APPENDIX A

ANALYSIS REPORT
 Solid Sample Analysis Report

Station
Date Sampled
Sample ID 1 2 3 4
Sample Appearance Solid Solid Solid Solid

Parameter with units

X-ray diffraction (%)
Fe3O4 25 20 25 25
FeO Not Detected Not Detected Not Detected Not Detected
a-Fe2O3 Not Detected Not Detected Not Detected Not Detected
a-FeOOH 15 15 15 15
y-FeOOH Not Detected 5 Not Detected Not Detected
FeCO3 Not Detected 5 Not Detected 15
FeS Not Detected Not Detected Not Detected Not Detected
Fe3S4 Not Detected Not Detected Not Detected Not Detected
a-Iron Not Detected Not Detected Not Detected Not Detected
a-SiO2 3 Not Detected 2 Not Detected
CaCO3 3 5 5 1
NaCl Not Detected Not Detected Not Detected Not Detected
Sulfur Not Detected 30 Not Detected Not Detected
Amorphous Balance Balance Balance Balance

Total Metals (ppm)

Chloride <4.9 16 103 57
Sulfate 54,000 43,000 3,700 44,000
Calcium 7,200 950 9,400 4,700
Chromium 160 11 98 240
Copper 190 40 150 220
Iron 110,000 17,000 65,000 20,000
Lead 170 25 8,100 160
Magnesium 660 70 230 310
Manganese 1,100 160 660 1,300
Sodium 2,100 1,500 12,000 <500
Nickel 170 15 100 110
Zinc 160 420 1 1

Bacteriology
Slime Bacteria No Growth No Growth No Growth No Growth
Fungi No Growth No Growth No Growth No Growth
Sulfate Reducing
Bacteria- 100,000 100,000 10,000 10,000
Bacteria/gram or ml of sludge
Nitrifying Bacteria None isolated None isolated None isolated None isolated
Iron-Oxidizing Bacteria None isolated None isolated None isolated None isolated
Biomass (ATP) – grams of
ATP/gram or ml of sludge < 6.3x10-11 < 2.4 x 10-10 < 2.6x10-10 < 6.3x10-11

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 Solid Sample Analysis Report

Sample ID: Date Collected:

Analyses/Method Result Rep. Limit Dil. Factor Date Analyzed Analyst Seq. #
Energy Dispersive X-Ray Spectrometry Units: %
Aluminum (Al) 0.1 0 1
Barium (Ba) ND 0 1
Bromine (Br) ND 0 1
Calcium (Ca) 0.68 0 1
Carbon (C) 28.72 0 1
Chlorine (Cl) 2.57 0 1
Chromium (Cr) ND 0 1
Iron (Fe) 17.01 0 1
Magnesium (Mg) ND 0 1
Manganese (Mn) ND 0 1
Nickel (Ni) ND 0 1
Oxygen (O) 31.71 0 1
Phosphorus (P) ND 0 1
Potassium (K) ND 0 1
Silicon (Si) ND 0 1
Sodium (Na) 1.89 0 1
Sulfur (S) 17.33 0 1
Zinc (Zn) ND 0 1

Ion Chromatography Units: mg/kg

Bromide ND 50 10
Chloride 4,580 500 100
Fluoride ND 50 10
Sulfate 57.6 50 10

Metals by Method 6010B, Total Units: mg/kg

Calcium 5,410 10 1
Chromium 110 1 1
Copper 80.2 1 1
Iron 189,000 40 20
Lead ND 500 100
Magnesium 390 10 1
Manganese 1,200 0.5 1
Nickel 30.9 2 1
Sodium 13,500 50 1
Zinc 90.6 2 1

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 Liquid Sample Analysis Report

Analyses Result RL Qual Units DF

Inorganic Anions E300.0

Bromide 600 10 H mg/L 100
Chloride 180,000 1,000 EH mg/L 5000
Fluoride ND 10 H mg/L 100
Nitrate ND 5.0 H mg/L 100
Nitrite ND 5.0 H mg/L 100
Ortho-Phosphate-P ND 100 H mg/L 100
Sulfate 210 10 H mg/L 100

Specific Gravity (Liquids, Hydrometer) ASTM-D891

Specific Gravity 1.2 0 1

Metals – Materials Science Group by ICP-OES SW6010R

Aluminum 584 0 H mg/kg 1
Barium 1,810 0 H mg/kg 1
Calcium 10,500 0 H mg/kg 1
Iron 3,400 0 H mg/kg 1
Magnesium 1,640 0 BH mg/kg 1
Manganese 20.3 0 H mg/kg 1
Phosphorus 65.1 0 H mg/kg 1
Potassium 382 0 BH mg/kg 1
Silicon 1.94 0 H mg/kg 1
Sodium 55,100 0 H mg/kg 1

Alkalinity A2320
Alkalinity, Total (as CaCO3) 780 10 H mg/L CaCO3 1

Total Dissolved Solids A2540C

Residue, Dissolved 270,000 5.0 BH mg/L 1

Qualifiers: */X Value exceeds Maximum Contaminant Level
E Value above quantitation range
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
S Spike Recovery outside accepted recovery limits
B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
RL Reporting Detection Limit

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