2.76 2.60 3.17 2.72 2.97
Median 2.75 2.60 3.45 2.73 2.95
Std Dev. 0.084 0.063 0.771 0.052 0.121
Rel.Std.Dev. 3.05% 2.43% 24.35% 1.93% 4.08%
PDM3 -7.99% -13.38% 5.50% -9.44% -1.17%
Analytical results for Cu in OREAS 623 (Certified Value 1.73 wt.%)

Cu Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
PF*OES PF*OES/MS PF*OES PF*OES PF*OES PF*OES
1 1 1.73 > 10000 1.79 1.87 1.65 1.68

1 2 1.71 > 10000 1.69 1.77 1.89 1.65
1 3 1.67 > 10000 1.71 2.12 1.92 1.63
1 4 1.69 > 10000 1.72 1.95 1.83 1.62
1 5 1.67 > 10000 1.82 2.26 1.81 1.70
1 6 1.69 > 10000 1.73 2.01 1.75 1.76
Mean 1.69 1.74 2.00 1.81 1.67
Median 1.69 1.73 1.98 1.82 1.67
Std Dev. 0.021 0.050 0.176 0.095 0.050
Rel.Std.Dev. 1.26% 2.89% 8.80% 5.27% 2.99%
PDM3 -1.99% 0.97% 15.65% 4.68% -3.08%
Z-Score (Absolute) 0.61 NA 0.14 3.85 1.07 0.89
Analytical results for Dy in OREAS 623 (Indicative Value 3.46 ppm)

Dy Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
PF*OES/MSPF*OES/MS PF*MS PF*MS
1 1 3.47 3.20 3.50 3.50

1 2 3.45 3.16 3.80 4.00
1 3 3.43 3.27 3.60 3.50
1 4 3.25 3.29 4.00 3.00
1 5 3.48 3.24 3.60 3.50
1 6 3.62 3.22 3.90 3.00
Mean 3.45 3.23 3.73 3.42
Median 3.46 3.23 3.70 3.50
Std Dev. 0.117 0.047 0.197 0.376
Rel.Std.Dev. 3.38% 1.47% 5.27% 11.02%
PDM3 -0.22% -6.58% 7.98% -1.18%
Z-Score (Absolute) 0.10 1.25 1.84 0.10
Analytical results for Er in OREAS 623 (Indicative Value 1.88 ppm)

Er Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 1.77 1.75 2.20 2.00

1 2 1.73 1.77 1.90 2.00
1 3 1.74 1.81 2.20 1.50
1 4 1.64 1.78 2.30 2.50
1 5 1.77 1.82 1.80 1.50
1 6 1.84 1.81 2.00 2.00
Mean 1.75 1.79 2.07 1.92
Median 1.76 1.80 2.10 2.00
Std Dev. 0.066 0.028 0.197 0.376
Rel.Std.Dev. 3.80% 1.54% 9.51% 19.64%
PDM3 -7.04% -4.80% 9.91% 1.93%
Z-Score (Absolute) 0.84 0.51 1.71 0.51
Analytical results for Eu in OREAS 623 (Indicative Value 1.6 ppm)
Eu Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 1.41 1.38 1.90 1.60

1 2 1.39 1.44 1.90 1.80
1 3 1.40 1.44 1.90 1.60
1 4 1.35 1.45 2.10 1.60
1 5 1.48 1.44 2.00 1.40
1 6 1.49 1.47 1.90 1.60
Mean 1.42 1.44 1.95 1.60
Median 1.40 1.44 1.90 1.60
Std Dev. 0.057 0.030 0.084 0.126
Rel.Std.Dev. 3.98% 2.10% 4.29% 7.91%
PDM3 -11.33% -10.30% 21.75% -0.11%
Z-Score (Absolute) 0.74 0.61 3.24 0.61
Analytical results for Fe in OREAS 623 (Certified Value 13.45 wt.%)

Fe Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 12.83 13.50 13.60 13.00 13.81 13.35

1 2 12.96 13.60 13.50 12.20 15.59 13.35
1 3 13.13 14.00 13.60 13.80 14.88 13.05
1 4 12.52 13.50 13.70 13.40 14.84 12.85
1 5 13.39 13.50 13.70 13.80 15.07 13.30
1 6 13.13 13.80 13.50 12.90 14.62 13.45
Mean 13.00 13.65 13.60 13.18 14.80 13.23
Median 13.05 13.55 13.60 13.20 14.86 13.33
Std Dev. 0.300 0.207 0.089 0.615 0.586 0.227
Rel.Std.Dev. 2.31% 1.52% 0.66% 4.66% 3.96% 1.72%
PDM3 -3.36% 1.51% 1.14% -1.96% 10.07% -1.65%
Z-Score (Absolute) 1.40 0.25 0.13 0.43 3.17 0.63
Analytical results for Ga in OREAS 623 (Certified Value 23.7 ppm)

Ga Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 23.2 27.0 20.0 < 2.5 23.3 24.0

1 2 23.7 26.0 20.0 < 2.5 21.7 26.0
1 3 23.1 27.0 20.0 < 2.5 22.4 24.0
1 4 22.3 27.0 20.0 < 2.5 22.3 26.0
1 5 22.6 28.0 20.0 < 2.5 22.5 25.0
1 6 22.4 28.0 20.0 6.0 22.7 22.0
Mean 22.9 27.2 20.0 6.0 22.5 24.5
Median 22.8 27.0 20.0 6.0 22.5 24.5
Std Dev. 0.6 0.8 0.0 0.5 1.5
Rel.Std.Dev. 2.43% 2.77% 0.00% 2.33% 6.19%
PDM3 -3.53% 14.63% -15.61% -74.68% -5.07% 3.38%
Z-Score (Absolute) 0.00 1.26 0.84 4.93 0.11 0.48
Analytical results for Gd in OREAS 623 (Indicative Value 4.39 ppm)

Gd Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 4.17 4.10 5.00 4.00

1 2 4.25 3.99 4.80 4.00
1 3 4.36 4.11 5.00 4.00
1 4 4.19 4.05 5.10 4.00
1 5 4.60 4.18 5.10 4.00
1 6 4.91 4.15 5.40 4.00
Mean 4.41 4.10 5.07 4.00
Median 4.30 4.11 5.05 4.00
Std Dev. 0.289 0.069 0.197 0.000
Rel.Std.Dev. 6.55% 1.67% 3.88% 0.00%
PDM3 0.38% -6.75% 15.33% -8.95%
Z-Score (Absolute) 0.52 0.52 2.68 0.83
Analytical results for Ge in OREAS 623 (Indicative Value 1.65 ppm)

Ge Round Replicate Lab Lab Lab Lab Lab
No No 02 04 05 13 14
PF*OES/MSPF*OES/MS PF*MS PF*OES/MS PF*MS
1 1 1.63 1.00 < 10 5.38 <1

1 2 1.74 1.00 < 10 4.91 <1
1 3 1.70 2.00 < 10 5.41 <1
1 4 1.58 2.00 < 10 5.16 <1
1 5 1.66 2.00 < 10 5.59 <1
1 6 1.55 2.00 < 10 4.92 <1
Mean 1.64 1.67 5.23
Median 1.64 2.00 5.27
Std Dev. 0.072 0.516 0.276
Rel.Std.Dev. 4.41% 30.98% 5.29%
PDM3 -0.77% 0.77% 215.99%
Z-Score (Absolute) 0.67 0.00 NA 94.75 NA
Analytical results for Hf in OREAS 623 (Indicative Value 4.51 ppm)

Hf Round Replicate Lab Lab Lab
No No 02 04 22
PF*OES/MSPF*OES/MS PF*MS
1 1 4.63 4.00 5.20

1 2 4.56 4.00 4.60
1 3 4.56 4.00 4.80
1 4 4.36 4.00 5.60
1 5 4.46 4.00 5.00
1 6 4.60 4.00 4.80
Mean 4.53 4.00 5.00
Median 4.56 4.00 4.90
Std Dev. 0.101 0.000 0.358
Rel.Std.Dev. 2.23% 0.00% 7.16%
PDM3 0.40% -11.29% 10.89%
Z-Score (Absolute) 0.00 0.75 0.67
Analytical results for Ho in OREAS 623 (Indicative Value 0.61 ppm)

Ho Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 0.65 0.59 0.60 0.60

1 2 0.65 0.61 0.60 0.60
1 3 0.63 0.64 0.60 0.60
1 4 0.62 0.62 0.60 0.60
1 5 0.64 0.62 0.60 0.80
1 6 0.66 0.61 0.70 0.60
Mean 0.64 0.62 0.62 0.63
Median 0.64 0.62 0.60 0.60
Std Dev. 0.014 0.016 0.041 0.082
Rel.Std.Dev. 2.18% 2.67% 6.62% 12.89%
PDM3 4.26% 0.21% 0.48% 3.20%
Z-Score (Absolute) 2.91 0.67 0.67 0.67
Analytical results for In in OREAS 623 (Certified Value 2.04 ppm)

In Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 2.29 1.90 < 10 2.20 1.83 2.00

1 2 2.28 2.00 < 10 2.50 2.14 2.00
1 3 2.25 2.10 < 10 2.40 1.90 1.90
1 4 2.19 1.90 < 10 2.80 2.01 2.40
1 5 2.58 2.00 < 10 2.40 1.93 2.10
1 6 2.28 2.00 < 10 4.60 2.02 1.90
Mean 2.31 1.98 2.82 1.97 2.05
Median 2.28 2.00 2.45 1.97 2.00
Std Dev. 0.134 0.075 0.895 0.109 0.187
Rel.Std.Dev. 5.81% 3.80% 31.79% 5.51% 9.13%
PDM3 12.99% -2.99% 37.77% -3.65% 0.27%
Analytical results for K in OREAS 623 (Certified Value 1.53 wt.%)
K Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 1.57 1.50 1.30 1.78 1.74 1.50

1 2 1.53 1.50 1.40 1.68 1.62 1.50
1 3 1.55 1.40 1.30 1.79 1.59 1.50
1 4 1.51 1.50 1.40 1.78 1.65 1.40
1 5 1.67 1.50 1.40 1.76 1.67 1.40
1 6 1.54 1.50 1.40 1.73 1.45 1.50
Mean 1.56 1.48 1.37 1.75 1.62 1.47
Median 1.54 1.50 1.40 1.77 1.64 1.50
Std Dev. 0.056 0.041 0.052 0.042 0.098 0.052
Rel.Std.Dev. 3.56% 2.75% 3.78% 2.38% 6.02% 3.52%
PDM3 2.29% -2.82% -10.47% 14.87% 6.13% -3.91%
Z-Score (Absolute) 0.11 0.34 1.27 1.80 0.74 0.48
Analytical results for La in OREAS 623 (Certified Value 24.9 ppm)

La Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 21 22
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*MS PF*MS
1 1 25.1 24.7 19.9 25.0 31.6 26.0

1 2 25.3 24.7 22.0 26.0 30.1 26.0
1 3 25.5 25.6 21.7 14.0 32.1 26.5
1 4 25.3 25.7 22.2 15.0 31.8 26.5
1 5 26.9 25.7 21.2 15.0 30.4 26.0
1 6 27.9 25.4 15.1 20.0 31.4 25.5
Mean 26.0 25.3 20.3 19.2 31.2 26.1
Median 25.4 25.5 21.5 17.5 31.5 26.0
Std Dev. 1.1 0.5 2.7 5.3 0.8 0.4
Rel.Std.Dev. 4.39% 1.89% 13.27% 27.89% 2.57% 1.44%
PDM3 4.54% 1.76% -18.15% -22.91% 25.63% 4.91%
Z-Score (Absolute) 0.10 0.10 1.22 1.87 1.61 0.13
Analytical results for Li in OREAS 623 (Certified Value 18 ppm)

Li Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
PF*OES/MSPF*OES/MS PF*OES PF*OES PF*OES PF*OES/MS
1 1 17.2 20.0 20.0 20.0 35.0 16.5

1 2 17.8 20.0 < 10 20.0 < 10 17.2
1 3 17.6 20.0 < 10 20.0 < 10 17.1
1 4 16.6 20.0 20.0 20.0 < 10 17.1
1 5 17.8 20.0 < 10 20.0 < 10 17.0
1 6 17.2 10.0 20.0 20.0 < 10 17.6
Mean 17.4 18.3 20.0 20.0 35.0 17.1
Median 17.4 20.0 20.0 20.0 35.0 17.1
Std Dev. 0.4 4.1 0.0 0.0 0.3
Rel.Std.Dev. 2.58% 22.27% 0.00% 0.00% 1.95%
PDM3 -3.31% 2.00% 11.27% 11.27% 94.73% -5.04%
Z-Score (Absolute) 0.66 0.66 0.66 0.66 8.25 0.82
Analytical results for Lu in OREAS 623 (Indicative Value 0.28 ppm)

Lu Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 0.29 0.25 0.30 0.20

1 2 0.30 0.27 0.30 0.20
1 3 0.29 0.28 0.90 0.20
1 4 0.29 0.27 0.60 0.40
1 5 0.29 0.28 0.50 0.20
1 6 0.30 0.28 < 0.25 0.20
Mean 0.30 0.27 0.52 0.23
Median 0.29 0.28 0.50 0.20
Std Dev. 0.006 0.012 0.249 0.082
Rel.Std.Dev. 1.95% 4.30% 47.88% 34.99%
PDM3 4.53% -4.06% 83.64% -17.60%
Z-Score (Absolute) 0.18 0.18 1.17 1.21
Analytical results for Mg in OREAS 623 (Certified Value 1.23 wt.%)

Mg Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 1.20 1.21 1.21 1.38 1.20 1.22

1 2 1.22 1.22 1.20 1.28 1.29 1.23
1 3 1.21 1.21 1.22 1.40 1.24 1.21
1 4 1.16 1.24 1.26 1.38 1.26 1.15
1 5 1.24 1.23 1.20 1.38 1.30 1.21
1 6 1.21 1.22 1.19 1.36 1.29 1.24
Mean 1.21 1.22 1.21 1.36 1.26 1.21
Median 1.21 1.22 1.21 1.38 1.28 1.21
Std Dev. 0.025 0.012 0.025 0.043 0.038 0.031
Rel.Std.Dev. 2.07% 0.96% 2.06% 3.13% 3.03% 2.57%
PDM3 -1.86% -0.63% -1.31% 10.89% 2.76% -1.50%
Z-Score (Absolute) 1.06 0.59 0.85 4.36 0.71 0.55
Analytical results for Mn in OREAS 623 (Certified Value 0.06 wt.%)

Mn Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 0.060 0.062 0.060 0.054 0.069 0.062

1 2 0.061 0.063 0.060 0.051 0.053 0.062
1 3 0.062 0.063 0.060 0.056 0.050 0.062
1 4 0.058 0.064 0.060 0.056 0.051 0.062
1 5 0.062 0.063 0.060 0.056 0.052 0.062
1 6 0.062 0.063 0.060 0.055 0.051 0.062
Mean 0.061 0.063 0.060 0.055 0.054 0.062
Median 0.062 0.063 0.060 0.055 0.051 0.062
Std Dev. 0.002 0.001 0.000 0.002 0.007 0.000
Rel.Std.Dev. 2.69% 1.00% 0.00% 3.60% 13.79% 0.00%
PDM3 0.40% 4.17% -0.79% -9.61% -10.52% 2.52%
Z-Score (Absolute) 0.07 0.46 0.22 1.27 2.24 0.22
Analytical results for Mo in OREAS 623 (Certified Value 10.2 ppm)

Mo Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*OES PF*OES/MS
1 1 10.8 10.0 < 10 < 10 < 10 10.0

1 2 10.7 11.0 < 10 < 10 < 10 9.2
1 3 10.8 11.0 < 10 < 10 < 10 9.6
1 4 10.4 11.0 10.0 < 10 < 10 9.4
1 5 12.1 11.0 < 10 < 10 < 10 9.7
1 6 10.7 11.0 10.0 < 10 < 10 9.3
Mean 10.9 10.8 10.0 9.5
Median 10.7 11.0 10.0 9.5
Std Dev. 0.584 0.408 0.000 0.296
Rel.Std.Dev. 5.35% 3.77% 0.00% 3.11%
PDM3 6.80% 6.16% -2.00% -6.67%
Z-Score (Absolute) 0.79 0.98 3.94 NA NA 0.56
Analytical results for Nb in OREAS 623 (Certified Value 10.4 ppm)

Nb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
PF*OES/MSPF*OES/MS PF*MS PF*MS PF*OES PF*OES/MS
1 1 10.7 9.0 < 10 15.0 < 10 10.8

1 2 10.8 9.0 < 10 17.0 < 10 10.7
1 3 10.2 9.0 < 10 16.0 < 10 11.1
1 4 10.5 9.0 10.0 16.0 < 10 11.2
1 5 10.6 10.0 < 10 15.0 < 10 11.6
1 6 10.4 10.0 < 10 9.0 < 10 11.1
Mean 10.5 9.3 10.0 14.7 11.1
Median 10.5 9.0 10.0 15.5 11.1
Std Dev. 0.196 0.516 2.875 0.328
Rel.Std.Dev. 1.86% 5.53% 19.60% 2.95%
PDM3 0.76% -10.58% -4.19% 40.52% 6.43%
Z-Score (Absolute) 0.00 1.35 0.59 6.02 NA 0.67
Analytical results for Nd in OREAS 623 (Certified Value 24.9 ppm)
Nd Round Replicate Lab Lab Lab Lab Lab
No No 02 04 06 21 22
1 1 22.8 22.2 26.1 27.8 23.0

1 2 22.4 22.1 28.9 26.8 25.5
1 3 22.9 22.9 28.0 27.6 26.5
1 4 21.8 22.5 28.8 26.8 23.5
1 5 23.5 23.0 27.1 26.0 21.5
1 6 24.4 22.4 19.9 27.1 25.0
Mean 23.0 22.5 26.5 27.0 24.2
Median 22.8 22.5 27.6 27.0 24.3
Std Dev. 0.900 0.366 3.387 0.646 1.835
Rel.Std.Dev. 3.92% 1.62% 12.80% 2.39% 7.59%
PDM3 -7.74% -9.53% 6.34% 8.55% -2.90%
Z-Score (Absolute) 0.49 0.67 1.48 1.16 0.00
Analytical results for Ni in OREAS 623 (Certified Value < 50 ppm)

Ni Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 27 5 < 50 20 -- < 50
1 2 24 <5 < 50 20 -- < 50
1 3 25 <5 < 50 20 -- < 50
1 4 26 <5 < 50 20 -- < 50
1 5 25 <5 < 50 20 -- < 50
1 6 31 6 < 50 20 -- < 50
Mean 26 6 20
Median 26 6 20
Std Dev. 2 1 0
Rel.Std.Dev. 8.86% 12.86% 0.00%
PDM3
Z-Score (Absolute) 0.67 1.82 NA 0.00 NA NA
Analytical results for P in OREAS 623 (Indicative Value 0.05 wt.%)

P Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 12
1 1 0.164 0.040 0.047 < 0.01 0.220 0.040

1 2 0.173 0.040 0.046 < 0.01 0.270 0.050
1 3 0.176 0.050 0.046 < 0.01 0.270 0.060
1 4 0.171 0.050 0.046 < 0.01 0.250 0.060
1 5 0.208 0.050 0.046 < 0.01 0.250 0.050
1 6 0.185 0.050 0.047 < 0.01 0.250 0.060
Mean 0.180 0.047 0.046 0.252 0.053
Median 0.175 0.050 0.046 0.250 0.055
Std Dev. 0.016 0.005 0.001 0.018 0.008
Rel.Std.Dev. 8.66% 11.07% 1.11% 7.29% 15.31%
PDM3 259.60% -6.51% -7.18% 404.17% 6.84%
Z-Score (Absolute) 11.89 0.66 0.69 NA 19.57 0.00
Analytical results for Pb in OREAS 623 (Certified Value 0.247 wt.%)

Pb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*OES PF*OES
1 1 0.269 0.251 0.253 0.205 0.217 0.240

1 2 0.262 0.253 0.251 0.188 0.258 0.260
1 3 0.264 0.251 0.243 0.217 0.251 0.250
1 4 0.251 0.257 0.250 0.210 0.255 0.230
1 5 0.259 0.255 0.250 0.206 0.257 0.230
1 6 0.262 0.257 0.241 0.201 0.251 0.240
Mean 0.261 0.254 0.248 0.205 0.248 0.242
Median 0.262 0.254 0.250 0.206 0.253 0.240
Std Dev. 0.006 0.003 0.005 0.010 0.016 0.012
Rel.Std.Dev. 2.37% 1.09% 1.94% 4.76% 6.29% 4.84%
PDM3 5.60% 2.72% 0.30% -17.30% 0.30% -2.27%
Z-Score (Absolute) 1.26 0.65 0.13 3.63 0.67 0.42
Analytical results for Pr in OREAS 623 (Certified Value 6.53 ppm)

Pr Round Replicate Lab Lab Lab Lab Lab
No No 02 04 06 21 22
1 1 6.32 5.80 6.40 6.90 6.20

1 2 6.38 5.80 7.00 7.30 6.00
1 3 6.33 6.08 6.80 7.30 6.20
1 4 6.22 6.03 7.00 7.60 6.00
1 5 6.70 6.15 6.60 7.30 6.20
1 6 6.84 5.98 4.70 7.90 5.80
Mean 6.47 5.97 6.42 7.38 6.07
Median 6.36 6.01 6.70 7.30 6.10
Std Dev. 0.245 0.146 0.873 0.337 0.163
Rel.Std.Dev. 3.79% 2.44% 13.60% 4.57% 2.69%
PDM3 -0.98% -8.52% -1.73% 13.07% -7.09%
Z-Score (Absolute) 0.00 0.83 0.50 1.55 0.67
Analytical results for Rb in OREAS 623 (Certified Value 67 ppm)

Rb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 13 14 21
PF*OES/MSPF*OES/MS PF*MS PF*OES/MS PF*MS PF*MS
1 1 65 67 71 63 65 68
1 2 65 66 76 61 69 69
1 3 65 67 75 61 69 68
1 4 62 68 77 61 69 66
1 5 64 67 72 62 69 65
1 6 66 69 41 63 67 66
Mean 65 67 68 62 68 67
Median 65 67 73 62 69 67
Std Dev. 1.2 0.9 13.5 0.7 1.8 1.5
Rel.Std.Dev. 1.79% 1.38% 19.77% 1.14% 2.62% 2.23%
PDM3 -3.21% 1.17% 2.57% -7.24% 1.67% 0.37%
Z-Score (Absolute) 0.67 0.15 1.95 1.43 0.43 0.00
Analytical results for Re in OREAS 623 (Indicative Value < 0.1 ppm)
Re Round Replicate Lab Lab Lab Lab Lab
No No 05 13 14 21 22
PF*MS PF*OES/MS PF*MS PF*MS PF*MS
1 1 < 10 < 0.1 < 0.1 <1 <1

1 2 < 10 < 0.1 < 0.1 <1 <1
1 3 < 10 < 0.1 < 0.1 <1 <1
1 4 < 10 < 0.1 < 0.1 <1 <1
1 5 < 10 < 0.1 < 0.1 <1 <1
1 6 < 10 < 0.1 < 0.1 <1 <1
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA NA NA NA

No No 05 06 11 12 13 14
PF*OES PF*OES PF*OES PF*OES PF*OES/MS PF*OES
1 1 9.02 7.95 8.76 9.81 8.05 9.26

1 2 8.73 7.62 8.65 10.10 8.32 9.13
1 3 8.73 8.81 8.51 10.50 8.13 9.30
1 4 9.11 8.28 8.48 10.00 8.17 9.10
1 5 9.12 8.86 8.69 10.00 8.38 9.34
1 6 8.95 8.41 8.64 10.20 8.10 9.20
Mean 8.94 8.32 8.62 10.10 8.19 9.22
Median 8.99 8.34 8.65 10.05 8.15 9.23
Std Dev. 0.177 0.483 0.107 0.234 0.131 0.095
Rel.Std.Dev. 1.97% 5.81% 1.24% 2.32% 1.60% 1.03%
PDM3 1.25% -5.79% -2.40% 14.36% -7.28% 4.40%
Z-Score (Absolute) 0.01 1.14 0.76 2.78 1.79 0.67
Analytical results for Sb in OREAS 623 (Certified Value 28 ppm)
Sb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 13 14
1 1 32.8 27.9 < 50 < 50 25.2 28.0

1 2 32.4 28.3 < 50 < 50 24.4 28.7
1 3 31.5 28.0 < 50 < 50 24.4 28.5
1 4 29.9 28.2 < 50 < 50 23.4 27.4
1 5 31.0 28.7 < 50 < 50 25.2 29.6
1 6 31.0 29.1 < 50 86.0 24.8 28.5
Mean 31.4 28.4 86.0 24.6 28.5
Median 31.2 28.3 86.0 24.6 28.5
Std Dev. 1.053 0.455 0.687 0.734
Rel.Std.Dev. 3.35% 1.60% 2.79% 2.58%
PDM3 12.34% 1.43% 207.51% -12.15% 1.73%
Analytical results for Sc in OREAS 623 (Certified Value < 10 ppm)

Sc Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 13 14
PF*OES/MSPF*OES/MS PF*OES PF*OES PF*OES/MS PF*OES
1 1 7.2 7.0 8.0 <5 <2 < 20

1 2 7.4 7.0 8.0 <5 <2 < 20
1 3 7.5 7.0 8.0 <5 <2 < 20
1 4 6.9 7.0 7.0 <5 <2 < 20
1 5 7.2 7.0 8.0 <5 <2 < 20
1 6 7.4 7.0 8.0 <5 <2 < 20
Mean 7.3 7.0 7.8
Median 7.3 7.0 8.0
Std Dev. 0.2 0.0 0.4
Rel.Std.Dev. 3.07% 0.00% 5.21%
PDM3
Z-Score (Absolute) 0.00 0.67 1.96 NA NA NA
Analytical results for Se in OREAS 623 (Indicative Value 15.6 ppm)

Se Round Replicate Lab Lab Lab Lab Lab Lab
No No 05 06 13 14 21 22
PF*MS PF*MS PF*OES/MS PF*MS PF*MS PF*MS
1 1 20.0 < 50 20.8 < 20 < 50 < 50

1 2 30.0 < 50 22.6 20.0 < 50 < 50
1 3 20.0 < 50 < 20 22.0 < 50 < 50
1 4 20.0 < 50 < 20 < 20 < 50 < 50
1 5 30.0 < 50 21.4 < 20 < 50 < 50
1 6 20.0 < 50 < 20 20.0 < 50 < 50
Mean 23.3 21.6 20.7
Median 20.0 21.4 20.0
Std Dev. 5.2 0.9 1.2
Rel.Std.Dev. 22.13% 4.36% 5.59%
PDM3 49.89% 38.76% 32.76%
Z-Score (Absolute) 10.88 NA 0.00 0.67 NA NA
Analytical results for Si in OREAS 623 (Certified Value 24.45 wt.%)

Si Round Replicate Lab Lab Lab Lab Lab Lab
No No 05 06 11 12 13 14
PF*OES PF*OES PF*OES PF*OES PF*OES/MS PF*OES
1 1 23.00 19.70 23.79 25.60 25.79 24.80

1 2 23.70 18.90 24.59 26.90 24.47 25.10
1 3 24.10 20.30 24.21 26.80 24.84 24.90
1 4 24.20 20.80 21.60 25.40 25.20 24.60
1 5 24.00 20.70 24.12 26.30 25.16 24.60
1 6 23.70 20.10 24.50 27.00 25.05 24.70
Mean 23.78 20.08 23.80 26.33 25.08 24.78
Median 23.85 20.20 24.17 26.55 25.11 24.75
Std Dev. 0.436 0.705 1.116 0.692 0.436 0.194
Rel.Std.Dev. 1.83% 3.51% 4.69% 2.63% 1.74% 0.78%
PDM3 -2.74% -17.87% -2.66% 7.69% 2.58% 1.35%
Z-Score (Absolute) 0.33 4.36 0.17 2.44 1.08 0.76
Analytical results for Sm in OREAS 623 (Indicative Value 5.26 ppm)

Sm Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 4.68 4.50 6.20 5.50

1 2 4.65 4.60 6.30 6.00
1 3 4.56 5.00 6.10 5.50
1 4 4.51 4.80 5.80 5.00
1 5 4.91 4.70 6.40 5.50
1 6 5.25 4.80 7.00 4.50
Mean 4.76 4.73 6.30 5.33
Median 4.67 4.75 6.25 5.50
Std Dev. 0.277 0.175 0.400 0.516
Rel.Std.Dev. 5.82% 3.70% 6.35% 9.68%
PDM3 -9.46% -9.96% 19.84% 1.45%
Z-Score (Absolute) 0.75 0.60 2.54 0.60
Analytical results for Sn in OREAS 623 (Indicative Value 9.4 ppm)

Sn Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*OES PF*OES/MS
1 1 12.52 10.00 < 10 < 50 < 50 < 100

1 2 12.35 10.00 < 10 < 50 64.00 < 100
1 3 12.24 11.00 < 10 < 50 < 50 < 100
1 4 11.99 10.00 < 10 < 50 < 50 < 100
1 5 13.28 10.00 10.00 < 50 < 50 < 100
1 6 12.16 10.00 < 10 < 50 < 50 < 100
Mean 12.42 10.17 10.00 64.00
Median 12.29 10.00 10.00 64.00
Std Dev. 0.457 0.408
Rel.Std.Dev. 3.68% 4.02%
PDM3 32.20% 8.18% 6.41% 581.02%
Z-Score (Absolute) 0.67 0.00 1.54 NA 4.43 NA
Analytical results for Sr in OREAS 623 (Certified Value 90 ppm)

Sr Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 13 14
1 1 94 90 80 83 105 87
1 2 91 90 70 115 98 90
1 3 93 90 70 66 100 89
1 4 90 90 80 66 105 89
1 5 97 90 90 70 108 92
1 6 93 90 90 108 101 88
Mean 93 90 80 85 103 89
Median 93 90 80 77 103 89
Std Dev. 2 0 9 22 4 2
Rel.Std.Dev. 2.61% 0.00% 11.18% 25.77% 3.79% 1.93%
PDM3 3.19% 0.10% -11.02% -5.83% 14.14% -0.83%
Z-Score (Absolute) 1.07 0.03 3.70 1.96 4.75 0.28
Analytical results for Ta in OREAS 623 (Indicative Value 0.87 ppm)

Ta Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
PF*OES/MSPF*OES/MS PF*MS PF*MS PF*OES PF*OES/MS
1 1 0.74 0.60 < 10 1.30 < 10 1.17

1 2 0.73 0.60 < 10 1.40 < 10 0.94
1 3 0.72 0.70 < 10 1.40 < 10 1.12
1 4 0.66 0.70 < 10 1.40 < 10 1.30
1 5 0.71 0.70 < 10 1.30 < 10 1.10
1 6 0.71 0.70 < 10 0.80 < 10 1.01
Mean 0.71 0.67 1.27 1.11
Median 0.71 0.70 1.35 1.11
Std Dev. 0.027 0.052 0.234 0.124
Rel.Std.Dev. 3.77% 7.75% 18.46% 11.24%
PDM3 -18.66% -23.75% 44.88% 26.72%
Z-Score (Absolute) 0.29 0.42 NA 1.69 NA 0.92
Analytical results for Tb in OREAS 623 (Indicative Value 0.62 ppm)
Tb Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 0.65 0.59 0.60 0.60

1 2 0.64 0.58 0.60 0.60
1 3 0.65 0.60 0.60 0.80
1 4 0.61 0.58 0.70 0.60
1 5 0.66 0.58 0.80 0.60
1 6 0.69 0.59 0.70 0.60
Mean 0.65 0.59 0.67 0.63
Median 0.65 0.59 0.65 0.60
Std Dev. 0.028 0.008 0.082 0.082
Rel.Std.Dev. 4.32% 1.39% 12.25% 12.89%
PDM3 4.92% -5.23% 7.69% 2.31%
Z-Score (Absolute) 0.80 0.91 0.54 0.54
Analytical results for Te in OREAS 623 (Indicative Value < 1 ppm)

Te Round Replicate Lab Lab Lab Lab Lab Lab
No No 05 06 13 14 21 22
PF*MS PF*MS PF*OES/MS PF*MS PF*MS PF*MS
1 1 < 10 1.00 <1 <2 <1 <1

1 2 < 10 1.00 <1 <2 <1 1.00
1 3 < 10 1.00 <1 <2 <1 1.00
1 4 < 10 1.00 <1 <2 <1 1.00
1 5 < 10 1.00 <1 <2 <1 1.00
1 6 < 10 <1 <1 <2 <1 <1
Mean 1.00 1.00
Median 1.00 1.00
Std Dev. 0.000 0.000
Rel.Std.Dev. 0.00% 0.00%
PDM3
Z-Score (Absolute) NA 0.67 NA NA NA 0.67
Analytical results for Th in OREAS 623 (Certified Value 7.29 ppm)

Th Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 8.00 7.30 < 10 5.60 7.25 7.60

1 2 7.91 7.10 < 10 6.10 6.91 7.40
1 3 7.72 7.40 < 10 6.00 6.90 7.40
1 4 7.29 7.60 < 10 6.10 7.00 7.50
1 5 7.60 7.60 < 10 5.90 7.10 7.70
1 6 8.33 7.40 < 10 3.60 7.19 7.20
Mean 7.81 7.40 5.55 7.06 7.47
Median 7.82 7.40 5.95 7.05 7.45
Std Dev. 0.357 0.190 0.973 0.147 0.175
Rel.Std.Dev. 4.57% 2.56% 17.53% 2.08% 2.35%
PDM3 7.16% 1.52% -23.86% -3.16% 2.43%
Analytical results for Ti in OREAS 623 (Certified Value 0.15 wt.%)

Ti Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
1 1 0.146 0.140 0.160 0.140 0.140 0.162

1 2 0.150 0.140 0.160 0.130 0.140 0.300
1 3 0.152 0.140 0.160 0.150 0.130 0.150
1 4 0.143 0.150 0.160 0.150 0.130 0.150
1 5 0.149 0.140 0.160 0.140 0.140 0.162
1 6 0.150 0.150 0.160 0.140 0.160 0.150
Mean 0.148 0.143 0.160 0.142 0.140 0.179
Median 0.150 0.140 0.160 0.140 0.140 0.156
Std Dev. 0.003 0.005 0.000 0.008 0.011 0.060
Rel.Std.Dev. 2.20% 3.60% 0.00% 5.31% 7.82% 33.28%
PDM3 -1.17% -4.50% 6.60% -5.61% -6.72% 19.26%
Z-Score (Absolute) 0.20 0.79 1.18 0.99 1.18 0.55
Analytical results for Tl in OREAS 623 (Certified Value 0.71 ppm)

Tl Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 0.87 0.70 < 10 0.60 0.59 0.80

1 2 0.86 0.70 < 10 0.70 0.59 0.70
1 3 0.82 0.70 < 10 0.60 0.56 0.70
1 4 0.81 0.70 < 10 0.70 0.58 0.80
1 5 0.82 0.70 < 10 0.60 0.59 0.70
1 6 0.83 0.70 < 10 0.90 0.55 0.60
Mean 0.84 0.70 0.68 0.58 0.72
Median 0.83 0.70 0.65 0.58 0.70
Std Dev. 0.022 0.000 0.117 0.015 0.075
Rel.Std.Dev. 2.59% 0.00% 17.11% 2.58% 10.50%
PDM3 17.86% -1.21% -3.56% -18.67% 1.14%
Analytical results for Tm in OREAS 623 (Indicative Value 0.24 ppm)

Tm Round Replicate Lab Lab Lab Lab
No No 02 04 21 22
1 1 0.28 0.25 < 0.25 0.20

1 2 0.29 0.25 < 0.25 0.20
1 3 0.29 0.26 < 0.25 < 0.2
1 4 0.27 0.26 0.30 0.20
1 5 0.28 0.24 < 0.25 0.40
1 6 0.29 0.26 0.30 0.40
Mean 0.28 0.25 0.30 0.28
Median 0.28 0.26 0.30 0.20
Std Dev. 0.010 0.008 0.000 0.110
Rel.Std.Dev. 3.49% 3.22% 0.00% 39.12%
PDM3 16.30% 4.67% 23.95% 15.68%
Z-Score (Absolute) 1.28 0.07 2.93 0.07
Analytical results for U in OREAS 623 (Certified Value 2.78 ppm)

U Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 3.13 2.66 < 10 1.80 2.80 2.60

1 2 3.02 2.69 < 10 2.00 2.63 2.50
1 3 3.09 2.63 < 10 1.90 2.54 2.70
1 4 2.85 2.79 < 10 2.00 2.65 2.70
1 5 2.89 2.74 < 10 1.80 2.72 2.70
1 6 3.06 2.77 < 10 1.00 2.60 2.60
Mean 3.01 2.71 1.75 2.66 2.63
Median 3.04 2.72 1.85 2.64 2.65
Std Dev. 0.113 0.063 0.378 0.092 0.082
Rel.Std.Dev. 3.75% 2.34% 21.61% 3.48% 3.10%
PDM3 8.14% -2.36% -37.03% -4.45% -5.24%
Analytical results for V in OREAS 623 (Indicative Value 34.1 ppm)

V Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 13 14
PF*OES/MSPF*OES/MS PF*OES PF*OES PF*OES/MS PF*OES
1 1 39.0 46.0 10.0 24.0 31.2 33.0

1 2 39.5 44.0 10.0 37.0 30.8 35.0
1 3 40.5 46.0 10.0 33.0 30.5 33.0
1 4 37.7 45.0 < 10 32.0 29.4 31.0
1 5 39.8 46.0 10.0 32.0 30.0 32.0
1 6 39.9 46.0 20.0 35.0 29.9 28.0
Mean 39.4 45.5 12.0 32.2 30.3 32.0
Median 39.7 46.0 10.0 32.5 30.2 32.5
Std Dev. 1.0 0.8 4.5 4.4 0.6 2.4
Rel.Std.Dev. 2.45% 1.84% 37.27% 13.82% 2.14% 7.40%
PDM3 15.70% 33.57% -64.77% -5.57% -11.03% -6.06%
Z-Score (Absolute) 0.71 1.30 2.12 0.02 0.16 0.00
Analytical results for W in OREAS 623 (Certified Value 4.22 ppm)
W Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 4.25 4.00 < 10 4.50 4.31 5.00

1 2 4.23 4.00 < 10 4.90 3.86 4.00
1 3 4.17 4.00 < 10 4.70 3.67 4.00
1 4 3.97 4.00 < 10 4.80 3.90 4.00
1 5 4.19 4.00 < 10 4.50 3.65 4.00
1 6 4.34 4.00 < 10 5.00 3.76 5.00
Mean 4.19 4.00 4.73 3.86 4.33
Median 4.21 4.00 4.75 3.81 4.00
Std Dev. 0.123 0.000 0.207 0.241 0.516
Rel.Std.Dev. 2.94% 0.00% 4.36% 6.26% 11.92%
PDM3 -0.72% -5.28% 12.08% -8.69% 2.61%
Analytical results for Y in OREAS 623 (Certified Value 19.1 ppm)

Y Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 06 09 13 14
PF*OES/MSPF*OES/MS PF*MS PF*OES PF*OES/MS PF*MS
1 1 18.1 18.9 20.4 29.0 17.6 18.8

1 2 18.0 18.7 22.0 <5 17.1 19.1
1 3 17.8 19.1 21.8 <5 16.6 19.0
1 4 17.5 19.1 22.4 <5 16.8 19.2
1 5 18.1 19.2 20.9 <5 16.6 19.3
1 6 18.4 19.6 20.8 <5 16.6 20.0
Mean 18.0 19.1 21.4 29.0 16.9 19.2
Median 18.0 19.1 21.4 29.0 16.7 19.2
Std Dev. 0.316 0.303 0.791 0.395 0.413
Rel.Std.Dev. 1.76% 1.59% 3.70% 2.34% 2.15%
PDM3 -6.05% -0.21% 11.72% 51.52% -11.68% 0.49%
Z-Score (Absolute) 0.81 0.12 1.29 5.99 1.56 0.04
Analytical results for Yb in OREAS 623 (Certified Value 1.76 ppm)

Yb Round Replicate Lab Lab Lab Lab Lab
No No 02 04 06 21 22
1 1 1.78 1.80 1.50 1.80 1.50

1 2 1.79 1.70 1.60 1.80 2.00
1 3 1.84 1.80 1.60 1.90 1.50
1 4 1.75 1.80 1.70 1.80 1.50
1 5 1.77 1.80 1.60 2.20 2.00
1 6 1.81 1.80 1.80 1.80 2.00
Mean 1.79 1.78 1.63 1.88 1.75
Median 1.79 1.80 1.60 1.80 1.75
Std Dev. 0.032 0.041 0.103 0.160 0.274
Rel.Std.Dev. 1.77% 2.29% 6.32% 8.51% 15.65%
PDM3 1.97% 1.60% -6.95% 7.29% -0.30%
Z-Score (Absolute) 0.13 0.00 3.03 0.74 0.67
Analytical results for Zn in OREAS 623 (Certified Value 1.03 wt.%)

Zn Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 11
PF*OES PF*OES/MS PF*OES PF*OES PF*OES PF*OES
1 1 1.07 1.00 1.03 0.85 0.96 1.06

1 2 1.07 0.99 1.04 0.80 1.09 1.05
1 3 1.07 > 10000 1.06 0.86 1.05 1.05
1 4 1.06 1.00 1.07 0.86 1.06 1.01
1 5 1.04 0.99 1.06 0.87 1.09 1.02
1 6 1.06 > 10000 1.04 0.85 1.05 1.05
Mean 1.06 0.99 1.05 0.85 1.05 1.04
Median 1.06 0.99 1.05 0.86 1.06 1.05
Std Dev. 0.010 0.005 0.015 0.024 0.046 0.020
Rel.Std.Dev. 0.98% 0.48% 1.48% 2.87% 4.42% 1.92%
PDM3 2.32% -3.95% 1.46% -18.02% 1.43% 0.50%
Z-Score (Absolute) 0.64 1.23 0.38 5.15 0.87 0.10
Analytical results for Zr in OREAS 623 (Indicative Value 167 ppm)

Zr Round Replicate Lab Lab Lab
No No 02 04 22
PF*OES/MSPF*OES/MS PF*MS
1 1 163 168 160

1 2 166 162 160
1 3 165 167 170
1 4 164 170 180
1 5 169 171 160
1 6 169 177 170
Mean 166 169 167
Median 166 169 165
Std Dev. 2 5 8
Rel.Std.Dev. 1.46% 2.93% 4.90%
PDM3 -0.82% 1.16% -0.34%
13 14 17 20 21 25
PF*OES/MS PF*OES PF*OES PF*OES PF*OES PF*OES
5.59 5.23 5.26 5.49 5.42 5.16

5.56 5.30 5.21 5.29 5.48 5.09
5.54 5.27 5.23 5.23 5.52 5.06
5.58 5.22 5.45 5.39 5.89 5.24
5.73 5.21 5.25 5.55 5.57 5.27
5.60 5.23 5.14 5.47 5.60 5.18
5.60 5.24 5.26 5.40 5.58 5.17
5.58 5.23 5.24 5.43 5.55 5.17
0.068 0.034 0.105 0.124 0.165 0.082
1.21% 0.66% 1.99% 2.29% 2.95% 1.58%
6.69% -0.12% 0.12% 2.92% 6.29% -1.58%
2.57 0.05 0.05 1.12 1.96 0.61
Lab Lab Lab Lab Lab Lab Lab

13 14 17 20 21 22 25
PF*OES/MS PF*MS PF*OES PF*OES PF*MS PF*MS PF*OES
76 85 100 80 75 100 100

76 81 100 80 80 80 100
73 84 100 80 80 80 100
73 84 100 < 70 75 100 100
75 87 < 100 < 70 75 80 100
75 84 100 80 75 90 100
75 84 100 80 77 88 100
75 84 100 80 75 85 100
1 2 0 0 3 10 0
1.79% 2.31% 0.00% 0.00% 3.37% 11.13% 0.00%
-13.31% -2.14% 16.27% -6.98% -10.86% 2.71% 16.27%
0.93 0.14 1.17 0.48 0.76 0.21 1.17
Lab Lab
14 22
PF*OES PF*MS
1456 1200
1458 1190
1447 1210
1438 1220
1434 1220
1431 1230
1444 1212
1443 1215
11 15
0.79% 1.21%
3.54% -13.12%
0.75 2.89
Lab Lab Lab

14 21 22
PF*MS PF*MS PF*MS
2.00 0.80 2.00

1.00 1.10 2.00
1.00 2.80 1.00
2.00 1.20 1.00
1.00 2.00 2.00
2.00 2.30 2.00
1.50 1.70 1.67
1.50 1.60 2.00
0.548 0.785 0.516
36.51% 46.17% 30.98%
-6.89% 5.53% 3.46%
1.24 0.11 0.11
Lab Lab
21 22
PF*MS PF*MS
18.5 16.0
17.4 18.0
17.5 18.0
18.2 18.0
19.3 18.0
18.8 18.0
18.3 17.7
18.4 18.0
0.741 0.816
4.06% 4.62%
3.31% -0.17%
0.52 0.15
Lab Lab Lab Lab Lab Lab Lab Lab

12 13 14 17 20 21 22 25
PF*OES PF*OES/MS PF*OES PF*OES PF*OES PF*OES PF*OES PF*OES
1.89 1.82 1.50 1.29 1.39 1.40 1.40 1.32

1.70 1.77 1.50 1.33 1.32 1.40 1.40 1.12
1.82 1.70 1.40 1.37 1.33 1.40 1.50 1.22
1.65 1.81 1.40 1.39 1.30 1.50 1.50 1.21
1.76 1.79 1.40 1.23 1.32 1.40 1.40 1.26
1.76 1.71 1.40 1.24 1.33 1.50 1.50 1.18
1.76 1.77 1.43 1.31 1.33 1.43 1.45 1.22
1.76 1.78 1.40 1.31 1.33 1.40 1.45 1.21
0.085 0.050 0.052 0.066 0.031 0.052 0.055 0.068
4.82% 2.83% 3.60% 5.03% 2.30% 3.60% 3.78% 5.60%
28.72% 28.90% 4.63% -4.53% -2.79% 4.63% 5.85% -11.05%
4.29 4.32 0.41 1.06 0.92 0.41 0.61 1.89
Lab Lab
21 22
PF*MS PF*MS
57 50
59 50
58 60
62 60
65 60
63 60
61 57
60 60
3.2 5.2
5.22% 9.11%
11.21% 3.79%
1.29 0.47

13 14 17 20 21 22 25
PF*OES/MS PF*OES PF*OES PF*OES PF*MS PF*OES PF*OES
220 228 220 230 252 220 220

221 231 230 220 253 220 230
218 233 220 220 251 220 230
218 232 220 220 246 220 220
220 231 220 220 234 200 220
223 229 230 220 238 220 220
220 231 223 222 246 217 223
220 231 220 220 249 220 220
2 2 5 4 8 8 5
0.87% 0.81% 2.31% 1.84% 3.24% 3.77% 2.31%
-2.35% 2.46% -0.80% -1.54% 9.12% -3.76% -0.80%
0.67 1.42 0.00 0.32 4.32 0.65 0.00
Lab Lab Lab Lab Lab

13 14 20 21 22
PF*OES/MS PF*OES PF*OES PF*OES PF*OES
< 50 < 50 < 60 35.0 < 50

< 50 < 50 < 60 40.0 < 50
< 50 < 50 < 60 35.0 < 50
< 50 < 50 < 60 35.0 < 50
< 50 < 50 < 60 40.0 < 50
< 50 < 50 < 60 35.0 < 50
36.7
35.0
2.6
7.04%
22.40%
NA NA NA 2.76 NA
Lab Lab
21 22
PF*MS PF*MS
3.60 < 10
3.40 < 10
3.70 < 10
3.60 < 10
3.30 < 10
3.30 < 10
3.48
3.50
0.172
4.94%
16.05%
2.04 NA

12 13 14 17 20 21 22 25
1.67 1.56 1.78 1.70 1.64 1.81 1.77 1.81

1.93 1.69 1.70 1.84 1.68 1.67 1.78 1.70
1.93 1.59 1.72 1.77 1.68 1.84 1.71 2.12
1.98 1.60 1.71 1.78 1.62 1.93 1.75 1.76
1.84 1.60 1.67 1.65 1.62 1.77 1.82 1.69
1.73 1.60 1.69 1.63 1.62 1.66 1.77 1.72
1.85 1.61 1.71 1.73 1.64 1.78 1.77 1.80
1.89 1.60 1.71 1.74 1.63 1.79 1.77 1.74
0.124 0.041 0.039 0.082 0.030 0.104 0.036 0.164
6.70% 2.57% 2.28% 4.73% 1.81% 5.82% 2.05% 9.12%
6.96% -6.89% -0.80% 0.11% -4.91% 3.10% 2.33% 4.16%
1.65 2.08 0.31 0.08 1.35 0.67 0.48 0.00
12 13 14 17 20 21 22 25
17.30 13.78 13.87 13.20 13.67 12.90 13.90 13.60

15.90 13.91 13.52 13.45 13.59 12.70 14.00 13.30
15.60 13.84 13.96 13.40 13.69 13.30 13.80 13.95
15.50 13.68 13.59 13.45 13.26 13.30 14.10 13.30
15.90 14.02 13.40 13.05 13.05 12.50 13.60 13.50
16.50 13.77 13.55 12.80 13.44 12.60 14.00 13.35
16.12 13.83 13.65 13.23 13.45 12.88 13.90 13.50
15.90 13.81 13.57 13.30 13.52 12.80 13.95 13.43
0.677 0.119 0.218 0.262 0.254 0.349 0.179 0.251
4.20% 0.86% 1.60% 1.98% 1.89% 2.71% 1.29% 1.86%
19.85% 2.87% 1.50% -1.65% 0.02% -4.19% 3.37% 0.39%
5.90 0.72 0.25 0.82 0.25 1.69 0.89 0.13
Lab
21
PF*MS
26.0
25.0
26.0
24.0
25.0
25.0
25.2
25.0
0.8
2.99%
6.20%
0.67
Lab Lab
21 22
PF*MS PF*MS
2.10 1.80
2.00 2.00
2.70 2.00
2.50 1.80
1.80 2.00
1.80 2.20
2.15 1.97
2.05 2.00
0.373 0.151
17.34% 7.66%
5.16% -3.81%
0.00 0.71
12 13 14 17 20 21 22 25
1.90 2.04 1.52 1.60 1.69 1.40 1.40 1.50

1.80 1.91 1.54 1.60 1.57 1.40 1.40 1.40
1.90 1.95 1.50 1.60 1.53 1.50 1.40 1.40
1.70 2.03 1.50 1.70 1.57 1.50 1.40 1.50
1.80 2.11 1.51 1.60 1.67 1.50 1.50 1.50
1.80 1.96 1.51 1.60 1.61 1.50 1.50 1.40
1.82 2.00 1.51 1.62 1.61 1.47 1.43 1.45
1.80 1.99 1.51 1.60 1.59 1.50 1.40 1.45
0.075 0.071 0.015 0.041 0.063 0.052 0.052 0.055
4.14% 3.55% 0.99% 2.53% 3.89% 3.52% 3.60% 3.78%
19.02% 30.97% -0.86% 5.91% 5.26% -3.91% -6.10% -5.01%
2.30 3.75 0.11 0.71 0.63 0.48 0.74 0.61
Lab Lab Lab Lab

14 20 21 22
PF*MS PF*OES PF*MS PF*MS
17.0 20.0 15.3 14.0

18.0 20.0 17.1 15.0
17.0 20.0 16.0 14.0
18.0 20.0 15.6 14.0
17.0 20.0 14.6 13.0
17.0 20.0 15.3 16.0
17.3 20.0 15.6 14.3
17.0 20.0 15.5 14.0
0.5 0.0 0.8 1.0
2.98% 0.00% 5.40% 7.21%
-3.56% 11.27% -12.93% -20.25%
0.69 0.66 1.54 2.20

12 13 14 17 20 21 22 25
1.52 1.24 1.24 1.25 1.25 1.54 1.22 1.22

1.43 1.20 1.25 1.24 1.25 1.51 1.22 1.23
1.55 1.20 1.25 1.25 1.24 1.48 1.24 1.20
1.34 1.16 1.24 1.27 1.26 1.53 1.26 1.22
1.38 1.21 1.24 1.24 1.23 1.56 1.24 1.23
1.50 1.22 1.25 1.22 1.24 1.56 1.24 1.22
1.45 1.20 1.25 1.24 1.25 1.53 1.24 1.22
1.46 1.20 1.25 1.25 1.25 1.54 1.24 1.22
0.083 0.025 0.005 0.018 0.010 0.031 0.015 0.011
5.73% 2.03% 0.44% 1.42% 0.84% 2.03% 1.22% 0.92%
18.21% -2.04% 1.27% 1.19% 1.27% 24.45% 0.59% -0.76%
6.65 1.13 0.14 0.12 0.14 9.05 0.12 0.63

12 13 14 17 20 21 22 25
PF*OES PF*OES/MS PF*OES PF*OES PF*OES PF*MS PF*OES PF*OES
0.078 0.058 0.065 0.054 0.060 0.068 0.060 0.062

0.071 0.057 0.066 0.054 0.060 0.066 0.060 0.062
0.079 0.057 0.065 0.054 0.060 0.066 0.062 0.062
0.069 0.056 0.064 0.054 0.061 0.065 0.060 0.062
0.071 0.057 0.065 0.054 0.059 0.062 0.060 0.062
0.076 0.057 0.064 0.054 0.061 0.065 0.062 0.062
0.074 0.057 0.065 0.054 0.060 0.065 0.061 0.062
0.074 0.057 0.065 0.054 0.060 0.066 0.060 0.062
0.004 0.001 0.000 0.000 0.001 0.002 0.001 0.000
5.67% 1.53% 0.70% 0.00% 1.25% 3.34% 1.70% 0.00%
22.36% -5.90% 7.29% -10.71% -0.51% 7.95% 0.31% 2.52%
2.96 0.92 0.89 1.54 0.18 0.98 0.07 0.22
Lab Lab
21 22
PF*OES PF*MS
10.0 10.0
10.0 10.0
15.0 10.0
10.0 10.0
10.0 10.0
10.0 10.0
10.8 10.0
10.0 10.0
2.041 0.000
18.84% 0.00%
6.16% -2.00%
0.00 0.00
Lab Lab Lab

14 21 22
PF*MS PF*MS PF*MS
11.0 < 10 10.0

12.0 < 10 10.0
11.0 < 10 10.0
12.0 < 10 10.0
12.0 < 10 10.0
12.0 < 10 10.0
11.7 10.0
12.0 10.0
0.516 0.000
4.43% 0.00%
11.78% -4.19%
1.31 NA 0.59
Lab Lab Lab Lab Lab
13 17 20 22 25
PF*OES/MS PF*OES PF*OES PF*OES PF*OES
< 20 < 50 < 20 < 50 < 50

< 20 < 50 < 20 < 50 < 50
< 20 < 50 < 20 < 50 < 50
< 20 < 50 30 < 50 < 50
< 20 < 50 < 20 < 50 < 50
< 20 70 < 20 < 50 < 50
70 30
70 30
NA 0.54 1.07 NA NA
Lab
22
PF*OES
0.050
0.060
0.050
0.060
0.050
0.050
0.053
0.050
0.005
9.68%
6.84%
0.00

12 13 14 17 20 21 22 25
PF*OES PF*OES/MS PF*MS PF*OES PF*OES PF*OES PF*MS PF*OES
0.235 0.233 0.256 0.230 0.340 0.237 0.254 0.250

0.255 0.236 0.265 0.240 0.330 0.241 0.252 0.240
0.250 0.231 0.254 0.230 0.330 0.238 0.254 0.240
0.245 0.234 0.255 0.230 0.330 0.244 0.256 0.240
0.240 0.232 0.259 0.240 0.310 0.250 0.254 0.240
0.245 0.236 0.245 0.230 0.340 0.248 0.256 0.250
0.245 0.234 0.256 0.233 0.330 0.243 0.254 0.243
0.245 0.233 0.255 0.230 0.330 0.243 0.254 0.240
0.007 0.002 0.006 0.005 0.011 0.005 0.002 0.005
2.89% 0.94% 2.49% 2.21% 3.32% 2.18% 0.59% 2.12%
-0.92% -5.53% 3.36% -5.64% 33.46% -1.73% 2.86% -1.59%
0.13 1.12 0.79 1.14 7.57 0.30 0.68 0.27
Lab
22
PF*MS
65
66
64
62
63
63
64
64
1.6
2.49%
-4.48%
0.91
Lab Lab Lab Lab Lab

17 20 21 22 25
PF*OES PF*OES PF*OES PF*OES PF*OES
8.90 8.90 7.84 9.14 9.29

9.21 8.88 7.64 9.28 8.95
9.06 8.75 8.14 9.06 9.96
9.04 8.80 8.42 9.18 9.22
8.74 8.83 8.16 9.24 9.09
8.69 8.95 7.64 9.10 8.96
8.94 8.85 7.97 9.17 9.25
8.97 8.86 7.99 9.16 9.16
0.201 0.073 0.317 0.084 0.376
2.24% 0.82% 3.97% 0.91% 4.06%
1.21% 0.21% -9.74% 3.77% 4.66%
0.00 0.21 2.31 0.54 0.39
Lab Lab
21 22
PF*OES PF*MS
< 50 30.0
< 50 30.0
< 50 30.0
< 50 30.0
< 50 30.0
< 50 30.0
30.0
30.0
0.000
0.00%
7.27%
NA 0.47
Lab Lab
21 22
PF*MS PF*OES
< 10 < 10
< 10 < 10
< 10 < 10
< 10 < 10
< 10 < 10
< 10 < 10
NA NA
Lab Lab Lab Lab
17 21 22 25
PF*OES PF*OES PF*OES PF*OES
23.61 36.80 23.80 24.31

23.42 35.60 23.90 23.28
23.61 36.70 24.00 23.51
24.12 36.90 24.20 24.21
23.51 36.40 23.70 24.40
23.00 35.70 23.90 23.89
23.55 36.35 23.92 23.93
23.56 36.55 23.90 24.05
0.361 0.568 0.172 0.457
1.53% 1.56% 0.72% 1.91%
-3.71% 48.65% -2.19% -2.12%
0.59 13.35 0.19 0.17
Lab Lab Lab Lab

14 20 21 22
PF*MS PF*OES PF*MS PF*MS
< 100 < 50 < 100 10.00

< 100 < 50 < 100 10.00
< 100 < 50 < 100 10.00
< 100 < 50 < 100 10.00
< 100 < 50 < 100 10.00
< 100 < 50 < 100 10.00
10.00
10.00
0.000
0.00%
6.41%
NA NA NA 0.05
Lab Lab
21 22
PF*MS PF*MS
93 89
97 89
90 89
90 91
88 89
90 92
91 90
90 89
3 1
3.40% 1.48%
1.58% -0.09%
0.11 0.03
Lab Lab Lab

14 21 22
PF*MS PF*MS PF*MS
0.70 < 10 0.50

1.10 < 10 0.50
1.30 < 10 1.00
0.80 < 10 0.50
0.70 < 10 0.50
0.80 < 10 0.50
0.90 0.58
0.80 0.50
0.245 0.204
27.22% 34.99%
2.94% -33.28%
0.29 NA 0.93
Lab Lab
21 22
PF*MS PF*MS
6.80 7.50
6.70 6.50
7.10 7.00
7.40 7.00
7.20 6.50
7.80 6.50
7.17 6.83
7.15 6.75
0.403 0.408
5.63% 5.97%
-1.69% -6.26%
0.00 0.75

12 13 14 17 20 21 22 25
0.200 0.161 0.150 0.150 0.149 0.150 0.160 0.150

0.190 0.155 0.150 0.150 0.143 0.150 0.160 0.150
0.210 0.156 0.150 0.150 0.141 0.150 0.160 0.150
0.180 0.153 0.150 0.150 0.146 0.150 0.160 0.150
0.190 0.156 0.150 0.150 0.144 0.150 0.170 0.150
0.200 0.156 0.150 0.138 0.145 0.150 0.160 0.156
0.195 0.156 0.150 0.148 0.145 0.150 0.162 0.151
0.195 0.156 0.150 0.150 0.145 0.150 0.160 0.150
0.010 0.003 0.000 0.005 0.003 0.000 0.004 0.002
5.38% 1.82% 0.00% 3.31% 1.89% 0.00% 2.53% 1.62%
29.92% 3.98% -0.06% -1.39% -3.61% -0.06% 7.71% 0.61%
5.32 0.72 0.00 0.02 0.63 0.00 1.38 0.10
Lab Lab
21 22
PF*MS PF*MS
0.70 <1
0.80 <1
0.80 <1
0.80 <1
0.90 <1
0.70 <1
0.78
0.80
0.075
9.61%
10.55%
0.71 NA
Lab Lab
21 22
PF*MS PF*MS
2.80 2.00
2.30 3.00
2.60 3.00
2.90 3.00
2.70 3.00
2.70 3.00
2.67 2.83
2.70 3.00
0.207 0.408
7.75% 14.41%
-4.04% 1.96%
0.00 4.82
Lab Lab
21 22
PF*OES PF*OES
25.0 < 50
25.0 < 50
25.0 < 50
30.0 < 50
25.0 < 50
25.0 < 50
25.8
25.0
2.0
7.90%
-24.16%
0.67 NA
Lab Lab
21 22
PF*MS PF*MS
<2 <5
2.00 <5
<2 <5
<2 <5
<2 <5
<2 <5
2.00
2.00
-52.64%
8.75 NA
Lab Lab
21 22
PF*MS PF*MS
19.0 20.0
19.9 20.0
20.4 20.0
19.2 21.0
18.8 20.0
18.8 20.0
19.3 20.2
19.1 20.0
0.657 0.408
3.39% 2.02%
1.10% 5.36%
0.04 0.54
12 13 14 17 20 21 22 25
1.08 1.02 1.11 0.98 1.02 1.17 1.05 1.06

1.11 1.01 1.06 0.97 1.00 0.99 1.03 1.01
1.14 1.02 1.06 0.98 1.01 1.00 1.06 1.02
1.07 1.01 1.05 0.99 0.98 1.07 1.05 1.04
1.07 1.01 1.06 0.97 0.95 1.14 1.00 1.05
1.10 1.00 1.05 0.95 0.98 1.06 1.01 1.02
1.10 1.01 1.07 0.97 0.99 1.07 1.03 1.03
1.09 1.01 1.06 0.98 0.99 1.07 1.04 1.03
0.027 0.006 0.024 0.014 0.025 0.074 0.024 0.020
2.50% 0.62% 2.29% 1.40% 2.53% 6.91% 2.34% 1.90%
5.81% -2.20% 2.98% -5.94% -4.38% 3.45% -0.15% -0.15%
1.68 0.71 0.56 1.83 1.36 0.40 0.10 0.10
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
22.7
11.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
5.25
12.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
86
13
Indicative
1.00
ppm
0.00
0.00
1
5
16
< 50
11
Certified
1.00
ppm
0.00
0.00
1
14
16
1395
14
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
1.61
12.00
Certified
1.00
ppm
1.00
2.00
1.0
19.0
16.0
17.7
15.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.37
16.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
55
17
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
49.9
18.0
Certified
1.00
ppm
0.00
0.00
1
19
16
225
19
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
30.0
20.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
3.00
21.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.73
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
3.46
13.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
1.88
14.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
1.60
15.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
13.45
23.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
23.7
24.0
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
4.39
16.00
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
1.65
17.00
Indicative
1.00
ppm
2.00
2.00
1.00
5.00
16.00
4.51
11.00
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
0.61
12.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.04
25.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.53
26.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
24.9
27.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
18.0
28.0
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
0.28
13.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.23
29.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.060
30.000
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
10.2
31.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
10.4
32.0
Certified
1.00
ppm
1.00
2.00
1.0
17.0
16.0
24.9
33.0
Certified
1.00
ppm
0.00
0.00
1
19
16
< 50
34
Indicative
1.00
wt.%
3.00
3.00
1.000
8.000
16.000
0.050
14.000
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.247
35.000
Certified
1.00
ppm
2.00
3.00
1.00
25.00
16.00
6.53
36.00
Certified
1.00
ppm
0.00
1.00
1
22
16
67
37
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
< 0.1
15.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
8.83
38.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
28.0
39.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
< 10
40.0
Indicative
1.00
ppm
1.00
1.00
1.0
10.0
16.0
15.6
16.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
24.45
41.00
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
5.26
17.00
Indicative
1.00
ppm
2.00
2.00
1.00
5.00
16.00
9.40
11.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
90
42
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
0.87
12.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
0.62
13.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
<1
14.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
7.29
43.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.150
44.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.71
45.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
0.24
15.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.78
46.00
Indicative
1.00
ppm
1.00
1.00
1.0
10.0
16.0
34.1
16.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
4.22
47.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
19.1
48.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.76
49.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.03
50.00
Indicative
1.00
ppm
0.00
0.00
1
11
16
167
17
No No 01 02 04 05 06 08
4A*OES 4A*OES/MS4A*OES/MS 4A*OES 4A*MS 4A*OES
1 1 20.0 23.5 20.4 21.0 15.5 21.0

1 2 20.0 22.6 20.1 21.0 15.1 21.0
1 3 20.0 23.7 21.2 20.0 15.4 21.0
1 4 20.0 23.3 21.2 21.0 15.5 22.0
1 5 20.0 22.7 20.6 20.0 14.9 21.0
1 6 20.0 23.4 21.9 20.0 16.0 21.0
Mean 20.0 23.2 20.9 20.5 15.4 21.2
Median 20.0 23.3 20.9 20.5 15.5 21.0
Std Dev. 0.000 0.440 0.657 0.548 0.379 0.408
Rel.Std.Dev. 0.00% 1.90% 3.14% 2.67% 2.46% 1.93%
PDM3 -1.96% 13.70% 2.45% 0.49% -24.51% 3.76%
Z-Score (Absolute) 0.42 2.81 0.49 0.08 5.07 0.76

No No 01 02 04 05 06 08
4A*OES 4A*OES/MS4A*OES/MS 4A*OES 4A*OES 4A*OES
1 1 4.59 5.28 5.03 5.08 6.12 4.57

1 2 4.25 5.24 5.06 4.88 5.12 4.50
1 3 4.62 5.19 5.16 5.12 5.52 4.49
1 4 4.68 5.08 4.98 4.96 5.77 4.49
1 5 4.43 5.25 5.04 4.93 5.39 4.56
1 6 4.73 5.17 5.01 5.10 5.52 4.51
Mean 4.55 5.20 5.05 5.01 5.57 4.52
Median 4.61 5.21 5.04 5.02 5.52 4.51
Std Dev. 0.179 0.070 0.062 0.101 0.341 0.036
Rel.Std.Dev. 3.93% 1.36% 1.23% 2.01% 6.12% 0.79%
PDM3 -9.71% 3.17% 0.15% -0.55% 10.60% -10.30%
Z-Score (Absolute) 1.40 0.48 0.04 0.06 1.25 1.49

No No 01 02 04 05 06 08
4A*OES 4A*OES/MS4A*OES/MS 4A*MS 4A*MS 4A*OES
1 1 80 75 75 65 82 50
1 2 90 76 76 70 81 70
1 3 80 76 77 71 82 80
1 4 90 77 76 70 82 60
1 5 90 74 75 68 79 80
1 6 80 76 79 66 86 60
Mean 85 76 76 68 82 67
Median 85 76 76 69 82 65
Std Dev. 5.5 1.0 1.5 2.6 2.3 12.1
Rel.Std.Dev. 6.44% 1.30% 1.97% 3.79% 2.78% 18.17%
PDM3 9.72% -2.43% -1.47% -11.90% 5.85% -13.94%
Z-Score (Absolute) 1.27 0.42 0.28 1.74 0.73 1.42
Analytical results for B in OREAS 623 (Indicative Value 0.75 ppm)

B Round Replicate Lab
No No 05
4A*MS
1 1 1.00
1 2 1.00
1 3 1.00
1 4 <1
1 5 <1
1 6 <1
Mean 1.00
Median 1.00
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 33.33%
Analytical results for Ba in OREAS 623 (Indicative Value 1198 ppm)

No No 01 04 05 06 08 09
4A*OES 4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES
1 1 1000 43 350 169 1040 763

1 2 960 45 187 149 910 680
1 3 1020 52 742 139 920 610
1 4 930 53 349 169 920 787
1 5 1020 59 375 200 1050 948
1 6 1030 41 318 171 870 533
Mean 993 49 387 166 952 720
Median 1010 49 350 169 920 722
Std Dev. 40 7 186 21 75 146
Rel.Std.Dev. 4.01% 14.21% 48.19% 12.67% 7.85% 20.31%
PDM3 -17.10% -95.92% -67.71% -86.13% -20.57% -39.89%
Z-Score (Absolute) 0.37 1.23 0.78 1.03 0.30 0.09
Analytical results for Be in OREAS 623 (Certified Value 1.39 ppm)

No No 01 02 04 05 06 08
1 1 < 10 1.57 1.20 2.00 1.40 < 10

1 2 < 10 1.44 1.30 1.00 1.40 < 10
1 3 < 10 1.46 1.30 2.00 1.40 < 10
1 4 < 10 1.47 1.30 1.00 1.40 < 10
1 5 < 10 1.34 1.40 1.00 1.30 < 10
1 6 < 10 1.57 1.30 2.00 1.40 < 10
Mean 1.47 1.30 1.50 1.38
Median 1.46 1.30 1.50 1.40
Std Dev. 0.087 0.063 0.548 0.041
Rel.Std.Dev. 5.89% 4.87% 36.51% 2.95%
PDM3 6.38% -6.24% 8.18% -0.23%
Z-Score (Absolute) NA 0.56 0.62 0.73 0.06 NA

No No 01 02 04 05 06 08
1 1 30.0 17.3 16.0 18.5 12.8 20.0

1 2 30.0 17.1 16.0 17.4 12.9 < 20
1 3 30.0 17.2 16.6 17.6 12.6 20.0
1 4 30.0 17.3 16.3 17.5 12.8 20.0
1 5 30.0 17.1 16.3 17.6 12.4 20.0
1 6 20.0 17.1 16.8 18.0 13.6 20.0
Mean 28.3 17.2 16.3 17.8 12.9 20.0
Median 30.0 17.1 16.3 17.6 12.8 20.0
Std Dev. 4.082 0.093 0.320 0.413 0.409 0.000
Rel.Std.Dev. 14.41% 0.54% 1.96% 2.33% 3.18% 0.00%
PDM3 59.88% -3.05% -7.84% 0.25% -27.49% 12.86%
Z-Score (Absolute) 4.16 0.35 0.70 0.18 2.17 0.79

No No 01 02 04 05 06 08
1 1 1.42 1.26 1.31 1.38 1.59 1.38

1 2 1.35 1.27 1.30 1.35 1.32 1.36
1 3 1.38 1.25 1.34 1.40 1.44 1.39
1 4 1.39 1.23 1.29 1.37 1.51 1.37
1 5 1.38 1.29 1.30 1.36 1.40 1.37
1 6 1.39 1.27 1.27 1.40 1.44 1.38
Mean 1.39 1.26 1.30 1.38 1.45 1.38
Median 1.38 1.27 1.30 1.38 1.44 1.38
Std Dev. 0.023 0.019 0.023 0.021 0.093 0.010
Rel.Std.Dev. 1.63% 1.48% 1.78% 1.50% 6.38% 0.76%
PDM3 0.69% -8.33% -5.37% 0.08% 5.42% -0.04%
Z-Score (Absolute) 0.14 1.64 1.05 0.02 1.08 0.00
No No 01 02 04 05 06 08
1 1 50 53 46 51 49 50
1 2 50 53 47 49 49 50
1 3 50 53 48 51 49 50
1 4 50 54 47 50 50 50
1 5 50 54 48 49 48 50
1 6 50 54 47 50 50 50
Mean 50 53 47 50 49 50
Median 50 53 47 50 49 50
Std Dev. 0.0 0.8 0.8 0.8 0.8 0.0
Rel.Std.Dev. 0.00% 1.43% 1.60% 1.62% 1.54% 0.00%
PDM3 -7.14% -0.85% -12.22% -6.80% -8.75% -7.14%
Z-Score (Absolute) 0.71 0.00 1.29 0.67 0.90 0.71

Ce Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 10 13
4A*OES/MS4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES/MS
1 1 46.0 41.0 42.4 35.8 51.0 45.5

1 2 44.9 41.2 35.5 36.6 51.0 45.5
1 3 45.1 42.8 43.6 36.6 51.0 44.8
1 4 44.1 40.8 42.8 36.6 51.0 45.9
1 5 46.1 42.6 41.2 35.1 51.0 45.1
1 6 43.3 40.9 41.9 37.3 51.0 44.6
Mean 44.9 41.6 41.2 36.3 51.0 45.2
Median 45.0 41.1 42.2 36.6 51.0 45.3
Std Dev. 1.1 0.9 2.9 0.8 0.0 0.5
Rel.Std.Dev. 2.46% 2.17% 7.09% 2.12% 0.00% 1.04%
PDM3 -1.59% -8.93% -9.63% -20.37% 11.78% -0.84%
Z-Score (Absolute) 0.03 0.63 0.48 1.55 1.05 0.03

No No 01 02 04 05 06 08
1 1 230 203 226 213 219 220

1 2 230 203 226 218 215 220
1 3 240 200 227 213 215 220
1 4 230 209 224 217 217 230
1 5 240 203 220 218 210 220
1 6 230 204 235 217 228 220
Mean 233 204 226 216 217 222
Median 230 203 226 217 216 220
Std Dev. 5 3 5 2 6 4
Rel.Std.Dev. 2.21% 1.44% 2.18% 1.10% 2.77% 1.84%
PDM3 5.31% -8.15% 2.15% -2.51% -1.91% 0.05%
Z-Score (Absolute) 1.23 1.95 0.48 0.62 0.48 0.02
Analytical results for Cr in OREAS 623 (Certified Value 24.8 ppm)

No No 01 02 04 05 06 08
4A*OES 4A*OES/MS4A*OES/MS 4A*MS 4A*OES 4A*OES
1 1 30.0 24.5 17.0 25.0 30.0 20.0

1 2 30.0 26.9 18.0 30.6 20.0 20.0
1 3 30.0 24.5 17.0 24.0 20.0 30.0
1 4 30.0 23.1 14.0 25.6 30.0 30.0
1 5 30.0 20.0 18.0 26.6 20.0 20.0
1 6 30.0 21.6 14.0 24.4 20.0 20.0
Mean 30.0 23.5 16.3 26.0 23.3 23.3
Median 30.0 23.8 17.0 25.3 20.0 20.0
Std Dev. 0.0 2.4 1.9 2.4 5.2 5.2
Rel.Std.Dev. 0.00% 10.40% 11.40% 9.29% 22.13% 22.13%
PDM3 20.82% -5.56% -34.22% 4.85% -6.03% -6.03%
Z-Score (Absolute) 0.84 0.22 1.38 0.05 0.24 0.24
Analytical results for Cs in OREAS 623 (Certified Value 2.85 ppm)

No No 02 04 05 06 13 14
4A*OES/MS4A*OES/MS 4A*MS 4A*MS 4A*OES/MS 4A*MS
1 1 2.75 3.00 2.92 2.70 2.73 2.80

1 2 2.86 3.00 2.83 2.76 2.72 2.90
1 3 2.81 3.00 2.87 2.71 2.69 2.90
1 4 2.85 3.00 2.92 2.73 2.74 2.80
1 5 2.89 3.00 2.86 2.65 2.82 2.90
1 6 2.85 3.00 2.97 2.78 2.80 2.90
Mean 2.84 3.00 2.90 2.72 2.75 2.87
Median 2.85 3.00 2.90 2.72 2.73 2.90
Std Dev. 0.050 0.000 0.051 0.046 0.052 0.052
Rel.Std.Dev. 1.75% 0.00% 1.76% 1.70% 1.90% 1.80%
PDM3 -0.62% 5.15% 1.47% -4.61% -3.59% 0.47%
Z-Score (Absolute) 0.07 1.31 0.33 1.29 1.02 0.07

No No 01 02 04 05 06 08
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES
1 1 1.72 1.88 1.64 1.76 1.85 1.77

1 2 1.72 1.79 1.66 1.78 1.86 1.80
1 3 1.66 1.71 1.84 1.67 1.55 1.84
1 4 1.73 1.78 1.77 1.70 1.62 1.85
1 5 1.71 1.82 1.66 1.65 1.71 1.72
1 6 1.68 1.87 2.07 1.76 1.72 1.67
Mean 1.70 1.81 1.77 1.72 1.72 1.78
Median 1.71 1.81 1.71 1.73 1.71 1.79
Std Dev. 0.027 0.063 0.165 0.054 0.123 0.070
Rel.Std.Dev. 1.60% 3.49% 9.30% 3.14% 7.15% 3.95%
PDM3 -1.77% 4.28% 2.26% -0.81% -0.91% 2.36%
Z-Score (Absolute) 0.39 1.88 0.16 0.03 0.06 1.16

No No 05 13 21 22
4A*MS 4A*OES/MS 4A*MS 4A*MS
1 1 3.30 2.67 3.00 3.35

1 2 3.00 2.72 3.10 3.20
1 3 3.10 2.75 3.00 3.20
1 4 3.50 2.88 3.10 3.35
1 5 3.30 2.82 3.00 3.40
1 6 3.30 2.81 3.00 3.30
Mean 3.25 2.77 3.03 3.30
Median 3.30 2.78 3.00 3.33
Std Dev. 0.176 0.076 0.052 0.084
Rel.Std.Dev. 5.42% 2.74% 1.70% 2.54%
PDM3 5.20% -10.21% -1.81% 6.82%
Z-Score (Absolute) 0.55 1.86 0.55 0.80

No No 05 13 21 22
1 1 1.80 1.51 1.50 1.75

1 2 1.60 1.46 1.50 1.65
1 3 1.70 1.53 1.60 1.65
1 4 1.90 1.57 1.60 1.70
1 5 1.80 1.57 1.50 1.60
1 6 1.90 1.58 1.50 1.60
Mean 1.78 1.54 1.53 1.66
Median 1.80 1.55 1.50 1.65
Std Dev. 0.117 0.046 0.052 0.058
Rel.Std.Dev. 6.56% 3.00% 3.37% 3.52%
PDM3 9.52% -5.54% -5.83% 1.85%
Z-Score (Absolute) 2.00 0.65 0.70 0.65
No No 05 13 21 22
1 1 1.21 1.33 1.38 1.50

1 2 1.16 1.32 1.38 1.45
1 3 1.19 1.31 1.40 1.45
1 4 1.27 1.39 1.48 1.45
1 5 1.23 1.34 1.43 1.50
1 6 1.25 1.38 1.41 1.55
Mean 1.22 1.34 1.41 1.48
Median 1.22 1.33 1.40 1.48
Std Dev. 0.040 0.033 0.038 0.041
Rel.Std.Dev. 3.30% 2.43% 2.67% 2.75%
PDM3 -10.74% -1.47% 3.54% 8.67%
Z-Score (Absolute) 1.57 0.33 0.33 1.02

No No 01 02 04 05 06 08
1 1 13.85 12.46 12.30 13.70 16.50 13.10

1 2 13.70 12.35 12.30 13.70 13.60 12.95
1 3 13.65 12.04 12.70 13.30 14.80 13.05
1 4 13.70 12.30 12.60 13.70 15.60 13.15
1 5 13.65 12.23 12.20 13.50 14.60 12.85
1 6 13.75 12.54 12.90 13.90 15.40 12.75
Mean 13.72 12.32 12.50 13.63 15.08 12.98
Median 13.70 12.32 12.45 13.70 15.10 13.00
Std Dev. 0.075 0.177 0.276 0.207 0.989 0.154
Rel.Std.Dev. 0.55% 1.43% 2.21% 1.52% 6.56% 1.19%
PDM3 2.19% -8.24% -6.87% 1.57% 12.37% -3.33%
Z-Score (Absolute) 0.19 1.99 1.70 0.06 1.88 0.96

No No 01 02 04 05 06 08
1 1 < 50 20.7 22.1 21.8 19.1 < 50

1 2 < 50 20.8 21.9 21.7 18.8 < 50
1 3 < 50 20.7 22.1 21.9 18.5 < 50
1 4 < 50 21.4 21.5 22.6 18.3 < 50
1 5 < 50 21.2 22.0 21.8 17.9 < 50
1 6 < 50 20.8 21.9 22.3 19.0 < 50
Mean 20.9 21.9 22.0 18.6
Median 20.8 22.0 21.9 18.7
Std Dev. 0.300 0.223 0.354 0.456
Rel.Std.Dev. 1.44% 1.02% 1.61% 2.45%
PDM3 -3.41% 1.14% 1.60% -14.17%
Analytical results for Gd in OREAS 623 (Indicative Value 4 ppm)

No No 05 13 21 22
1 1 3.90 3.86 4.30 4.00

1 2 3.50 3.92 4.40 4.00
1 3 3.70 3.85 4.30 4.00
1 4 4.00 3.93 4.40 4.00
1 5 3.80 3.91 4.30 4.00
1 6 3.70 3.99 4.20 4.00
Mean 3.77 3.91 4.32 4.00
Median 3.75 3.91 4.30 4.00
Std Dev. 0.175 0.052 0.075 0.000
Rel.Std.Dev. 4.65% 1.34% 1.74% 0.00%
PDM3 -5.79% -2.22% 7.96% 0.04%
Z-Score (Absolute) 1.09 0.26 2.09 0.26

Ge Round Replicate Lab Lab Lab Lab Lab
No No 05 13 14 16 19
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*OES/MS
1 1 0.30 0.69 0.70 1.10 0.40

1 2 0.30 0.66 0.70 1.10 0.50
1 3 0.30 0.68 0.80 1.10 0.60
1 4 0.30 0.58 0.80 1.10 0.50
1 5 0.30 0.60 0.80 1.10 0.40
1 6 0.30 0.57 0.80 1.20 0.70
Mean 0.30 0.63 0.77 1.12 0.52
Median 0.30 0.63 0.80 1.10 0.50
Std Dev. 0.000 0.053 0.052 0.041 0.117
Rel.Std.Dev. 0.00% 8.36% 6.74% 3.66% 22.63%
PDM3 -54.74% -4.83% 15.67% 68.47% -22.05%
Z-Score (Absolute) 1.64 0.00 0.67 2.33 0.57
Analytical results for Hf in OREAS 623 (Certified Value 3.97 ppm)

Hf Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 14
1 1 3.86 3.61 3.70 4.28 4.04 3.90

1 2 4.00 3.59 3.80 4.37 4.05 4.00
1 3 3.91 3.73 3.60 4.35 4.08 3.90
1 4 3.91 3.52 3.70 4.39 3.99 4.00
1 5 3.93 3.70 3.60 4.21 4.07 4.00
1 6 3.82 3.55 3.80 4.48 4.16 3.90
Mean 3.91 3.62 3.70 4.35 4.07 3.95
Median 3.91 3.60 3.70 4.36 4.06 3.95
Std Dev. 0.062 0.083 0.089 0.093 0.056 0.055
Rel.Std.Dev. 1.59% 2.29% 2.42% 2.14% 1.37% 1.39%
PDM3 -1.75% -9.01% -6.92% 9.35% 2.29% -0.63%
Z-Score (Absolute) 0.26 1.93 1.44 2.29 0.67 0.00
Analytical results for Hg in OREAS 623 (Indicative Value 0.56 ppm)

Hg Round Replicate Lab
No No 05
4A*MS
1 1 0.44
1 2 0.56
1 3 0.53
1 4 0.68
1 5 0.63
1 6 0.53
Mean 0.56
Median 0.55
Std Dev. 0.084
Rel.Std.Dev. 15.00%
PDM3 0.00%

No No 05 13 21 22
1 1 0.60 0.49 0.55 0.60

1 2 0.60 0.51 0.54 0.58
1 3 0.60 0.52 0.54 0.60
1 4 0.70 0.52 0.56 0.64
1 5 0.60 0.51 0.52 0.58
1 6 0.60 0.54 0.53 0.60
Mean 0.62 0.52 0.54 0.60
Median 0.60 0.51 0.54 0.60
Std Dev. 0.041 0.015 0.014 0.022
Rel.Std.Dev. 6.62% 2.99% 2.62% 3.65%
PDM3 9.39% -8.64% -4.21% 6.43%
Z-Score (Absolute) 0.67 1.24 0.67 0.67
No No 02 04 05 06 13 14
1 1 2.14 1.97 1.80 2.13 1.94 2.34

1 2 2.07 1.96 1.80 2.02 1.89 2.05
1 3 2.14 2.13 1.80 2.10 1.79 2.13
1 4 2.26 2.20 1.80 2.17 1.85 2.27
1 5 2.02 1.97 1.90 2.07 1.98 2.13
1 6 2.22 2.48 1.70 2.27 1.95 2.00
Mean 2.14 2.12 1.80 2.13 1.90 2.15
Median 2.14 2.05 1.80 2.12 1.91 2.13
Std Dev. 0.089 0.203 0.063 0.087 0.070 0.129
Rel.Std.Dev. 4.16% 9.60% 3.51% 4.08% 3.67% 6.01%
PDM3 2.13% 1.04% -14.15% 1.44% -9.34% 2.71%
Z-Score (Absolute) 0.86 0.35 3.46 0.67 2.18 1.01

No No 01 02 04 05 06 08
1 1 1.50 1.49 1.29 1.40 1.64 1.60

1 2 1.40 1.48 1.31 1.34 1.39 1.60
1 3 1.40 1.49 1.33 1.38 1.50 1.60
1 4 1.40 1.45 1.29 1.33 1.57 1.60
1 5 1.40 1.49 1.32 1.32 1.47 1.60
1 6 1.40 1.46 1.28 1.36 1.49 1.60
Mean 1.42 1.48 1.30 1.36 1.51 1.60
Median 1.40 1.48 1.30 1.35 1.50 1.60
Std Dev. 0.041 0.018 0.020 0.031 0.086 0.000
Rel.Std.Dev. 2.88% 1.19% 1.51% 2.27% 5.70% 0.00%
PDM3 -2.41% 1.81% -10.22% -6.66% 4.01% 10.21%
Z-Score (Absolute) 0.30 0.18 1.19 0.79 0.43 1.14

No No 01 02 04 05 06 08
1 1 < 50 20.7 19.0 19.0 14.5 < 50

1 2 < 50 20.2 19.0 13.7 14.7 < 50
1 3 < 50 19.0 19.9 20.9 14.6 < 50
1 4 < 50 19.3 18.8 18.6 14.8 < 50
1 5 < 50 20.8 20.2 18.5 14.1 < 50
1 6 < 50 19.3 18.4 18.7 14.9 < 50
Mean 19.9 19.2 18.2 14.6
Median 19.8 19.0 18.7 14.6
Std Dev. 0.8 0.7 2.4 0.3
Rel.Std.Dev. 3.87% 3.58% 13.13% 1.94%
PDM3 -7.70% -10.84% -15.40% -32.26%
Analytical results for Li in OREAS 623 (Certified Value 15.7 ppm)

No No 02 04 05 06 09 13
1 1 14.8 13.0 14.8 14.7 27.0 17.4

1 2 14.8 13.0 15.3 14.5 28.0 17.5
1 3 14.8 13.0 14.6 14.3 26.0 17.3
1 4 14.5 13.0 14.9 14.2 27.0 17.1
1 5 14.8 14.0 14.6 13.8 28.0 17.2
1 6 14.5 14.0 14.4 14.7 28.0 17.2
Mean 14.7 13.3 14.8 14.4 27.3 17.3
Median 14.8 13.0 14.7 14.4 27.5 17.2
Std Dev. 0.164 0.516 0.314 0.344 0.816 0.144
Rel.Std.Dev. 1.11% 3.87% 2.13% 2.40% 2.99% 0.84%
PDM3 -6.48% -15.21% -6.09% -8.63% 73.83% 9.83%
Z-Score (Absolute) 0.65 1.57 0.61 0.88 7.87 1.08
Analytical results for Lu in OREAS 623 (Certified Value 0.24 ppm)

Lu Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 19
4A*OES/MS4A*OES/MS 4A*MS 4A*MS 4A*OES/MS4A*OES/MS
1 1 0.26 0.22 0.20 0.17 0.23 0.24

1 2 0.31 0.23 0.20 0.17 0.22 0.22
1 3 0.22 0.24 0.20 0.17 0.23 0.24
1 4 0.22 0.22 0.20 0.17 0.24 0.23
1 5 0.23 0.24 0.20 0.16 0.23 0.23
1 6 0.27 0.22 0.30 0.18 0.23 0.25
Mean 0.25 0.23 0.22 0.17 0.23 0.24
Median 0.24 0.23 0.20 0.17 0.23 0.24
Std Dev. 0.034 0.010 0.041 0.006 0.007 0.010
Rel.Std.Dev. 13.70% 4.31% 18.84% 3.72% 3.18% 4.46%
PDM3 2.42% -6.21% -11.00% -30.17% -5.59% -3.47%
Z-Score (Absolute) 0.70 0.17 0.65 2.58 0.11 0.11

No No 01 02 04 05 06 08
1 1 1.07 1.23 1.09 1.16 1.54 1.13

1 2 1.02 1.21 1.10 1.16 1.28 1.11
1 3 1.05 1.19 1.10 1.17 1.38 1.11
1 4 1.06 1.18 1.08 1.16 1.45 1.12
1 5 1.02 1.22 1.13 1.13 1.35 1.12
1 6 1.07 1.21 1.11 1.15 1.42 1.11
Mean 1.05 1.21 1.10 1.16 1.40 1.12
Median 1.06 1.21 1.10 1.16 1.40 1.12
Std Dev. 0.023 0.016 0.017 0.014 0.089 0.008
Rel.Std.Dev. 2.21% 1.34% 1.56% 1.19% 6.35% 0.73%
PDM3 -12.72% 0.48% -8.28% -3.84% 16.84% -7.03%
Z-Score (Absolute) 1.65 0.13 1.05 0.45 2.03 0.88

No No 01 02 04 05 06 08
1 1 0.063 0.058 0.053 0.056 0.076 0.059

1 2 0.061 0.057 0.054 0.060 0.064 0.059
1 3 0.062 0.056 0.054 0.057 0.069 0.060
1 4 0.062 0.056 0.054 0.058 0.072 0.059
1 5 0.064 0.057 0.055 0.058 0.067 0.059
1 6 0.061 0.058 0.055 0.059 0.070 0.059
Mean 0.062 0.057 0.054 0.058 0.070 0.059
Median 0.062 0.057 0.054 0.058 0.069 0.059
Std Dev. 0.001 0.001 0.001 0.001 0.004 0.000
Rel.Std.Dev. 1.88% 1.47% 1.30% 2.44% 6.25% 0.69%
PDM3 3.69% -4.46% -9.68% -3.26% 16.12% -1.31%
Z-Score (Absolute) 0.61 0.85 1.79 0.63 2.85 0.28

No No 01 02 04 05 06 08
1 1 < 10 9.55 7.81 9.91 10.50 10.00

1 2 < 10 9.69 7.91 9.66 10.30 10.00
1 3 < 10 9.86 8.16 9.05 10.40 10.00
1 4 < 10 10.24 8.57 8.96 10.30 10.00
1 5 < 10 9.49 7.99 9.04 9.90 10.00
1 6 < 10 10.12 8.96 8.95 10.80 10.00
Mean 9.83 8.23 9.26 10.37 10.00
Median 9.78 8.08 9.05 10.35 10.00
Std Dev. 0.306 0.445 0.415 0.294 0.000
Rel.Std.Dev. 3.11% 5.40% 4.48% 2.84% 0.00%
PDM3 2.90% -13.78% -3.01% 8.56% 4.72%
Analytical results for Na in OREAS 623 (Certified Value 1.12 wt.%)
Na Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 04 05 06 08
1 1 1.14 1.12 0.94 1.05 1.27 1.11

1 2 1.11 1.12 0.94 1.04 1.06 1.10
1 3 1.13 1.10 0.96 1.07 1.14 1.09
1 4 1.11 1.09 0.93 1.03 1.21 1.10
1 5 1.12 1.12 0.95 1.02 1.13 1.10
1 6 1.13 1.07 0.95 1.08 1.14 1.10
Mean 1.12 1.10 0.95 1.05 1.16 1.10
Median 1.13 1.11 0.94 1.05 1.14 1.10
Std Dev. 0.012 0.019 0.010 0.023 0.073 0.006
Rel.Std.Dev. 1.08% 1.73% 1.11% 2.21% 6.26% 0.57%
PDM3 -0.01% -1.67% -15.88% -6.68% 3.11% -2.09%
Z-Score (Absolute) 0.12 0.37 2.55 1.14 0.36 0.44
Analytical results for Nb in OREAS 623 (Certified Value 8.58 ppm)

No No 02 04 05 06 13 14
1 1 8.51 7.90 8.80 8.20 8.94 8.50

1 2 8.81 8.00 8.80 8.60 9.05 8.80
1 3 9.23 8.20 8.80 8.70 9.47 8.80
1 4 8.94 8.00 8.90 8.30 9.45 8.90
1 5 9.29 8.20 8.70 8.10 9.42 9.30
1 6 8.92 7.80 8.80 8.30 9.32 9.10
Mean 8.95 8.02 8.80 8.37 9.28 8.90
Median 8.93 8.00 8.80 8.30 9.37 8.85
Std Dev. 0.286 0.160 0.063 0.234 0.227 0.276
Rel.Std.Dev. 3.19% 2.00% 0.72% 2.79% 2.44% 3.10%
PDM3 4.31% -6.57% 2.56% -2.49% 8.11% 3.73%
Z-Score (Absolute) 0.46 0.72 0.27 0.27 0.88 0.40
Analytical results for Nd in OREAS 623 (Indicative Value 22.3 ppm)

Nd Round Replicate Lab Lab Lab Lab
No No 05 13 21 22
1 1 20.2 23.0 22.5 23.0

1 2 18.5 23.3 23.4 22.4
1 3 19.8 23.5 23.0 23.4
1 4 20.5 23.7 23.1 23.7
1 5 19.7 23.7 22.4 22.7
1 6 20.0 23.9 22.0 23.2
Mean 19.8 23.5 22.7 23.1
Median 19.9 23.6 22.8 23.1
Std Dev. 0.7 0.3 0.5 0.5
Rel.Std.Dev. 3.49% 1.27% 2.29% 2.05%
PDM3 -11.44% 5.26% 1.77% 3.26%
Z-Score (Absolute) 4.94 1.06 0.29 0.29
Analytical results for Ni in OREAS 623 (Certified Value 16.8 ppm)

No No 01 02 04 05 06 08
1 1 10.0 14.6 15.3 18.4 22.0 10.0

1 2 10.0 16.7 16.1 19.2 19.0 10.0
1 3 10.0 15.7 15.8 17.7 17.0 10.0
1 4 10.0 16.2 15.8 18.9 20.0 10.0
1 5 10.0 13.8 15.6 18.3 19.0 20.0
1 6 10.0 15.5 14.9 18.8 18.0 10.0
Mean 10.0 15.4 15.6 18.5 19.2 11.7
Median 10.0 15.6 15.7 18.6 19.0 10.0
Std Dev. 0.0 1.1 0.4 0.5 1.7 4.1
Rel.Std.Dev. 0.00% 6.84% 2.74% 2.87% 8.99% 34.99%
PDM3 -40.55% -8.44% -7.35% 10.29% 13.95% -30.64%
Z-Score (Absolute) 2.17 0.55 0.50 0.39 0.57 1.67
Analytical results for P in OREAS 623 (Certified Value 0.043 wt.%)

No No 01 02 04 05 06 08
1 1 0.043 0.047 0.036 0.044 < 0.002 0.045

1 2 0.043 0.045 0.033 0.044 0.002 0.043
1 3 0.042 0.049 0.035 0.046 < 0.002 0.045
1 4 0.043 0.051 0.034 0.044 < 0.002 0.045
1 5 0.043 0.042 0.034 0.044 < 0.002 0.042
1 6 0.042 0.050 0.040 0.044 < 0.002 0.044
Mean 0.043 0.047 0.035 0.044 0.002 0.044
Median 0.043 0.048 0.035 0.044 0.002 0.045
Std Dev. 0.001 0.003 0.003 0.001 0.001
Rel.Std.Dev. 1.21% 6.92% 7.08% 1.84% 2.87%
PDM3 -1.21% 9.35% -18.19% 2.65% -95.37% 1.88%
Z-Score (Absolute) 0.24 0.73 1.99 0.11 8.87 0.04

No No 01 02 04 05 06 08
1 1 0.255 0.262 0.245 0.260 0.266 0.254

1 2 0.248 0.261 0.247 0.241 0.270 0.250
1 3 0.248 0.260 0.250 0.249 0.229 0.250
1 4 0.244 0.260 0.245 0.247 0.235 0.250
1 5 0.244 0.262 0.257 0.255 0.257 0.250
1 6 0.247 0.257 0.251 0.257 0.228 0.252
Mean 0.248 0.260 0.249 0.252 0.248 0.251
Median 0.248 0.260 0.249 0.252 0.246 0.250
Std Dev. 0.004 0.002 0.005 0.007 0.019 0.002
Rel.Std.Dev. 1.63% 0.77% 1.84% 2.82% 7.70% 0.67%
PDM3 -0.84% 4.24% -0.24% 0.70% -0.90% 0.50%
Z-Score (Absolute) 0.69 1.75 0.40 0.05 0.72 0.05
Analytical results for Pr in OREAS 623 (Indicative Value 5.79 ppm)

Pr Round Replicate Lab Lab Lab Lab
No No 05 13 21 22
1 1 5.50 5.93 6.12 5.70

1 2 4.80 6.09 6.12 5.60
1 3 5.40 6.03 6.17 5.68
1 4 5.50 6.09 6.13 5.74
1 5 5.20 5.98 6.36 5.58
1 6 5.30 6.08 6.21 5.74
Mean 5.28 6.03 6.19 5.67
Median 5.35 6.05 6.15 5.69
Std Dev. 0.264 0.067 0.093 0.069
Rel.Std.Dev. 5.00% 1.12% 1.50% 1.21%
PDM3 -8.81% 4.14% 6.75% -2.08%
Z-Score (Absolute) 1.50 0.47 0.87 0.47
Analytical results for Rb in OREAS 623 (Certified Value 62 ppm)

No No 02 04 05 06 13 14
1 1 60 61 61 64 66 64
1 2 62 61 58 65 66 67
1 3 61 62 61 65 66 67
1 4 61 61 62 64 66 67
1 5 63 62 61 62 67 67
1 6 61 59 61 66 67 68
Mean 61 61 61 64 66 67
Median 61 61 61 65 66 67
Std Dev. 1.0 0.9 1.6 1.3 0.6 1.2
Rel.Std.Dev. 1.57% 1.49% 2.56% 2.09% 0.92% 1.83%
PDM3 -1.88% -2.16% -2.75% 3.43% 6.35% 6.88%
Z-Score (Absolute) 0.01 0.05 0.00 0.78 1.22 1.30
Re Round Replicate Lab Lab Lab Lab Lab Lab
No No 05 13 14 16 20 22
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*MS
1 1 0.015 < 0.002 < 0.05 < 0.05 < 0.005 < 0.1
1 2 0.016 < 0.002 < 0.05 < 0.05 < 0.005 < 0.1
1 3 0.016 < 0.002 < 0.05 < 0.05 0.006 < 0.1
1 4 0.020 < 0.002 < 0.05 < 0.05 0.008 < 0.1
1 5 0.018 < 0.002 < 0.05 < 0.05 < 0.005 < 0.1
1 6 0.021 < 0.002 < 0.05 < 0.05 < 0.005 < 0.1
Mean 0.018 0.007
Median 0.017 0.007
Std Dev. 0.002 0.001
Rel.Std.Dev. 13.71% 20.20%
PDM3
Z-Score (Absolute) 0.67 NA NA NA 0.67 NA

No No 01 02 04 05 06 08
1 1 9.05 >5 >5 8.13 > 50000 9.17

1 2 8.94 >5 >5 8.16 > 50000 9.19
1 3 8.87 >5 >5 8.34 > 50000 9.20
1 4 8.94 >5 >5 8.10 > 50000 9.28
1 5 8.91 >5 >5 8.13 > 50000 9.00
1 6 8.95 >5 >5 8.23 > 50000 8.88
Mean 8.94 8.18 9.12
Median 8.94 8.15 9.18
Std Dev. 0.060 0.089 0.149
Rel.Std.Dev. 0.67% 1.09% 1.64%
PDM3 -1.27% -9.68% 0.68%
Z-Score (Absolute) 0.67 NA NA 3.58 NA 0.00
Analytical results for Sb in OREAS 623 (Certified Value 27.6 ppm)

No No 01 02 04 05 06 08
1 1 < 50 29.3 27.0 30.0 27.9 < 50

1 2 < 50 29.6 27.3 30.5 28.1 < 50
1 3 < 50 28.2 27.4 29.4 28.0 < 50
1 4 < 50 29.4 27.1 30.5 28.1 < 50
1 5 < 50 29.2 27.8 30.3 26.9 < 50
1 6 < 50 28.7 26.8 28.7 28.5 < 50
Mean 29.1 27.2 29.9 27.9
Median 29.2 27.2 30.2 28.1
Std Dev. 0.503 0.350 0.718 0.538
Rel.Std.Dev. 1.73% 1.29% 2.40% 1.93%
PDM3 5.25% -1.39% 8.26% 1.08%
Analytical results for Sc in OREAS 623 (Certified Value 8.32 ppm)

No No 01 02 04 05 06 08
1 1 10.00 6.49 7.30 8.00 7.50 10.00

1 2 10.00 6.63 7.20 8.00 7.40 10.00
1 3 10.00 6.49 7.30 8.00 7.30 10.00
1 4 10.00 6.78 7.30 8.00 7.40 10.00
1 5 10.00 6.84 7.40 8.00 7.20 10.00
1 6 10.00 6.71 7.10 8.00 7.60 10.00
Mean 10.00 6.66 7.27 8.00 7.40 10.00
Median 10.00 6.67 7.30 8.00 7.40 10.00
Std Dev. 0.000 0.147 0.103 0.000 0.141 0.000
Rel.Std.Dev. 0.00% 2.21% 1.42% 0.00% 1.91% 0.00%
PDM3 20.21% -19.98% -12.65% -3.84% -11.05% 20.21%
Z-Score (Absolute) 1.45 0.92 0.49 0.03 0.39 1.45
Analytical results for Se in OREAS 623 (Certified Value 18.7 ppm)

No No 02 04 05 06 09 13
1 1 18.6 17.0 19.5 19.0 103.0 20.5

1 2 16.2 18.0 20.6 19.0 97.0 19.8
1 3 17.9 17.0 18.6 19.0 82.0 19.7
1 4 18.5 19.0 18.7 19.0 93.0 20.1
1 5 16.8 17.0 17.7 18.0 109.0 20.1
1 6 18.7 20.0 18.1 21.0 110.0 20.5
Mean 17.8 18.0 18.9 19.2 99.0 20.1
Median 18.2 17.5 18.7 19.0 100.0 20.1
Std Dev. 1.048 1.265 1.044 0.983 10.640 0.352
Rel.Std.Dev. 5.89% 7.03% 5.54% 5.13% 10.75% 1.75%
PDM3 -4.73% -3.55% 1.10% 2.71% 430.50% 7.81%
Z-Score (Absolute) 0.61 0.48 0.04 0.00 47.72 0.79

No No 05 13 21 22
1 1 4.20 4.73 4.80 4.75

1 2 3.90 4.67 4.90 4.85
1 3 4.10 4.79 4.90 4.80
1 4 4.30 4.93 5.10 5.05
1 5 4.10 5.14 4.70 4.85
1 6 4.20 5.00 4.80 4.70
Mean 4.13 4.88 4.87 4.83
Median 4.15 4.86 4.85 4.82
Std Dev. 0.137 0.179 0.137 0.121
Rel.Std.Dev. 3.31% 3.67% 2.81% 2.51%
PDM3 -14.94% 0.39% 0.15% -0.54%
Z-Score (Absolute) 21.36 0.85 0.50 0.50
Analytical results for Sn in OREAS 623 (Certified Value 5.94 ppm)

No No 02 04 05 06 09 10
4A*OES/MS4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES
1 1 5.95 5.70 5.80 6.00 < 20 6.00

1 2 5.71 5.70 5.58 6.00 < 20 6.00
1 3 5.70 5.70 5.44 6.00 < 20 6.00
1 4 5.96 6.10 5.47 6.00 < 20 7.00
1 5 5.72 5.80 5.33 5.90 < 20 6.00
1 6 5.88 6.50 5.59 6.20 < 20 6.00
Mean 5.82 5.92 5.53 6.02 6.17
Median 5.80 5.75 5.53 6.00 6.00
Std Dev. 0.126 0.325 0.162 0.098 0.408
Rel.Std.Dev. 2.16% 5.49% 2.92% 1.63% 6.62%
PDM3 -1.97% -0.33% -6.76% 1.35% 3.88%
Analytical results for Sr in OREAS 623 (Certified Value 80 ppm)

No No 01 02 04 05 06 08
1 1 80 78 67 62 82 90
1 2 70 76 66 55 82 90
1 3 70 69 68 70 82 90
1 4 80 74 65 63 81 80
1 5 70 72 68 62 79 90
1 6 80 73 64 63 84 80
Mean 75 74 66 63 82 87
Median 75 73 66 62 82 90
Std Dev. 5.5 3.1 1.6 4.8 1.5 5.2
Rel.Std.Dev. 7.30% 4.18% 2.34% 7.71% 1.85% 5.96%
PDM3 -6.04% -7.76% -16.83% -21.63% 2.34% 8.58%
Z-Score (Absolute) 0.83 1.01 1.93 2.42 0.02 0.66
Analytical results for Ta in OREAS 623 (Certified Value < 1 ppm)
No No 02 04 05 06 13 14
1 1 0.65 0.83 0.50 0.95 0.90 0.60

1 2 0.69 0.84 0.60 0.95 0.93 0.61
1 3 0.69 0.87 0.50 0.98 0.99 0.62
1 4 0.68 0.84 0.50 0.92 0.95 0.61
1 5 0.72 0.88 0.50 0.89 0.94 0.65
1 6 0.68 0.83 0.60 0.95 0.95 0.61
Mean 0.68 0.85 0.53 0.94 0.94 0.62
Median 0.68 0.84 0.50 0.95 0.94 0.61
Std Dev. 0.022 0.021 0.052 0.031 0.032 0.018
Rel.Std.Dev. 3.21% 2.52% 9.68% 3.30% 3.43% 2.84%
PDM3
Z-Score (Absolute) 0.32 0.32 0.90 0.67 0.68 0.60
Analytical results for Tb in OREAS 623 (Certified Value 0.53 ppm)

Tb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 19
1 1 0.45 0.53 0.50 0.35 0.50 0.48

1 2 0.46 0.55 0.50 0.36 0.52 0.47
1 3 0.46 0.56 0.50 0.35 0.53 0.47
1 4 0.46 0.54 0.50 0.36 0.53 0.50
1 5 0.48 0.57 0.50 0.35 0.54 0.47
1 6 0.45 0.55 0.50 0.37 0.55 0.49
Mean 0.46 0.55 0.50 0.36 0.53 0.48
Median 0.46 0.55 0.50 0.36 0.53 0.48
Std Dev. 0.012 0.014 0.000 0.008 0.017 0.013
Rel.Std.Dev. 2.62% 2.57% 0.00% 2.29% 3.18% 2.64%
PDM3 -12.80% 4.08% -5.39% -32.51% -0.01% -9.17%
Z-Score (Absolute) 0.92 0.62 0.24 2.72 0.24 0.59
Analytical results for Te in OREAS 623 (Certified Value 0.58 ppm)

No No 02 04 05 06 10 13
1 1 0.53 0.62 0.60 0.50 <5 0.50

1 2 0.58 0.63 1.00 0.50 <5 0.52
1 3 0.63 0.65 0.80 0.50 <5 0.52
1 4 0.59 0.56 0.60 0.60 <5 0.50
1 5 0.59 0.60 0.80 0.50 <5 0.53
1 6 0.62 0.64 0.80 0.60 <5 0.51
Mean 0.59 0.62 0.77 0.53 0.51
Median 0.59 0.63 0.80 0.50 0.51
Std Dev. 0.036 0.033 0.151 0.052 0.012
Rel.Std.Dev. 6.12% 5.30% 19.64% 9.68% 2.30%
PDM3 1.15% 5.96% 31.73% -8.36% -11.86%

No No 01 02 04 05 06 08
1 1 < 50 6.41 5.70 4.60 5.46 < 50

1 2 < 50 6.48 5.50 5.20 5.64 < 50
1 3 < 50 6.71 5.50 5.30 5.58 < 50
1 4 < 50 6.41 5.60 4.40 5.54 < 50
1 5 < 50 7.05 6.10 4.10 5.33 < 50
1 6 < 50 6.36 5.90 4.20 5.63 < 50
Mean 6.57 5.72 4.63 5.53
Median 6.44 5.65 4.50 5.56
Std Dev. 0.267 0.240 0.509 0.118
Rel.Std.Dev. 4.07% 4.20% 10.98% 2.13%
PDM3 2.61% -10.71% -27.63% -13.62%
Analytical results for Ti in OREAS 623 (Certified Value 0.139 wt.%)

No No 01 02 04 05 06 08
1 1 0.140 0.125 0.110 0.160 0.110 0.140

1 2 0.130 0.127 0.110 0.160 0.096 0.140
1 3 0.140 0.122 0.110 0.170 0.107 0.140
1 4 0.140 0.121 0.110 0.160 0.107 0.140
1 5 0.140 0.126 0.110 0.150 0.099 0.140
1 6 0.140 0.124 0.110 0.160 0.100 0.140
Mean 0.138 0.124 0.110 0.160 0.103 0.140
Median 0.140 0.125 0.110 0.160 0.104 0.140
Std Dev. 0.004 0.002 0.000 0.006 0.006 0.000
Rel.Std.Dev. 2.95% 1.87% 0.00% 3.95% 5.39% 0.00%
PDM3 -0.76% -10.92% -21.08% 14.79% -25.99% 0.44%
Z-Score (Absolute) 0.10 1.18 2.26 1.55 2.79 0.03

No No 01 02 04 05 06 08
1 1 < 50 0.80 0.76 0.90 0.60 < 50

1 2 < 50 0.78 0.78 0.80 0.60 < 50
1 3 < 50 0.79 0.77 0.80 0.60 < 50
1 4 < 50 0.79 0.74 0.80 0.60 < 50
1 5 < 50 0.79 0.79 0.80 0.60 < 50
1 6 < 50 0.77 0.76 0.80 0.60 < 50
Mean 0.78 0.77 0.82 0.60
Median 0.79 0.77 0.80 0.60
Std Dev. 0.010 0.018 0.041 0.000
Rel.Std.Dev. 1.22% 2.28% 5.00% 0.00%
PDM3 6.61% 4.14% 10.94% -18.50%

Tm Round Replicate Lab Lab Lab Lab
No No 05 13 21 22
1 1 0.30 0.23 0.23 0.24

1 2 0.20 0.20 0.23 0.24
1 3 0.30 0.22 0.23 0.24
1 4 0.30 0.22 0.23 0.24
1 5 0.30 0.22 0.22 0.26
1 6 0.30 0.22 0.23 0.24
Mean 0.28 0.22 0.23 0.24
Median 0.30 0.22 0.23 0.24
Std Dev. 0.041 0.009 0.004 0.008
Rel.Std.Dev. 14.41% 3.98% 1.79% 3.36%
PDM3 16.46% -10.33% -6.15% 0.02%
Z-Score (Absolute) 2.55 0.95 0.40 0.40

No No 01 02 04 05 06 08
1 1 < 50 2.70 2.63 2.60 2.02 < 50

1 2 < 50 2.71 2.55 2.50 2.08 < 50
1 3 < 50 2.69 2.65 2.50 2.02 < 50
1 4 < 50 2.68 2.58 2.70 2.05 < 50
1 5 < 50 2.72 2.71 2.60 1.98 < 50
1 6 < 50 2.68 2.53 2.60 2.10 < 50
Mean 2.70 2.61 2.58 2.04
Median 2.69 2.61 2.60 2.04
Std Dev. 0.015 0.068 0.075 0.044
Rel.Std.Dev. 0.57% 2.59% 2.91% 2.16%
PDM3 2.57% -0.78% -1.73% -22.34%
Analytical results for V in OREAS 623 (Certified Value 26 ppm)
No No 01 02 04 05 06 08
1 1 30.0 29.6 27.0 27.0 31.0 30.0

1 2 30.0 29.0 27.0 26.0 26.0 20.0
1 3 30.0 28.9 28.0 27.0 27.0 20.0
1 4 20.0 29.0 26.0 26.0 29.0 30.0
1 5 30.0 29.1 27.0 27.0 27.0 30.0
1 6 20.0 29.0 25.0 26.0 29.0 30.0
Mean 26.7 29.1 26.7 26.5 28.2 26.7
Median 30.0 29.0 27.0 26.5 28.0 30.0
Std Dev. 5.2 0.2 1.0 0.5 1.8 5.2
Rel.Std.Dev. 19.36% 0.81% 3.87% 2.07% 6.51% 19.36%
PDM3 2.60% 12.03% 2.60% 1.96% 8.37% 2.60%
Z-Score (Absolute) 0.08 0.82 0.08 0.03 0.53 0.08

No No 01 04 05 06 08 09
4A*OES 4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES
1 1 < 50 4.40 3.80 4.10 < 50 < 20

1 2 < 50 4.50 3.90 4.20 < 50 < 20
1 3 < 50 4.70 4.00 4.30 < 50 < 20
1 4 < 50 4.50 3.90 4.20 < 50 < 20
1 5 < 50 4.60 3.90 4.10 < 50 < 20
1 6 < 50 4.70 3.80 4.40 < 50 < 20
Mean 4.57 3.88 4.22
Median 4.55 3.90 4.20
Std Dev. 0.121 0.075 0.117
Rel.Std.Dev. 2.65% 1.94% 2.77%
PDM3 6.79% -9.19% -1.39%
Z-Score (Absolute) NA 0.87 0.75 0.04 NA NA

No No 02 04 05 06 09 12
4A*OES/MS4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*OES
1 1 13.2 12.8 16.0 12.7 12.0 20.0

1 2 13.4 12.9 14.0 12.8 13.0 20.0
1 3 13.2 13.2 16.0 12.7 11.0 20.0
1 4 13.3 12.9 16.0 12.5 11.0 20.0
1 5 13.5 12.9 16.0 12.2 15.0 20.0
1 6 13.2 12.7 16.0 13.2 13.0 20.0
Mean 13.3 12.9 15.7 12.7 12.5 20.0
Median 13.3 12.9 16.0 12.7 12.5 20.0
Std Dev. 0.123 0.167 0.816 0.331 1.517 0.000
Rel.Std.Dev. 0.92% 1.30% 5.21% 2.61% 12.13% 0.00%
PDM3 -0.38% -3.32% 17.41% -4.95% -6.32% 49.88%
Z-Score (Absolute) 0.09 0.43 1.95 0.62 0.77 5.68

Yb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 19
1 1 1.39 1.50 1.50 1.10 1.38 1.50

1 2 1.39 1.50 1.30 1.10 1.42 1.50
1 3 1.39 1.50 1.40 1.10 1.44 1.50
1 4 1.37 1.40 1.50 1.10 1.43 1.50
1 5 1.40 1.50 1.40 1.00 1.51 1.50
1 6 1.34 1.50 1.50 1.10 1.50 1.50
Mean 1.38 1.48 1.43 1.08 1.45 1.50
Median 1.39 1.50 1.45 1.10 1.44 1.50
Std Dev. 0.021 0.041 0.082 0.041 0.050 0.000
Rel.Std.Dev. 1.50% 2.75% 5.70% 3.77% 3.45% 0.00%
PDM3 -6.25% 0.80% -2.59% -26.38% -1.50% 1.94%
Z-Score (Absolute) 0.97 0.19 0.37 4.29 0.19 0.38

No No 01 02 04 05 06 08
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES
1 1 1.07 1.02 0.91 1.01 1.15 1.04

1 2 1.03 1.03 0.94 1.01 1.10 1.02
1 3 1.02 1.05 0.91 1.01 0.95 1.05
1 4 1.04 1.05 0.92 1.00 0.97 1.03
1 5 1.02 1.06 0.95 1.01 1.04 1.03
1 6 1.03 1.07 0.98 1.02 0.98 1.04
Mean 1.04 1.05 0.94 1.01 1.03 1.03
Median 1.03 1.05 0.93 1.01 1.01 1.03
Std Dev. 0.019 0.019 0.029 0.006 0.080 0.009
Rel.Std.Dev. 1.81% 1.78% 3.07% 0.63% 7.77% 0.85%
PDM3 0.74% 1.88% -8.91% -1.69% 0.37% 0.58%
Z-Score (Absolute) 0.12 0.78 3.15 0.52 0.61 0.31
Analytical results for Zr in OREAS 623 (Certified Value 150 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 09 13
1 1 148 142 155 155 156 149

1 2 147 140 157 158 157 149
1 3 148 147 152 156 156 150
1 4 144 142 154 155 150 150
1 5 147 146 155 150 160 151
1 6 144 135 153 161 154 151
Mean 146 142 154 156 156 150
Median 147 142 155 156 156 150
Std Dev. 2 4 2 4 3 1
Rel.Std.Dev. 1.03% 3.05% 1.13% 2.35% 2.14% 0.65%
PDM3 -2.31% -5.14% 3.10% 4.11% 3.88% 0.25%
Z-Score (Absolute) 0.50 0.99 0.43 0.61 0.57 0.06
09 10 11 12 13 14 15 16 17
4A*AAS 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES
21.0 21.2 20.0 20.0 20.3 20.8 19.0 19.9 19.0

21.0 21.7 21.0 20.0 20.1 19.9 18.3 20.5 20.0
21.0 21.1 21.0 20.0 20.3 20.0 19.3 20.3 21.0
21.0 21.9 20.0 20.0 20.3 20.4 19.1 19.8 20.0
22.0 21.2 21.0 20.0 20.6 19.9 18.8 20.9 20.0
21.0 21.3 19.0 20.0 20.3 20.3 29.0 20.5 20.0
21.2 21.4 20.3 20.0 20.3 20.2 20.6 20.3 20.0
21.0 21.3 20.5 20.0 20.3 20.2 19.1 20.4 20.0
0.408 0.322 0.816 0.000 0.147 0.354 4.160 0.412 0.632
1.93% 1.51% 4.02% 0.00% 0.72% 1.75% 20.21% 2.03% 3.16%
3.76% 4.90% -0.33% -1.96% -0.39% -0.90% 0.92% -0.41% -1.96%
0.76 0.99 0.08 0.42 0.10 0.20 1.54 0.10 0.42

09 10 11 12 13 14 15 16 17
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES
4.99 5.30 6.77 5.43 5.40 5.10 5.35 5.44 4.23

5.10 5.19 6.78 5.14 5.43 5.29 5.22 5.44 4.35
4.71 5.25 7.25 5.47 5.36 5.24 5.29 5.46 4.56
4.81 5.31 6.57 5.64 5.47 5.28 5.28 5.46 4.33
5.03 5.25 5.94 5.52 5.45 5.24 5.22 5.28 4.26
5.09 5.24 5.35 5.25 5.40 5.30 5.22 5.39 4.41
4.96 5.26 6.44 5.41 5.42 5.24 5.26 5.41 4.36
5.01 5.25 6.67 5.45 5.41 5.26 5.25 5.44 4.34
0.159 0.041 0.683 0.183 0.037 0.074 0.053 0.069 0.119
3.22% 0.79% 10.61% 3.38% 0.68% 1.41% 1.01% 1.28% 2.72%
-1.67% 4.33% 27.86% 7.32% 7.51% 4.06% 4.40% 7.39% -13.55%
0.23 0.65 4.08 1.08 1.11 0.69 0.66 1.09 1.96

09 10 11 12 13 14 15 16 17
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES
96 61 210 80 77 82 81 79 70
91 73 190 80 77 80 79 78 70
81 70 170 80 77 81 82 81 60
89 71 170 90 76 81 81 80 60
102 71 180 80 77 83 79 81 60
98 73 190 80 76 80 81 79 < 50
93 70 185 82 77 81 81 80 64
94 71 185 80 77 81 81 80 60
7.5 4.5 15.2 4.1 0.5 1.2 1.3 1.2 5.5
8.04% 6.43% 8.20% 5.00% 0.64% 1.44% 1.61% 1.52% 8.56%
19.83% -9.86% 138.80% 5.42% -0.86% 4.77% 3.97% 2.84% -17.39%
2.68 1.14 19.26 0.67 0.20 0.58 0.47 0.31 2.50

10 11 13 16 17 20 22 23 24
4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*MS 4A*OES 4A*OES
827 380 1286 1070 1060 39 1140 950 16

815 370 1385 1080 1160 28 1110 1210 15
820 340 1271 1080 1210 14 1190 1160 14
842 340 1396 1060 1160 14 1130 1180 14
845 340 1297 1100 1150 18 1270 1130 16
458 400 1333 1090 1160 12 1240 1070 17
768 362 1328 1080 1150 21 1180 1117 15
824 355 1315 1080 1160 16 1165 1145 16
152 26 52 14 49 11 64 95 1
19.83% 7.09% 3.95% 1.31% 4.26% 50.84% 5.47% 8.47% 7.90%
-35.92% -69.82% 10.84% -9.86% -4.02% -98.26% -1.52% -6.80% -98.72%
0.09 0.70 0.93 0.52 0.66 1.28 0.68 0.58 1.28

09 11 13 14 15 16 17 19 20
4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*MS
<3 < 10 1.39 1.40 <5 1.40 < 10 1.50 1.00

<3 < 10 1.38 1.50 <5 1.40 < 10 1.50 1.00
<3 < 10 1.32 1.60 <5 1.40 < 10 1.40 1.00
<3 < 10 1.45 1.50 <5 1.40 < 10 1.40 <1
<3 < 10 1.35 1.50 <5 1.40 < 10 1.40 2.00
<3 < 10 1.37 1.20 1.40 < 10 1.70 <1
1.38 1.45 1.40 1.48 1.25
1.38 1.50 1.40 1.45 1.00
0.043 0.138 0.000 0.117 0.500
3.14% 9.51% 0.00% 7.88% 40.00%
-0.67% 4.57% 0.97% 6.98% -9.85%
NA NA 0.10 0.73 NA 0.06 NA 0.62 0.96

09 10 11 13 14 15 16 17 19
4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES/MS
40.0 18.0 < 20 16.9 18.3 27.0 16.5 20.0 18.2

46.0 18.0 < 20 17.2 18.3 30.5 16.6 20.0 17.9
42.0 18.0 < 20 17.0 18.0 28.8 17.2 20.0 18.1
41.0 19.0 < 20 17.0 17.9 24.5 16.8 < 20 18.3
40.0 19.0 < 20 17.3 18.4 28.3 17.5 30.0 18.0
48.0 19.0 < 20 17.3 17.7 26.5 16.8 20.0 17.7
42.8 18.5 17.1 18.1 27.6 16.9 22.0 18.0
41.5 18.5 17.1 18.1 27.6 16.8 20.0 18.1
3.371 0.548 0.155 0.291 2.066 0.379 4.472 0.216
7.87% 2.96% 0.91% 1.61% 7.49% 2.25% 20.33% 1.20%
141.70% 4.39% -3.55% 2.04% 55.65% -4.64% 24.14% 1.76%
10.02 0.18 NA 0.39 0.01 3.85 0.47 0.79 0.01

09 11 12 13 14 15 16 17 19
4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS
1.32 1.54 1.47 1.47 1.31 1.50 1.32 1.34 1.33

1.34 1.53 1.40 1.47 1.36 1.45 1.31 1.36 1.32
1.26 1.61 1.46 1.42 1.35 1.49 1.32 1.38 1.35
1.30 1.51 1.50 1.46 1.38 1.54 1.32 1.33 1.33
1.34 1.46 1.44 1.43 1.36 1.42 1.29 1.32 1.33
1.34 1.40 1.41 1.41 1.39 1.49 1.31 1.37 1.36
1.32 1.51 1.45 1.44 1.36 1.48 1.31 1.35 1.34
1.33 1.52 1.45 1.45 1.36 1.49 1.32 1.35 1.33
0.032 0.072 0.038 0.027 0.026 0.040 0.012 0.024 0.015
2.43% 4.77% 2.61% 1.85% 1.91% 2.71% 0.89% 1.75% 1.13%
-4.28% 9.66% 5.17% 4.98% -1.33% 7.78% -4.64% -1.85% -2.82%
0.67 1.62 1.03 0.99 0.25 1.54 0.91 0.36 0.55
09 10 11 12 13 14 15 16 19
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES/MS
54 54 60 58 54 59 57 50 55
54 53 60 54 54 58 55 49 55
51 54 60 58 54 57 57 49 56
52 53 50 60 53 57 56 49 57
54 54 50 58 55 58 55 49 55
53 53 50 58 55 58 58 48 56
53 53 55 58 54 58 56 49 56
54 53 55 58 54 58 56 49 56
1.3 0.4 5.5 2.0 0.7 1.0 1.2 0.7 0.9
2.39% 0.73% 9.96% 3.41% 1.26% 1.76% 2.18% 1.35% 1.56%
-1.57% -0.86% 2.14% 7.10% 0.28% 7.48% 4.36% -8.81% 3.66%
0.08 0.00 0.34 1.06 0.13 0.94 0.59 0.90 0.45
Lab Lab Lab Lab

19 20 21 22
4A*OES/MS 4A*MS 4A*MS 4A*MS
47.9 41.0 50.8 56.0

47.1 39.0 53.6 53.4
47.8 42.0 51.9 53.3
49.3 40.0 52.8 54.6
48.1 41.0 48.8 53.1
49.4 43.0 49.9 55.3
48.3 41.0 51.3 54.3
48.0 41.0 51.3 54.0
0.9 1.4 1.8 1.2
1.88% 3.45% 3.53% 2.21%
5.78% -10.14% 12.44% 18.98%
0.57 0.72 1.11 1.64

09 10 11 12 13 14 15 16 17
202 215 220 245 217 220 233 209 200

200 217 230 255 213 222 230 213 210
195 215 230 240 211 218 233 224 210
194 215 220 250 215 227 240 219 210
201 213 220 240 217 226 232 223 200
198 215 220 240 216 219 245 217 210
198 215 223 245 215 222 235 218 207
199 215 220 243 216 221 233 218 210
3 1 5 6 2 4 6 6 5
1.65% 0.59% 2.31% 2.58% 1.05% 1.61% 2.43% 2.66% 2.50%
-10.48% -2.96% 0.80% 10.58% -3.00% 0.19% 6.22% -1.83% -6.72%
2.50 0.73 0.16 2.47 0.74 0.02 1.23 0.46 1.62

09 10 11 12 13 14 15 16 17
12.0 29.0 50.0 20.0 26.7 22.0 29.8 26.0 30.0

15.0 29.0 60.0 20.0 25.6 23.0 29.8 26.0 20.0
10.0 29.0 40.0 20.0 26.9 25.0 29.8 26.0 30.0
6.0 32.0 30.0 20.0 26.8 26.0 29.5 24.0 40.0
11.0 29.0 40.0 20.0 26.7 27.0 28.3 24.0 20.0
17.0 32.0 30.0 20.0 27.5 24.0 27.8 25.0 60.0
11.8 30.0 41.7 20.0 26.7 24.5 29.1 25.2 33.3
11.5 29.0 40.0 20.0 26.7 24.5 29.6 25.5 30.0
3.9 1.5 11.7 0.0 0.6 1.9 0.9 1.0 15.1
32.69% 5.16% 28.06% 0.00% 2.22% 7.64% 3.06% 3.91% 45.17%
-52.34% 20.82% 67.81% -19.45% 7.53% -1.33% 17.30% 1.35% 34.24%
2.11 0.84 2.74 0.78 0.34 0.05 0.70 0.06 0.52
Lab Lab Lab Lab

16 19 21 22
2.90 2.96 2.68 2.80

2.90 3.08 2.80 2.80
2.90 2.93 2.79 2.90
2.90 3.16 2.83 2.90
2.70 2.90 2.61 2.90
2.80 2.90 2.73 2.90
2.85 2.99 2.74 2.87
2.90 2.95 2.76 2.90
0.084 0.107 0.083 0.052
2.94% 3.59% 3.04% 1.80%
-0.11% 4.74% -3.97% 0.47%
0.09 1.21 1.12 0.07

09 10 11 12 13 14 15 16 17
> 10000 1.76 1.70 1.88 1.73 1.84 1.73 1.73 1.66
> 10000 1.73 1.75 1.64 1.73 1.73 1.78 1.78 1.72
> 10000 1.72 1.91 1.77 1.75 1.73 1.73 1.79 1.72
-- 1.72 1.67 1.81 1.74 1.75 1.80 1.77 1.73
> 10000 1.74 1.69 1.73 1.73 1.73 1.76 1.79 1.69
> 10000 1.73 1.63 1.79 1.75 1.66 1.82 1.77 1.71
1.74 1.72 1.77 1.74 1.74 1.77 1.77 1.71
1.73 1.69 1.78 1.74 1.73 1.77 1.78 1.71
0.016 0.099 0.081 0.010 0.058 0.038 0.022 0.026
0.92% 5.75% 4.56% 0.56% 3.34% 2.16% 1.26% 1.52%
0.08% -0.57% 2.07% 0.23% 0.41% 2.09% 2.17% -1.68%
NA 0.31 0.74 1.05 0.36 0.00 1.06 1.09 0.35
09 10 11 12 13 14 15 16 17
14.17 13.88 13.00 14.80 13.92 13.33 13.32 13.40 12.30

14.49 13.75 13.15 15.60 13.83 13.49 13.31 13.50 12.75
13.96 13.76 13.65 14.80 13.89 13.44 13.34 13.90 13.20
13.75 13.70 12.75 15.20 13.89 13.84 13.71 13.60 12.80
14.12 13.69 12.75 14.80 14.15 13.59 13.24 14.10 12.50
14.41 13.88 12.35 14.40 14.04 13.43 13.39 13.50 12.85
14.15 13.78 12.94 14.93 13.95 13.52 13.38 13.67 12.73
14.15 13.76 12.88 14.80 13.91 13.47 13.33 13.55 12.78
0.276 0.085 0.441 0.413 0.121 0.178 0.168 0.273 0.309
1.95% 0.61% 3.41% 2.77% 0.87% 1.32% 1.25% 2.00% 2.43%
5.42% 2.64% -3.58% 11.26% 3.95% 0.73% -0.29% 1.82% -5.14%
0.87 0.29 1.01 2.09 0.56 0.11 0.32 0.12 1.34

11 13 14 15 16 17 19 21 22
4A*OES 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*MS 4A*MS
< 50 23.2 22.3 31.0 23.0 < 50 21.7 20.9 22.2

< 50 22.9 22.8 31.2 23.3 < 50 21.5 21.3 21.6
< 50 23.4 22.5 31.8 23.5 < 50 21.7 20.8 22.0
< 50 23.0 22.0 32.5 23.7 < 50 22.8 20.2 22.0
< 50 23.4 23.2 31.8 22.7 < 50 21.6 19.2 21.6
< 50 23.4 22.6 32.0 23.2 < 50 22.6 19.6 22.2
23.2 22.6 31.7 23.2 22.0 20.3 21.9
23.3 22.6 31.8 23.3 21.7 20.5 22.0
0.217 0.413 0.554 0.356 0.564 0.814 0.273
0.94% 1.83% 1.75% 1.53% 2.56% 4.00% 1.25%
6.99% 4.14% 46.39% 7.22% 1.45% -6.17% 1.22%
NA 0.77 0.37 6.23 0.80 NA 0.00 1.06 0.03
Lab Lab Lab Lab Lab

16 19 20 21 22
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS
4.50 4.84 3.70 3.86 4.00

4.30 4.62 3.80 4.11 4.00
4.40 4.63 4.00 3.96 4.20
4.30 4.48 3.90 3.71 4.20
4.30 4.40 4.00 3.79 4.00
4.30 4.77 3.90 3.76 4.00
4.35 4.62 3.88 3.86 4.07
4.30 4.63 3.90 3.82 4.00
0.084 0.167 0.117 0.148 0.103
1.92% 3.61% 3.01% 3.83% 2.54%
9.43% 16.31% -2.31% -2.77% 2.31%
2.31 3.89 0.39 0.49 0.67
15 16 19 20 21 22
4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS
<5 1.84 2.02 1.96 2.02 2.00

<5 1.88 2.02 2.12 2.06 1.98
<5 1.90 2.14 2.50 2.05 2.04
<5 1.89 2.07 2.12 2.11 2.04
<5 1.90 2.04 2.17 2.09 2.04
<5 1.87 2.15 2.24 2.21 2.26
1.88 2.07 2.19 2.09 2.06
1.88 2.05 2.15 2.08 2.04
0.023 0.059 0.180 0.067 0.101
1.21% 2.82% 8.23% 3.19% 4.91%
-10.33% -1.11% 4.22% -0.31% -1.74%
NA 2.44 0.00 0.62 0.21 0.67

09 10 11 12 13 14 15 16 17
1.60 1.49 1.50 1.65 1.30 1.44 1.62 1.41 1.30

1.64 1.45 1.50 1.47 1.31 1.50 1.60 1.40 1.40
1.53 1.49 1.60 1.61 1.28 1.51 1.60 1.39 1.40
1.74 1.50 1.50 1.68 1.27 1.49 1.60 1.41 1.30
1.73 1.48 1.50 1.57 1.33 1.50 1.60 1.36 1.30
1.64 1.48 1.50 1.57 1.32 1.52 1.60 1.39 1.40
1.65 1.48 1.52 1.59 1.30 1.49 1.60 1.39 1.35
1.64 1.48 1.50 1.59 1.30 1.50 1.60 1.40 1.35
0.079 0.017 0.041 0.074 0.024 0.029 0.009 0.019 0.055
4.82% 1.15% 2.69% 4.64% 1.83% 1.91% 0.58% 1.34% 4.06%
13.43% 1.89% 4.47% 9.64% -10.35% 2.96% 10.39% -4.02% -7.01%
1.51 0.19 0.48 1.07 1.21 0.40 1.16 0.48 0.82

09 10 11 13 15 17 19 20 21
4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*MS
< 20 25.0 < 50 26.6 24.5 < 50 23.1 18.0 24.8

< 20 26.0 < 50 26.6 24.5 < 50 22.1 17.6 26.0
< 20 23.0 < 50 26.6 24.5 < 50 23.2 17.7 25.8
< 20 25.0 < 50 26.8 24.5 < 50 23.9 17.4 25.7
< 20 25.0 < 50 26.5 24.0 < 50 22.7 18.3 24.2
< 20 25.0 < 50 26.7 24.0 < 50 23.6 18.0 24.5
24.8 26.7 24.3 23.1 17.8 25.2
25.0 26.6 24.5 23.2 17.9 25.3
1.0 0.1 0.3 0.6 0.3 0.8
3.96% 0.46% 1.06% 2.78% 1.83% 3.02%
15.22% 23.67% 12.90% 7.18% -17.26% 16.76%
NA 0.81 NA 1.13 0.62 NA 0.35 0.80 0.80

14 15 16 19 20 21 22
4A*MS 4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*OES 4A*MS
15.2 17.0 15.1 16.0 17.5 18.0 16.0

15.5 17.0 15.4 17.0 15.8 18.0 15.5
16.0 16.0 15.2 17.0 17.0 18.0 15.5
15.5 19.0 15.6 16.0 18.0 18.0 16.0
16.1 17.0 15.0 16.0 14.3 17.0 15.5
15.6 17.0 15.3 18.0 16.6 17.0 15.5
15.7 17.2 15.3 16.7 16.5 17.7 15.7
15.6 17.0 15.3 16.5 16.8 18.0 15.5
0.339 0.983 0.216 0.816 1.329 0.516 0.258
2.17% 5.73% 1.42% 4.90% 8.04% 2.92% 1.65%
-0.47% 9.17% -2.91% 5.99% 5.15% 12.35% -0.37%
0.01 0.76 0.27 0.67 0.58 1.35 0.00
Lab Lab
21 22
4A*MS 4A*MS
0.27 0.28
0.27 0.28
0.25 0.30
0.24 0.28
0.25 0.28
0.29 0.28
0.26 0.28
0.26 0.28
0.018 0.008
7.01% 2.88%
7.48% 16.38%
1.21 2.10

09 10 11 12 13 14 15 16 17
1.18 1.20 1.32 1.41 1.28 1.14 1.31 1.27 1.07

1.20 1.18 1.33 1.35 1.27 1.20 1.29 1.26 1.11
1.12 1.17 1.38 1.39 1.27 1.19 1.30 1.28 1.16
1.15 1.21 1.31 1.46 1.29 1.21 1.30 1.27 1.11
1.19 1.18 1.26 1.39 1.29 1.20 1.28 1.24 1.09
1.20 1.18 1.16 1.38 1.27 1.22 1.29 1.26 1.12
1.17 1.19 1.29 1.40 1.28 1.19 1.29 1.26 1.11
1.19 1.18 1.32 1.39 1.28 1.20 1.29 1.27 1.11
0.032 0.015 0.076 0.037 0.008 0.027 0.010 0.014 0.030
2.73% 1.30% 5.86% 2.63% 0.61% 2.29% 0.79% 1.08% 2.73%
-2.31% -1.20% 7.68% 16.28% 6.50% -0.63% 7.75% 5.18% -7.58%
0.25 0.10 1.40 2.12 0.94 0.10 1.11 0.77 0.96

09 10 11 12 13 14 15 16 17
0.050 0.059 0.062 0.068 0.056 0.059 0.075 0.059 0.058

0.060 0.059 0.063 0.066 0.056 0.062 0.091 0.059 0.059
0.050 0.059 0.064 0.068 0.057 0.061 0.077 0.060 0.060
0.050 0.059 0.062 0.070 0.056 0.064 0.076 0.059 0.058
0.060 0.059 0.061 0.069 0.056 0.062 0.076 0.059 0.057
0.050 0.060 0.060 0.067 0.056 0.063 0.075 0.059 0.060
0.053 0.059 0.062 0.068 0.056 0.062 0.078 0.059 0.059
0.050 0.059 0.062 0.068 0.056 0.062 0.076 0.059 0.059
0.005 0.000 0.001 0.002 0.000 0.002 0.006 0.000 0.001
9.68% 0.53% 2.28% 2.36% 0.69% 2.57% 8.02% 0.65% 2.06%
-11.04% -1.31% 3.41% 13.20% -6.10% 2.94% 30.63% -1.37% -2.15%
2.03 0.28 0.56 2.32 1.15 0.48 4.69 0.29 0.43

09 10 11 12 13 14 15 16 17
15.00 10.00 10.00 10.00 8.96 9.80 6.50 9.30 10.00

17.00 11.00 10.00 15.00 9.07 9.20 6.50 9.10 10.00
17.00 10.00 10.00 10.00 8.87 9.30 6.75 9.70 10.00
15.00 10.00 10.00 15.00 8.98 9.90 6.75 9.40 10.00
16.00 10.00 10.00 10.00 9.11 9.80 6.50 9.60 10.00
17.00 10.00 10.00 15.00 8.79 9.50 6.00 9.40 10.00
16.17 10.17 10.00 12.50 8.96 9.58 6.50 9.42 10.00
16.50 10.00 10.00 12.50 8.97 9.65 6.50 9.40 10.00
0.983 0.408 0.000 2.739 0.118 0.293 0.274 0.214 0.000
6.08% 4.02% 0.00% 21.91% 1.32% 3.05% 4.21% 2.27% 0.00%
69.30% 6.46% 4.72% 30.90% -6.14% 0.36% -31.93% -1.39% 4.72%
10.45 0.56 0.29 4.40 1.42 0.40 5.48 0.67 0.29
09 10 11 12 13 14 15 16 17
1.21 1.12 1.03 1.25 1.01 1.09 1.19 1.19 1.03

1.24 1.19 1.02 1.15 1.03 1.14 1.17 1.20 1.06
1.17 1.15 1.03 1.25 1.01 1.13 1.17 1.19 1.11
1.21 1.16 1.02 1.29 0.99 1.15 1.18 1.20 1.05
1.22 1.11 1.02 1.22 1.02 1.14 1.15 1.15 1.04
1.22 1.11 0.98 1.20 1.03 1.16 1.17 1.18 1.07
1.21 1.14 1.02 1.23 1.01 1.14 1.17 1.18 1.06
1.21 1.14 1.02 1.23 1.02 1.14 1.17 1.19 1.06
0.023 0.032 0.019 0.048 0.014 0.024 0.015 0.019 0.028
1.91% 2.78% 1.83% 3.95% 1.42% 2.11% 1.28% 1.58% 2.67%
7.85% 1.38% -9.50% 9.19% -9.68% 1.12% 4.22% 5.48% -5.65%
1.09 0.10 1.47 1.29 1.60 0.18 0.53 0.82 0.98

15 16 19 20 21 22 24
4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*OES
7.50 8.10 9.50 8.40 9.70 8.50 7.00

7.75 8.10 9.60 8.00 9.60 8.50 6.00
7.50 8.00 9.40 8.70 9.60 8.50 8.00
7.50 8.10 10.10 8.10 9.70 8.50 7.00
7.25 8.10 9.60 8.90 9.50 9.00 7.00
7.50 7.90 9.90 8.30 9.60 8.50 8.00
7.50 8.05 9.68 8.40 9.62 8.58 7.17
7.50 8.10 9.60 8.35 9.60 8.50 7.00
0.158 0.084 0.264 0.346 0.075 0.204 0.753
2.11% 1.04% 2.73% 4.12% 0.78% 2.38% 10.50%
-12.59% -6.18% 12.86% -2.10% 12.08% 0.04% -16.47%
1.37 0.67 1.39 0.23 1.31 0.00 1.50
09 10 11 12 13 14 15 16 17
11.0 14.0 30.0 20.0 17.4 14.0 15.0 21.0 10.0

13.0 15.0 30.0 20.0 16.9 14.0 14.8 21.0 20.0
10.0 15.0 20.0 20.0 17.1 14.0 15.3 21.0 20.0
11.0 14.0 20.0 20.0 17.2 14.0 15.0 20.0 20.0
12.0 14.0 20.0 20.0 17.1 13.0 14.0 20.0 20.0
11.0 15.0 20.0 20.0 17.3 15.0 14.0 21.0 30.0
11.3 14.5 23.3 20.0 17.2 14.0 14.7 20.7 20.0
11.0 14.5 20.0 20.0 17.1 14.0 14.9 21.0 20.0
1.0 0.5 5.2 0.0 0.2 0.6 0.5 0.5 6.3
9.11% 3.78% 22.13% 0.00% 1.02% 4.52% 3.68% 2.50% 31.62%
-32.62% -13.79% 38.73% 18.91% 2.05% -16.76% -12.80% 22.87% 18.91%
1.77 0.82 0.82 0.82 0.03 0.97 0.77 1.02 0.23

09 10 11 12 13 14 15 16 17
0.040 0.045 0.042 0.050 0.032 0.048 0.061 0.057 0.041

0.040 0.046 0.045 0.055 0.031 0.047 0.061 0.058 0.042
0.040 0.049 0.050 0.050 0.033 0.049 0.062 0.060 0.044
0.030 0.046 0.044 0.050 0.032 0.048 0.061 0.059 0.042
0.050 0.046 0.044 0.050 0.033 0.048 0.059 0.060 0.042
0.040 0.048 0.043 0.050 0.033 0.047 0.059 0.059 0.042
0.040 0.047 0.045 0.051 0.032 0.048 0.061 0.059 0.042
0.040 0.046 0.044 0.050 0.032 0.048 0.061 0.059 0.042
0.006 0.002 0.003 0.002 0.001 0.001 0.001 0.001 0.001
15.81% 3.56% 6.28% 4.02% 1.71% 1.59% 1.82% 1.99% 2.33%
-7.38% 8.21% 3.42% 17.70% -25.56% 10.41% 40.35% 36.23% -2.37%
0.81 0.62 0.04 1.32 2.47 0.82 3.57 3.19 0.35

09 10 11 12 13 14 15 16 17
0.223 0.253 0.254 0.262 0.244 0.281 0.268 0.254 0.234

0.220 0.252 0.252 0.245 0.244 0.272 0.260 0.254 0.242
0.208 0.258 0.255 0.255 0.245 0.259 0.266 0.255 0.252
0.211 0.259 0.250 0.245 0.248 0.258 0.268 0.258 0.239
0.223 0.253 0.249 0.255 0.246 0.265 0.263 0.250 0.236
0.218 0.249 0.239 0.251 0.246 0.267 0.264 0.254 0.246
0.217 0.254 0.250 0.252 0.246 0.267 0.265 0.254 0.242
0.219 0.253 0.251 0.253 0.246 0.266 0.265 0.254 0.241
0.006 0.004 0.006 0.007 0.002 0.008 0.003 0.003 0.007
2.90% 1.52% 2.31% 2.61% 0.64% 3.16% 1.24% 1.01% 2.77%
-13.07% 1.63% 0.03% 0.96% -1.66% 6.94% 6.04% 1.76% -3.31%
6.58 0.50 0.14 0.18 1.09 3.05 2.62 0.56 1.88
Lab Lab Lab Lab Lab

16 19 20 21 22
4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS
61 63 55 57 68
61 62 58 58 69
60 62 61 57 68
62 66 57 55 67
59 62 59 54 63
61 65 60 54 65
61 64 58 56 67
61 63 59 56 67
1.1 1.7 2.1 1.8 2.3
1.80% 2.62% 3.62% 3.19% 3.39%
-2.89% 1.93% -6.34% -10.43% 6.93%
0.16 0.56 0.67 1.29 1.31
11 12 13 14 15 16 17 19 20
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*MS
9.25 9.47 8.66 9.07 9.40 9.06 8.37 >5 7.80

9.39 9.49 8.67 9.12 9.47 9.18 8.67 >5 7.70
9.83 9.29 8.44 9.18 9.46 9.14 9.01 >5 8.20
9.11 9.64 8.78 9.43 9.42 9.17 8.75 >5 7.60
9.24 9.02 8.58 9.23 9.45 9.13 8.54 >5 8.10
8.93 9.19 8.54 9.13 9.59 9.06 8.73 >5 8.00
9.29 9.35 8.61 9.20 9.46 9.12 8.68 7.90
9.25 9.38 8.62 9.16 9.46 9.14 8.70 7.90
0.306 0.226 0.115 0.128 0.067 0.052 0.215 0.237
3.29% 2.42% 1.34% 1.39% 0.70% 0.57% 2.48% 3.00%
2.57% 3.22% -4.92% 1.52% 4.48% 0.72% -4.20% -12.79%
0.66 0.88 1.94 0.29 1.31 0.01 1.69 NA 4.66

09 10 11 13 14 15 16 17 19
22.0 21.0 < 50 25.7 29.3 11.8 27.3 < 50 28.8

22.0 21.0 < 50 25.5 28.6 12.3 27.4 < 50 28.4
18.0 21.0 < 50 25.4 28.6 13.0 27.5 < 50 29.0
15.0 21.0 < 50 25.7 29.1 12.8 27.6 < 50 31.0
23.0 21.0 < 50 25.8 29.3 11.3 26.5 < 50 28.6
17.0 20.0 < 50 25.8 29.7 8.0 26.9 < 50 30.2
19.5 20.8 25.6 29.1 11.5 27.2 29.3
20.0 21.0 25.7 29.2 12.0 27.4 28.9
3.271 0.408 0.145 0.434 1.830 0.420 1.033
16.77% 1.96% 0.56% 1.49% 15.92% 1.54% 3.52%
-29.39% -24.57% -7.13% 5.37% -58.36% -1.51% 6.21%
2.73 2.26 NA 0.55 0.67 5.32 0.00 NA 0.76

09 10 11 12 13 14 15 16 17
<5 7.00 10.00 8.00 7.97 7.00 <5 7.00 10.00

<5 7.00 10.00 7.00 7.66 8.00 <5 7.00 10.00
<5 7.00 10.00 7.00 7.93 7.00 <5 7.00 10.00
<5 7.00 10.00 8.00 7.81 8.00 <5 7.00 10.00
<5 7.00 10.00 8.00 7.94 8.00 <5 7.00 10.00
<5 7.00 10.00 7.00 7.89 8.00 <5 7.00 10.00
7.00 10.00 7.50 7.87 7.67 7.00 10.00
7.00 10.00 7.50 7.91 8.00 7.00 10.00
0.000 0.000 0.548 0.118 0.516 0.000 0.000
0.00% 0.00% 7.30% 1.50% 6.74% 0.00% 0.00%
-15.86% 20.21% -9.85% -5.44% -7.84% -15.86% 20.21%
NA 0.67 1.45 0.32 0.03 0.20 NA 0.67 1.45

14 15 16 19 20 21 22
4A*MS 4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS
22.0 15.5 17.0 19.0 20.0 17.0 20.0

20.0 15.0 17.0 18.0 21.0 18.0 15.0
22.0 15.8 18.0 19.0 22.0 18.0 15.0
21.0 15.5 17.0 20.0 20.0 19.0 20.0
23.0 15.5 19.0 18.0 22.0 17.0 20.0
19.0 16.0 18.0 20.0 21.0 17.0 20.0
21.2 15.5 17.7 19.0 21.0 17.7 18.3
21.5 15.5 17.5 19.0 21.0 17.5 20.0
1.472 0.332 0.816 0.894 0.894 0.816 2.582
6.95% 2.14% 4.62% 4.71% 4.26% 4.62% 14.08%
13.42% -16.72% -5.33% 1.81% 12.53% -5.33% -1.76%
1.41 1.94 0.67 0.12 1.31 0.67 0.28
13 14 15 16 19 20 21 22 24
4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*OES
5.60 6.10 <5 6.20 6.00 5.50 5.70 6.00 5.00

5.73 6.10 <5 6.80 6.10 5.60 6.00 7.00 5.00
5.88 6.10 <5 6.30 6.00 6.10 5.90 6.00 3.00
5.80 6.20 <5 6.50 6.50 5.70 6.20 6.00 5.00
5.72 6.20 <5 6.20 5.90 6.20 5.60 9.00 7.00
5.87 5.90 <5 6.10 6.20 6.20 5.70 6.00 5.00
5.77 6.10 6.35 6.12 5.88 5.85 6.67 5.00
5.76 6.10 6.25 6.05 5.90 5.80 6.00 5.00
0.107 0.110 0.259 0.214 0.319 0.226 1.211 1.265
1.85% 1.80% 4.08% 3.49% 5.42% 3.86% 18.17% 25.30%
-2.87% 2.75% 6.97% 3.04% -0.90% -1.46% 12.30% -15.78%
0.67 1.25 NA 2.69 1.35 0.00 0.19 0.67 5.09

09 10 11 13 14 15 16 17 19
83 85 70 85 81 116 84 80 87
84 85 70 85 84 115 85 80 87
77 85 70 86 86 117 83 80 86
77 83 70 86 85 117 85 80 84
83 84 70 87 87 116 81 80 89
85 85 70 87 85 120 84 80 88
82 85 70 86 85 117 84 80 87
83 85 70 86 85 117 84 80 87
3.6 0.8 0.0 0.9 2.0 1.8 1.5 0.0 1.5
4.37% 0.99% 0.00% 1.04% 2.38% 1.57% 1.81% 0.00% 1.72%
2.11% 5.87% -12.30% 7.81% 6.28% 46.27% 4.74% 0.23% 8.73%
0.00 0.38 1.47 0.58 0.43 4.50 0.27 0.19 0.67
Lab Lab Lab Lab
16 20 21 22
4A*MS 4A*MS 4A*MS 4A*MS
0.99 0.60 1.01 0.70

0.97 0.60 1.06 0.60
0.97 0.60 1.02 0.60
0.97 0.50 0.96 0.70
0.97 0.60 0.94 0.60
0.94 0.60 0.94 0.60
0.97 0.58 0.99 0.63
0.97 0.60 0.99 0.60
0.016 0.041 0.049 0.052
1.65% 7.00% 4.97% 8.15%
0.78 0.70 0.86 0.51
Lab Lab
21 22
4A*MS 4A*MS
0.62 0.54
0.65 0.54
0.62 0.54
0.64 0.56
0.60 0.58
0.61 0.58
0.62 0.56
0.62 0.55
0.019 0.020
2.99% 3.53%
17.95% 5.34%
1.88 0.73

14 16 19 20 21 22
4A*MS 4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS
0.60 0.50 0.56 0.80 0.50 0.60

0.60 0.40 0.58 0.60 0.50 0.60
0.60 0.50 0.57 0.60 0.60 0.60
0.70 0.50 0.63 0.50 0.70 0.60
0.70 0.50 0.54 0.70 0.60 0.60
0.60 0.50 0.63 0.80 0.70 0.60
0.63 0.48 0.59 0.67 0.60 0.60
0.60 0.50 0.58 0.65 0.60 0.60
0.052 0.041 0.037 0.121 0.089 0.000
8.15% 8.45% 6.37% 18.17% 14.91% 0.00%
8.82% -16.95% 0.52% 14.55% 3.09% 3.09%
0.67 2.36 0.30 1.35 0.00 0.00

09 11 13 14 16 17 19 20 21
4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*MS 4A*MS
< 20 < 50 6.54 6.82 7.03 < 50 7.20 6.10 7.35

< 20 < 50 6.57 7.29 6.89 < 50 7.00 5.60 7.37
< 20 < 50 6.58 6.99 6.86 < 50 7.30 6.00 7.34
< 20 < 50 6.65 6.83 6.77 < 50 7.50 5.60 7.86
< 20 < 50 6.55 7.20 6.90 < 50 7.10 6.00 7.69
< 20 < 50 6.63 7.07 6.81 < 50 7.40 6.00 7.64
6.59 7.03 6.88 7.25 5.88 7.54
6.57 7.03 6.88 7.25 6.00 7.51
0.046 0.192 0.090 0.187 0.223 0.219
0.70% 2.73% 1.31% 2.58% 3.79% 2.90%
2.87% 9.86% 7.41% 13.24% -8.10% 17.80%
NA NA 0.15 0.31 0.15 NA 0.53 0.86 0.82

09 10 11 12 13 14 15 16 17
0.140 0.142 0.120 0.160 0.145 0.127 0.120 0.140 0.130

0.150 0.140 0.120 0.150 0.145 0.136 0.120 0.139 0.130
0.130 0.138 0.120 0.160 0.155 0.137 0.125 0.144 0.130
0.140 0.144 0.120 0.165 0.156 0.147 0.125 0.142 0.130
0.140 0.139 0.120 0.160 0.157 0.147 0.125 0.137 0.130
0.140 0.141 0.120 0.155 0.157 0.145 0.120 0.135 0.130
0.140 0.140 0.120 0.158 0.152 0.140 0.123 0.139 0.130
0.140 0.140 0.120 0.160 0.155 0.141 0.123 0.139 0.130
0.006 0.002 0.000 0.005 0.006 0.008 0.003 0.003 0.000
4.52% 1.44% 0.00% 3.26% 3.66% 5.73% 2.24% 2.34% 0.00%
0.44% 0.77% -13.91% 13.59% 9.33% 0.36% -12.12% 0.08% -6.73%
0.03 0.06 1.50 1.42 0.97 0.02 1.31 0.01 0.74

10 11 13 14 15 16 17 19 20
<5 < 50 0.68 0.93 < 10 0.63 < 50 0.73 0.70

<5 < 50 0.68 0.89 < 10 0.63 < 50 0.73 0.70
<5 < 50 0.67 0.86 < 10 0.62 < 50 0.73 0.80
<5 < 50 0.69 0.85 < 10 0.64 < 50 0.76 0.70
<5 < 50 0.67 0.86 < 10 0.65 < 50 0.75 0.80
<5 < 50 0.68 0.88 < 10 0.63 < 50 0.75 0.80
0.68 0.88 0.63 0.74 0.75
0.68 0.87 0.63 0.74 0.75
0.008 0.029 0.010 0.013 0.055
1.24% 3.33% 1.63% 1.79% 7.30%
-8.14% 19.31% -13.97% 0.75% 1.88%
NA NA 0.99 1.73 NA 1.57 NA 0.11 0.00

09 11 13 14 16 17 19 20 21
4A*OES 4A*OES 4A*OES/MS 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*MS 4A*MS
< 20 < 50 2.46 2.54 2.55 < 50 2.70 2.50 2.85

< 20 < 50 2.49 2.65 2.58 < 50 2.70 2.40 2.85
< 20 < 50 2.44 2.60 2.58 < 50 2.70 2.60 2.83
< 20 < 50 2.48 2.54 2.54 < 50 2.80 2.50 2.81
< 20 < 50 2.46 2.57 2.52 < 50 2.60 2.60 2.84
< 20 < 50 2.46 2.50 2.55 < 50 2.80 2.60 2.81
2.47 2.57 2.55 2.72 2.53 2.83
2.46 2.55 2.55 2.70 2.55 2.84
0.019 0.053 0.023 0.075 0.082 0.018
0.79% 2.06% 0.92% 2.77% 3.22% 0.65%
-6.21% -2.37% -2.87% 3.34% -3.63% 7.71%
NA NA 0.70 0.10 0.18 NA 0.80 0.30 1.48
09 10 11 12 13 14 15 16 17
31.0 24.0 30.0 30.0 26.6 24.0 22.8 26.0 20.0

31.0 23.0 20.0 30.0 25.9 27.0 22.0 26.0 20.0
30.0 23.0 20.0 30.0 26.0 25.0 22.3 26.0 20.0
29.0 24.0 30.0 30.0 25.8 26.0 22.0 27.0 20.0
31.0 24.0 20.0 30.0 25.9 27.0 22.0 26.0 20.0
31.0 24.0 20.0 30.0 25.5 26.0 22.0 27.0 20.0
30.5 23.7 23.3 30.0 25.9 25.8 22.2 26.3 20.0
31.0 24.0 20.0 30.0 25.9 26.0 22.0 26.0 20.0
0.8 0.5 5.2 0.0 0.4 1.2 0.3 0.5 0.0
2.74% 2.18% 22.13% 0.00% 1.42% 4.53% 1.37% 1.96% 0.00%
17.35% -8.94% -10.22% 15.43% -0.16% -0.60% -14.71% 1.32% -23.05%
1.24 0.83 0.93 1.09 0.14 0.18 1.32 0.03 1.94

10 11 13 14 15 16 17 19 20
5.00 < 50 3.96 3.90 < 10 4.50 < 50 4.10 3.40

5.00 < 50 4.02 4.00 < 10 4.50 < 50 4.30 4.00
5.00 < 50 4.28 4.00 < 10 4.60 < 50 4.20 3.80
5.00 < 50 4.14 4.20 < 10 4.50 < 50 4.20 3.70
5.00 < 50 4.13 4.10 < 10 4.50 < 50 4.10 3.80
5.00 < 50 4.14 4.00 < 10 4.30 < 50 4.30 4.00
5.00 4.11 4.03 4.48 4.20 3.78
5.00 4.14 4.00 4.50 4.20 3.80
0.000 0.112 0.103 0.098 0.089 0.223
0.00% 2.72% 2.56% 2.19% 2.13% 5.89%
16.93% -3.84% -5.68% 4.84% -1.78% -11.53%
1.90 NA 0.21 0.40 NA 0.67 NA 0.00 0.99

13 14 15 16 19 20 21 22 24
4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*OES
14.3 13.9 9.3 13.2 14.1 12.4 12.5 17.1 11.0

14.1 14.7 9.3 13.2 13.2 13.8 13.0 16.7 11.0
14.2 13.7 8.7 13.4 13.7 14.9 12.9 17.0 11.0
14.2 14.3 9.0 13.5 14.2 13.2 12.6 16.5 11.0
14.4 14.2 9.2 13.3 13.4 15.1 12.4 16.8 11.0
14.2 13.9 9.3 13.8 14.0 14.3 12.3 16.7 11.0
14.2 14.1 9.1 13.4 13.8 13.9 12.6 16.8 11.0
14.2 14.1 9.3 13.4 13.9 14.1 12.6 16.8 11.0
0.083 0.360 0.267 0.228 0.403 1.033 0.279 0.219 0.000
0.58% 2.55% 2.92% 1.70% 2.93% 7.40% 2.21% 1.30% 0.00%
6.65% 5.79% -31.51% 0.42% 3.17% 4.54% -5.45% 25.90% -17.56%
0.72 0.62 3.67 0.00 0.32 0.47 0.67 2.93 2.07
Lab Lab
21 22
4A*MS 4A*MS
1.60 1.90
1.60 1.85
1.60 1.75
1.60 1.85
1.50 1.75
1.60 1.85
1.58 1.83
1.60 1.85
0.041 0.061
2.58% 3.36%
7.60% 24.02%
1.31 4.01

09 10 11 12 13 14 15 16 17
> 10000 1.04 1.06 1.07 1.02 1.05 1.08 1.08 0.98
> 10000 1.01 1.05 1.00 1.00 1.04 1.05 1.07 1.00
1.00 1.02 1.07 1.05 1.00 1.01 1.07 1.08 1.01
-- 1.03 1.04 1.08 1.02 1.02 1.08 1.08 0.97
> 10000 1.01 1.04 1.04 1.01 1.01 1.05 1.04 0.97
> 10000 1.00 1.01 1.03 1.01 1.04 1.06 1.06 1.00
1.00 1.02 1.04 1.05 1.01 1.03 1.06 1.07 0.99
1.00 1.02 1.05 1.05 1.01 1.03 1.06 1.08 0.99
0.015 0.020 0.029 0.009 0.017 0.012 0.016 0.018
1.51% 1.88% 2.76% 0.93% 1.61% 1.11% 1.50% 1.81%
-2.70% -0.71% 1.64% 1.72% -1.53% 0.24% 3.54% 3.99% -3.81%
0.89 0.17 0.69 0.72 0.46 0.18 1.39 1.55 1.30

14 15 16 19 20 21 22 24
4A*MS 4A*OES 4A*MS 4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES
148 142 161 178 150 145 144 117

155 142 160 175 147 147 142 119
153 144 159 182 151 145 147 119
153 142 161 177 150 142 145 119
157 140 154 175 155 142 143 117
154 139 157 183 154 143 144 124
153 141 159 178 151 144 144 119
153 142 160 178 150 144 144 119
3 2 3 3 3 2 2 3
2.16% 1.26% 1.72% 1.93% 1.78% 1.39% 1.19% 2.15%
2.35% -5.69% 6.00% 19.14% 0.94% -3.80% -3.69% -20.39%
0.30 1.09 0.93 3.21 0.06 0.76 0.74 3.74
19 20 21 22 23 24 25
4A*OES 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES
20.0 20.8 18.2 21.5 22.0 18.6 21.0

22.0 20.7 18.8 21.0 21.0 18.4 21.0
21.0 22.8 17.7 20.5 21.0 18.3 21.0
21.0 21.5 19.0 20.5 21.0 18.8 22.0
21.0 22.3 17.6 20.5 21.0 17.6 22.0
22.0 21.9 17.9 21.0 20.0 18.8 22.0
21.2 21.7 18.2 20.8 21.0 18.4 21.5
21.0 21.7 18.0 20.8 21.0 18.5 21.5
0.753 0.831 0.583 0.408 0.632 0.449 0.548
3.56% 3.84% 3.20% 1.96% 3.01% 2.44% 2.55%
3.76% 6.21% -10.78% 2.12% 2.94% -9.72% 5.39%
0.76 1.26 2.24 0.42 0.59 2.02 1.10

19 20 21 22 23 24 25
4A*OES/MS 4A*MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES
4.86 4.99 4.84 5.05 4.01 4.56 3.42

5.04 4.92 5.03 5.01 5.07 4.62 3.47
5.02 5.16 4.92 5.12 4.87 4.63 4.31
4.84 4.90 4.92 5.16 5.10 4.61 4.51
4.95 5.07 4.97 5.13 5.14 4.69 4.28
5.03 5.08 5.06 5.15 4.67 4.78 4.69
4.96 5.02 4.96 5.10 4.81 4.65 4.11
4.98 5.03 4.95 5.13 4.97 4.63 4.30
0.089 0.101 0.081 0.060 0.430 0.077 0.539
1.79% 2.01% 1.63% 1.17% 8.94% 1.65% 13.10%
-1.64% -0.38% -1.64% 1.27% -4.55% -7.76% -18.37%
0.22 0.04 0.22 0.20 0.18 1.11 2.66

19 20 21 22 23 24 25
4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES
76 71 76 80 70 58 90
76 70 74 78 80 56 80
77 78 76 79 80 56 80
80 71 76 79 80 51 80
77 78 75 79 80 55 80
79 75 74 81 80 60 80
78 74 75 79 78 56 82
77 73 76 79 80 56 80
1.6 3.7 1.0 1.0 4.1 3.0 4.1
2.12% 4.95% 1.31% 1.30% 5.21% 5.42% 5.00%
0.04% -4.69% -2.97% 2.41% 1.12% -27.71% 5.42%
0.07 0.73 0.49 0.25 0.07 3.94 0.67
Lab
25
4A*OES
570
570
590
590
550
590
577
580
16
2.83%
-51.87%
0.34
Lab Lab Lab Lab Lab

21 22 23 24 25
4A*MS 4A*MS 4A*OES 4A*OES 4A*OES
1.20 1.50 < 10 1.00 < 10

1.10 1.50 < 10 1.00 < 10
1.10 1.60 < 10 1.00 < 10
1.00 1.50 < 10 1.00 < 10
1.00 1.50 < 10 1.00 < 10
1.10 1.40 < 10 1.00 < 10
1.08 1.50 1.00
1.10 1.50 1.00
0.075 0.063 0.000
6.95% 4.22% 0.00%
-21.87% 8.18% -27.88%
2.08 0.73 NA 2.64 NA

20 21 22 23 24 25
4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES
18.7 16.4 17.4 20.0 9.0 < 20

18.4 16.9 17.1 20.0 10.0 20.0
20.4 16.1 17.3 30.0 11.0 20.0
19.7 17.1 17.5 30.0 9.0 30.0
20.3 15.9 17.1 < 20 10.0 < 20
20.2 16.3 17.5 20.0 10.0 30.0
19.6 16.5 17.3 24.0 9.8 25.0
20.0 16.4 17.4 20.0 10.0 25.0
0.866 0.464 0.183 5.477 0.753 5.774
4.41% 2.82% 1.06% 22.82% 7.66% 23.09%
10.69% -7.18% -2.29% 35.43% -44.51% 41.07%
0.63 0.65 0.30 0.79 3.33 2.81

20 21 22 23 24 25
4A*MS 4A*OES 4A*OES 4A*OES 4A*OES 4A*OES
1.32 1.39 1.38 1.41 1.22 1.33

1.32 1.43 1.37 1.48 1.23 1.34
1.35 1.39 1.38 1.43 1.24 1.39
1.31 1.41 1.41 1.47 1.24 1.40
1.34 1.45 1.43 1.46 1.23 1.39
1.37 1.43 1.40 1.38 1.25 1.38
1.34 1.42 1.39 1.44 1.24 1.37
1.33 1.42 1.39 1.44 1.23 1.38
0.023 0.024 0.023 0.039 0.010 0.029
1.69% 1.71% 1.62% 2.69% 0.85% 2.13%
-2.95% 2.99% 1.42% 4.57% -10.22% -0.28%
0.57 0.60 0.29 0.91 2.01 0.05
20 21 22 23 24 25
4A*MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES
58 54 57 60 52 60
58 53 55 60 52 60
58 54 55 60 52 60
60 51 55 60 53 60
59 51 55 60 51 60
59 51 54 50 54 60
59 52 55 58 52 60
59 52 55 60 52 60
0.8 1.5 0.8 4.1 1.0 0.0
1.37% 2.88% 1.45% 7.00% 1.87% 0.00%
9.01% -2.81% 2.30% 8.33% -2.99% 11.43%
1.12 0.22 0.36 1.39 0.24 1.39

19 20 21 22 23 24 25
225 214 233 225 220 212 230

230 217 241 225 230 212 230
225 227 228 225 230 213 230
226 209 241 230 230 215 230
231 235 239 220 230 206 230
221 221 239 225 220 219 230
227 221 237 225 227 213 230
226 219 239 225 230 213 230
4 9 5 3 5 4 0
1.64% 4.24% 2.21% 1.41% 2.28% 2.00% 0.00%
2.26% -0.44% 6.89% 1.55% 2.30% -3.94% 3.81%
0.51 0.13 1.79 0.34 0.52 0.96 0.87

19 20 21 22 23 24 25
27.0 20.0 20.0 20.0 30.0 14.0 30.0

28.0 20.0 25.0 20.0 30.0 19.0 30.0
28.0 21.0 20.0 20.0 30.0 21.0 30.0
30.0 22.0 20.0 20.0 30.0 18.0 30.0
27.0 21.0 25.0 20.0 30.0 23.0 30.0
30.0 21.0 25.0 20.0 30.0 23.0 30.0
28.3 20.8 22.5 20.0 30.0 19.7 30.0
28.0 21.0 22.5 20.0 30.0 20.0 30.0
1.4 0.8 2.7 0.0 0.0 3.4 0.0
4.82% 3.61% 12.17% 0.00% 0.00% 17.52% 0.00%
14.11% -16.10% -9.38% -19.45% 20.82% -20.80% 20.82%
0.57 0.65 0.38 0.78 0.84 0.84 0.84

19 20 21 22 23 24 25
4A*OES 4A*OES 4A*AAS 4A*OES 4A*OES 4A*OES 4A*OES
1.79 1.67 1.69 1.72 1.86 1.70 1.64

1.80 1.67 1.70 1.67 1.75 1.76 1.78
1.77 1.59 1.69 1.71 1.69 1.78 1.70
1.79 1.77 1.84 1.69 1.71 1.78 1.71
1.76 1.67 1.64 1.71 1.66 1.75 1.91
1.81 1.72 1.63 1.77 1.65 1.77 1.79
1.79 1.68 1.70 1.71 1.72 1.76 1.75
1.79 1.67 1.69 1.71 1.70 1.76 1.74
0.020 0.059 0.075 0.034 0.077 0.028 0.095
1.15% 3.53% 4.43% 1.97% 4.48% 1.59% 5.40%
2.96% -3.00% -2.06% -1.29% -0.81% 1.27% 1.06%
1.38 0.85 1.11 0.21 0.03 0.75 0.67
19 20 21 22 23 24 25
12.23 13.69 13.30 13.70 13.05 12.04 12.95

12.25 13.48 13.80 13.30 13.35 12.12 13.55
12.24 14.55 13.10 13.50 13.05 12.24 13.60
12.22 13.55 13.60 13.70 13.25 12.36 13.60
12.27 14.33 13.80 13.80 13.15 11.81 13.90
12.26 14.14 13.70 13.90 12.70 12.29 13.65
12.25 13.96 13.55 13.65 13.09 12.14 13.54
12.25 13.92 13.65 13.70 13.10 12.18 13.60
0.019 0.445 0.288 0.217 0.225 0.200 0.315
0.15% 3.19% 2.13% 1.59% 1.72% 1.65% 2.33%
-8.77% 3.98% 0.95% 1.69% -2.47% -9.53% 0.89%
2.10 0.57 0.06 0.09 0.78 2.26 0.11
Lab Lab
23 25
4A*OES 4A*OES
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
NA NA
19 20 21 22 23 24 25
1.62 1.44 1.38 1.47 1.40 1.22 1.30

1.64 1.45 1.42 1.45 1.40 1.24 1.30
1.60 1.39 1.43 1.46 1.40 1.24 1.40
1.62 1.44 1.38 1.47 1.40 1.24 1.40
1.58 1.43 1.38 1.49 1.40 1.24 1.30
1.61 1.50 1.39 1.47 1.30 1.31 1.40
1.61 1.44 1.40 1.47 1.38 1.25 1.35
1.62 1.44 1.38 1.47 1.40 1.24 1.35
0.020 0.035 0.023 0.013 0.041 0.031 0.055
1.27% 2.46% 1.61% 0.91% 2.95% 2.50% 4.06%
11.02% -0.69% -3.79% 1.14% -4.71% -14.01% -7.01%
1.23 0.10 0.46 0.10 0.56 1.72 0.82
Lab Lab Lab Lab

22 23 24 25
4A*MS 4A*OES 4A*OES 4A*OES
25.1 < 50 19.0 < 50

24.6 < 50 18.0 < 50
24.7 < 50 19.0 < 50
24.9 < 50 18.0 < 50
24.6 < 50 19.0 < 50
25.1 < 50 19.0 < 50
24.8 18.7
24.8 19.0
0.2 0.5
0.94% 2.77%
15.22% -13.39%
0.73 NA 0.62 NA

19 20 21 22 23 24 25
1.13 1.21 1.23 1.20 1.04 1.16 0.99

1.15 1.20 1.26 1.19 1.18 1.17 1.00
1.14 1.24 1.22 1.21 1.15 1.18 1.10
1.14 1.20 1.22 1.23 1.18 1.17 1.11
1.13 1.22 1.22 1.22 1.18 1.15 1.08
1.17 1.25 1.24 1.20 1.11 1.21 1.13
1.14 1.22 1.23 1.21 1.14 1.17 1.07
1.14 1.21 1.23 1.21 1.17 1.17 1.09
0.015 0.021 0.016 0.015 0.056 0.021 0.059
1.32% 1.72% 1.30% 1.22% 4.93% 1.76% 5.54%
-4.81% 1.57% 2.55% 0.60% -5.09% -2.31% -11.05%
0.58 0.28 0.41 0.15 0.40 0.25 1.43

19 20 21 22 23 24 25
0.064 0.062 0.065 0.060 0.062 0.055 0.061

0.064 0.059 0.066 0.059 0.063 0.056 0.062
0.064 0.060 0.064 0.059 0.061 0.056 0.064
0.066 0.062 0.064 0.060 0.062 0.056 0.063
0.064 0.060 0.066 0.059 0.062 0.056 0.063
0.066 0.063 0.065 0.059 0.059 0.058 0.062
0.065 0.061 0.065 0.059 0.062 0.056 0.063
0.064 0.061 0.065 0.059 0.062 0.056 0.063
0.001 0.001 0.001 0.001 0.001 0.001 0.001
1.72% 2.15% 1.55% 0.87% 2.24% 1.65% 1.68%
7.83% 1.86% 8.22% -1.31% 2.58% -6.23% 4.25%
1.36 0.28 1.43 0.28 0.56 1.28 0.71

19 20 21 22 23 24 25
4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES
9.90 9.30 9.50 9.00 10.00 8.00 10.00

9.80 9.10 9.70 8.50 10.00 8.00 10.00
10.30 10.40 9.60 9.00 10.00 8.00 10.00
10.60 9.00 9.70 9.00 10.00 9.00 10.00
9.70 10.60 9.10 8.50 10.00 8.00 10.00
10.30 9.70 8.90 9.00 10.00 8.00 10.00
10.10 9.68 9.42 8.83 10.00 8.17 10.00
10.10 9.50 9.55 9.00 10.00 8.00 10.00
0.352 0.679 0.337 0.258 0.000 0.408 0.000
3.49% 7.02% 3.58% 2.92% 0.00% 5.00% 0.00%
5.77% 1.40% -1.39% -7.50% 4.72% -14.48% 4.72%
0.45 0.24 0.67 1.64 0.29 2.73 0.29
19 20 21 22 23 24 25
1.42 1.11 1.20 1.14 1.08 1.00 1.11

1.46 1.09 1.24 1.13 1.12 1.00 1.12
1.42 1.16 1.20 1.17 1.09 1.01 1.13
1.41 1.08 1.22 1.18 1.11 1.01 1.14
1.39 1.18 1.25 1.13 1.11 1.02 1.12
1.43 1.22 1.25 1.14 1.07 1.04 1.13
1.42 1.14 1.23 1.15 1.10 1.01 1.13
1.42 1.14 1.23 1.14 1.10 1.01 1.13
0.023 0.054 0.023 0.021 0.020 0.015 0.010
1.63% 4.73% 1.91% 1.86% 1.79% 1.49% 0.93%
26.55% 1.49% 9.19% 2.22% -2.38% -9.80% 0.14%
3.95 0.11 1.29 0.22 0.48 1.62 0.10
19 20 21 22 23 24 25
17.0 17.5 14.0 20.0 10.0 16.0 10.0

16.3 16.7 13.0 20.0 20.0 16.0 20.0
16.7 17.3 15.0 25.0 20.0 17.0 20.0
17.9 17.0 15.0 20.0 20.0 17.0 20.0
16.4 18.1 14.0 20.0 20.0 19.0 20.0
17.2 18.0 14.0 15.0 20.0 19.0 20.0
16.9 17.4 14.2 20.0 18.3 17.3 18.3
16.9 17.4 14.0 20.0 20.0 17.0 20.0
0.6 0.6 0.8 3.2 4.1 1.4 4.1
3.50% 3.16% 5.31% 15.81% 22.27% 7.88% 22.27%
0.58% 3.65% -15.77% 18.91% 9.00% 3.05% 9.00%
0.10 0.06 0.92 0.82 0.32 0.03 0.32

19 20 21 22 23 24 25
0.041 0.043 0.050 0.050 0.044 0.038 0.042

0.041 0.045 0.048 0.045 0.044 0.037 0.042
0.042 0.048 0.049 0.045 0.043 0.038 0.044
0.042 0.042 0.051 0.050 0.044 0.039 0.044
0.042 0.045 0.048 0.045 0.042 0.035 0.051
0.044 0.047 0.048 0.045 0.041 0.037 0.043
0.042 0.045 0.049 0.047 0.043 0.037 0.044
0.042 0.045 0.049 0.045 0.044 0.038 0.044
0.001 0.002 0.001 0.003 0.001 0.001 0.003
2.12% 5.07% 2.49% 5.53% 2.94% 3.66% 7.64%
-2.87% 4.20% 12.69% 8.05% -0.44% -13.56% 2.65%
0.39 0.25 1.03 0.61 0.17 1.37 0.17

19 20 21 22 23 24 25
4A*OES/MS 4A*MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES
0.265 0.256 0.240 0.248 0.251 0.239 0.247

0.277 0.247 0.249 0.252 0.261 0.241 0.248
0.273 0.260 0.244 0.250 0.254 0.241 0.251
0.270 0.251 0.240 0.252 0.256 0.243 0.251
0.272 0.252 0.242 0.249 0.259 0.236 0.246
0.267 0.254 0.243 0.246 0.246 0.247 0.244
0.271 0.253 0.243 0.249 0.255 0.241 0.248
0.271 0.253 0.243 0.250 0.255 0.241 0.248
0.004 0.004 0.003 0.002 0.005 0.004 0.003
1.63% 1.76% 1.38% 0.94% 2.15% 1.54% 1.12%
8.40% 1.39% -2.71% -0.10% 1.90% -3.45% -0.77%
3.76 0.38 1.59 0.34 0.63 1.95 0.66
Lab Lab Lab Lab Lab
21 22 23 24 25
4A*OES 4A*OES 4A*OES 4A*OES 4A*OES
> 50000 9.03 9.41 8.50 8.77

> 50000 8.97 9.40 8.50 9.25
> 50000 8.98 9.24 8.60 9.07
> 50000 9.12 9.27 8.60 9.14
> 50000 9.10 9.20 8.20 9.50
> 50000 9.10 9.01 8.80 9.12
9.05 9.26 8.53 9.14
9.07 9.25 8.55 9.13
0.066 0.147 0.197 0.238
0.73% 1.59% 2.30% 2.61%
-0.09% 2.17% -5.80% 0.92%
NA 0.27 0.52 2.24 0.08

20 21 22 23 24 25
4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES
29.0 26.0 17.0 < 50 28.0 < 50

27.9 21.5 19.2 < 50 26.0 < 50
27.9 19.3 18.4 < 50 27.0 < 50
26.2 24.9 18.8 < 50 26.0 < 50
28.3 22.6 18.6 < 50 24.0 < 50
28.4 23.0 18.0 < 50 28.0 < 50
28.0 22.9 18.3 26.5
28.1 22.8 18.5 26.5
0.948 2.393 0.766 1.517
3.39% 10.46% 4.18% 5.72%
1.20% -17.14% -33.62% -4.05%
0.39 1.28 3.15 NA 0.25 NA

19 20 21 22 23 24 25
6.50 8.00 7.80 7.00 10.00 10.00 10.00

6.60 8.00 7.30 7.00 10.00 10.00 10.00
6.50 8.00 8.20 7.00 10.00 10.00 10.00
6.60 8.00 9.20 7.00 10.00 10.00 10.00
6.60 8.00 8.70 7.00 10.00 10.00 10.00
6.70 8.00 8.20 7.00 10.00 11.00 10.00
6.58 8.00 8.23 7.00 10.00 10.17 10.00
6.60 8.00 8.20 7.00 10.00 10.00 10.00
0.075 0.000 0.665 0.000 0.000 0.408 0.000
1.14% 0.00% 8.08% 0.00% 0.00% 4.02% 0.00%
-20.86% -3.84% -1.03% -15.86% 20.21% 22.21% 20.21%
0.97 0.03 0.20 0.67 1.45 1.56 1.45
20 21 22 23 24 25
4A*MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES
66 89 88 80 64 70
68 92 87 80 67 80
72 90 89 80 67 80
72 92 88 80 66 80
70 93 87 80 68 80
71 96 87 80 68 80
70 92 87 80 67 78
71 92 87 80 67 80
2.4 2.4 1.0 0.0 1.5 4.1
3.44% 2.66% 1.11% 0.00% 2.26% 5.21%
-12.51% 15.26% 9.52% 0.23% -16.48% -1.86%
1.49 1.34 0.76 0.19 1.89 0.19
Lab Lab Lab Lab
22 23 24 25
6.70 < 50 11.00 < 50

6.80 < 50 11.00 < 50
7.00 < 50 10.00 < 50
6.90 < 50 11.00 < 50
7.00 < 50 11.00 < 50
7.00 < 50 11.00 < 50
6.90 10.83
6.95 11.00
0.126 0.408
1.83% 3.77%
7.78% 69.21%
0.17 NA 4.16 NA

19 20 21 22 23 24 25
0.130 0.138 0.144 0.150 0.150 0.120 0.130

0.130 0.135 0.145 0.140 0.150 0.130 0.140
0.130 0.138 0.146 0.150 0.140 0.130 0.140
0.130 0.138 0.144 0.150 0.150 0.130 0.140
0.130 0.145 0.154 0.160 0.150 0.130 0.140
0.140 0.145 0.151 0.150 0.140 0.130 0.140
0.132 0.140 0.147 0.150 0.147 0.128 0.138
0.130 0.138 0.146 0.150 0.150 0.130 0.140
0.004 0.004 0.004 0.006 0.005 0.004 0.004
3.10% 2.98% 2.84% 4.22% 3.52% 3.18% 2.95%
-5.54% 0.32% 5.70% 7.61% 5.22% -7.93% -0.76%
0.61 0.01 0.59 0.79 0.53 0.87 0.10
Lab Lab Lab Lab

21 22 23 25
4A*MS 4A*MS 4A*OES 4A*OES
0.80 0.70 < 50 < 50

0.80 0.70 < 50 < 50
0.70 0.70 < 50 < 50
0.80 0.70 < 50 < 50
0.70 0.70 < 50 < 50
0.70 0.70 < 50 < 50
0.75 0.70
0.75 0.70
0.055 0.000
7.30% 0.00%
1.88% -4.91%
0.00 0.67 NA NA
Lab Lab Lab Lab

22 23 24 25
2.70 < 50 < 20 < 50

2.70 < 50 < 20 < 50
2.80 < 50 < 20 < 50
2.70 < 50 < 20 < 50
2.80 < 50 < 20 < 50
2.70 < 50 < 20 < 50
2.73
2.70
0.052
1.89%
3.97%
0.90 NA NA NA
19 20 21 22 23 24 25
24.0 26.0 21.0 25.0 30.0 22.0 30.0

24.0 27.0 23.0 25.0 30.0 23.0 30.0
25.0 27.0 22.0 25.0 30.0 23.0 30.0
25.0 26.0 20.0 25.0 30.0 23.0 30.0
25.0 27.0 20.0 25.0 30.0 22.0 30.0
26.0 27.0 20.0 25.0 30.0 24.0 30.0
24.8 26.7 21.0 25.0 30.0 22.8 30.0
25.0 27.0 20.5 25.0 30.0 23.0 30.0
0.8 0.5 1.3 0.0 0.0 0.8 0.0
3.03% 1.94% 6.02% 0.00% 0.00% 3.30% 0.00%
-4.45% 2.60% -19.20% -3.81% 15.43% -12.15% 15.43%
0.48 0.08 1.64 0.43 1.09 1.09 1.09
Lab Lab Lab Lab Lab

21 22 23 24 25
4A*MS 4A*MS 4A*OES 4A*OES 4A*OES
4.60 3.00 < 50 <4 < 50

4.70 3.00 < 50 <4 < 50
4.40 3.00 < 50 <4 < 50
4.50 3.00 < 50 <4 < 50
4.30 3.00 < 50 <4 < 50
4.40 3.00 < 50 <4 < 50
4.48 3.00
4.45 3.00
0.147 0.000
3.28% 0.00%
4.84% -29.84%
0.67 2.86 NA NA NA
19 20 21 22 23 24 25
4A*OES 4A*OES 4A*AAS 4A*OES 4A*OES 4A*OES 4A*OES
1.04 0.99 1.00 1.00 1.03 1.07 1.02

1.07 1.00 1.01 0.99 1.04 1.08 1.02
1.05 0.97 1.00 0.99 1.01 1.07 1.03
1.03 0.99 1.01 1.01 1.03 1.08 1.03
1.03 0.99 1.02 1.02 1.02 1.10 1.03
1.05 1.00 1.02 1.01 0.97 1.10 1.01
1.04 0.99 1.01 1.00 1.02 1.08 1.02
1.04 0.99 1.01 1.01 1.03 1.08 1.03
0.012 0.011 0.010 0.012 0.025 0.014 0.008
1.20% 1.11% 0.98% 1.21% 2.43% 1.26% 0.80%
1.54% -3.64% -1.75% -2.34% -1.02% 5.45% -0.39%
0.66 1.23 0.54 0.76 0.05 2.08 0.05
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
20.4
52.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
5.04
53.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
77
54
Indicative
1.00
ppm
2.00
2.00
1.00
5.00
16.00
0.75
19.00
Indicative
1.00
ppm
0.00
0.00
1
14
16
1198
20
Certified
1.00
ppm
2.00
2.00
1.00
6.00
16.00
1.39
55.00
Certified
1.00
ppm
1.00
2.00
1.0
19.0
16.0
17.7
56.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.38
57.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
54
58
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
45.6
59.0
Certified
1.00
ppm
0.00
0.00
1
19
16
222
60
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
24.8
61.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.85
62.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.73
63.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
3.09
21.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
1.63
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
1.36
23.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
13.42
64.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
21.7
65.0
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
4.00
19.00
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
0.66
20.00
Certified
1.00
ppm
2.00
3.00
1.00
5.00
16.00
3.97
66.00
Indicative
1.00
ppm
2.00
2.00
1.00
15.00
16.00
0.56
21.00
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
0.56
22.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.10
67.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.45
68.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
21.6
69.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
15.7
70.0
Certified
1.00
ppm
2.00
2.00
1.00
7.00
16.00
0.24
71.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.20
72.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.060
73.000
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
9.55
74.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.12
75.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
8.58
76.00
Indicative
1.00
ppm
1.00
1.00
1.0
17.0
16.0
22.3
23.0
Certified
1.00
ppm
1.00
1.00
1.0
19.0
16.0
16.8
77.0
Certified
1.00
wt.%
3.00
3.00
1.000
8.000
16.000
0.043
78.000
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.250
79.000
Indicative
1.00
ppm
2.00
2.00
1.00
25.00
16.00
5.79
19.00
Certified
1.00
ppm
0.00
1.00
1
22
16
62
80
Indicative
1.00
ppm
3.00
3.00
1.000
9.000
16.000
< 0.05
20.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
9.06
81.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
27.6
82.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
8.32
83.00
Certified
1.00
ppm
1.00
2.00
1.0
10.0
16.0
18.7
84.0
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
4.86
21.00
Certified
1.00
ppm
2.00
3.00
1.00
5.00
16.00
5.94
85.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
80
86
Certified
1.00
ppm
2.00
2.00
1.00
6.00
16.00
<1
87.00
Certified
1.00
ppm
2.00
2.00
1.00
7.00
16.00
0.53
88.00
Certified
1.00
ppm
2.00
2.00
1.00
8.00
16.00
0.58
89.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
6.40
90.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.139
91.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.74
92.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
0.24
22.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.63
93.00
Certified
1.00
ppm
1.00
1.00
1.0
10.0
16.0
26.0
94.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
4.28
95.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
13.3
96.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.47
97.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.03
98.00
Certified
1.00
ppm
0.00
0.00
1
11
16
150
99
No No 06 08 10 13 14 15
1 1 16.9 21.0 21.0 20.4 19.5 20.9

1 2 19.3 21.0 20.0 20.8 19.3 20.8
1 3 16.7 21.0 21.0 20.1 18.9 19.4
1 4 18.2 21.0 23.0 20.4 20.9 20.2
1 5 17.5 21.0 20.0 20.6 20.8 20.8
1 6 17.8 21.0 21.0 20.7 21.9 19.9
Mean 17.7 21.0 21.0 20.5 20.2 20.3
Median 17.7 21.0 21.0 20.5 20.2 20.5
Std Dev. 0.948 0.000 1.095 0.263 1.160 0.623
Rel.Std.Dev. 5.35% 0.00% 5.22% 1.28% 5.74% 3.06%
PDM3 -14.00% 1.84% 1.84% -0.66% -1.96% -1.35%
Z-Score (Absolute) 3.55 0.78 0.25 0.09 0.26 0.09

No No 06 10 13 14 15 16
1 1 86 68 72 107 78 81
1 2 96 73 68 90 80 81
1 3 77 73 72 84 77 82
1 4 91 75 71 82 77 80
1 5 86 69 72 103 79 80
1 6 88 68 72 77 76 80
Mean 87 71 71 91 78 81
Median 87 71 72 87 78 81
Std Dev. 6 3 2 12 2 1
Rel.Std.Dev. 7.23% 4.27% 2.33% 13.31% 1.97% 1.01%
PDM3 11.02% -9.74% -9.34% 15.04% -1.06% 2.54%
Z-Score (Absolute) 0.71 0.72 0.64 0.99 0.12 0.12
Analytical results for Bi in OREAS 623 (Indicative Value 9.17 ppm)

Bi Round Replicate Lab
No No 08
3A*OES
1 1 10.00
1 2 10.00
1 3 < 10
1 4 10.00
1 5 10.00
1 6 10.00
Mean 10.00
Median 10.00
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 9.09%
Analytical results for Co in OREAS 623 (Indicative Value 218 ppm)

Co Round Replicate Lab
No No 08
3A*OES
1 1 220
1 2 220
1 3 220
1 4 220
1 5 220
1 6 210
Mean 218
Median 220
Std Dev. 4
Rel.Std.Dev. 1.87%
PDM3 0.00%

No No 06 08 10 13 14 15
1 1 1.58 1.71 1.76 1.65 1.69 1.77

1 2 1.84 1.72 1.73 1.66 1.71 1.76
1 3 1.53 1.81 1.72 1.68 1.70 1.74
1 4 1.72 1.72 1.79 1.67 1.79 1.74
1 5 1.57 1.74 1.74 1.65 1.75 1.76
1 6 1.73 1.65 1.86 1.66 1.71 1.73
Mean 1.66 1.72 1.77 1.66 1.72 1.75
Median 1.65 1.72 1.75 1.66 1.71 1.75
Std Dev. 0.120 0.051 0.052 0.011 0.038 0.015
Rel.Std.Dev. 7.24% 2.98% 2.93% 0.63% 2.18% 0.88%
PDM3 -4.50% -1.05% 1.71% -4.60% -0.92% 0.51%
Z-Score (Absolute) 2.90 0.47 0.71 2.97 0.38 0.64

No No 06 08 10 13 14 15
1 1 12.30 13.20 13.43 13.39 13.33 13.68

1 2 14.40 13.15 13.66 13.40 13.68 13.76
1 3 11.90 13.35 13.33 13.19 13.58 13.70
1 4 13.60 13.20 13.63 13.14 13.70 13.57
1 5 12.30 13.35 13.50 13.57 13.71 13.55
1 6 13.30 13.00 13.41 13.38 13.83 13.65
Mean 12.97 13.21 13.49 13.35 13.64 13.65
Median 12.80 13.20 13.47 13.39 13.69 13.66
Std Dev. 0.958 0.132 0.130 0.158 0.171 0.081
Rel.Std.Dev. 7.39% 1.00% 0.96% 1.18% 1.25% 0.59%
PDM3 -3.29% -1.48% 0.64% -0.46% 1.72% 1.83%
Z-Score (Absolute) 0.72 0.63 0.22 0.22 0.65 0.69

No No 06 08 10 13 14 15
1 1 5.00 10.00 < 20 9.00 10.00 7.75

1 2 7.00 10.00 < 20 8.00 11.00 7.75
1 3 6.00 10.00 < 20 6.58 10.00 8.00
1 4 7.00 10.00 < 20 5.64 11.00 8.00
1 5 5.00 10.00 < 20 8.20 10.00 8.00
1 6 7.00 10.00 < 20 6.58 8.00 7.75
Mean 6.17 10.00 7.33 10.00 7.88
Median 6.50 10.00 7.29 10.00 7.88
Std Dev. 0.983 0.000 1.263 1.095 0.137
Rel.Std.Dev. 15.94% 0.00% 17.23% 10.95% 1.74%
PDM3 -26.79% 18.72% -12.95% 18.72% -6.51%
Analytical results for Ni in OREAS 623 (Indicative Value 15 ppm)

Ni Round Replicate Lab
No No 08
3A*OES
1 1 10.0
1 2 20.0
1 3 20.0
1 4 10.0
1 5 10.0
1 6 20.0
Mean 15.0
Median 15.0
Std Dev. 5.5
Rel.Std.Dev. 36.51%
PDM3 0.00%
No No 06 08 10 13 14 15
1 1 0.192 0.254 0.255 0.247 0.261 0.263

1 2 0.221 0.250 0.254 0.238 0.260 0.256
1 3 0.191 0.251 0.255 0.235 0.251 0.256
1 4 0.217 0.253 0.260 0.243 0.248 0.258
1 5 0.200 0.253 0.253 0.242 0.257 0.255
1 6 0.205 0.251 0.251 0.237 0.261 0.257
Mean 0.204 0.252 0.255 0.240 0.256 0.258
Median 0.203 0.252 0.254 0.240 0.258 0.257
Std Dev. 0.013 0.002 0.003 0.004 0.006 0.003
Rel.Std.Dev. 6.14% 0.61% 1.15% 1.82% 2.18% 1.19%
PDM3 -18.58% 0.41% 1.47% -4.34% 2.15% 2.65%
Z-Score (Absolute) 6.72 0.14 0.53 1.57 0.77 0.95

No No 06 08 10 13 14 15
1 1 0.90 1.05 1.05 0.98 1.02 1.03

1 2 1.05 1.04 1.08 0.99 1.04 1.03
1 3 0.90 1.04 1.08 0.96 1.02 1.02
1 4 1.03 1.05 1.07 0.99 1.00 1.01
1 5 0.92 1.03 1.03 0.97 1.02 1.02
1 6 0.98 1.03 1.02 0.97 1.04 1.02
Mean 0.96 1.04 1.06 0.98 1.03 1.02
Median 0.95 1.04 1.06 0.98 1.02 1.02
Std Dev. 0.069 0.008 0.026 0.009 0.016 0.009
Rel.Std.Dev. 7.12% 0.79% 2.49% 0.91% 1.54% 0.89%
PDM3 -5.58% 1.93% 3.63% -4.03% 0.63% 0.30%
Z-Score (Absolute) 1.28 0.31 0.67 0.96 0.04 0.04
Lab Lab Lab Lab
16 21 23 24
3A*OES 3A*OES 3A*OES 3A*AAS
20.1 19.0 22.0 21.0

19.9 17.0 21.0 21.0
19.6 16.0 22.0 21.0
19.9 20.0 21.0 21.0
20.2 16.0 21.0 21.0
20.2 13.0 21.0 21.0
20.0 16.8 21.3 21.0
20.0 16.5 21.0 21.0
0.232 2.483 0.516 0.000
1.16% 14.75% 2.42% 0.00%
-3.09% -18.36% 3.46% 1.84%
0.57 4.75 1.22 0.78
Lab Lab
21 23
3A*OES 3A*OES
67 87
64 92
66 89
71 81
64 76
55 88
65 86
65 88
5 6
8.25% 6.89%
-18.01% 8.69%
1.30 0.55
Lab Lab Lab Lab
16 21 23 24
1.75 1.80 1.97 1.76

1.75 1.64 1.73 1.73
1.76 1.71 1.77 1.74
1.78 1.93 1.89 1.77
1.73 1.70 1.69 1.71
1.78 1.74 1.70 1.75
1.76 1.75 1.79 1.74
1.76 1.72 1.75 1.74
0.019 0.101 0.114 0.021
1.10% 5.77% 6.34% 1.20%
1.05% 0.77% 2.97% 0.14%
1.02 0.62 0.92 0.38
Lab Lab Lab Lab

16 21 23 24
13.60 12.90 12.05 13.88

13.80 12.50 11.90 13.72
13.60 12.70 12.05 13.44
13.70 13.10 12.05 13.76
13.80 12.80 11.75 13.36
13.80 12.90 11.80 13.52
13.72 12.82 11.93 13.61
13.75 12.85 11.98 13.62
0.098 0.204 0.137 0.203
0.72% 1.59% 1.14% 1.49%
2.31% -4.40% -10.99% 1.54%
0.89 1.80 4.44 0.58
Lab Lab Lab

16 21 24
3A*OES 3A*OES 3A*AAS
9.00 < 10 < 10

8.00 < 10 < 10
9.00 < 10 < 10
10.00 < 10 20.00
9.00 < 10 < 10
10.00 < 10 < 10
9.17 20.00
9.00 20.00
0.753
8.21%
8.82% 137.43%
0.00 NA 5.66
Lab Lab Lab Lab
16 21 23 24
0.250 0.252 0.240 0.260

0.249 0.245 0.250 0.250
0.249 0.250 0.250 0.260
0.250 0.246 0.240 0.260
0.251 0.246 0.240 0.250
0.251 0.249 0.250 0.250
0.250 0.248 0.245 0.255
0.250 0.248 0.245 0.255
0.001 0.003 0.005 0.005
0.36% 1.11% 2.24% 2.15%
-0.39% -1.18% -2.38% 1.61%
0.14 0.43 0.86 0.58
Lab Lab Lab Lab

16 21 23 24
1.08 0.99 0.99 1.27

1.08 0.98 1.02 1.15
1.06 1.00 1.03 1.18
1.09 0.99 1.01 1.19
1.08 0.99 1.04 1.19
1.08 1.00 1.02 1.20
1.08 0.99 1.02 1.20
1.08 0.99 1.02 1.19
0.010 0.009 0.017 0.040
0.91% 0.87% 1.69% 3.33%
5.86% -2.71% -0.03% 17.48%
1.15 0.68 0.10 3.31
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
20.6
101.0
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
79
102
Indicative
1.00
ppm
2.00
2.00
1.00
19.00
16.00
9.17
25.00
Indicative
1.00
ppm
0.00
0.00
1
19
16
218
25
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.74
103.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
13.41
104.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
8.42
105.00
Indicative
1.00
ppm
1.00
1.00
1.0
19.0
16.0
15.0
25.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.251
106.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.02
107.00
No No 01 02 04 05 06 07
AR*OES AR*OES/MSAR*OES/MS AR*OES AR*MS AR*OES
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 21.0 20.8 21.8 19.0 18.7 21.0
1 2 21.0 21.2 21.6 20.0 19.3 21.0
1 3 21.0 19.9 21.7 21.0 18.9 22.0
1 4 21.0 21.3 21.7 20.0 18.9 20.0
1 5 21.0 20.2 21.1 20.0 19.0 21.0
1 6 21.0 20.4 21.4 20.0 19.0 22.0
Mean 21.0 20.7 21.6 20.0 19.0 21.2
Median 21.0 20.6 21.7 20.0 19.0 21.0
Std Dev. 0.000 0.577 0.259 0.632 0.197 0.753
Rel.Std.Dev. 0.00% 2.79% 1.20% 3.16% 1.04% 3.56%
PDM3 2.83% 1.13% 5.52% -2.07% -7.13% 3.64%
Z-Score (Absolute) 0.38 0.07 0.88 0.52 1.45 0.53

No No 01 02 04 05 06 08
AR*OES AR*OES/MSAR*OES/MS AR*OES AR*OES AR*OES
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 1.87 1.78 1.73 1.72 2.11 1.68
1 2 1.87 1.69 1.76 1.79 2.14 1.65
1 3 1.89 1.75 1.80 1.82 2.21 1.69
1 4 1.94 1.76 1.75 1.77 2.18 1.71
1 5 1.91 1.78 1.72 1.87 2.10 1.73
1 6 1.91 1.81 1.71 1.83 2.23 1.70
Mean 1.90 1.76 1.75 1.80 2.16 1.69
Median 1.90 1.77 1.74 1.81 2.16 1.70
Std Dev. 0.027 0.041 0.033 0.052 0.053 0.027
Rel.Std.Dev. 1.43% 2.31% 1.87% 2.90% 2.47% 1.61%
PDM3 5.33% -2.26% -3.18% -0.13% 19.94% -6.05%
Z-Score (Absolute) 1.37 0.53 0.77 0.00 5.05 1.49

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 80 74 71 70 71 60
1 2 60 76 73 71 73 90
1 3 90 70 70 73 72 70
1 4 90 73 69 73 73 90
1 5 80 72 68 75 73 80
1 6 90 70 70 70 72 90
Mean 82 73 70 72 72 80
Median 85 72 70 72 73 85
Std Dev. 11.7 2.3 1.7 2.0 0.8 12.6
Rel.Std.Dev. 14.31% 3.15% 2.45% 2.78% 1.13% 15.81%
PDM3 7.85% -4.25% -7.34% -4.92% -4.48% 5.65%
Z-Score (Absolute) 1.15 0.32 0.70 0.40 0.35 0.88
Analytical results for Au in OREAS 623 (Certified Value 0.797 ppm)

Au Round Replicate Lab Lab Lab Lab Lab Lab
No No 00 01 05 06 08 09
INAA AR*MS AR*GFAAS AR*AAS AR*MS AR*AAS
1.0g 25g 25g 25g 25g 50g
1 1 0.829 0.800 0.753 0.820 0.830 0.902
1 2 0.836 0.780 0.746 0.770 0.820 0.818
1 3 0.866 0.770 0.791 0.740 0.820 0.823
1 4 0.828 0.770 0.755 0.770 0.840 0.832
1 5 0.873 0.750 0.760 0.810 0.800 0.821
1 6 0.866 0.780 0.734 0.790 0.870 N.A.
7 0.853
8 0.846
9 0.796
10 0.822
11 0.813
12 0.838
13 0.802
14 0.846
15 0.838
16 0.852
17 0.874
18 0.857
19 0.842
20 0.840
Mean 0.841 0.775 0.757 0.783 0.830 0.839
Median 0.841 0.775 0.754 0.780 0.825 0.823
Std Dev. 0.022 0.016 0.019 0.029 0.024 0.035
Rel.Std.Dev. 2.59% 2.12% 2.53% 3.76% 2.85% 4.23%
PDM3 5.54% -2.72% -5.04% -1.68% 4.18% 5.34%
Analytical results for B in OREAS 623 (Certified Value < 10 ppm)

B Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 09 13 14
AR*OES/MSAR*OES/MS AR*OES AR*OES AR*OES/MS AR*MS
0.25g 0.25g 0.5g 10g 20g 0.5g
1 1 93.9 < 10 < 10 < 10 < 10 < 20
1 2 96.7 < 10 < 10 < 10 < 10 < 20
1 3 90.9 < 10 < 10 < 10 < 10 < 20
1 4 92.2 < 10 < 10 < 10 < 10 < 20
1 5 91.7 < 10 < 10 < 10 < 10 < 20
1 6 91.5 < 10 < 10 < 10 < 10 < 20
Mean 92.8
Median 92.0
Std Dev. 2.2
Rel.Std.Dev. 2.33%
PDM3
Z-Score (Absolute) NA NA NA NA NA NA
Analytical results for Ba in OREAS 623 (Indicative Value 241 ppm)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 240 33 46 12 29 240
1 2 240 29 59 12 30 230
1 3 240 31 47 11 29 240
1 4 250 25 51 11 29 240
1 5 240 37 44 < 10 29 240
1 6 250 38 57 < 10 31 240
Mean 243 32 51 12 30 238
Median 240 32 49 12 29 240
Std Dev. 5 5 6 1 1 4
Rel.Std.Dev. 2.12% 14.80% 12.15% 5.02% 2.84% 1.71%
PDM3 1.08% -86.62% -78.95% -95.22% -87.75% -1.00%
Z-Score (Absolute) 1.08 0.65 0.50 0.82 0.67 1.05
Analytical results for Be in OREAS 623 (Certified Value 0.37 ppm)

No No 01 02 04 05 06 08
AR*OES AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 <5 0.38 0.30 0.50 0.30 <5
1 2 <5 0.35 0.40 0.70 0.30 <5
1 3 <5 0.27 0.30 0.70 0.30 <5
1 4 <5 0.31 0.30 0.50 0.30 <5
1 5 <5 0.28 0.40 0.50 0.30 <5
1 6 <5 0.36 0.30 0.60 0.30 <5
Mean 0.32 0.33 0.58 0.30
Median 0.33 0.30 0.55 0.30
Std Dev. 0.046 0.052 0.098 0.000
Rel.Std.Dev. 14.03% 15.49% 16.85% 0.00%
PDM3 -12.11% -9.76% 57.92% -18.78%

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 20.0 17.5 17.0 18.6 14.4 20.0
1 2 10.0 18.2 17.1 18.1 14.6 20.0
1 3 10.0 17.3 16.7 19.5 14.3 < 10
1 4 10.0 17.5 16.6 18.6 14.5 < 10
1 5 10.0 17.5 16.4 19.4 14.6 10.0
1 6 10.0 17.4 16.7 18.4 14.7 10.0
Mean 11.7 17.5 16.8 18.8 14.5 15.0
Median 10.0 17.5 16.7 18.6 14.6 15.0
Std Dev. 4.1 0.3 0.3 0.6 0.1 5.8
Rel.Std.Dev. 34.99% 1.92% 1.55% 2.99% 1.01% 38.49%
PDM3 -30.82% 4.03% -0.67% 11.29% -13.92% -11.05%
Z-Score (Absolute) 3.24 0.00 0.44 0.67 1.67 1.40

No No 01 02 04 05 06 08
AR*OES AR*OES/MSAR*OES/MS AR*MS AR*OES AR*OES
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 1.13 1.05 0.96 1.12 1.06 1.13
1 2 1.15 0.99 0.99 1.09 1.11 1.13
1 3 1.14 1.03 0.99 1.16 1.15 1.14
1 4 1.14 1.04 0.99 1.14 1.12 1.14
1 5 1.13 1.05 0.98 1.03 1.08 1.14
1 6 1.13 1.06 0.96 1.14 1.15 1.13
Mean 1.14 1.04 0.98 1.11 1.11 1.13
Median 1.13 1.05 0.98 1.13 1.12 1.13
Std Dev. 0.008 0.024 0.015 0.047 0.037 0.005
Rel.Std.Dev. 0.72% 2.31% 1.50% 4.24% 3.29% 0.48%
PDM3 4.42% -4.72% -10.12% 2.28% 2.13% 4.27%
Z-Score (Absolute) 0.44 0.75 1.64 0.35 0.11 0.41

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 54 53 46 50 49 53
1 2 54 50 49 48 49 53
1 3 55 51 47 52 49 52
1 4 56 52 47 49 48 52
1 5 56 52 47 52 50 53
1 6 55 51 48 50 49 53
Mean 55 52 47 50 49 53
Median 55 52 47 50 49 53
Std Dev. 0.9 0.9 1.0 1.7 0.5 0.5
Rel.Std.Dev. 1.63% 1.77% 2.14% 3.36% 1.11% 0.98%
PDM3 4.82% -1.59% -10.08% -4.39% -6.71% 0.38%
Z-Score (Absolute) 0.68 0.13 1.20 0.48 0.77 0.12

Ce Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 10 13
AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES AR*OES/MS
0.25g 0.25g 0.5g 0.4g 40g 20g
1 1 35.1 32.6 40.7 27.3 41.0 42.3
1 2 33.9 35.0 39.0 26.2 40.0 42.6
1 3 34.7 33.1 42.3 27.3 40.0 41.8
1 4 34.9 33.7 39.6 26.5 40.0 41.7
1 5 35.5 32.1 41.2 27.9 41.0 42.4
1 6 36.1 32.8 40.8 27.4 41.0 42.3
Mean 35.0 33.2 40.6 27.1 40.5 42.2
Median 35.0 33.0 40.8 27.3 40.5 42.3
Std Dev. 0.7 1.0 1.2 0.6 0.5 0.4
Rel.Std.Dev. 2.11% 3.08% 2.89% 2.32% 1.35% 0.86%
PDM3 -3.72% -8.70% 11.59% -25.51% 11.32% 15.89%
Z-Score (Absolute) 0.18 0.46 0.69 1.42 0.67 0.93

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 217 205 200 216 212 228
1 2 224 203 206 219 217 226
1 3 225 194 201 229 211 229
1 4 227 194 200 221 218 228
1 5 223 197 195 226 218 225
1 6 222 194 203 215 216 221
Mean 223 198 201 221 215 226
Median 224 195 201 220 217 227
Std Dev. 3 5 4 6 3 3
Rel.Std.Dev. 1.53% 2.65% 1.82% 2.51% 1.43% 1.29%
PDM3 3.34% -8.32% -6.93% 2.41% -0.21% 4.81%
Z-Score (Absolute) 0.50 1.25 1.05 0.36 0.04 0.72
Analytical results for Cr in OREAS 623 (Certified Value 19.4 ppm)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 22.0 20.5 16.0 16.0 18.0 21.0
1 2 21.0 20.0 18.0 18.0 16.0 17.0
1 3 22.0 18.2 18.0 20.0 17.0 18.0
1 4 30.0 17.5 18.0 20.0 17.0 19.0
1 5 21.0 17.5 20.0 21.0 16.0 20.0
1 6 21.0 22.0 20.0 20.0 16.0 21.0
Mean 22.8 19.3 18.3 19.2 16.7 19.3
Median 21.5 19.1 18.0 20.0 16.5 19.5
Std Dev. 3.5 1.8 1.5 1.8 0.8 1.6
Rel.Std.Dev. 15.53% 9.54% 8.21% 9.57% 4.90% 8.45%
PDM3 17.64% -0.65% -5.55% -1.25% -14.13% -0.40%
Z-Score (Absolute) 1.39 0.03 0.67 0.31 1.80 0.00
Analytical results for Cs in OREAS 623 (Certified Value 0.75 ppm)

No No 02 04 05 06 13 16
AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES/MS AR*MS
0.25g 0.25g 0.5g 0.4g 20g 40g
1 1 0.73 0.60 0.88 0.60 0.81 0.91
1 2 0.69 0.66 0.82 0.59 0.83 0.90
1 3 0.70 0.63 0.91 0.62 0.81 0.90
1 4 0.71 0.63 0.86 0.59 0.80 0.93
1 5 0.71 0.60 0.96 0.61 0.82 0.93
1 6 0.71 0.62 0.88 0.60 0.82 0.93
Mean 0.71 0.62 0.88 0.60 0.82 0.92
Median 0.71 0.63 0.88 0.60 0.81 0.92
Std Dev. 0.013 0.023 0.047 0.012 0.010 0.015
Rel.Std.Dev. 1.85% 3.61% 5.34% 1.94% 1.19% 1.64%
PDM3 -5.94% -17.17% 17.60% -20.05% 8.50% 21.81%
Z-Score (Absolute) 0.37 0.84 0.63 0.96 0.24 0.81

No No 01 02 04 05 06 07
AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES
01g 0.5g 0.25g 0.5g 0.2g 01g
1 1 1.78 1.74 1.63 1.66 1.63 1.69
1 2 1.78 1.76 1.79 1.74 1.75 1.80
1 3 1.74 1.76 1.78 1.67 1.72 1.78
1 4 1.73 1.89 1.76 1.72 1.87 1.68
1 5 1.72 1.85 1.62 1.65 1.88 1.69
1 6 1.66 1.81 1.69 1.80 1.69 1.71
Mean 1.73 1.80 1.71 1.71 1.76 1.72
Median 1.73 1.79 1.73 1.69 1.74 1.70
Std Dev. 0.043 0.059 0.076 0.058 0.100 0.049
Rel.Std.Dev. 2.46% 3.28% 4.42% 3.39% 5.69% 2.84%
PDM3 0.42% 4.48% -0.74% -1.03% 1.87% -0.01%
Z-Score (Absolute) 0.14 1.63 0.28 0.39 0.67 0.02

No No 05 13 21 22
AR*MS AR*OES/MS AR*MS AR*MS
0.5g 20g 0.4g 01g
1 1 2.30 1.89 1.49 1.50
1 2 2.30 1.84 1.46 1.63
1 3 2.50 1.79 1.37 1.50
1 4 2.30 1.74 1.41 1.47
1 5 2.50 1.78 1.46 1.52
1 6 2.40 1.79 1.49 1.52
Mean 2.38 1.81 1.45 1.52
Median 2.35 1.79 1.46 1.51
Std Dev. 0.098 0.050 0.048 0.055
Rel.Std.Dev. 4.13% 2.76% 3.29% 3.64%
PDM3 33.54% 1.24% -18.94% -14.65%
Z-Score (Absolute) 2.73 0.57 0.78 0.57

No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 1.20 0.88 0.73 0.73
1 2 1.10 0.90 0.75 0.77
1 3 1.20 0.86 0.67 0.75
1 4 1.10 0.90 0.68 0.74
1 5 1.20 0.86 0.76 0.76
1 6 1.20 0.90 0.76 0.75
Mean 1.17 0.88 0.73 0.75
Median 1.20 0.89 0.74 0.75
Std Dev. 0.052 0.019 0.040 0.014
Rel.Std.Dev. 4.43% 2.20% 5.57% 1.89%
PDM3 32.45% 0.09% -17.69% -14.85%
Z-Score (Absolute) 3.02 0.57 0.78 0.57

No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 1.00 1.07 0.78 0.86
1 2 0.90 1.07 0.78 0.89
1 3 1.10 1.04 0.70 0.86
1 4 1.00 1.02 0.74 0.85
1 5 1.00 1.02 0.79 0.89
1 6 1.00 1.05 0.83 0.88
Mean 1.00 1.05 0.77 0.87
Median 1.00 1.05 0.78 0.87
Std Dev. 0.063 0.023 0.045 0.017
Rel.Std.Dev. 6.32% 2.17% 5.81% 2.00%
PDM3 9.04% 14.01% -16.04% -4.84%
Z-Score (Absolute) 0.42 0.93 1.22 0.42

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 13.30 12.90 12.30 12.30 12.90 13.40
1 2 13.45 13.20 12.20 11.70 14.00 13.50
1 3 13.45 12.60 13.10 12.90 13.90 13.35
1 4 13.60 12.60 12.70 12.60 13.60 13.45
1 5 13.45 12.70 12.50 13.20 12.90 13.35
1 6 13.35 12.60 11.90 12.50 13.70 13.15
Mean 13.43 12.77 12.45 12.53 13.50 13.37
Median 13.45 12.65 12.40 12.55 13.65 13.38
Std Dev. 0.103 0.242 0.418 0.516 0.486 0.121
Rel.Std.Dev. 0.77% 1.90% 3.36% 4.12% 3.60% 0.91%
PDM3 3.24% -1.88% -4.32% -3.68% 3.75% 2.73%
Z-Score (Absolute) 0.66 0.64 1.04 0.90 0.78 0.55

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 < 50 12.5 10.8 12.5 11.6 < 50
1 2 < 50 11.9 11.5 12.4 11.8 < 50
1 3 < 50 12.2 11.0 12.1 11.7 < 50
1 4 < 50 12.0 10.8 12.9 11.7 < 50
1 5 < 50 12.2 10.7 13.2 11.9 < 50
1 6 < 50 12.0 11.0 12.5 11.6 < 50
Mean 12.2 11.0 12.6 11.7
Median 12.1 10.9 12.5 11.7
Std Dev. 0.216 0.288 0.390 0.117
Rel.Std.Dev. 1.78% 2.62% 3.09% 1.00%
PDM3 2.09% -7.89% 5.83% -1.59%
Analytical results for Gd in OREAS 623 (Indicative Value 2.75 ppm)

No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 3.00 2.94 2.71 2.40
1 2 2.80 3.01 2.72 2.48
1 3 3.10 2.80 2.58 2.41
1 4 3.00 2.79 2.64 2.41
1 5 3.10 3.01 2.60 2.47
1 6 2.90 2.94 2.68 2.41
Mean 2.98 2.92 2.66 2.43
Median 3.00 2.94 2.66 2.41
Std Dev. 0.117 0.099 0.058 0.035
Rel.Std.Dev. 3.92% 3.40% 2.18% 1.45%
PDM3 8.65% 6.16% -3.31% -11.50%
Z-Score (Absolute) 0.81 0.53 0.53 1.46

Ge Round Replicate Lab Lab Lab Lab
No No 02 04 05 19
AR*OES/MSAR*OES/MS AR*MS AR*OES/MS
0.25g 0.25g 0.5g 0.25g
1 1 0.15 0.20 0.30 < 0.1
1 2 0.15 0.20 0.30 < 0.1
1 3 0.14 0.20 0.30 < 0.1
1 4 0.16 0.20 0.30 < 0.1
1 5 0.16 0.20 0.20 < 0.1
1 6 0.15 0.20 0.30 < 0.1
Mean 0.15 0.20 0.28
Median 0.15 0.20 0.30
Std Dev. 0.008 0.000 0.041
Rel.Std.Dev. 5.01% 0.00% 14.41%
PDM3 -29.30% -8.28% 29.94%
Z-Score (Absolute) 0.67 0.00 1.47 NA
Analytical results for Hf in OREAS 623 (Certified Value 1.32 ppm)

Hf Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 16
0.25g 0.25g 0.5g 0.4g 20g 40g
1 1 1.31 1.36 1.70 0.99 1.52 1.25
1 2 1.29 1.45 1.50 0.92 1.50 1.27
1 3 1.27 1.33 1.70 1.01 1.46 1.37
1 4 1.28 1.35 1.60 0.98 1.44 1.22
1 5 1.29 1.30 1.80 1.02 1.47 1.28
1 6 1.34 1.31 1.70 0.96 1.49 1.29
Mean 1.30 1.35 1.67 0.98 1.48 1.28
Median 1.29 1.34 1.70 0.99 1.48 1.28
Std Dev. 0.026 0.054 0.103 0.036 0.027 0.051
Rel.Std.Dev. 2.03% 4.00% 6.20% 3.71% 1.80% 3.95%
PDM3 -1.67% 2.47% 26.50% -25.62% 12.35% -2.85%
Z-Score (Absolute) 0.00 0.20 1.35 1.15 0.67 0.06
Analytical results for Hg in OREAS 623 (Certified Value 0.83 ppm)

Hg Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 <5 0.67 0.83 0.72 0.70 <5
1 2 <5 0.73 0.87 0.68 0.70 <5
1 3 <5 0.78 0.84 0.73 0.80 <5
1 4 <5 0.76 0.86 0.72 0.70 <5
1 5 5.00 0.75 0.84 0.72 0.80 <5
1 6 <5 0.81 0.89 0.71 0.70 <5
Mean 5.00 0.75 0.86 0.71 0.73
Median 5.00 0.76 0.85 0.72 0.70
Std Dev. 0.048 0.023 0.018 0.052
Rel.Std.Dev. 6.45% 2.64% 2.45% 7.04%
PDM3 502.78% -9.48% 3.08% -14.00% -11.59%
Z-Score (Absolute) 30.78 0.68 0.09 0.91 0.81 NA

No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 0.40 0.33 0.26 0.29
1 2 0.40 0.33 0.24 0.29
1 3 0.40 0.32 0.25 0.28
1 4 0.40 0.33 0.25 0.28
1 5 0.50 0.33 0.26 0.27
1 6 0.40 0.33 0.27 0.30
Mean 0.42 0.33 0.26 0.28
Median 0.40 0.33 0.26 0.28
Std Dev. 0.041 0.004 0.010 0.009
Rel.Std.Dev. 9.80% 1.28% 4.11% 3.09%
PDM3 31.81% 3.17% -19.33% -10.37%
Z-Score (Absolute) 1.81 0.41 0.94 0.41

No No 02 04 05 06 13 15
AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES/MS AR*OES
0.25g 0.25g 0.5g 0.4g 20g 0.5g
1 1 2.07 2.00 1.93 1.86 1.98 <5
1 2 2.04 1.81 1.84 2.00 1.98 <5
1 3 1.95 1.72 2.00 1.93 1.95 <5
1 4 2.03 1.74 1.99 1.97 2.01 <5
1 5 2.04 1.70 2.01 1.90 2.06 <5
1 6 2.00 1.75 1.93 1.93 1.98 <5
Mean 2.02 1.79 1.95 1.93 1.99
Median 2.03 1.75 1.96 1.93 1.98
Std Dev. 0.040 0.111 0.064 0.050 0.037
Rel.Std.Dev. 1.99% 6.21% 3.29% 2.57% 1.85%
PDM3 4.32% -7.77% 0.66% -0.29% 2.81%

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 0.200 0.167 0.160 0.190 0.126 0.190
1 2 0.200 0.157 0.170 0.190 0.124 0.180
1 3 0.200 0.163 0.170 0.200 0.133 0.190
1 4 0.200 0.163 0.170 0.190 0.130 0.190
1 5 0.200 0.173 0.160 0.210 0.123 0.190
1 6 0.200 0.175 0.160 0.200 0.131 0.190
Mean 0.200 0.166 0.165 0.197 0.128 0.188
Median 0.200 0.165 0.165 0.195 0.128 0.190
Std Dev. 0.000 0.007 0.005 0.008 0.004 0.004
Rel.Std.Dev. 0.00% 4.07% 3.32% 4.15% 3.18% 2.17%
PDM3 14.14% -5.08% -5.84% 12.23% -27.05% 7.48%
Z-Score (Absolute) 0.77 0.20 0.24 0.67 1.31 0.43

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 < 50 17.5 15.2 17.0 13.6 < 50
1 2 < 50 16.6 16.4 18.0 13.1 < 50
1 3 < 50 16.9 15.5 18.0 13.6 < 50
1 4 < 50 16.9 15.8 18.0 13.2 < 50
1 5 < 50 17.4 15.1 19.0 13.8 < 50
1 6 < 50 17.4 15.4 18.0 13.5 < 50
Mean 17.1 15.6 18.0 13.5
Median 17.1 15.5 18.0 13.6
Std Dev. 0.3 0.5 0.6 0.3
Rel.Std.Dev. 2.01% 3.06% 3.51% 1.97%
PDM3 -4.24% -12.89% 0.73% -24.64%
Analytical results for Li in OREAS 623 (Certified Value 10 ppm)

No No 02 04 05 09 13 15
AR*OES/MSAR*OES/MS AR*MS AR*OES AR*OES/MS AR*OES
0.25g 0.25g 0.5g 10g 20g 0.5g
1 1 9.8 9.0 10.9 13.0 10.3 10.0
1 2 9.5 9.0 11.3 12.0 10.2 10.0
1 3 9.6 10.0 10.8 13.0 10.1 10.0
1 4 9.7 9.0 10.7 13.0 9.7 10.0
1 5 9.8 9.0 9.9 12.0 9.8 10.0
1 6 9.9 9.0 9.6 12.0 9.9 10.0
Mean 9.7 9.2 10.5 12.5 10.0 10.0
Median 9.7 9.0 10.8 12.5 10.0 10.0
Std Dev. 0.1 0.4 0.6 0.5 0.3 0.0
Rel.Std.Dev. 1.50% 4.45% 6.14% 4.38% 2.56% 0.00%
PDM3 -3.35% -8.68% 4.93% 24.52% -0.28% -0.38%
Z-Score (Absolute) 0.50 1.69 1.08 5.06 0.02 0.00
Analytical results for Lu in OREAS 623 (Certified Value 0.12 ppm)

Lu Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 19
AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES/MSAR*OES/MS
0.25g 0.25g 0.5g 0.4g 20g 0.25g
1 1 0.12 0.11 0.10 0.09 0.12 0.11
1 2 0.12 0.12 0.10 0.08 0.12 0.12
1 3 0.12 0.11 0.10 0.09 0.13 0.11
1 4 0.12 0.11 0.10 0.08 0.12 0.11
1 5 0.12 0.11 0.10 0.09 0.12 0.11
1 6 0.12 0.11 0.10 0.09 0.12 0.10
Mean 0.12 0.11 0.10 0.09 0.12 0.11
Median 0.12 0.11 0.10 0.09 0.12 0.11
Std Dev. 0.002 0.004 0.000 0.005 0.001 0.006
Rel.Std.Dev. 1.91% 3.66% 0.00% 5.96% 1.21% 5.75%
PDM3 4.02% -4.14% -14.15% -25.60% 6.64% -5.57%
Z-Score (Absolute) 0.51 0.40 1.50 2.77 0.80 0.55

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 1.05 1.26 1.08 1.11 1.36 1.00
1 2 1.06 1.22 1.10 1.04 1.43 0.99
1 3 1.08 1.16 1.13 1.13 1.50 1.01
1 4 1.09 1.14 1.10 1.08 1.44 1.01
1 5 1.08 1.25 1.08 1.14 1.38 1.02
1 6 1.08 1.27 1.08 1.10 1.47 1.00
Mean 1.07 1.22 1.10 1.10 1.43 1.01
Median 1.08 1.23 1.09 1.11 1.44 1.01
Std Dev. 0.015 0.055 0.020 0.036 0.053 0.010
Rel.Std.Dev. 1.40% 4.49% 1.80% 3.30% 3.70% 1.04%
PDM3 -3.23% 9.70% -1.27% -0.82% 28.93% -9.39%
Z-Score (Absolute) 0.45 1.80 0.11 0.03 5.14 1.52

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 0.059 0.060 0.052 0.056 0.053 0.058
1 2 0.061 0.057 0.053 0.054 0.055 0.057
1 3 0.059 0.058 0.054 0.058 0.056 0.058
1 4 0.059 0.059 0.053 0.056 0.056 0.058
1 5 0.059 0.060 0.052 0.059 0.054 0.058
1 6 0.059 0.059 0.052 0.056 0.057 0.057
Mean 0.059 0.059 0.053 0.057 0.055 0.058
Median 0.059 0.059 0.053 0.056 0.055 0.058
Std Dev. 0.001 0.001 0.001 0.002 0.001 0.001
Rel.Std.Dev. 1.38% 1.46% 1.70% 3.35% 2.40% 0.90%
PDM3 4.28% 3.28% -7.38% -0.65% -3.19% 1.35%
Z-Score (Absolute) 0.59 0.52 1.43 0.20 0.66 0.17

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 7.00 10.28 9.33 8.48 7.00 7.00
1 2 8.00 11.00 9.16 6.87 6.60 7.00
1 3 8.00 9.70 8.04 8.74 8.60 7.00
1 4 9.00 10.05 8.01 7.95 7.50 9.00
1 5 10.00 9.21 6.43 9.45 8.20 7.00
1 6 8.00 9.32 7.48 7.14 8.10 6.00
Mean 8.33 9.93 8.08 8.11 7.67 7.17
Median 8.00 9.87 8.02 8.22 7.80 7.00
Std Dev. 1.033 0.666 1.079 0.983 0.769 0.983
Rel.Std.Dev. 12.39% 6.71% 13.36% 12.13% 10.02% 13.72%
PDM3 -0.50% 18.52% -3.58% -3.23% -8.46% -14.43%
Z-Score (Absolute) 0.07 1.36 0.14 0.12 0.47 1.17
Analytical results for Na in OREAS 623 (Certified Value 0.068 wt.%)

Na Round Replicate Lab Lab Lab Lab Lab Lab
No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 0.080 0.084 0.070 0.075 0.050 0.090
1 2 0.080 0.077 0.070 0.073 0.049 0.080
1 3 0.080 0.078 0.070 0.079 0.055 0.090
1 4 0.090 0.078 0.070 0.076 0.053 0.090
1 5 0.090 0.084 0.060 0.081 0.049 0.090
1 6 0.090 0.085 0.060 0.076 0.053 0.090
Mean 0.085 0.081 0.067 0.077 0.052 0.088
Median 0.085 0.081 0.070 0.076 0.052 0.090
Std Dev. 0.005 0.004 0.005 0.003 0.003 0.004
Rel.Std.Dev. 6.44% 4.41% 7.75% 3.75% 4.87% 4.62%
PDM3 24.91% 19.28% -2.03% 12.67% -24.32% 29.81%
Z-Score (Absolute) 1.73 1.36 0.03 0.93 1.49 2.06
Analytical results for Nb in OREAS 623 (Certified Value < 1 ppm)

No No 02 04 05 06 13 15
AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES/MS AR*OES
0.25g 0.25g 0.5g 0.4g 20g 0.5g
1 1 0.86 0.53 0.80 0.40 1.04 <5
1 2 0.80 0.60 0.80 0.40 1.01 <5
1 3 0.80 0.49 0.90 0.40 0.99 <5
1 4 0.78 0.51 1.00 0.40 0.97 <5
1 5 0.83 0.47 1.00 0.40 0.96 <5
1 6 0.85 0.50 0.90 0.40 1.01 <5
Mean 0.82 0.52 0.90 0.40 1.00
Median 0.82 0.51 0.90 0.40 1.00
Std Dev. 0.033 0.045 0.089 0.000 0.030
Rel.Std.Dev. 4.01% 8.80% 9.94% 0.00% 3.03%
PDM3
Analytical results for Nd in OREAS 623 (Indicative Value 16 ppm)

Nd Round Replicate Lab Lab Lab Lab
No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 18.1 19.4 12.1 14.5
1 2 17.4 18.9 12.4 14.6
1 3 18.5 18.6 12.5 14.1
1 4 17.8 18.9 12.8 14.1
1 5 18.0 19.4 12.5 14.2
1 6 18.3 19.5 13.7 14.2
Mean 18.0 19.1 12.7 14.3
Median 18.1 19.2 12.5 14.2
Std Dev. 0.4 0.4 0.6 0.2
Rel.Std.Dev. 2.15% 1.93% 4.37% 1.50%
PDM3 12.82% 19.72% -20.68% -10.56%
Z-Score (Absolute) 0.52 0.83 1.03 0.52
Analytical results for Ni in OREAS 623 (Certified Value 15.6 ppm)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 19.0 15.8 14.5 < 30 16.0 14.0
1 2 15.0 15.2 15.3 < 30 16.0 9.0
1 3 13.0 14.5 15.6 < 30 15.0 <5
1 4 18.0 14.2 15.6 < 30 16.0 5.0
1 5 27.0 14.6 16.4 < 30 16.0 8.0
1 6 19.0 16.4 16.4 < 30 15.0 11.0
Mean 18.5 15.1 15.6 15.7 9.4
Median 18.5 14.9 15.6 16.0 9.0
Std Dev. 4.8 0.8 0.7 0.5 3.4
Rel.Std.Dev. 25.98% 5.62% 4.59% 3.30% 35.76%
PDM3 18.40% -3.25% 0.06% 0.27% -39.84%
Z-Score (Absolute) 0.75 0.34 0.01 NA 0.02 4.05
Analytical results for P in OREAS 623 (Certified Value 0.04 wt.%)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 0.042 0.037 0.043 0.039 < 0.002 0.036
1 2 0.044 0.041 0.041 0.039 < 0.002 0.040
1 3 0.040 0.037 0.042 0.040 < 0.002 0.036
1 4 0.041 0.036 0.042 0.041 < 0.002 0.039
1 5 0.041 0.037 0.041 0.041 < 0.002 0.039
1 6 0.041 0.037 0.042 0.040 < 0.002 0.039
Mean 0.042 0.037 0.042 0.040 0.038
Median 0.041 0.037 0.042 0.040 0.039
Std Dev. 0.001 0.002 0.001 0.001 0.002
Rel.Std.Dev. 3.32% 4.69% 1.80% 2.24% 4.51%
PDM3 4.39% -6.17% 5.23% 0.62% -3.99%

No No 01 02 04 05 06 07
01g 0.25g 0.25g 0.5g 0.2g 01g
1 1 0.245 0.261 0.251 0.244 0.240 0.255
1 2 0.245 0.253 0.259 0.244 0.280 0.253
1 3 0.248 0.260 0.252 0.245 0.270 0.254
1 4 0.255 0.260 0.250 0.242 0.290 0.254
1 5 0.252 0.259 0.248 0.247 0.260 0.255
1 6 0.254 0.262 0.251 0.243 0.260 0.263
Mean 0.250 0.259 0.252 0.244 0.267 0.256
Median 0.250 0.260 0.251 0.244 0.265 0.255
Std Dev. 0.004 0.003 0.004 0.002 0.018 0.004
Rel.Std.Dev. 1.78% 1.20% 1.49% 0.71% 6.57% 1.44%
PDM3 -0.70% 3.07% 0.10% -2.95% 5.99% 1.62%
Z-Score (Absolute) 0.01 0.98 0.05 0.60 1.26 0.45
Analytical results for Pd in OREAS 623 (Indicative Value < 10 ppb)

Pd Round Replicate Lab
No No 13
AR*OES/MS
20g
1 1 < 10
1 2 < 10
1 3 < 10
1 4 < 10
1 5 < 10
1 6 < 10
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Pr in OREAS 623 (Indicative Value 4.33 ppm)

Pr Round Replicate Lab Lab Lab Lab
No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 5.00 4.80 3.35 3.96
1 2 4.70 4.77 3.47 4.40
1 3 5.10 4.69 3.51 4.29
1 4 4.80 4.72 3.60 3.83
1 5 4.90 4.85 3.51 3.97
1 6 5.00 4.83 3.83 4.39
Mean 4.92 4.78 3.54 4.14
Median 4.95 4.79 3.51 4.13
Std Dev. 0.147 0.064 0.161 0.249
Rel.Std.Dev. 2.99% 1.33% 4.55% 6.01%
PDM3 13.53% 10.34% -18.14% -4.41%
Z-Score (Absolute) 0.79 0.55 1.69 0.55
Analytical results for Pt in OREAS 623 (Indicative Value < 5 ppb)

Pt Round Replicate Lab
No No 13
AR*OES/MS
20g
1 1 <5
1 2 <5
1 3 <5
1 4 <5
1 5 <5
1 6 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Rb in OREAS 623 (Indicative Value 8.08 ppm)

No No 02 04 05 06 13 16
0.25g 0.25g 0.5g 0.4g 20g 40g
1 1 7.25 6.60 11.10 5.80 10.72 11.90
1 2 7.39 7.30 10.60 5.74 10.63 11.70
1 3 7.35 6.80 11.60 5.99 10.51 12.30
1 4 7.71 6.80 11.30 5.80 10.25 12.50
1 5 7.43 6.50 12.50 5.93 10.53 12.50
1 6 7.69 6.60 11.60 5.89 10.37 12.20
Mean 7.47 6.77 11.45 5.86 10.50 12.18
Median 7.41 6.70 11.45 5.85 10.52 12.25
Std Dev. 0.188 0.288 0.635 0.094 0.170 0.325
Rel.Std.Dev. 2.52% 4.25% 5.54% 1.61% 1.62% 2.67%
PDM3 -7.61% -16.29% 41.65% -27.53% 29.93% 50.72%
Z-Score (Absolute) 0.36 0.63 1.00 0.90 0.67 1.25
Re Round Replicate Lab Lab Lab Lab Lab
No No 05 13 16 19 21
AR*MS AR*OES/MS AR*MS AR*OES/MS AR*MS
0.5g 20g 40g 0.25g 0.4g
1 1 < 0.01 < 0.001 < 0.05 < 0.002 < 0.05
1 2 < 0.01 0.001 < 0.05 < 0.002 < 0.05
1 3 < 0.01 < 0.001 < 0.05 < 0.002 < 0.05
1 4 < 0.01 < 0.001 < 0.05 < 0.002 < 0.05
1 5 < 0.01 < 0.001 < 0.05 < 0.002 < 0.05
1 6 < 0.01 < 0.001 < 0.05 < 0.002 < 0.05
Mean 0.001
Median 0.001
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA NA NA NA

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 9.23 >5 >5 7.48 > 25000 9.37
1 2 9.27 >5 >5 7.43 > 25000 9.62
1 3 9.33 >5 >5 8.03 > 25000 9.32
1 4 9.35 >5 >5 8.39 > 25000 9.47
1 5 9.27 >5 >5 8.59 > 25000 9.47
1 6 9.18 >5 >5 7.76 > 25000 9.25
Mean 9.27 7.95 9.42
Median 9.27 7.90 9.42
Std Dev. 0.063 0.477 0.131
Rel.Std.Dev. 0.68% 6.00% 1.40%
PDM3 6.00% -9.15% 7.66%
Z-Score (Absolute) 0.65 NA NA 0.81 NA 0.81
Analytical results for Sb in OREAS 623 (Certified Value 20.2 ppm)

No No 02 04 05 06 09 10
AR*OES/MSAR*OES/MS AR*MS AR*MS AR*OES AR*OES
0.25g 0.25g 0.5g 0.4g 10g 40g
1 1 19.7 14.1 23.5 23.0 20.0 18.0
1 2 18.9 15.4 21.7 23.2 9.0 17.0
1 3 19.3 14.9 24.3 23.2 20.0 17.0
1 4 19.1 14.7 21.7 23.0 9.0 17.0
1 5 18.5 14.6 25.7 23.8 13.0 17.0
1 6 18.9 15.5 22.1 23.5 16.0 17.0
Mean 19.0 14.9 23.2 23.3 14.5 17.2
Median 19.0 14.8 22.8 23.2 14.5 17.0
Std Dev. 0.4 0.5 1.6 0.3 5.0 0.4
Rel.Std.Dev. 2.09% 3.53% 7.03% 1.34% 34.55% 2.38%
PDM3 -5.67% -26.34% 14.78% 15.36% -28.16% -14.95%
Z-Score (Absolute) 0.25 1.20 0.69 0.72 0.66 0.71
Analytical results for Sc in OREAS 623 (Certified Value 4.63 ppm)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 5.00 3.84 4.10 4.00 4.90 <5
1 2 5.00 4.11 4.50 4.00 4.90 <5
1 3 5.00 4.01 4.30 5.00 4.90 <5
1 4 5.00 4.20 4.30 4.00 5.00 <5
1 5 5.00 4.19 4.20 5.00 5.00 <5
1 6 5.00 4.28 4.40 5.00 5.00 <5
Mean 5.00 4.11 4.30 4.50 4.95
Median 5.00 4.15 4.30 4.50 4.95
Std Dev. 0.000 0.159 0.141 0.548 0.055
Rel.Std.Dev. 0.00% 3.87% 3.29% 12.17% 1.11%
PDM3 8.00% -11.33% -7.12% -2.80% 6.92%
Analytical results for Se in OREAS 623 (Certified Value 18.6 ppm)

No No 02 04 05 06 09 13
0.25g 0.25g 0.5g 0.4g 10g 20g
1 1 19.7 20.0 19.4 19.0 97.0 21.2
1 2 22.7 19.0 17.6 19.0 87.0 20.7
1 3 18.5 18.0 21.0 19.0 88.0 20.5
1 4 18.9 17.0 19.9 20.0 94.0 20.8
1 5 18.8 18.0 20.7 19.0 86.0 21.4
1 6 17.9 17.0 18.5 19.0 100.0 21.0
Mean 19.4 18.2 19.5 19.2 92.0 20.9
Median 18.8 18.0 19.7 19.0 91.0 20.9
Std Dev. 1.7 1.2 1.3 0.4 5.8 0.4
Rel.Std.Dev. 8.82% 6.44% 6.67% 2.13% 6.34% 1.71%
PDM3 4.48% -2.19% 5.08% 3.20% 395.34% 12.72%
Z-Score (Absolute) 0.03 0.30 0.32 0.16 33.19 0.96

No No 05 13 21 22
0.5g 20g 0.4g 01g
1 1 3.60 3.86 3.18 2.87
1 2 3.40 3.85 3.25 2.96
1 3 3.70 3.66 3.10 2.85
1 4 3.60 3.76 3.18 2.84
1 5 3.70 3.75 3.06 2.89
1 6 3.60 3.82 2.97 2.89
Mean 3.60 3.78 3.12 2.88
Median 3.60 3.79 3.14 2.88
Std Dev. 0.110 0.074 0.101 0.043
Rel.Std.Dev. 3.04% 1.95% 3.22% 1.48%
PDM3 7.54% 13.03% -6.70% -13.87%
Z-Score (Absolute) 0.49 0.86 0.49 0.98
Analytical results for Sn in OREAS 623 (Certified Value 4.07 ppm)

No No 02 04 05 06 09 13
0.25g 0.25g 0.5g 0.4g 10g 20g
1 1 4.12 3.10 3.98 3.50 < 10 3.86
1 2 4.54 3.20 3.75 3.70 < 10 3.91
1 3 4.07 2.80 4.17 3.60 < 10 3.76
1 4 3.93 3.00 4.04 3.60 < 10 3.73
1 5 3.80 2.70 4.29 3.70 < 10 3.67
1 6 3.87 2.90 4.08 3.60 < 10 3.79
Mean 4.05 2.95 4.05 3.62 3.79
Median 4.00 2.95 4.06 3.60 3.77
Std Dev. 0.265 0.187 0.183 0.075 0.087
Rel.Std.Dev. 6.53% 6.34% 4.52% 2.08% 2.30%
PDM3 -0.35% -27.48% -0.39% -11.09% -6.94%
Analytical results for Sr in OREAS 623 (Certified Value 14.2 ppm)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 8.0 14.5 12.7 14.0 14.4 16.0
1 2 10.0 14.6 13.4 15.0 13.7 13.0
1 3 14.0 14.5 13.6 15.0 14.0 13.0
1 4 13.0 14.0 13.2 15.0 12.7 21.0
1 5 13.0 15.6 13.0 15.0 6.5 16.0
1 6 13.0 14.7 12.9 15.0 14.1 18.0
Mean 11.8 14.7 13.1 14.8 12.6 16.2
Median 13.0 14.6 13.1 15.0 13.9 16.0
Std Dev. 2.3 0.5 0.3 0.4 3.0 3.1
Rel.Std.Dev. 19.58% 3.58% 2.53% 2.75% 24.10% 18.93%
PDM3 -16.59% 3.26% -7.43% 4.56% -11.42% 13.95%
Z-Score (Absolute) 1.25 0.23 0.87 0.36 0.40 0.63
Analytical results for Ta in OREAS 623 (Certified Value < 0.05 ppm)
No No 02 04 05 06 13 16
0.25g 0.25g 0.5g 0.4g 20g 40g
1 1 < 0.05 < 0.05 < 0.05 < 0.05 < 0.01 < 0.05
1 2 < 0.05 < 0.05 < 0.05 < 0.05 < 0.01 < 0.05
1 3 < 0.05 < 0.05 < 0.05 < 0.05 < 0.01 < 0.05
1 4 < 0.05 < 0.05 < 0.05 < 0.05 < 0.01 < 0.05
1 5 < 0.05 < 0.05 < 0.05 < 0.05 < 0.01 < 0.05
1 6 < 0.05 < 0.05 < 0.05 < 0.05 < 0.01 < 0.05
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA NA NA NA NA
Analytical results for Tb in OREAS 623 (Certified Value 0.34 ppm)

Tb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 19
0.25g 0.25g 0.5g 0.4g 20g 0.25g
1 1 0.35 0.30 0.40 0.21 0.37 0.31
1 2 0.35 0.32 0.30 0.22 0.36 0.33
1 3 0.35 0.30 0.40 0.22 0.34 0.31
1 4 0.36 0.31 0.40 0.22 0.36 0.32
1 5 0.36 0.30 0.40 0.22 0.37 0.33
1 6 0.37 0.30 0.40 0.22 0.36 0.31
Mean 0.36 0.31 0.38 0.22 0.36 0.32
Median 0.35 0.30 0.40 0.22 0.36 0.32
Std Dev. 0.009 0.008 0.041 0.004 0.011 0.010
Rel.Std.Dev. 2.42% 2.74% 10.65% 1.87% 2.94% 3.09%
PDM3 4.24% -10.78% 12.14% -36.13% 5.03% -6.88%
Z-Score (Absolute) 0.57 0.97 1.38 3.58 0.65 0.57
Analytical results for Te in OREAS 623 (Certified Value 0.57 ppm)

No No 02 04 05 06 10 13
0.25g 0.25g 0.5g 0.4g 40g 20g
1 1 0.62 0.63 0.47 0.50 <2 0.51
1 2 0.71 0.64 0.68 0.50 <2 0.53
1 3 0.66 0.64 0.76 0.50 <2 0.50
1 4 0.66 0.60 0.70 0.50 <2 0.52
1 5 0.63 0.61 0.76 0.60 <2 0.52
1 6 0.63 0.58 0.49 0.50 <2 0.48
Mean 0.65 0.62 0.64 0.52 0.51
Median 0.65 0.62 0.69 0.50 0.52
Std Dev. 0.033 0.024 0.131 0.041 0.020
Rel.Std.Dev. 5.06% 3.93% 20.31% 7.90% 3.84%
PDM3 14.60% 8.48% 13.17% -9.11% -10.14%

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 < 100 5.03 4.70 5.10 3.45 < 100
1 2 < 100 4.85 5.00 4.90 3.37 < 100
1 3 < 100 4.98 4.80 5.30 3.45 < 100
1 4 < 100 4.92 4.80 4.90 3.45 < 100
1 5 < 100 5.10 4.80 5.20 3.50 < 100
1 6 < 100 5.15 4.80 5.10 3.42 < 100
Mean 5.00 4.82 5.08 3.44
Median 5.00 4.80 5.10 3.45
Std Dev. 0.110 0.098 0.160 0.043
Rel.Std.Dev. 2.20% 2.04% 3.15% 1.25%
PDM3 6.08% 2.12% 7.77% -27.07%
Analytical results for Ti in OREAS 623 (Certified Value < 0.06 wt.%)
No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 0.050 0.032 0.030 0.046 0.017 0.050
1 2 0.050 0.029 0.040 0.045 0.016 0.050
1 3 0.050 0.031 0.030 0.048 0.018 0.050
1 4 0.050 0.030 0.030 0.048 0.018 0.050
1 5 0.050 0.033 0.030 0.057 0.016 0.050
1 6 0.050 0.034 0.030 0.053 0.017 0.050
Mean 0.050 0.032 0.032 0.049 0.017 0.050
Median 0.050 0.032 0.030 0.048 0.017 0.050
Std Dev. 0.000 0.002 0.004 0.005 0.001 0.000
Rel.Std.Dev. 0.00% 5.81% 12.89% 9.28% 5.26% 0.00%
PDM3
Z-Score (Absolute) 1.20 0.01 0.00 1.17 0.96 1.20

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 < 50 0.29 0.26 0.32 0.20 < 50
1 2 < 50 0.29 0.25 0.30 0.20 < 50
1 3 < 50 0.29 0.24 0.32 0.20 < 50
1 4 < 50 0.28 0.24 0.32 0.20 < 50
1 5 < 50 0.28 0.24 0.33 0.20 < 50
1 6 < 50 0.28 0.25 0.31 0.20 < 50
Mean 0.28 0.25 0.32 0.20
Median 0.29 0.25 0.32 0.20
Std Dev. 0.005 0.008 0.010 0.000
Rel.Std.Dev. 1.77% 3.31% 3.26% 0.00%
PDM3 10.61% -3.99% 23.26% -22.15%

Tm Round Replicate Lab Lab Lab
No No 05 13 22
AR*MS AR*OES/MS AR*MS
0.5g 20g 01g
1 1 0.20 0.12 0.11
1 2 0.20 0.12 0.12
1 3 0.20 0.11 0.11
1 4 0.20 0.12 0.11
1 5 0.20 0.13 0.11
1 6 0.20 0.12 0.11
Mean 0.20 0.12 0.11
Median 0.20 0.12 0.11
Std Dev. 0.000 0.005 0.006
Rel.Std.Dev. 0.00% 3.90% 5.70%
PDM3 41.21% -15.35% -24.10%

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 < 50 1.52 1.30 1.60 0.97 < 50
1 2 < 50 1.47 1.33 1.50 0.94 < 50
1 3 < 50 1.51 1.27 1.60 0.98 < 50
1 4 < 50 1.48 1.28 1.50 0.97 < 50
1 5 < 50 1.58 1.25 1.70 0.97 < 50
1 6 < 50 1.58 1.24 1.60 1.00 < 50
Mean 1.52 1.28 1.58 0.97
Median 1.52 1.28 1.60 0.97
Std Dev. 0.046 0.033 0.075 0.019
Rel.Std.Dev. 3.03% 2.59% 4.75% 2.00%
PDM3 6.20% -10.91% 10.34% -32.28%
Analytical results for V in OREAS 623 (Certified Value 15.8 ppm)

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 14.0 14.2 17.0 17.0 15.0 17.0
1 2 17.0 13.4 17.0 16.0 16.0 15.0
1 3 15.0 13.9 17.0 18.0 16.0 18.0
1 4 16.0 14.0 17.0 17.0 16.0 15.0
1 5 15.0 13.7 17.0 19.0 15.0 18.0
1 6 16.0 14.0 17.0 17.0 16.0 18.0
Mean 15.5 13.9 17.0 17.3 15.7 16.8
Median 15.5 14.0 17.0 17.0 16.0 17.5
Std Dev. 1.049 0.280 0.000 1.033 0.516 1.472
Rel.Std.Dev. 6.77% 2.02% 0.00% 5.96% 3.30% 8.74%
PDM3 -1.88% -12.22% 7.61% 9.72% -0.83% 6.56%
Z-Score (Absolute) 0.14 1.09 0.72 0.92 0.05 0.63

No No 01 02 04 05 06 08
01g 0.25g 0.25g 0.5g 0.4g 01g
1 1 < 50 3.09 2.60 2.50 2.40 < 50
1 2 < 50 3.10 2.80 2.40 2.30 < 50
1 3 < 50 3.04 2.60 2.60 2.30 < 50
1 4 < 50 3.11 2.60 2.50 2.30 < 50
1 5 < 50 3.04 2.50 2.70 2.30 < 50
1 6 < 50 3.03 2.50 2.60 2.30 < 50
Mean 3.07 2.60 2.55 2.32
Median 3.07 2.60 2.55 2.30
Std Dev. 0.034 0.110 0.105 0.041
Rel.Std.Dev. 1.11% 4.21% 4.11% 1.76%
PDM3 17.18% -0.75% -2.65% -11.56%

No No 02 04 05 06 09 13
AR*OES/MSAR*OES/MS AR*OES AR*MS AR*OES AR*OES/MS
0.25g 0.25g 0.5g 0.4g 10g 20g
1 1 7.85 7.01 8.00 5.97 5.00 8.43
1 2 7.64 7.62 8.00 5.77 5.00 8.43
1 3 7.75 7.20 8.00 6.11 5.00 8.35
1 4 7.85 7.13 8.00 5.95 5.00 8.34
1 5 7.77 7.01 9.00 6.08 5.00 8.48
1 6 7.86 7.04 8.00 5.99 5.00 8.27
Mean 7.79 7.17 8.17 5.98 5.00 8.38
Median 7.81 7.09 8.00 5.98 5.00 8.39
Std Dev. 0.085 0.234 0.408 0.120 0.000 0.077
Rel.Std.Dev. 1.09% 3.26% 5.00% 2.01% 0.00% 0.91%
PDM3 4.80% -3.51% 9.93% -19.53% -32.70% 12.84%
Z-Score (Absolute) 0.00 0.67 0.36 1.72 2.65 0.57

Yb Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 06 13 19
0.25g 0.25g 0.5g 0.4g 20g 0.25g
1 1 0.82 0.80 0.80 0.50 0.84 0.80
1 2 0.75 0.90 0.80 0.50 0.79 0.80
1 3 0.76 0.80 0.80 0.60 0.81 0.80
1 4 0.76 0.80 0.80 0.60 0.82 0.80
1 5 0.76 0.80 0.90 0.60 0.84 0.80
1 6 0.77 0.80 0.80 0.60 0.85 0.80
Mean 0.77 0.82 0.82 0.57 0.82 0.80
Median 0.76 0.80 0.80 0.60 0.83 0.80
Std Dev. 0.024 0.041 0.041 0.052 0.023 0.000
Rel.Std.Dev. 3.17% 5.00% 5.00% 9.11% 2.83% 0.00%
PDM3 -3.72% 2.23% 2.23% -29.07% 3.15% 0.14%
Z-Score (Absolute) 1.73 0.00 0.00 13.09 1.35 0.00

No No 01 02 04 05 06 07
AR*OES AR*OES AR*OES/MS AR*OES AR*OES AR*OES
01g 0.5g 0.25g 0.5g 0.2g 01g
1 1 1.02 1.06 0.91 1.01 0.96 1.03
1 2 1.03 1.05 0.98 1.01 1.08 1.03
1 3 1.02 1.07 0.96 1.02 1.04 1.04
1 4 1.03 1.08 0.96 1.01 1.11 1.02
1 5 1.01 1.09 0.93 1.03 1.07 1.03
1 6 1.03 1.04 0.96 1.01 0.97 1.05
Mean 1.02 1.07 0.95 1.02 1.04 1.03
Median 1.03 1.07 0.96 1.01 1.06 1.03
Std Dev. 0.008 0.019 0.024 0.008 0.061 0.010
Rel.Std.Dev. 0.80% 1.76% 2.51% 0.82% 5.89% 1.00%
PDM3 0.86% 4.96% -6.45% 0.04% 2.34% 1.84%
Z-Score (Absolute) 0.12 1.18 1.76 0.09 0.51 0.38
Analytical results for Zr in OREAS 623 (Certified Value 50 ppm)

Zr Round Replicate Lab Lab Lab Lab Lab Lab
No No 02 04 05 09 13 14
AR*OES/MSAR*OES/MS AR*OES AR*OES AR*OES/MS AR*MS
0.25g 0.25g 0.5g 10g 20g 0.5g
1 1 56 49 60 48 57 51
1 2 52 53 62 49 56 50
1 3 53 51 64 49 55 51
1 4 53 52 62 49 55 50
1 5 54 49 68 47 56 50
1 6 55 49 66 46 55 51
Mean 54 50 64 48 56 50
Median 54 50 63 49 56 50
Std Dev. 1.3 1.6 2.9 1.3 0.8 0.4
Rel.Std.Dev. 2.50% 3.17% 4.62% 2.64% 1.38% 0.82%
PDM3 6.69% -0.22% 26.21% -4.84% 10.19% -0.25%
Z-Score (Absolute) 1.02 0.00 3.89 0.67 1.53 0.00
08 09 10 11 13 14 15 16 17
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*MS AR*OES
01g 10g 40g 01g 20g 0.5g 0.5g 40g 01g
22.0 21.0 18.2 20.0 19.7 19.4 17.7 19.8 20.0
22.0 22.0 18.7 20.0 19.6 18.8 17.5 19.6 20.2
21.0 22.0 18.5 20.0 19.5 19.7 17.2 20.2 20.1
21.0 22.0 18.1 19.0 19.7 19.2 17.2 19.5 19.9
21.0 22.0 18.2 21.0 19.6 19.4 17.0 20.1 19.5
21.0 22.0 18.3 19.0 19.7 19.4 17.3 19.8 20.2
21.3 21.8 18.3 19.8 19.6 19.3 17.3 19.8 20.0
21.0 22.0 18.3 20.0 19.6 19.4 17.3 19.8 20.1
0.516 0.408 0.225 0.753 0.073 0.319 0.213 0.273 0.264
2.42% 1.87% 1.23% 3.80% 0.37% 1.65% 1.23% 1.38% 1.32%
4.46% 6.91% -10.23% -2.89% -3.87% -5.49% -15.25% -2.89% -2.15%
0.68 1.13 2.02 0.67 0.85 1.05 2.94 0.67 0.53

09 10 11 13 14 15 16 17 19
AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*OES AR*OES AR*OES/MS
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
1.68 1.82 1.86 1.95 1.75 1.61 1.86 1.77 1.84
1.64 1.83 1.89 1.96 1.73 1.60 1.82 1.76 1.82
1.65 1.79 1.85 2.00 1.79 1.58 1.86 1.73 1.80
1.65 1.85 1.88 1.99 1.71 1.56 1.84 1.77 1.80
1.63 1.80 1.90 1.98 1.78 1.56 1.84 1.73 1.84
1.62 1.84 1.88 1.96 1.75 1.56 1.87 1.76 1.85
1.65 1.82 1.88 1.97 1.75 1.58 1.85 1.75 1.83
1.65 1.83 1.88 1.97 1.75 1.57 1.85 1.76 1.83
0.021 0.024 0.019 0.020 0.030 0.023 0.018 0.019 0.022
1.26% 1.29% 0.99% 1.02% 1.71% 1.46% 0.99% 1.06% 1.19%
-8.73% 1.19% 4.12% 9.50% -2.81% -12.61% 2.55% -2.72% 1.26%
2.16 0.33 1.07 2.42 0.67 3.14 0.67 0.65 0.35

09 10 11 13 14 15 16 17 19
AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*MS AR*OES AR*OES/MS
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
82 73 110 71 80 64 73 78 74
82 77 60 72 77 66 73 78 78
79 74 80 74 80 64 75 76 73
88 77 70 73 78 64 72 77 75
88 73 70 71 79 63 75 75 77
82 73 100 70 80 64 72 77 73
84 75 82 72 79 64 73 77 75
82 74 75 71 79 64 73 77 75
3.7 2.0 19.4 1.4 1.1 1.0 1.1 1.2 2.1
4.40% 2.65% 23.76% 1.89% 1.38% 1.59% 1.56% 1.52% 2.80%
10.27% -1.62% 7.85% -5.23% 3.93% -15.37% -3.11% 1.46% -0.96%
1.44 0.00 0.72 0.44 0.67 1.73 0.18 0.37 0.08

11 12 13 14 15 16 17 20 21
AR*MS AR*MS AR*MS AR*MS AR*AAS AR*AAS AR*MS AR*MS AR*AAS
25g 40g 25g 25g 30g 30g 25g 0.5g 25g
0.840 0.829 0.797 0.811 0.710 0.770 0.840 0.742 0.780
0.840 0.828 0.765 0.814 0.660 0.770 0.850 0.758 0.670
0.760 0.848 0.761 0.794 0.710 0.760 0.860 0.798 0.570
0.870 0.840 0.780 0.798 0.640 0.750 0.850 0.795 0.730
0.860 0.867 0.805 0.807 0.640 0.770 0.850 0.771 0.650
0.830 0.850 0.806 0.783 0.630 0.780 0.840 0.780 0.760
0.833 0.844 0.786 0.801 0.665 0.767 0.848 0.774 0.693

0.840 0.844 0.788 0.803 0.650 0.770 0.850 0.775 0.700
0.039 0.015 0.020 0.012 0.036 0.010 0.008 0.022 0.079
4.66% 1.74% 2.54% 1.46% 5.44% 1.35% 0.89% 2.81% 11.34%
4.60% 5.90% -1.39% 0.56% -16.53% -3.77% 6.48% -2.85% -12.97%
1.27 1.18 0.00 0.32 2.45 0.39 1.27 0.24 1.03
Lab Lab Lab Lab

17 19 20 24
AR*OES AR*OES/MS AR*MS AR*OES
01g 0.25g 0.5g 0.5g
< 10 < 10 < 20 < 20
< 10 < 10 < 20 < 20
< 10 < 10 < 20 < 20
< 10 < 10 < 20 < 20
< 10 < 10 < 20 < 20
< 10 < 10 < 20 < 20
NA NA NA NA

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
52 191 180 219 113 12 219 30 140
49 196 180 216 98 12 224 30 133
53 188 170 226 112 12 234 30 136
49 171 180 225 102 12 226 30 130
49 193 180 220 125 11 229 30 132
45 173 170 217 120 12 219 40 140
50 185 177 220 112 12 225 32 135
49 190 180 219 112 12 225 30 135
3 11 5 4 10 0 6 4 4
5.68% 5.76% 2.92% 1.89% 9.06% 3.50% 2.60% 12.89% 3.12%
-79.44% -23.02% -26.62% -8.50% -53.67% -95.15% -6.47% -86.85% -43.85%
0.51 0.60 0.53 0.89 0.00 0.82 0.93 0.67 0.19

09 11 13 15 16 17 19 21 23
AR*OES AR*OES AR*OES/MS AR*OES AR*MS AR*OES AR*OES/MS AR*OES AR*OES
10g 01g 20g 0.5g 40g 01g 0.25g 0.4g 01g
<1 <5 0.44 < 10 < 0.5 < 0.5 0.40 < 0.5 <5
<1 <5 0.44 < 10 < 0.5 < 0.5 0.50 < 0.5 <5
<1 <5 0.43 < 10 < 0.5 < 0.5 0.50 < 0.5 <5
<1 <5 0.41 < 10 < 0.5 < 0.5 0.50 < 0.5 <5
<1 <5 0.42 < 10 < 0.5 < 0.5 0.40 < 0.5 <5
<1 <5 0.39 < 10 < 0.5 < 0.5 0.50 < 0.5 <5
0.42 0.47
0.43 0.50
0.017 0.052
4.02% 11.07%
14.31% 26.34%
NA NA 0.46 NA NA NA 0.92 NA NA

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
44.0 18.0 20.0 16.3 17.3 29.5 16.8 17.0 17.7
40.0 18.0 10.0 16.2 16.7 26.0 16.3 20.0 18.3
39.0 18.0 20.0 15.8 17.5 27.5 16.6 18.0 17.8
43.0 18.0 30.0 15.7 17.2 25.0 16.5 20.0 17.8
41.0 19.0 10.0 15.7 17.4 26.0 16.9 20.0 18.3
41.0 18.0 30.0 15.9 17.3 22.5 16.2 19.0 17.6
41.3 18.2 20.0 15.9 17.2 26.1 16.6 19.0 17.9
41.0 18.0 20.0 15.9 17.3 26.0 16.6 19.5 17.8
1.9 0.4 8.9 0.2 0.3 2.4 0.3 1.3 0.3
4.50% 2.25% 44.72% 1.45% 1.74% 9.03% 1.65% 6.66% 1.81%
145.11% 7.73% 18.60% -5.49% 2.10% 54.68% -1.86% 12.67% 6.22%
13.11 0.34 1.40 0.89 0.18 4.71 0.55 0.80 0.20

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
1.06 1.11 1.18 1.09 1.09 0.91 0.96 1.04 1.14
1.03 1.12 1.18 1.09 1.11 0.90 0.99 1.03 1.12
1.04 1.09 1.14 1.11 1.11 0.89 0.99 1.02 1.11
1.05 1.11 1.16 1.11 1.08 0.89 0.98 1.03 1.13
1.04 1.10 1.18 1.11 1.09 0.88 0.98 1.01 1.14
1.03 > 40 1.16 1.11 1.09 0.89 0.98 1.04 1.13
1.04 1.11 1.17 1.10 1.10 0.89 0.98 1.03 1.13
1.04 1.11 1.17 1.11 1.09 0.89 0.98 1.03 1.13
0.012 0.011 0.016 0.008 0.012 0.012 0.011 0.012 0.012
1.12% 1.03% 1.40% 0.70% 1.12% 1.30% 1.12% 1.14% 1.04%
-4.30% 1.61% 7.18% 1.37% 0.60% -18.16% -9.97% -5.53% 3.66%
0.81 0.03 0.83 0.00 0.11 2.79 1.62 0.98 0.33

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
52 51 57 54 52 41 46 46 58
51 51 58 54 51 41 45 46 58
52 51 56 53 52 41 47 46 57
52 50 57 54 49 41 46 46 57
52 50 58 55 52 40 45 46 58
52 50 56 54 51 41 46 47 58
52 50 57 54 51 41 46 46 58
52 50 57 54 51 41 46 46 58
0.4 0.3 0.9 0.8 1.1 0.3 0.5 0.5 0.5
0.79% 0.68% 1.57% 1.41% 2.21% 0.72% 1.18% 1.03% 0.85%
-1.21% -4.07% 8.63% 2.96% -2.70% -22.35% -12.84% -12.04% 9.85%
0.08 0.44 1.16 0.45 0.17 2.75 1.55 1.45 1.32
Lab Lab Lab Lab Lab

14 16 19 21 22
AR*MS AR*MS AR*OES/MS AR*MS AR*MS
0.5g 40g 0.25g 0.4g 01g
35.0 43.6 38.5 28.9 36.1
34.4 42.5 40.1 28.2 37.1
35.3 43.5 39.1 26.6 35.8
34.5 45.3 38.9 27.4 35.8
34.5 43.1 39.5 29.1 36.0
35.0 43.2 38.2 30.3 36.3
34.8 43.5 39.0 28.4 36.2
34.7 43.4 39.0 28.5 36.1
0.4 0.9 0.7 1.3 0.5
1.08% 2.18% 1.75% 4.62% 1.35%
-4.42% 19.65% 7.33% -21.90% -0.55%
0.22 1.09 0.45 1.21 0.00

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
205 212 216 218 233 147 200 205 235
204 217 221 218 233 147 204 205 236
206 213 219 215 229 144 203 204 231
207 217 220 214 234 144 200 204 229
206 216 223 215 233 143 205 199 238
209 215 217 215 236 144 207 208 232
206 215 219 216 233 145 203 204 233
206 216 220 215 233 144 204 205 233
2 2 3 2 2 1 3 3 3
0.84% 0.98% 1.18% 0.76% 0.92% 1.02% 1.37% 1.43% 1.43%
-4.46% -0.37% 1.64% 0.04% 7.96% -32.96% -5.85% -5.39% 8.13%
0.67 0.06 0.24 0.00 1.19 4.95 0.88 0.81 1.21

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
15.0 19.0 21.0 19.9 19.4 25.0 22.0 17.0 21.0
14.0 19.0 21.0 20.3 19.3 24.5 22.0 19.0 21.0
17.0 18.0 19.0 19.7 23.3 28.0 22.0 17.0 19.0
15.0 18.0 19.0 19.9 19.1 26.0 22.0 18.0 20.0
15.0 21.0 19.0 19.8 19.4 24.0 22.0 18.0 22.0
15.0 21.0 19.0 19.6 18.7 26.0 22.0 17.0 19.0
15.2 19.3 19.7 19.9 19.9 25.6 22.0 17.7 20.3
15.0 19.0 19.0 19.8 19.4 25.5 22.0 17.5 20.5
1.0 1.4 1.0 0.2 1.7 1.4 0.0 0.8 1.2
6.48% 7.07% 5.25% 1.11% 8.57% 5.59% 0.00% 4.62% 5.96%
-21.86% -0.40% 1.32% 2.32% 2.35% 31.80% 13.34% -8.98% 4.76%
3.06 0.00 0.22 0.36 0.10 4.21 1.80 1.12 0.67
Lab Lab Lab

19 21 22
AR*OES/MS AR*MS AR*MS
0.25g 0.4g 01g
0.87 0.56 0.76
0.96 0.55 0.80
0.86 0.54 0.76
0.89 0.54 0.76
0.91 0.58 0.78
0.87 0.56 0.78
0.89 0.56 0.77
0.88 0.56 0.77
0.037 0.015 0.016
4.17% 2.73% 2.11%
18.71% -26.25% 2.77%
0.67 1.23 0.00

08 09 11 13 14 15 16 17 19
AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*MS AR*OES/AAS AR*OES
01g 10g 01g 20g 0.5g 0.5g 40g 0.5g 0.25g
1.76 > 10000 1.62 1.68 1.63 1.52 1.75 1.83 1.76
1.91 > 10000 1.71 1.69 1.61 1.48 1.71 1.74 1.76
1.71 > 10000 1.67 1.68 1.69 1.46 1.71 1.69 1.76
1.76 -- 1.70 1.67 1.70 1.46 1.73 1.74 1.76
1.71 > 10000 1.71 1.66 1.65 1.47 1.72 1.69 1.76
1.64 > 10000 1.69 1.69 1.65 1.46 1.73 1.93 1.79
1.75 1.68 1.68 1.65 1.47 1.73 1.77 1.76
1.73 1.69 1.68 1.65 1.46 1.73 1.74 1.76
0.089 0.037 0.009 0.034 0.024 0.015 0.094 0.013
5.10% 2.20% 0.56% 2.08% 1.63% 0.88% 5.35% 0.72%
1.29% -2.43% -2.75% -4.11% -14.50% 0.04% 2.45% 2.27%
0.46 NA 0.62 1.02 1.52 5.53 0.00 0.19 0.82
09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
13.41 13.49 12.85 13.28 12.86 11.59 13.40 12.05 12.18
13.13 13.57 13.20 13.58 12.81 11.32 13.40 12.10 11.83
13.08 13.50 12.85 13.29 12.85 11.37 13.60 12.00 12.20
13.24 13.58 13.10 13.38 12.86 11.16 13.50 12.05 12.08
13.10 13.55 13.25 13.45 13.08 11.12 13.60 11.75 12.22
13.30 13.58 13.05 13.66 12.85 11.30 13.50 12.30 12.02
13.21 13.55 13.05 13.44 12.88 11.31 13.50 12.04 12.09
13.18 13.56 13.08 13.41 12.86 11.31 13.50 12.05 12.13
0.130 0.040 0.170 0.155 0.097 0.167 0.089 0.177 0.148
0.98% 0.30% 1.30% 1.15% 0.76% 1.48% 0.66% 1.47% 1.23%
1.53% 4.10% 0.30% 3.29% -0.97% -13.10% 3.75% -7.45% -7.10%
0.28 0.86 0.00 0.67 0.29 3.02 0.78 1.75 1.67

11 13 14 15 16 17 19 20 21
AR*OES AR*OES/MS AR*MS AR*OES AR*MS AR*OES AR*OES/MS AR*MS AR*MS
01g 20g 0.5g 0.5g 40g 01g 0.25g 0.5g 0.4g
< 50 13.3 12.0 22.5 15.3 10.0 13.2 12.0 10.6
< 50 13.3 12.0 22.0 15.4 10.0 13.5 12.0 10.7
< 50 13.1 12.4 21.5 15.7 10.0 12.9 12.0 9.9
< 50 13.1 12.3 22.0 15.9 10.0 13.6 12.0 10.2
< 50 13.2 12.3 21.5 16.4 10.0 13.4 12.0 10.8
< 50 12.9 11.7 22.0 16.3 10.0 13.1 12.0 10.8
13.1 12.1 21.9 15.8 10.0 13.3 12.0 10.5
13.1 12.2 22.0 15.8 10.0 13.3 12.0 10.6
0.155 0.264 0.376 0.455 0.000 0.264 0.000 0.369
1.18% 2.18% 1.72% 2.87% 0.00% 1.99% 0.00% 3.51%
10.42% 1.77% 84.08% 32.99% -16.01% 11.57% 0.79% -11.81%
NA 0.62 0.15 7.21 2.64 1.74 0.73 0.24 1.37
Lab Lab Lab
19 21 22
0.25g 0.4g 01g
1.22 1.52 1.00
1.29 1.48 1.20
1.21 1.47 1.00
1.28 1.45 1.00
1.28 1.47 1.20
1.25 1.51 1.00
1.26 1.48 1.07
1.27 1.48 1.00
0.034 0.027 0.103
2.70% 1.79% 9.68%
-4.74% 12.59% -19.04%
0.15 0.69 0.84

11 13 14 17 19 20 21 22 23
AR*OES AR*OES/MS AR*MS AR*OES AR*OES/MS AR*MS AR*MS AR*MS AR*OES
01g 20g 0.5g 01g 0.25g 0.5g 0.4g 01g 01g
<5 0.86 0.94 1.00 0.76 0.78 0.70 0.86 <5
<5 0.83 0.91 1.00 0.75 0.84 0.80 0.84 <5
<5 0.82 0.89 2.00 0.77 0.84 0.70 0.84 <5
<5 0.86 0.82 1.00 0.75 0.78 0.80 0.84 <5
6.00 0.81 0.88 1.00 0.75 0.79 0.80 0.88 <5
<5 0.81 0.84 1.00 0.74 0.80 0.80 0.89 <5
6.00 0.83 0.88 1.17 0.75 0.81 0.77 0.86
6.00 0.82 0.89 1.00 0.75 0.80 0.80 0.85
0.026 0.044 0.408 0.010 0.028 0.052 0.022
3.13% 5.03% 34.99% 1.37% 3.49% 6.74% 2.60%
623.34% 0.22% 6.09% 40.65% -9.18% -2.95% -7.57% 3.48%
38.18 0.09 0.27 1.16 0.67 0.28 0.57 0.11 NA
Lab Lab Lab Lab

16 19 21 22
40g 0.25g 0.4g 01g
1.83 2.04 1.52 1.99
1.82 2.15 1.53 1.94
1.85 2.03 1.60 1.89
1.79 2.05 1.55 1.88
1.86 2.16 1.60 2.05
1.86 2.04 1.64 1.93
1.84 2.08 1.57 1.95
1.84 2.05 1.58 1.94
0.027 0.060 0.047 0.064
1.49% 2.88% 3.00% 3.29%
-5.28% 7.28% -18.79% 0.48%
1.01 1.19 3.39 0.00

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
0.150 0.206 0.170 0.233 0.170 0.180 0.216 0.160 0.180
0.150 0.207 0.190 0.229 0.160 0.180 0.202 0.160 0.170
0.150 0.203 0.180 0.246 0.170 0.180 0.210 0.150 0.170
0.150 0.209 0.180 0.238 0.160 0.180 0.204 0.160 0.170
0.140 0.209 0.190 0.239 0.170 0.175 0.204 0.150 0.170
0.140 0.205 0.190 0.238 0.160 0.170 0.209 0.160 0.180
0.147 0.207 0.183 0.237 0.165 0.178 0.208 0.157 0.173
0.150 0.207 0.185 0.238 0.165 0.180 0.207 0.160 0.170
0.005 0.002 0.008 0.006 0.005 0.004 0.005 0.005 0.005
3.52% 1.09% 4.45% 2.44% 3.32% 2.36% 2.51% 3.30% 2.98%
-16.30% 17.91% 4.62% 35.44% -5.84% 1.29% 18.42% -10.59% -1.08%
0.77 0.96 0.29 1.85 0.24 0.12 0.99 0.48 0.00

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
11.0 22.0 < 50 21.3 18.0 16.0 19.6 20.0 19.8
12.0 22.0 < 50 21.1 16.9 16.0 19.5 20.0 20.4
12.0 22.0 < 50 20.6 17.9 15.5 20.0 20.0 20.1
11.0 22.0 < 50 20.8 17.3 15.0 20.7 20.0 19.9
11.0 22.0 < 50 21.2 17.9 15.5 21.5 20.0 20.3
11.0 22.0 < 50 21.1 17.8 15.0 21.5 20.0 19.5
11.3 22.0 21.0 17.6 15.5 20.5 20.0 20.0
11.0 22.0 21.1 17.8 15.5 20.4 20.0 20.0
0.5 0.0 0.3 0.4 0.4 0.9 0.0 0.3
4.56% 0.00% 1.24% 2.52% 2.89% 4.42% 0.00% 1.67%
-36.58% 23.11% 17.54% -1.47% -13.26% 14.53% 11.92% 11.92%
2.13 1.59 NA 1.25 0.11 0.67 1.06 0.90 0.90
Lab Lab Lab

16 19 22
AR*MS AR*OES/MS AR*MS
40g 0.25g 01g
8.9 10.0 10.2
8.6 10.0 10.6
8.6 9.0 9.8
8.7 9.0 9.8
8.0 10.0 9.9
8.4 10.0 10.8
8.5 9.7 10.2
8.6 10.0 10.1
0.3 0.5 0.4
3.61% 5.34% 4.23%
-14.99% -3.70% 1.44%
2.97 0.67 0.37
Lab Lab
21 22
AR*MS AR*MS
0.4g 01g
0.12 0.12
0.13 0.13
0.13 0.12
0.13 0.12
0.13 0.13
0.13 0.12
0.13 0.12
0.13 0.12
0.004 0.004
3.18% 3.73%
10.17% 3.02%
1.19 0.40

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
1.09 1.11 1.11 1.08 1.21 1.23 1.10 1.03 1.17
1.07 1.11 1.13 1.08 1.16 1.21 1.07 1.03 1.15
1.07 1.09 1.10 1.08 1.18 1.21 1.09 1.02 1.13
1.08 1.11 1.13 1.09 1.19 1.21 1.08 1.04 1.15
1.07 1.11 1.14 1.11 1.19 1.20 1.08 1.01 1.13
1.06 1.11 1.13 1.08 1.19 1.21 1.11 1.05 1.14
1.07 1.11 1.12 1.09 1.19 1.21 1.09 1.03 1.14
1.07 1.11 1.13 1.08 1.19 1.21 1.09 1.03 1.15
0.010 0.008 0.015 0.012 0.016 0.010 0.015 0.014 0.015
0.96% 0.74% 1.34% 1.10% 1.38% 0.85% 1.35% 1.37% 1.32%
-3.23% -0.22% 1.28% -2.14% 6.99% 9.40% -1.87% -7.13% 3.24%
0.45 0.07 0.33 0.26 1.33 1.75 0.21 1.13 0.67

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
0.050 0.057 0.057 0.057 0.057 0.049 0.051 0.052 0.061
0.050 0.057 0.059 0.057 0.057 0.049 0.049 0.052 0.064
0.050 0.056 0.057 0.057 0.059 0.049 0.050 0.052 0.063
0.050 0.058 0.058 0.057 0.057 0.048 0.049 0.052 0.062
0.050 0.057 0.059 0.059 0.058 0.048 0.049 0.051 0.063
0.050 0.057 0.058 0.057 0.058 0.048 0.050 0.053 0.061
0.050 0.057 0.058 0.058 0.058 0.049 0.050 0.052 0.062
0.050 0.057 0.058 0.057 0.058 0.049 0.049 0.052 0.062
0.000 0.000 0.001 0.001 0.001 0.001 0.001 0.001 0.001
0.00% 0.86% 1.54% 1.02% 1.54% 1.11% 1.70% 1.12% 1.86%
-12.13% 0.44% 1.93% 1.15% 1.17% -14.59% -12.89% -8.79% 9.43%
2.30 0.00 0.27 0.13 0.13 2.75 2.44 1.69 1.64

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
15.00 10.00 <5 8.89 8.95 6.00 9.10 8.00 9.79
15.00 10.00 <5 9.02 9.23 6.00 8.80 8.00 10.25
15.00 11.00 <5 8.72 9.62 6.00 9.10 8.00 9.65
14.00 10.00 <5 8.86 8.85 6.00 8.70 8.00 9.95
14.00 10.00 <5 8.60 9.41 6.00 9.00 8.00 10.28
14.00 10.00 <5 8.91 9.43 6.00 8.80 9.00 9.89
14.50 10.17 8.83 9.25 6.00 8.92 8.17 9.97
14.50 10.00 8.88 9.32 6.00 8.90 8.00 9.92
0.548 0.408 0.150 0.298 0.000 0.172 0.408 0.251
3.78% 4.02% 1.69% 3.23% 0.00% 1.93% 5.00% 2.52%
73.13% 21.39% 5.48% 10.43% -28.36% 6.47% -2.49% 19.02%
5.06 1.55 NA 0.47 0.81 1.82 0.54 0.07 1.39

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
0.060 0.060 < 0.05 0.083 0.067 0.070 0.070 0.060 0.070
0.060 0.060 < 0.05 0.082 0.067 0.070 0.070 0.060 0.070
0.060 0.060 < 0.05 0.079 0.066 0.070 0.070 0.060 0.070
0.060 0.070 < 0.05 0.080 0.066 0.070 0.070 0.060 0.070
0.060 0.060 < 0.05 0.082 0.066 0.065 0.070 0.060 0.070
0.060 0.060 < 0.05 0.081 0.066 0.065 0.070 0.060 0.070
0.060 0.062 0.081 0.066 0.068 0.070 0.060 0.070
0.060 0.060 0.081 0.066 0.070 0.070 0.060 0.070
0.000 0.004 0.001 0.001 0.003 0.000 0.000 0.000
0.00% 6.62% 1.70% 0.78% 3.78% 0.00% 0.00% 0.00%
-11.82% -9.38% 19.11% -2.52% 0.42% 2.87% -11.82% 2.87%
0.67 0.51 NA 1.35 0.06 0.13 0.29 0.67 0.29
Lab Lab Lab Lab

16 19 21 22
40g 0.25g 0.4g 01g
1.10 0.79 0.80 0.60
1.10 0.84 0.80 0.80
1.10 0.80 0.80 0.60
1.10 0.76 0.80 0.60
1.10 0.84 0.80 0.60
1.10 0.79 0.90 0.60
1.10 0.80 0.82 0.63
1.10 0.80 0.80 0.60
0.000 0.031 0.041 0.082
0.00% 3.91% 5.00% 12.89%
1.04 0.00 0.01 0.71

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
11.0 15.0 33.0 16.0 16.1 12.5 15.7 14.0 17.3
11.0 15.0 27.0 16.4 15.7 12.0 15.5 15.0 17.8
12.0 16.0 29.0 16.3 15.5 14.0 16.2 13.0 16.4
11.0 15.0 25.0 16.2 15.5 12.5 15.6 14.0 17.7
11.0 16.0 25.0 16.3 15.7 11.5 16.0 14.0 18.0
11.0 15.0 20.0 16.1 15.4 12.5 16.8 13.0 17.3
11.2 15.3 26.5 16.2 15.7 12.5 16.0 13.8 17.4
11.0 15.0 26.0 16.2 15.6 12.5 15.9 14.0 17.5
0.4 0.5 4.4 0.1 0.3 0.8 0.5 0.8 0.6
3.66% 3.37% 16.49% 0.84% 1.60% 6.69% 3.03% 5.44% 3.28%
-28.53% -1.86% 69.60% 3.78% 0.16% -20.00% 2.19% -11.46% 11.47%
2.90 0.20 7.04 0.37 0.01 2.04 0.21 1.17 1.15

09 10 11 13 14 16 17 19 20
AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*OES AR*OES/MS AR*MS
10g 40g 01g 20g 0.5g 40g 01g 0.25g 0.5g
0.030 0.039 0.043 0.033 0.039 0.053 0.040 0.042 0.037
0.040 0.034 0.041 0.033 0.038 0.053 0.040 0.043 0.033
0.030 0.038 0.043 0.033 0.037 0.051 0.040 0.041 0.036
0.030 0.039 0.044 0.032 0.039 0.052 0.038 0.041 0.034
0.040 0.038 0.044 0.032 0.037 0.051 0.039 0.043 0.036
0.040 0.038 0.039 0.031 0.042 0.054 0.041 0.040 0.036
0.035 0.038 0.042 0.032 0.039 0.052 0.040 0.042 0.035
0.035 0.038 0.043 0.032 0.038 0.053 0.040 0.041 0.036
0.005 0.002 0.002 0.001 0.002 0.001 0.001 0.001 0.002
15.65% 4.46% 4.65% 2.52% 4.58% 2.31% 2.60% 2.37% 4.26%
-11.96% -5.50% 6.49% -19.08% -2.69% 31.65% -0.22% 4.44% -11.12%
0.00 0.77 0.99 3.34 0.56 5.25 0.14 0.65 1.99

08 09 10 11 13 14 15 16 17
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*MS AR*OES
01g 10g 40g 01g 20g 0.5g 0.5g 40g 01g
0.252 0.219 0.244 0.255 0.242 0.247 0.143 0.237 0.226
0.246 0.218 0.245 0.255 0.241 0.236 0.147 0.233 0.225
0.255 0.222 0.246 0.249 0.245 0.246 0.148 0.237 0.221
0.254 0.221 0.242 0.252 0.245 0.237 0.144 0.233 0.225
0.254 0.223 0.241 0.255 0.245 0.247 0.144 0.237 0.219
0.254 0.222 0.244 0.251 0.243 0.245 0.146 0.241 0.226
0.253 0.221 0.244 0.253 0.243 0.243 0.145 0.236 0.224
0.254 0.222 0.244 0.254 0.244 0.246 0.145 0.237 0.225
0.003 0.002 0.002 0.003 0.002 0.005 0.002 0.003 0.003
1.32% 0.88% 0.86% 1.01% 0.67% 2.21% 1.23% 1.27% 1.32%
0.36% -12.26% -3.10% 0.49% -3.24% -3.36% -42.24% -6.06% -11.10%
0.41 3.05 0.64 0.31 0.68 0.71 10.94 1.42 2.75
Lab Lab Lab
19 21 22
0.25g 0.4g 01g
8.50 5.13 8.80
8.60 5.24 9.20
8.30 5.22 9.00
8.60 5.44 8.60
8.70 5.58 8.60
8.40 5.66 8.80
8.52 5.38 8.83
8.55 5.34 8.80
0.147 0.214 0.234
1.73% 3.99% 2.65%
5.36% -33.46% 9.28%
0.00 1.07 0.11

11 13 14 15 16 17 19 20 21
AR*OES AR*OES/MS AR*MS AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES
01g 20g 0.5g 0.5g 40g 01g 0.25g 0.5g 0.4g
9.50 8.43 >5 6.92 > 50000 9.03 >5 8.32 > 25000
9.69 8.36 >5 6.94 > 50000 9.10 >5 7.86 > 25000
9.44 8.09 >5 6.80 > 50000 8.96 >5 8.37 > 25000
9.67 8.44 >5 6.80 > 50000 8.96 >5 7.91 > 25000
9.76 8.28 >5 6.78 > 50000 8.76 >5 7.94 > 25000
9.66 8.55 >5 6.84 > 50000 9.14 >5 7.92 > 25000
9.62 8.36 6.84 8.99 8.05
9.67 8.40 6.82 9.00 7.93
0.123 0.156 0.071 0.135 0.228
1.28% 1.87% 1.04% 1.50% 2.83%
9.98% -4.43% -21.74% 2.80% -7.93%
1.04 0.36 NA 2.03 NA 0.34 NA 0.70 NA

13 14 15 16 17 19 20 21 22
AR*OES/MS AR*MS AR*OES AR*MS AR*OES AR*OES/MS AR*MS AR*OES AR*MS
20g 0.5g 0.5g 40g 01g 0.25g 0.5g 0.4g 01g
17.4 27.8 12.5 23.5 23.0 20.8 18.3 22.0 25.8
17.8 27.8 11.5 23.8 22.0 22.5 17.1 22.0 25.0
17.6 27.5 13.5 24.8 21.0 20.4 18.6 22.0 24.4
17.7 25.7 14.5 24.6 22.0 20.6 17.1 20.0 23.9
17.8 27.8 13.5 24.7 18.0 21.4 18.9 19.0 24.1
17.5 27.7 14.0 23.2 25.0 20.8 18.6 20.0 24.5
17.6 27.4 13.3 24.1 21.8 21.1 18.1 20.8 24.6
17.7 27.7 13.5 24.2 22.0 20.8 18.5 21.0 24.5
0.2 0.8 1.1 0.7 2.3 0.8 0.8 1.3 0.7
1.00% 3.01% 8.18% 2.85% 10.61% 3.71% 4.41% 6.38% 2.81%
-12.61% 35.58% -34.35% 19.40% 8.17% 4.30% -10.32% 3.22% 21.96%
0.57 1.72 1.57 0.90 0.39 0.14 0.46 0.16 1.02

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
<3 4.00 5.00 5.44 4.85 <5 4.00 4.00 4.80
<3 4.00 5.00 5.49 5.00 <5 4.00 4.00 4.80
<3 4.00 <5 5.40 4.80 <5 4.00 4.00 4.70
<3 4.00 5.00 5.50 4.76 <5 4.00 4.00 4.70
<3 4.00 5.00 5.50 4.82 <5 4.00 4.00 4.70
<3 4.00 5.00 5.38 5.17 <5 4.00 4.00 4.80
4.00 5.00 5.45 4.90 4.00 4.00 4.75
4.00 5.00 5.46 4.84 4.00 4.00 4.75
0.000 0.000 0.053 0.156 0.000 0.000 0.055
0.00% 0.00% 0.97% 3.18% 0.00% 0.00% 1.15%
-13.60% 8.00% 17.71% 5.84% -13.60% -13.60% 2.60%
NA 1.33 0.59 1.46 0.30 NA 1.33 1.33 0.11

14 15 16 19 20 21 22
AR*MS AR*OES AR*MS AR*OES/MS AR*MS AR*MS AR*MS
0.5g 0.5g 40g 0.25g 0.5g 0.4g 01g
14.3 13.5 17.0 20.0 18.7 16.0 20.0
15.4 13.5 18.0 21.0 20.1 17.0 20.0
15.3 12.5 17.0 20.0 20.8 17.0 20.0
14.2 13.0 17.0 21.0 18.5 16.0 18.0
15.2 13.5 18.0 22.0 18.4 16.0 20.0
15.3 12.5 17.0 21.0 18.4 15.0 20.0
15.0 13.1 17.3 20.8 19.2 16.2 19.7
15.3 13.3 17.0 21.0 18.6 16.0 20.0
0.5 0.5 0.5 0.8 1.0 0.8 0.8
3.66% 3.76% 2.98% 3.61% 5.41% 4.66% 4.15%
-19.51% -29.56% -6.68% 12.17% 3.11% -12.96% 5.89%
1.76 2.60 0.67 0.91 0.00 1.20 0.38
Lab Lab Lab Lab Lab

15 16 19 21 22
AR*OES AR*MS AR*OES/MS AR*OES AR*MS
0.5g 40g 0.25g 0.4g 01g
<5 4.20 4.30 4.00 4.20
<5 4.20 4.50 4.00 4.20
<5 4.00 4.50 4.00 4.10
<5 4.20 4.10 4.00 3.90
<5 4.00 4.50 4.00 4.30
<5 4.10 4.10 4.00 4.10
4.12 4.33 4.00 4.13
4.15 4.40 4.00 4.15
0.098 0.197 0.000 0.137
2.39% 4.54% 0.00% 3.31%
1.20% 6.53% -1.66% 1.61%
NA 0.54 2.33 0.43 0.67

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
13.0 14.0 8.0 14.8 14.5 35.5 14.4 13.0 14.1
12.0 14.0 8.0 14.7 14.2 35.5 14.0 14.0 14.8
12.0 14.0 13.0 14.5 14.2 35.0 14.7 13.0 13.9
12.0 15.0 13.0 14.5 14.3 34.5 14.6 14.0 14.4
12.0 14.0 10.0 14.5 14.3 34.5 15.1 13.0 14.6
12.0 14.0 9.0 14.3 14.3 35.0 14.9 13.0 14.2
12.2 14.2 10.2 14.6 14.3 35.0 14.6 13.3 14.3
12.0 14.0 9.5 14.5 14.3 35.0 14.6 13.0 14.3
0.4 0.4 2.3 0.2 0.1 0.4 0.4 0.5 0.3
3.36% 2.88% 22.79% 1.34% 0.64% 1.28% 2.65% 3.87% 2.32%
-14.24% -0.14% -28.34% 2.66% 0.61% 146.71% 3.03% -6.02% 1.03%
1.57 0.12 3.01 0.17 0.04 14.93 0.20 0.72 0.00
Lab Lab Lab

19 21 22
0.25g 0.4g 01g
< 0.05 < 0.05 0.010
< 0.05 < 0.05 0.005
< 0.05 < 0.05 0.005
< 0.05 < 0.05 0.005
< 0.05 < 0.05 0.010
< 0.05 < 0.05 0.010
0.008
0.008
0.003
36.51%
NA NA NA
Lab Lab
21 22
AR*MS AR*MS
0.4g 01g
0.36 0.31
0.36 0.32
0.35 0.31
0.35 0.31
0.35 0.32
0.37 0.33
0.36 0.31
0.36 0.31
0.008 0.009
2.29% 2.74%
4.34% -8.10%
0.58 0.70

14 16 19 20 21 22
AR*MS AR*MS AR*OES/MS AR*MS AR*MS AR*MS
0.5g 40g 0.25g 0.5g 0.4g 01g
0.54 0.43 0.59 0.60 0.50 0.54
0.56 0.42 0.63 0.60 0.60 0.52
0.55 0.45 0.61 0.70 0.60 0.54
0.65 0.45 0.57 0.50 0.60 0.52
0.56 0.47 0.67 0.50 0.60 0.56
0.52 0.47 0.63 0.60 0.60 0.54
0.56 0.45 0.62 0.58 0.58 0.54
0.56 0.45 0.62 0.60 0.60 0.54
0.045 0.020 0.035 0.075 0.041 0.015
7.99% 4.55% 5.68% 12.90% 7.00% 2.81%
-0.91% -21.14% 8.48% 2.61% 2.61% -5.60%
0.54 1.95 0.48 0.00 0.00 0.67

09 11 13 14 16 17 19 20 21
AR*OES AR*OES AR*OES/MS AR*MS AR*MS AR*OES AR*OES/MS AR*MS AR*MS
10g 01g 20g 0.5g 40g 01g 0.25g 0.5g 0.4g
< 10 < 100 4.67 4.58 5.18 < 20 4.80 4.10 4.38
< 10 < 100 4.59 4.45 5.02 < 20 5.00 4.10 4.39
< 10 < 100 4.42 4.64 5.17 < 20 4.60 4.30 4.31
< 10 < 100 4.43 4.50 5.03 < 20 4.80 4.20 4.37
< 10 < 100 4.47 4.65 5.17 < 20 4.90 4.10 4.30
< 10 < 100 4.43 4.56 5.12 < 20 4.70 4.00 4.46
4.50 4.56 5.12 4.80 4.13 4.37
4.45 4.57 5.15 4.80 4.10 4.38
0.104 0.078 0.073 0.141 0.103 0.058
2.30% 1.71% 1.42% 2.95% 2.50% 1.34%
-4.61% -3.25% 8.45% 1.77% -12.37% -7.39%
NA NA 0.68 0.53 0.75 NA 0.02 1.52 0.98

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
0.030 0.046 < 0.05 0.061 0.034 0.030 0.045 0.030 0.040
0.030 0.044 < 0.05 0.062 0.033 0.030 0.047 0.030 0.040
0.030 0.044 < 0.05 0.060 0.034 0.030 0.049 0.030 0.040
0.030 0.046 < 0.05 0.060 0.031 0.030 0.046 0.030 0.040
0.030 0.046 < 0.05 0.061 0.032 0.030 0.047 0.030 0.040
0.020 0.046 < 0.05 0.060 0.033 0.030 0.044 0.030 0.040
0.028 0.045 0.061 0.033 0.030 0.046 0.030 0.040
0.030 0.046 0.061 0.033 0.030 0.046 0.030 0.040
0.004 0.001 0.001 0.001 0.000 0.002 0.000 0.000
14.41% 2.00% 0.97% 3.53% 0.00% 3.63% 0.00% 0.00%
0.22 0.90 NA 1.91 0.08 0.11 0.96 0.11 0.55

10 11 13 14 15 16 17 19 20
AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*MS AR*OES AR*OES/MS AR*MS
40g 01g 20g 0.5g 0.5g 40g 01g 0.25g 0.5g
<5 < 50 0.25 0.27 < 10 0.22 < 10 0.27 0.20
<5 < 50 0.23 0.26 < 10 0.21 < 10 0.26 0.20
<5 < 50 0.23 0.27 < 10 0.22 < 10 0.25 0.30
<5 < 50 0.23 0.27 < 10 0.22 < 10 0.26 0.30
<5 < 50 0.24 0.27 < 10 0.23 < 10 0.27 0.20
<5 < 50 0.24 0.27 < 10 0.23 < 10 0.25 0.30
0.24 0.27 0.22 0.26 0.25
0.23 0.27 0.22 0.26 0.25
0.007 0.004 0.008 0.009 0.055
2.96% 1.52% 3.40% 3.44% 21.91%
-7.95% 4.45% -13.72% 1.20% -2.69%
NA NA 0.50 0.67 NA 1.04 NA 0.37 0.00
09 11 13 14 16 17 19 21 22
AR*OES AR*OES AR*OES/MS AR*MS AR*MS AR*OES AR*OES/MS AR*MS AR*MS
10g 01g 20g 0.5g 40g 01g 0.25g 0.4g 01g
< 10 < 50 1.48 1.34 1.52 < 10 1.44 1.49 1.28
< 10 < 50 1.47 1.34 1.47 < 10 1.50 1.48 1.38
< 10 < 50 1.43 1.38 1.53 < 10 1.45 1.45 1.32
< 10 < 50 1.39 1.30 1.48 < 10 1.49 1.48 1.32
< 10 < 50 1.42 1.34 1.51 < 10 1.46 1.46 1.32
< 10 < 50 1.40 1.36 1.51 < 10 1.43 1.50 1.32
1.43 1.34 1.50 1.46 1.48 1.32
1.42 1.34 1.51 1.46 1.48 1.32
0.035 0.027 0.023 0.028 0.019 0.032
2.47% 1.98% 1.56% 1.91% 1.26% 2.42%
-0.23% -6.38% 4.77% 1.87% 2.91% -7.77%
NA NA 0.11 0.77 0.42 NA 0.11 0.22 1.01

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
21.0 17.0 18.0 17.7 16.0 13.0 18.0 15.0 15.0
21.0 16.0 15.0 17.8 16.0 13.0 17.0 15.0 15.0
21.0 17.0 16.0 17.2 16.0 13.0 17.0 15.0 14.0
21.0 17.0 17.0 18.0 15.0 13.0 17.0 15.0 15.0
22.0 17.0 16.0 18.2 16.0 13.0 17.0 14.0 15.0
22.0 17.0 16.0 17.8 16.0 13.0 17.0 15.0 15.0
21.3 16.8 16.3 17.8 15.8 13.0 17.2 14.8 14.8
21.0 17.0 16.0 17.8 16.0 13.0 17.0 15.0 15.0
0.516 0.408 1.033 0.352 0.408 0.000 0.408 0.408 0.408
2.42% 2.43% 6.32% 1.98% 2.58% 0.00% 2.38% 2.75% 2.75%
35.04% 6.56% 3.39% 12.58% 0.23% -17.71% 8.67% -6.10% -6.10%
3.23 0.63 0.34 1.18 0.05 1.59 0.82 0.53 0.53

09 10 11 13 14 15 16 17 19
10g 40g 01g 20g 0.5g 0.5g 40g 01g 0.25g
< 10 <2 < 50 2.68 2.56 <5 2.50 < 10 2.80
< 10 <2 < 50 2.58 2.55 <5 2.80 < 10 2.90
< 10 <2 < 50 2.59 2.69 <5 2.70 < 10 2.70
< 10 <2 < 50 2.58 2.53 <5 2.80 < 10 2.70
< 10 <2 < 50 2.54 2.64 <5 2.80 < 10 2.90
< 10 <2 < 50 2.70 2.61 <5 2.60 < 10 2.80
2.61 2.60 2.70 2.80
2.59 2.59 2.75 2.80
0.063 0.061 0.126 0.089
2.41% 2.36% 4.68% 3.19%
-0.27% -0.87% 3.07% 6.89%
NA NA NA 0.04 0.01 NA 0.34 NA 0.67
Lab Lab Lab Lab Lab

15 16 19 21 22
AR*OES AR*MS AR*OES/MS AR*MS AR*MS
0.5g 40g 0.25g 0.4g 01g
7.00 8.52 7.90 5.24 7.91
7.00 8.36 7.97 5.32 8.08
7.00 8.76 8.05 5.59 7.69
7.00 8.63 7.97 5.48 7.52
7.00 8.80 8.17 5.52 7.78
7.00 8.77 7.83 5.73 7.80
7.00 8.64 7.98 5.48 7.80
7.00 8.70 7.97 5.50 7.79
0.000 0.173 0.118 0.179 0.190
0.00% 2.00% 1.48% 3.26% 2.44%
-5.77% 16.30% 7.44% -26.24% 4.95%
0.75 0.81 0.19 2.20 0.01
Lab Lab
21 22
AR*MS AR*MS
0.4g 01g
0.80 0.69
0.80 0.73
0.80 0.69
0.80 0.71
0.80 0.72
0.80 0.71
0.80 0.71
0.80 0.71
0.000 0.016
0.00% 2.26%
0.14% -11.33%
0.00 5.14

08 09 10 11 13 14 15 16 17
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*MS AR*OES AR*OES AR*OES
01g 10g 40g 01g 20g 0.5g 0.5g 40g 01g
1.03 > 10000 0.96 1.34 0.96 1.02 0.80 1.04 0.96
1.02 0.99 0.97 1.04 0.97 1.02 0.79 1.01 0.96
1.04 0.99 0.96 1.00 0.97 1.03 0.80 1.05 0.97
1.03 -- 0.97 1.01 0.97 0.97 0.79 1.01 0.99
1.03 0.99 0.97 1.02 0.97 1.03 0.78 1.01 0.95
1.02 1.00 0.97 1.01 0.96 1.00 0.79 1.03 0.98
1.03 0.99 0.96 1.07 0.97 1.01 0.79 1.03 0.97
1.03 0.99 0.97 1.02 0.97 1.02 0.79 1.02 0.96
0.008 0.004 0.005 0.133 0.002 0.023 0.007 0.018 0.014
0.73% 0.36% 0.54% 12.45% 0.22% 2.23% 0.89% 1.72% 1.50%
1.35% -2.38% -4.97% 5.42% -4.81% -0.46% -22.27% 1.02% -4.60%
0.25 0.71 1.37 0.07 1.33 0.00 5.82 0.17 1.28
Lab Lab Lab Lab Lab

15 16 19 21 22
AR*OES AR*MS AR*OES/MS AR*OES AR*MS
0.5g 40g 0.25g 0.4g 01g
51 49 48 45 54
51 50 51 46 55
50 51 48 46 54
50 49 49 43 53
50 51 51 42 53
49 50 48 42 54
50 50 49 44 54
50 50 49 44 54
0.9 0.6 1.2 1.9 0.8
1.76% 1.22% 2.39% 4.26% 1.40%
-1.21% -1.14% -2.50% -13.43% 6.72%
0.14 0.13 0.33 1.94 1.02
19 20 21 22 23 24 25
AR*OES AR*MS AR*OES AR*MS AR*OES AR*OES AR*OES
0.25g 0.5g 0.4g 01g 01g 0.5g 01g
22.0 22.3 18.0 21.6 21.0 19.3 21.0
21.0 21.2 18.6 21.4 21.0 20.4 21.0
21.0 21.7 20.3 20.9 20.0 21.1 22.0
22.0 21.5 19.2 20.4 21.0 23.5 22.0
21.0 21.0 17.2 21.3 20.0 20.8 21.0
20.0 21.1 18.0 21.3 20.0 21.1 21.0
21.2 21.5 18.6 21.2 20.5 21.0 21.3
21.0 21.4 18.3 21.3 20.5 21.0 21.0
0.753 0.484 1.088 0.432 0.548 1.382 0.516
3.56% 2.26% 5.86% 2.04% 2.67% 6.57% 2.42%
3.64% 5.11% -9.17% 3.56% 0.38% 2.99% 4.46%
0.53 0.80 1.82 0.65 0.07 0.41 0.68

20 21 22 23 24 25
AR*MS AR*OES AR*OES AR*OES AR*OES AR*OES
0.5g 0.4g 01g 01g 0.5g 01g
1.81 1.94 1.76 1.73 1.61 2.08
1.75 1.91 1.78 1.74 1.78 2.09
1.83 1.92 1.76 1.75 2.04 2.07
1.77 1.90 1.75 1.80 2.03 2.06
1.77 1.90 1.76 1.71 1.80 1.83
1.73 1.91 1.75 1.80 1.79 2.03
1.78 1.91 1.76 1.76 1.84 2.03
1.77 1.91 1.76 1.75 1.80 2.07
0.037 0.015 0.011 0.037 0.165 0.099
2.10% 0.79% 0.62% 2.12% 8.98% 4.86%
-1.43% 6.16% -2.35% -2.63% 2.18% 12.45%
0.33 1.58 0.56 0.63 0.58 3.71

20 21 22 23 24 25
AR*MS AR*MS AR*MS AR*OES AR*OES AR*OES
0.5g 0.4g 01g 01g 0.5g 01g
77 79 82 70 78 60
73 79 81 90 84 80
76 74 80 80 81 60
73 74 80 80 94 50
75 77 82 90 85 60
72 76 83 80 85 60
74 77 81 82 85 62
74 77 82 80 85 60
1.9 2.3 1.2 7.5 5.4 9.8
2.61% 2.95% 1.53% 9.22% 6.38% 15.94%
-1.73% 1.02% 7.45% 7.85% 11.59% -18.56%
0.01 0.32 1.10 1.15 1.61 2.65
Lab Lab Lab

22 23 25
AR*MS AR*MS AR*MS
40g 25g 25g
0.838 0.790 0.760
0.823 0.680 0.790
0.799 0.810 0.760
0.823 0.830 0.740
0.826 0.790 0.780
0.804 0.760 0.780
0.819 0.777 0.768

0.823 0.790 0.770
0.015 0.053 0.018
1.78% 6.80% 2.39%
2.78% -2.51% -3.56%
0.67 0.21 0.35
Lab Lab Lab Lab
20 23 24 25
AR*MS AR*OES AR*OES AR*OES
0.5g 01g 0.5g 01g
36 220 11 300
54 220 8 300
49 220 46 290
43 230 40 290
55 210 7 230
53 230 7 290
48 222 20 283
51 220 10 290
7 8 18 27
15.46% 3.40% 91.28% 9.38%
-79.92% -7.92% -91.76% 17.69%
0.52 0.90 0.75 1.49
Lab
25
AR*OES
01g
<5
<5
<5
<5
<5
<5
NA

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
18.5 17.6 17.3 20.0 12.0 20.0
18.2 17.4 17.4 20.0 15.0 20.0
19.0 16.1 17.4 30.0 12.0 20.0
18.5 16.4 17.9 20.0 12.0 20.0
18.3 17.2 17.9 20.0 15.0 20.0
17.7 17.4 17.7 30.0 12.0 10.0
18.4 17.0 17.6 23.3 13.0 18.3
18.4 17.3 17.5 20.0 12.0 20.0
0.4 0.6 0.3 5.2 1.5 4.1
2.33% 3.61% 1.52% 22.13% 11.92% 22.27%
8.92% 0.91% 4.37% 38.37% -22.91% 8.72%
0.45 0.29 0.03 3.19 2.50 0.44

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
1.03 1.09 1.17 1.11 0.99 1.16
1.03 1.05 1.17 1.10 1.06 1.17
1.02 1.05 1.16 1.12 1.14 1.17
1.01 1.05 1.16 1.11 1.15 1.16
1.01 1.06 1.17 1.09 1.06 1.13
1.04 1.05 1.16 1.16 1.08 1.15
1.02 1.06 1.17 1.12 1.08 1.16
1.03 1.05 1.17 1.11 1.07 1.16
0.012 0.016 0.005 0.024 0.059 0.015
1.18% 1.51% 0.47% 2.18% 5.46% 1.30%
-5.99% -2.77% 7.03% 2.43% -0.78% 6.26%
1.05 0.67 0.81 0.03 0.31 0.70

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
54 56 56 52 52 55
54 56 55 51 59 55
57 54 53 52 60 56
56 55 51 54 60 55
56 53 52 51 60 55
54 54 54 53 60 54
55 54 53 52 58 55
55 54 53 52 60 55
1.2 1.1 1.8 1.2 3.2 0.6
2.15% 2.08% 3.43% 2.24% 5.46% 1.15%
4.76% 3.84% 1.49% -0.58% 11.40% 4.82%
0.67 0.56 0.26 0.00 1.82 0.68

20 21 22 23 24 25
AR*MS AR*MS AR*OES AR*OES AR*OES AR*OES
0.5g 0.4g 01g 01g 0.5g 01g
207 214 220 210 210 225
202 219 219 215 220 229
206 218 218 213 219 227
200 219 219 219 254 231
204 219 221 206 224 224
200 224 216 219 226 228
203 219 219 214 226 227
203 219 219 214 222 228
3 3 2 5 15 3
1.55% 1.46% 0.79% 2.40% 6.66% 1.14%
-5.86% 1.41% 1.41% -0.98% 4.50% 5.35%
0.88 0.21 0.21 0.15 0.27 0.80

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
16.0 20.0 20.0 20.0 14.0 23.0
15.0 19.0 20.0 20.0 19.0 22.0
17.0 19.0 20.0 23.0 25.0 20.0
19.0 19.0 20.0 22.0 20.0 21.0
16.0 18.0 15.0 19.0 18.0 23.0
30.0 19.0 15.0 25.0 18.0 20.0
18.8 19.0 18.3 21.5 19.0 21.5
16.5 19.0 20.0 21.0 18.5 21.5
5.6 0.6 2.6 2.3 3.6 1.4
29.93% 3.33% 14.08% 10.50% 18.83% 6.41%
-2.97% -2.11% -5.55% 10.77% -2.11% 10.77%
1.84 0.22 0.67 1.46 0.22 1.46

20 21 22 23 24 25
AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES
01g 0.4g 01g 01g 01g 01g
1.77 > 5000 1.69 1.63 1.64 1.70
1.72 > 5000 1.65 1.70 1.75 1.68
1.75 > 5000 1.62 1.65 1.76 1.77
1.83 > 5000 1.67 1.63 1.85 1.78
1.88 > 5000 1.71 1.59 1.78 1.72
1.79 > 5000 1.64 1.66 1.78 1.73
1.79 1.66 1.64 1.76 1.73
1.78 1.66 1.64 1.77 1.73
0.060 0.033 0.037 0.070 0.038
3.35% 2.00% 2.25% 3.99% 2.20%
3.83% -3.54% -4.80% 2.13% 0.28%
1.39 NA 1.31 1.77 1.30 0.09
20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
13.51 13.00 13.90 12.30 13.37 12.95
12.83 13.00 13.90 12.55 12.68 12.95
13.47 13.10 13.70 12.45 13.89 13.05
13.04 12.90 13.80 12.80 15.22 13.15
12.97 13.00 14.10 12.20 12.85 12.65
12.58 13.10 13.70 12.65 12.92 12.90
13.07 13.02 13.85 12.49 13.49 12.94
13.00 13.00 13.85 12.50 13.15 12.95
0.364 0.075 0.152 0.222 0.955 0.169
2.78% 0.58% 1.10% 1.78% 7.08% 1.30%
0.42% 0.04% 6.44% -4.00% 3.66% -0.54%
0.03 0.06 1.39 0.97 0.16 0.19
Lab Lab Lab Lab

22 23 24 25
01g 01g 0.5g 01g
12.4 < 50 21.0 < 50
12.6 < 50 20.0 < 50
12.4 < 50 28.0 < 50
11.8 < 50 59.0 < 50
12.4 < 50 <5 < 50
12.6 < 50 7.0 < 50
12.4 27.0
12.4 21.0
0.294 19.429
2.38% 71.96%
3.87% 126.78%
0.12 NA 5.02 NA
Lab Lab
24 25
AR*OES AR*OES
0.5g 01g
<1 <5
<1 <5
<1 <5
<1 <5
<1 <5
1.00 <5
1.00
1.00
20.56%
1.16 NA
20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
0.140 0.165 0.160 0.190 0.120 0.300
0.140 0.165 0.160 0.190 0.140 0.290
0.140 0.166 0.150 0.200 0.180 0.280
0.140 0.162 0.160 0.200 0.180 0.280
0.140 0.165 0.150 0.190 0.140 0.200
0.140 0.166 0.150 0.210 0.140 0.280
0.140 0.165 0.155 0.197 0.150 0.272
0.140 0.165 0.155 0.195 0.140 0.280
0.000 0.001 0.005 0.008 0.024 0.036
0.00% 0.89% 3.53% 4.15% 16.33% 13.25%
-20.11% -5.93% -11.55% 12.23% -14.40% 55.03%
0.96 0.25 0.53 0.67 0.67 3.26

20 21 22 23 24 25
AR*MS AR*OES AR*MS AR*OES AR*OES AR*OES
0.5g 0.4g 01g 01g 0.5g 01g
17.0 17.9 18.4 < 50 15.0 < 50
16.0 16.2 18.8 < 50 15.0 < 50
16.0 16.2 18.3 < 50 17.0 < 50
16.0 17.1 18.2 < 50 16.0 < 50
16.0 17.6 18.5 < 50 15.0 < 50
16.0 17.1 18.8 < 50 15.0 < 50
16.2 17.0 18.5 15.5
16.0 17.1 18.5 15.0
0.4 0.7 0.3 0.8
2.53% 4.13% 1.37% 5.40%
-9.53% -4.78% 3.52% -13.26%
0.44 0.15 0.37 NA 0.67 NA
20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
1.15 1.05 1.21 0.98 1.09 1.10
1.11 1.03 1.21 0.99 1.16 1.10
1.14 1.04 1.21 1.00 1.26 1.11
1.13 1.04 1.21 1.02 1.28 1.11
1.12 1.01 1.19 0.97 1.17 1.06
1.07 1.00 1.19 1.01 1.19 1.09
1.12 1.03 1.20 1.00 1.19 1.10
1.13 1.04 1.21 0.99 1.18 1.10
0.028 0.019 0.010 0.019 0.070 0.019
2.53% 1.89% 0.86% 1.88% 5.85% 1.71%
0.98% -7.28% 8.49% -10.29% 7.44% -1.27%
0.28 1.16 1.59 1.68 1.41 0.00

20 21 22 23 24 25
AR*MS AR*MS AR*OES AR*OES AR*OES AR*OES
0.5g 0.4g 01g 01g 0.5g 01g
0.056 0.055 0.060 0.054 0.052 0.061
0.055 0.054 0.059 0.054 0.059 0.061
0.056 0.056 0.061 0.055 0.062 0.060
0.055 0.053 0.059 0.054 0.062 0.059
0.055 0.051 0.059 0.054 0.056 0.059
0.054 0.054 0.060 0.057 0.057 0.058
0.055 0.054 0.060 0.055 0.058 0.060
0.055 0.054 0.059 0.054 0.058 0.060
0.001 0.002 0.001 0.001 0.004 0.001
1.54% 3.08% 1.03% 2.22% 6.44% 2.03%
-3.25% -5.62% 4.57% -3.93% 1.76% 4.86%
0.67 1.11 0.75 0.95 0.24 0.81

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
9.20 8.10 10.70 7.00 8.00 8.00
7.40 8.30 10.60 8.00 8.00 7.00
8.60 7.60 10.60 7.00 7.00 8.00
8.30 7.60 9.70 7.00 8.00 6.00
8.60 8.60 10.50 7.00 8.00 7.00
8.10 8.00 10.20 7.00 8.00 6.00
8.37 8.03 10.38 7.17 7.83 7.00
8.45 8.05 10.55 7.00 8.00 7.00
0.602 0.393 0.376 0.408 0.408 0.894
7.20% 4.90% 3.62% 5.70% 5.21% 12.78%
-0.10% -4.08% 23.98% -14.43% -6.47% -16.42%
0.09 0.18 1.84 0.88 0.34 1.01

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
0.055 0.068 0.070 0.050 0.050 0.100
0.054 0.068 0.060 0.060 0.060 0.100
0.054 0.068 0.060 0.060 0.080 0.100
0.054 0.067 0.060 0.070 0.080 0.090
0.054 0.068 0.060 0.050 0.060 0.080
0.052 0.067 0.060 0.060 0.060 0.100
0.054 0.067 0.062 0.058 0.065 0.095
0.054 0.068 0.060 0.060 0.060 0.100
0.001 0.001 0.004 0.008 0.012 0.008
1.83% 0.77% 6.62% 12.90% 18.84% 8.81%
-20.89% -1.05% -9.38% -14.27% -4.48% 39.61%
1.27 0.03 0.51 0.83 0.19 2.70

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
14.7 14.0 18.0 14.0 13.0 16.0
14.2 14.0 17.0 14.0 16.0 23.0
14.9 15.0 19.0 19.0 18.0 15.0
15.4 14.0 19.0 20.0 17.0 16.0
14.4 13.0 18.0 17.0 16.0 15.0
21.0 14.0 19.0 17.0 16.0 16.0
15.8 14.0 18.3 16.8 16.0 16.8
14.8 14.0 18.5 17.0 16.0 16.0
2.6 0.6 0.8 2.5 1.7 3.1
16.47% 4.52% 4.45% 14.75% 10.46% 18.18%
0.91% -10.40% 17.34% 7.74% 2.40% 7.74%
0.60 1.06 1.75 0.77 0.23 0.03
Lab Lab Lab Lab Lab

21 22 23 24 25
AR*OES AR*OES AR*OES AR*OES AR*OES
0.4g 01g 01g 0.5g 01g
0.043 0.042 0.038 0.034 0.041
0.042 0.042 0.040 0.037 0.041
0.042 0.040 0.040 0.041 0.041
0.041 0.042 0.040 0.043 0.042
0.042 0.042 0.039 0.038 0.033
0.041 0.042 0.039 0.039 0.041
0.042 0.042 0.039 0.039 0.040
0.042 0.042 0.040 0.039 0.041
0.001 0.001 0.001 0.003 0.003
1.77% 1.96% 2.08% 8.12% 8.46%
4.60% 4.81% -1.06% -2.73% 0.20%
0.67 0.71 0.28 0.57 0.51

19 20 21 22 23 24 25
AR*OES/MS AR*OES AR*OES AR*MS AR*OES AR*OES AR*OES
0.25g 01g 0.4g 01g 01g 0.5g 01g
0.272 0.250 0.267 0.229 0.243 0.240 0.257
0.268 0.250 0.253 0.228 0.246 0.251 0.258
0.269 0.250 0.249 0.221 0.246 0.273 0.256
0.273 0.250 0.256 0.222 0.251 0.271 0.255
0.275 0.250 0.258 0.222 0.239 0.252 0.251
0.276 0.250 0.255 0.227 0.249 0.254 0.249
0.272 0.250 0.256 0.225 0.246 0.257 0.254
0.272 0.250 0.256 0.225 0.246 0.253 0.256
0.003 0.000 0.006 0.004 0.004 0.013 0.004
1.20% 0.00% 2.36% 1.58% 1.74% 5.00% 1.40%
8.23% -0.63% 1.89% -10.64% -2.35% 2.05% 1.09%
2.34 0.01 0.67 2.62 0.44 0.71 0.46
Lab Lab Lab Lab
22 23 24 25
AR*OES AR*OES AR*OES AR*OES
01g 01g 0.5g 01g
8.76 8.62 7.38 9.20
8.77 8.91 8.00 9.20
8.60 8.75 7.49 9.34
8.43 8.99 8.62 9.43
8.61 8.53 8.00 9.21
8.38 8.83 8.10 9.18
8.59 8.77 7.93 9.26
8.61 8.79 8.00 9.21
0.162 0.174 0.450 0.101
1.89% 1.99% 5.67% 1.09%
-1.77% 0.29% -9.32% 5.87%
0.10 0.10 0.83 0.64
Lab
24
AR*OES
0.5g
18.0
14.0
27.0
27.0
15.0
16.0
19.5
17.0
6.0
30.55%
-3.39%
0.14

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
4.30 4.70 4.00 <5 6.00 5.00
4.30 4.50 4.00 <5 5.00 5.00
4.30 4.10 4.00 <5 6.00 5.00
4.10 4.50 4.00 5.00 6.00 5.00
4.60 5.10 4.00 <5 5.00 5.00
4.20 4.90 4.00 5.00 5.00 5.00
4.30 4.63 4.00 5.00 5.50 5.00
4.30 4.60 4.00 5.00 5.50 5.00
0.167 0.350 0.000 0.000 0.548 0.000
3.89% 7.56% 0.00% 0.00% 9.96% 0.00%
-7.12% 0.08% -13.60% 8.00% 18.80% 8.00%
0.75 0.11 1.33 0.59 1.56 0.59
20 21 22 23 24 25
AR*MS AR*OES AR*MS AR*OES AR*OES AR*OES
0.5g 0.4g 01g 01g 0.5g 01g
12.0 16.8 13.5 15.0 12.0 17.0
12.0 16.4 13.8 14.0 14.0 18.0
13.0 16.8 13.2 15.0 16.0 18.0
12.0 16.9 13.3 17.0 16.0 14.0
12.0 17.1 13.1 15.0 14.0 12.0
12.0 17.2 13.5 16.0 14.0 21.0
12.2 16.9 13.4 15.3 14.3 16.7
12.0 16.9 13.4 15.0 14.0 17.5
0.4 0.3 0.3 1.0 1.5 3.2
3.36% 1.66% 1.89% 6.74% 10.50% 19.22%
-14.24% 18.89% -5.55% 8.08% 1.03% 17.48%
1.57 1.83 0.67 0.72 0.00 1.06
Lab Lab Lab Lab
22 23 24 25
01g 01g 0.5g 01g
4.28 < 100 7.00 < 100
4.96 < 100 7.00 < 100
4.76 < 100 7.00 < 100
4.68 < 100 8.00 < 100
4.74 < 100 8.00 < 100
4.78 < 100 8.00 < 100
4.70 7.50
4.75 7.50
0.226 0.548
4.81% 7.30%
-0.35% 59.01%
0.02 NA 6.25 NA

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
0.016 0.031 0.035 < 0.05 0.018 0.060
0.016 0.030 0.035 < 0.05 0.022 0.060
0.017 0.030 0.030 < 0.05 0.021 0.060
0.016 0.031 0.030 < 0.05 0.020 0.060
0.017 0.031 0.030 < 0.05 0.022 0.050
0.016 0.032 0.030 < 0.05 0.022 0.050
0.016 0.031 0.032 0.021 0.057
0.016 0.031 0.030 0.022 0.060
0.001 0.001 0.003 0.002 0.005
3.16% 2.45% 8.15% 7.69% 9.11%
1.01 0.07 0.00 NA 0.67 1.64
Lab Lab Lab Lab Lab

21 22 23 24 25
AR*MS AR*MS AR*OES AR*OES AR*OES
0.4g 01g 01g 0.5g 01g
0.30 0.25 < 50 <5 < 50
0.30 0.29 < 50 <5 < 50
0.30 0.23 < 50 <5 < 50
0.30 0.24 < 50 <5 < 50
0.30 0.24 < 50 <5 < 50
0.30 0.25 < 50 <5 < 50
0.30 0.25
0.30 0.25
0.000 0.021
0.00% 8.39%
16.77% -2.69%
1.84 0.29 NA NA NA
Lab Lab
23 25
AR*OES AR*OES
01g 01g
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
< 50 < 50
NA NA
Lab Lab Lab Lab Lab

20 21 23 24 25
AR*MS AR*OES AR*OES AR*OES AR*OES
0.5g 0.4g 01g 0.5g 01g
16.0 14.0 14.0 13.0 21.0
15.0 14.0 15.0 14.0 18.0
16.0 15.0 15.0 15.0 19.0
16.0 14.0 15.0 15.0 21.0
16.0 14.0 16.0 14.0 16.0
15.0 14.0 17.0 14.0 19.0
15.7 14.2 15.3 14.2 19.0
16.0 14.0 15.0 14.0 19.0
0.516 0.408 1.033 0.753 1.897
3.30% 2.88% 6.74% 5.31% 9.99%
-0.83% -10.32% -2.94% -10.32% 20.27%
0.05 0.92 0.24 0.92 1.30

20 21 22 23 24 25
0.5g 0.4g 01g 01g 0.5g 01g
2.00 1.70 3.00 < 50 <2 < 50
2.20 1.80 3.00 < 50 <2 < 50
1.90 1.60 2.90 < 50 <2 < 50
1.90 1.80 2.90 < 50 <2 < 50
2.00 1.80 3.00 < 50 <2 < 50
2.00 1.80 3.00 < 50 <2 < 50
2.00 1.75 2.97
2.00 1.80 3.00
0.110 0.084 0.052
5.48% 4.78% 1.74%
-23.65% -33.19% 13.25%
2.02 2.76 1.24 NA NA NA

19 20 21 22 23 24 25
AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES AR*OES
0.25g 01g 0.4g 01g 01g 01g 01g
1.04 1.05 > 5000 1.00 1.00 1.00 1.06
1.02 1.04 > 5000 1.00 0.99 1.06 1.07
1.02 1.05 > 5000 0.99 1.00 1.09 1.07
1.06 1.04 > 5000 1.00 1.00 1.06 1.06
1.06 1.04 > 5000 0.99 0.98 1.09 1.03
1.07 1.05 > 5000 0.99 1.04 1.04 1.04
1.05 1.05 1.00 1.00 1.06 1.05
1.05 1.05 0.99 1.00 1.06 1.06
0.020 0.005 0.003 0.020 0.034 0.014
1.95% 0.52% 0.34% 2.03% 3.20% 1.33%
3.04% 2.99% -1.92% -1.59% 4.14% 3.65%
0.69 0.67 NA 0.59 0.50 0.97 0.84
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
20.4
109.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.80
110.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
76
111
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.797
112.000
Certified
1.00
ppm
1.00
1.00
1.0
5.0
16.0
< 10
113.0
Indicative
1.00
ppm
0.00
0.00
1
14
16
241
27
Certified
1.00
ppm
2.00
2.00
1.00
6.00
16.00
0.37
114.00
Certified
1.00
ppm
1.00
1.00
1.0
19.0
16.0
16.9
115.0
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.09
116.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
52
117
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
36.4
118.0
Certified
1.00
ppm
0.00
0.00
1
19
16
216
119
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
19.4
120.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.75
121.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.72
122.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
1.78
28.00
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
0.88
29.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
0.92
30.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
13.01
123.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
11.9
124.0
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
2.75
31.00
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
0.22
27.00
Certified
1.00
ppm
2.00
2.00
1.00
5.00
16.00
1.32
125.00
Certified
1.00
ppm
2.00
2.00
1.00
15.00
16.00
0.83
126.00
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
0.32
28.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.94
127.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.175
128.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
17.9
129.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
10.0
130.0
Certified
1.00
ppm
2.00
3.00
1.00
7.00
16.00
0.12
131.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.11
132.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.057
133.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
8.38
134.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.068
135.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
<1
136.00
Indicative
1.00
ppm
1.00
1.00
1.0
17.0
16.0
16.0
29.0
Certified
1.00
ppm
1.00
1.00
1.0
19.0
16.0
15.6
137.0
Certified
1.00
wt.%
3.00
3.00
1.000
8.000
16.000
0.040
138.000
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.252
139.000
Indicative
1.00
ppb
0.00
0.00
1
1
16
< 10
30
Indicative
1.00
ppm
2.00
2.00
1.00
25.00
16.00
4.33
31.00
Indicative
1.00
ppb
0.00
0.00
1
1
16
<5
27
Indicative
1.00
ppm
2.00
2.00
1.00
22.00
16.00
8.08
28.00
Indicative
1.00
ppm
3.00
3.00
1.000
9.000
16.000
< 0.05
29.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
8.75
140.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
20.2
141.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
4.63
142.00
Certified
1.00
ppm
1.00
1.00
1.0
10.0
16.0
18.6
143.0
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
3.35
30.00
Certified
1.00
ppm
2.00
3.00
1.00
5.00
16.00
4.07
144.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
14.2
145.0
Certified
1.00
ppm
3.00
3.00
1.000
6.000
16.000
< 0.05
146.000
Certified
1.00
ppm
2.00
3.00
1.00
7.00
16.00
0.34
147.00
Certified
1.00
ppm
2.00
2.00
1.00
8.00
16.00
0.57
148.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
4.72
149.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
< 0.06
150.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.26
151.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
0.14
31.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.43
152.00
Certified
1.00
ppm
1.00
2.00
1.0
10.0
16.0
15.8
153.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
2.62
154.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
7.43
155.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.80
156.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.01
157.00
Certified
1.00
ppm
0.00
1.00
1
11
16
50
158
Certified
Ag, Silver (ppm) 20.6 0.67 20.2 21.0 19.6 21.6
As, Arsenic (ppm) 79 10 71 86 75 82
Cu, Copper (wt.%) 1.74 0.042 1.73 1.75 1.68 1.80
Fe, Iron (wt.%) 13.41 0.400 13.18 13.64 13.06 13.76
Pb, Lead (wt.%) 0.251 0.007 0.247 0.255 0.245 0.257
Zn, Zinc (wt.%) 1.02 0.043 0.99 1.05 0.99 1.05
Ag, Silver (ppm) 20.4 1.15 20.0 20.9 19.8 21.0
Al, Aluminium (wt.%) 1.80 0.091 1.76 1.84 1.75 1.85
As, Arsenic (ppm) 76 6.8 73 78 73 78
Au, Gold (ppm) 0.797 0.038 0.778 0.816 0.783 0.810
B, Boron (ppm) < 10 IND IND IND IND IND
Bi, Bismuth (ppm) 16.9 2.4 16.0 17.7 16.1 17.6
Ca, Calcium (wt.%) 1.09 0.060 1.06 1.12 1.07 1.11
Cd, Cadmium (ppm) 52 3.7 51 54 51 54
Ce, Cerium (ppm) 36.4 5.2 32.8 40.0 35.3 37.5
Co, Cobalt (ppm) 216 11 211 221 211 221
Cr, Chromium (ppm) 19.4 2.1 18.7 20.1 18.4 20.4
Cs, Cesium (ppm) 0.75 0.13 0.65 0.86 0.72 0.79
Cu, Copper (wt.%) 1.72 0.066 1.70 1.75 1.68 1.77
Fe, Iron (wt.%) 13.01 0.546 12.78 13.25 12.75 13.28
Ga, Gallium (ppm) 11.9 1.03 11.2 12.6 11.5 12.3
Hf, Hafnium (ppm) 1.32 0.21 1.15 1.48 1.24 1.40
Hg, Mercury (ppm) 0.83 0.08 0.77 0.89 0.79 0.87
In, Indium (ppm) 1.94 0.107 1.85 2.03 1.84 2.04
K, Potassium (wt.%) 0.175 0.027 0.163 0.188 0.170 0.181
La, Lanthanum (ppm) 17.9 2.4 16.5 19.2 17.1 18.6
Li, Lithium (ppm) 10.0 1.1 9.2 10.9 9.5 10.5
Lu, Lutetium (ppm) 0.12 0.010 0.11 0.13 IND IND
Mg, Magnesium (wt.%) 1.11 0.070 1.08 1.14 1.08 1.14
Mn, Manganese (wt.%) 0.057 0.003 0.056 0.058 0.055 0.058
Na, Sodium (wt.%) 0.068 0.011 0.063 0.073 0.066 0.070
Nb, Niobium (ppm) <1 IND IND IND IND IND
Ni, Nickel (ppm) 15.6 1.7 14.9 16.3 14.9 16.3
P, Phosphorus (wt.%) 0.040 0.002 0.039 0.041 0.038 0.042
Pb, Lead (wt.%) 0.252 0.010 0.247 0.256 0.246 0.257
S, Sulphur (wt.%) 8.75 0.630 8.33 9.16 8.47 9.03
Sb, Antimony (ppm) 20.2 4.1 18.1 22.2 19.3 21.0
Sc, Scandium (ppm) 4.63 0.53 4.38 4.88 4.46 4.80
Se, Selenium (ppm) 18.6 1.9 17.3 19.8 16.9 20.2
Sn, Tin (ppm) 4.07 0.213 3.92 4.22 3.78 4.36
Sr, Strontium (ppm) 14.2 1.5 13.6 14.8 13.7 14.6
Ta, Tantalum (ppm) < 0.05 IND IND IND IND IND
Tb, Terbium (ppm) 0.34 0.032 0.31 0.37 0.32 0.36
Te, Tellurium (ppm) 0.57 0.08 0.53 0.61 0.51 0.63
Th, Thorium (ppm) 4.72 0.325 4.49 4.95 4.53 4.90
Ti, Titanium (wt.%) < 0.06 IND IND IND IND IND
Tl, Thallium (ppm) 0.26 0.04 0.23 0.28 0.24 0.27
U, Uranium (ppm) 1.43 0.104 1.36 1.51 1.37 1.50
V, Vanadium (ppm) 15.8 1.52 15.1 16.5 IND IND
W, Tungsten (ppm) 2.62 0.30 2.40 2.84 2.49 2.75
Y, Yttrium (ppm) 7.43 1.01 6.69 8.17 7.18 7.67
Zn, Zinc (wt.%) 1.01 0.038 1.00 1.03 1.00 1.03
Zr, Zirconium (ppm) 50 3.4 48 53 49 52
Certified
4-Acid Digestion
Ag, Silver (ppm) 20.4 1.06 19.9 20.9 19.6 21.2
Co, Cobalt (ppm) 222 10 217 226 215 228
Cu, Copper (wt.%) 1.73 0.064 1.72 1.75 1.67 1.80
Fe, Iron (wt.%) 13.42 0.778 13.09 13.76 13.11 13.73
Pb, Lead (wt.%) 0.250 0.007 0.247 0.252 0.243 0.256
Zn, Zinc (wt.%) 1.03 0.030 1.02 1.04 1.00 1.05
Ag, Silver (ppm) 20.6 0.67 20.2 21.0 19.6 21.6
Cu, Copper (wt.%) 1.74 0.042 1.73 1.75 1.68 1.80
Fe, Iron (wt.%) 13.41 0.400 13.18 13.64 13.06 13.76
Pb, Lead (wt.%) 0.251 0.007 0.247 0.255 0.245 0.257
Zn, Zinc (wt.%) 1.02 0.043 0.99 1.05 0.99 1.05
Ag, Silver (ppm) 20.4 1.15 20.0 20.9 19.8 21.0
Co, Cobalt (ppm) 216 11 211 221 211 221
Cu, Copper (wt.%) 1.72 0.066 1.70 1.75 1.68 1.77
Fe, Iron (wt.%) 13.01 0.546 12.78 13.25 12.75 13.28
Pb, Lead (wt.%) 0.252 0.010 0.247 0.256 0.246 0.257
Zn, Zinc (wt.%) 1.01 0.038 1.00 1.03 1.00 1.03

OREAS 623 Datapack

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OREAS 623 Datapack

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Table 1.

Abbreviations used for OREAS 623

Batch & Limits

3-acid (HNO3-HCIO4-HCI) digest with AAS finish

- Outlying individual values

- Outlying laboratory batch data sets and superfluous limit values

Batch & Limits

Laboratory Name and Location

Acme (BV), Santiago, Chile

- Outlying individual values

- Outlying laboratory batch data sets and superfluous limit values

Constituent Unit Value Constituent Unit Value Constituent Unit Value

Certified Absolute Standard Deviations Relative Standard Deviations 5% window

Analytical results for Pd in OREAS 623 (Indicative Value < 5 ppb)

Analytical results for Pt in OREAS 623 (Indicative Value < 5 ppb)

0.861 0.842 0.860 0.868 0.873 0.857 0.815 0.837 0.872

0.863 0.838 0.802 0.805 0.748 0.846 0.811 0.770 0.821

Analytical results for S in OREAS 623 (Certified Value 9.07 wt.%)

1 1 9.27 9.21 9.27 8.73 8.03 9.33

9.15 9.06 8.89 8.50 9.03 8.92 9.04 9.23 8.82

9.00 8.82 9.27 9.04 9.10 8.98

1 1 24.4 18.0 20.0 < 20 20.0 25.0

Analytical results for Al in OREAS 623 (Certified Value 5.25 wt.%)

1 1 5.25 5.02 5.09 4.61 5.17 5.27

Analytical results for As in OREAS 623 (Certified Value 86 ppm)

Analytical results for B in OREAS 623 (Indicative Value < 50 ppm)

1 1 < 50 < 50 < 20 20

Analytical results for Ba in OREAS 623 (Certified Value 1395 ppm)

1 1 1356 1400 1300 1277 1620 1408

Analytical results for Be in OREAS 623 (Indicative Value 1.61 ppm)

1 1 <5 <5 < 10 1.70 11.00 1.52

Analytical results for Bi in OREAS 623 (Certified Value 17.7 ppm)

1 1 18.1 17.0 20.0 10.1 15.8 18.6

Analytical results for Ca in OREAS 623 (Certified Value 1.37 wt.%)

1 1 1.38 1.40 1.38 1.94 1.31 1.37

Analytical results for Ce in OREAS 623 (Certified Value 49.9 ppm)

1 1 50.0 51.1 39.2 50.2 52.0

Analytical results for Co in OREAS 623 (Certified Value 225 ppm)

1 1 240 245 230 190 206 230

Analytical results for Cr in OREAS 623 (Certified Value 30 ppm)

1 1 32.1 20.0 < 100 30.0 46.0 30.0

Analytical results for Cs in OREAS 623 (Certified Value 3 ppm)

1 1 2.88 2.60 < 10 3.40 2.73 2.90

Analytical results for Cu in OREAS 623 (Certified Value 1.73 wt.%)

1 1 1.73 > 10000 1.79 1.87 1.65 1.68

Analytical results for Dy in OREAS 623 (Indicative Value 3.46 ppm)

1 1 3.47 3.20 3.50 3.50

Analytical results for Er in OREAS 623 (Indicative Value 1.88 ppm)

1 1 1.77 1.75 2.20 2.00

1 1 1.41 1.38 1.90 1.60

Analytical results for Fe in OREAS 623 (Certified Value 13.45 wt.%)

1 1 12.83 13.50 13.60 13.00 13.81 13.35

Analytical results for Ga in OREAS 623 (Certified Value 23.7 ppm)

1 1 23.2 27.0 20.0 < 2.5 23.3 24.0

Analytical results for Gd in OREAS 623 (Indicative Value 4.39 ppm)

1 1 4.17 4.10 5.00 4.00

Analytical results for Ge in OREAS 623 (Indicative Value 1.65 ppm)

1 1 1.63 1.00 < 10 5.38 <1

Analytical results for Hf in OREAS 623 (Indicative Value 4.51 ppm)

1 1 4.63 4.00 5.20

Analytical results for Ho in OREAS 623 (Indicative Value 0.61 ppm)

1 1 0.65 0.59 0.60 0.60

Analytical results for In in OREAS 623 (Certified Value 2.04 ppm)