Professional Documents
Culture Documents
ASM Lab Record Book
ASM Lab Record Book
COLLEGE OF ENGINEERING
BENGALURU – 19
(AUTONOMOUS INSTITUTE AFFILIATED TO VTU)
RECORD BOOK
for
CERTIFICATE
Introduction 1
iii
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
INTRODUCTION
Testing of materials is nothing but evaluation of material properties.
Knowledge of material properties is very essential in characterizing the same. There
are a variety of materials in the market which finds application in several
machines/equipments/general use/ engineering use etc. Materials can be classified as
metals and non metals.
Metals can be classified as ferrous (all iron containing metals such as cast iron,
steel, S.G. Iron) and non-ferrous (without iron such as aluminium, copper,
magnesium).
Examples for non-metals are glass, wood, plastic, ceramics etc. Metals are
characterized by their good electrical and thermal properties and non-metals are
characterized by poor thermal and electrical properties. Metals have good properties in
tension, compression, bending, ductility etc. Hence, they are used extensively in
practice. Ex. Automobile parts, Machine parts, general engineering applications. Non
metals also find application in industries and house hold use.
Metals are generally evaluated for mechanical properties such as Tensile
strength, compression strength, hardness etc. Various equipments such as Universal
Testing Machine, hardness tester are used for the purpose. Mechanical testing of
materials is required to assess the performance of a new material as compared with
available materials.
Metals are given heat treatment to enhance the properties as a result of
structural changes. Annealing, Normalizing, Tempering etc., are some of the heat
treatment methods.
In metallographic examination of metals micro aspects of metals are studied
under a microscope. Mainly grain structure and phases are studied. Each metal has its
own structure which distinguishes itself from others. This is used to characterize the
metal. Structure can be photographed and recorded for future reference. For this a
metallurgical microscope is used. In general metals are observed under a magnification
of 100X or 500X.
In this book test procedures for evaluating different mechanical properties and
metallographic examination is given. General guidelines regarding content for writing
lab record are:
1) Aim, 2) Apparatus required, 3) Theory, 4) Procedure, 5) Apparatus
sketch (unruled-page), 6) Specimen sketch (unruled-page), 7) Initial observations
(unruled-page), 8) Tabular column (unruled-page), 9) Specimen calculations
(unruled-page), 10) Result & 11) Learning outcomes.
1
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 1
TENSILE TEST
Objective:
The objective of this experiment is to conduct uniaxial tension test on different
materials and to determine their mechanical properties.
Experimental Procedure:
1. Measure the diameter of the specimen in three locations and determine the mean.
2. Mark the centre of the specimen and the gauge length using a steel rule and a
punch. Note: To accurately compare elongation values between tests, the gage lengths must
be the same.
3. Attach the extensometer to the specimen to record the extension during loading.
4. Fix the specimen in the shackles.
5. Fix the arrangement to UTM.
6. Apply the tensile load gradually.
7. Record the load for every one division (1.27 mm) of the specimen with reference
to the extensometer until the specimen breaks.
8. Carefully remove the specimen and inspect the shape near the failure surface.
Make notes about the appearance of the failure surface. If you have a digital
camera take picture of the failure surfaces and include it in your record.
9. Carefully put the two pieces of the specimen together and measure the final
length of the specimen.
10. Measure the diameter of the specimen at the failure location.
11. Plot the stress vs. strain graph and calculate the necessary parameters i.e., yield
point, yield stress, upper yield stress, lower yield stress, 0.2% offset yield stress,
Maximum Load, Ultimate tensile stress, Breaking load, Breaking stress, %
Elongation, Cross section area at fracture, %Reduction in area, Young's modulus.
Data Sheet:
Material Name Material Type
(ductile/brittle)
Initial Observations:
Sl. No. Particulars Value
1. Overall length of specimen _______________ mm
2. Shoulder length of specimen _______________ mm
3. Initial gage length of the specimen, Lo _______________ mm
4. Initial diameter of the specimen, Do _______________ mm
2
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
3
Slope of the
4 linear portion of
5 the Stress vs.
Strain curve
6
10
11
12
13
14
15
16
17
18
Final Observations:
Sl.No. Particulars Value
1. Final gage (or shoulder) length of the specimen, Lf
_______________ mm
2. Final diameter of the specimen, Df
_______________ mm
3
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
==================================================
Material Name Material Type (ductile/brittle)
Initial Observations:
Sl. No. Particulars Value
1. Overall length of specimen
_______________ mm
2. Shoulder length of specimen
_______________ mm
3. Gage length of the specimen, L0
_______________ mm
4. Initial diameter of the specimen, D0
_______________ mm
7
Slope of the
8 linear portion
9 of the Stress
vs. Strain curve
10
11
12
13
14
15
16
17
4
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
18
Final Observations:
Sl. Particulars Value
No.
1. Final gage (or shoulder) length of the specimen, Lf
_______________ mm
2. Final diameter of the specimen, Df
_______________ mm
Formulae:
D 2
Area of Cross Section, A = mm 2
4
P
Stress, = N / mm 2
Ao
;
L
Strain, =
Lo
L f − Lo
% Elongation in length = 100
Lo
;
Ao − A f
% Reduction in Cross section area = 100
Ao
5
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
6
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
7
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
8
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 2
COMPRESSION TEST
Objective:
The objective of the experiment is to conduct compression test on different materials
and to determine their mechanical properties.
Experimental Procedure:
1. Determine the mean length and mean diameter of the specimen.
2. Fix the compression shackles to the upper and lower cross heads of the UTM.
3. Place the specimen axially on the bottom shackles.
4. Fix the specimen between the shackles by adjusting the upper cross-head.
5. Adjust the dial indicator to zero.
6. Apply the load gradually. Record the load at different intervals. Continue the
experiment until the specimen breaks.
7. Record the corresponding load for decrease in length of 0.5mm for M.S. and Al
and 0.25mm for C.I.
8. Measure the final length and diameter of the specimen.
9. Plot the stress vs. strain graph and calculate the necessary parameters.
Data Sheet:
Material Name Material Type (ductile/brittle)
Initial Observations:
Sl. No. Particulars Value
1. Initial length of the specimen, Lo
_______________ mm
2. Initial diameter of the specimen, Do
_______________ mm
9
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
10
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Final Observations:
Sl. No. Particulars Value
1. Final length of the specimen, Lf
_______________ mm
2. Final diameter of the specimen, Df
_______________ mm
==================================================
Initial Observations:
Sl. No. Particulars Value
1. Initial length of the specimen, Lo
_______________ mm
2. Initial diameter of the specimen, Do
_______________ mm
10
11
12
11
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
13
14
15
16
17
18
19
20
21
22
23
24
Final Observations:
Sl. Particulars Value
No.
1. Final gage (or shoulder) length of the specimen, Lf
_______________ mm
2. Final diameter of the specimen, Df
_______________ mm
Formulae:
D 2 P L
Area of Cross Section, A = mm 2 Stress, = N / mm 2 Strain, =
4 ; Ao Lo
;
Lo − L f A f − Ao
% Reduction in length = 100 % Increase in Cross section area = 100
Lo Ao
;
12
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
13
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
14
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
15
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 3
SHEAR TEST
Objective:
The objective of this experiment is to conduct shear test on different materials and to
determine the shear strength of the materials.
Experimental Procedure:
1. Determine the mean diameter of the specimen.
2. Fix the top and the bottom shackles in position.
3. Insert the specimen into the holes of the top and bottom shackles.
4. Grip the specimen in position and close the release valve.
5. Apply the tensile load to the specimen perpendicular to its axis gradually until
breaking.
6. Note the breaking load or shear load when the specimen breaks.
7. Determine the shear-strengths of all the materials and compare them using a
histogram.
Data Sheet:
Diameter, D Shear Load F Shear strength,
Sl. No. Material
(mm) in kgf N s (N/mm2)
1. MILD STEEL
2. CAST – IRON
3. ALUMINIUM
4. COPPER
5. BRASS
Formulae:
D 2
Area of Cross Section, A = mm 2
4
P
Stress, s = N / mm 2
2A
16
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
17
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 4
IZOD IMPACT TEST
Objective:
The objective of this experiment is to determine the impact strength of different
materials through Izod test.
Experimental Procedure:
Caution: Be extra careful while operating the machine. Avoid being in the path of
swinging hammer.
1. Measure the dimensions of the specimen and the notch.
2. Insert the specimen in the shackles.
3. Fix the shackles with the specimen in the vice provided at the bottom using the
gripper and the gauge. The notch should face the pendulum i.e. tension side.
4. Lift the swinging weight of the pendulum manually to a fixed length i.e. up to the
lever and lock it.
5. Bring the pointer to the zero position.
6. Release the pendulum by operating the lever provided at that place.
7. As the specimen is broken and the pendulum returns back, hold it in position
manually.
8. Note down the impact energy of the specimen as recorded by the pointer in kg-m
on the graduated scale.
Data Sheet:
Initial Observations:
Sl. No. Particulars Value
1. Weight of the hammer
_______________ kg
2. Height of the initial position of the hammer
_______________
3. Swinging angle of the hammer
_______________ deg
CAST –
2.
IRON
ALUMINI
3.
UM
18
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Formulae:
D2
− cos −1 D − d + D − d Dd − d 2 10 −6 m 2
Cross Sectional Area at impact pt , AI =
4 D 180 2
E
Impact Strength = J / m2
AI
Worksheet
19
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 5
CHARPY IMPACT TEST
Objective:
The objective of this experiment is to determine the impact strength of different
materials through Charpy test.
Experimental Procedure:
Caution: Be extra careful while operating the machine. Avoid being in the path of
swinging hammer.
1. Measure the dimensions of the specimen & the notch.
2. Lift the pendulum and fix it in its highest position. Secure it in that position by
using the hook.
3. Place the specimen in the provided shackles/support in such a way that, the notch
should face away from the pendulum.
4. Bring the pointer to the maximum position.
5. Release the pendulum by operating the lever provided at that place.
6. As the specimen is broken and the pendulum returns back, stop its swing by
periodically pressing the side brake.
7. Note down the impact energy of the specimen as recorded by the pointer in Joules
on the graduated scale.
Data Sheet:
Initial Observations:
Sl. No. Particulars Value
1. Weight of the hammer
_______________ kg
2. Height of the initial position of the hammer
_______________
3. Swinging angle of the hammer
_______________ deg
Cross-
sectional
Width, Thick Notch Impact Impact
Sl. Area at
Material w ness, t Depth, d Energy, Strength
No. Impact
(mm) (mm) (mm) E (J) J/m2
Point,
AI(m2)
1. MILD STEEL
2. ALUMINIUM
3. BRASS
4. COPPER
20
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Formulae:
Cross Sectional Area at impact pt , AI = w (t − d ) 10 −6 m 2
E
Impact Strength = J / m2
AI
Worksheet
21
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 6
BRINELL HARDNESS TEST
Objective:
The objective of this experiment is to determine the Brinell hardness number (BHN)
of different materials.
Experimental Procedure:
1. Identify the given material by inspection.
2. Calculate the load to be applied using the formula P/D2 = K.
K - constant - depending on the material (5 - 30 ) whether it is soft or hard. For
soft metals like Al = 5 , Cu = 10 , For hard metals like Steel = 30 , Cast Iron =
30.
D - diameter of the indentor ball.
P - Load required for indentation.
If the thickness of the material being tested is T > 6 mm then D = 10mm ,
if T = 3 - 6 mm then D= 5mm and T < 3mm then D = 2.5 mm.
3. Adjust the load in the pan of the machine as per the calculation.
4. Insert the indentor ball into the shackles and fix it into the loading arm.
5. Adjust the time of loading from the scale provided in the machine by operating
the lever up and down.
6. Lift the specimen kept on the table of the machine up using a round plate, until it
makes contact with the indentor ball.
7. Initial adjustment of the table is to be made such that prior to applying the load
the specimen surface just touches the surface of the indentor.
8. Now apply the load by operating the lever in the machine.
9. The duration of the load that is applied is a function of the material
t=15 sec for 3000 kg for cast iron, mild steel etc.
t=30 sec for 1000 kg for Brass, copper etc.
t=30 sec for 500 kg for Aluminium etc.
10. Take out the specimen and measure the diameter of indentation by using a
microscope.
11. Calculate the BHN using the below formula and tabulate the results:
2P
BHN =
D D − D 2 − d 2
Data sheet:
Initial Observations:
Sl. No. Particulars Value
1. Dead weight (equivalent) of the load pan
_______________ kg
2. Weight (equivalent) of load billet
_______________ kg
3. Machine time (constant)
_______________ s
4. Least count of travelling microscope
_______________ mm
22
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
2 Cast Iron
3 Aluminium
4 Brass
5 Copper
Worksheet
23
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
24
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 7
ROCKWELL HARDNESS TEST
Objective:
The objective of this experiment is to determine the Rockwell Hardness of different
materials.
Experimental Procedure:
1. Insert the ball-indentor of required diameter in the holder.
2. Clean the surface of the specimen by removing dirt / dust / oil / grease.
3. Rotate the lever such that, the indentor just makes the contact with the surface of
the specimen.
4. Set the load to the required value by turning the load selector dial.
5. Wait for 15 seconds and then release the load by pulling the lever.
6. The needle in the hardness-indicator starts to rotate back. Note down the reading
once the needle stabilizes.
7. Tabulate the values and compare.
Data sheet:
Sl Material used Diameter of Applied Scale Rockwell
No for testing indentor load Hardness
D (inch) (kg) number
1 Mild steel
2 Cast Iron
3 Aluminium
4 Brass
5 Copper
25
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 8
BENDING TEST
Objective:
The objective of this experiment is to conduct bending test on different materials and
to determine Young's modulus, Maximum bending stress and Radius of bending.
Experimental Procedure:
1. Measure the dimensions of the specimen.
2. Mark the center and the gauge length of the specimen.
3. Fix the specimen is on the two supports such that the two supports coincide with
the end markings of the specimen [the supports are movable within the slot]
4. Apply the load on to the specimen gradually. (normal to the axis of the specimen)
5. Record the applied load for each one division deflection of the specimen.
6. Continue the experiment up to 20 divisions of deflection.
7. Draw a graph of load v/s deflection and calculate the necessary parameters.
Data Sheet:
Ductile Material
Initial Observations:
Sl. No. Particulars Value
1. Length of specimen between the supports, L _______________ m
2. Breadth of the specimen, b _______________ m
3. Depth of the specimen, d _______________ m
26
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
10
11
12
13
14
15
16
17
18
Brittle Material
Initial Observations:
Sl. No. Particulars Value
1. Length of specimen between the supports, L
_______________ m
2. Breadth of the specimen, b
_______________ m
3. Depth of the specimen, d
_______________ m
27
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
10
11
12
13
14
15
16
17
18
Formulae:
bd 3 4 wL
Moment of Inertia, I = m Max Bending Moment , M b max = N .m
12 4
M bmax y M bmax d 2
Maximum Bending Stress, bmax = = N / m2
I bd 3 12
L3 w EI
Young' s Modulus, E = N / m2 Radius of Curvature, R = m
48I slope M bmax
28
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
29
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
30
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
31
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
EXPERIMENT NO - 9
TORSION TEST
Objective:
The object of this experiment is to conduct torsion test on different materials and to
determine the mechanical properties of materials in torsion.
Experimental Procedure:
1. Measure the dimensions of the specimen.
2. Insert the specimen in torsion shackles, and fix this to the torsion testing machine.
3. Set the reading of torsion testing machine to zero manually.
4. Attach a graph sheet and a graph plotter (or pencils) to the circumference of the
drum.
5. Apply the load gradually by operating the motor, which rotates the worm.
6. Once the specimen breaks, using the plotted graph calculate the necessary
parameters. (machine constant -545.5 kg-cm)
Note: Draw coloured chalk line marks parallel to the axis of the specimen and
observe the same after the test.
Data Sheet:
Initial Observations:
Sl. No. Particulars Value
1. Machine constant (x - axis)
_______________
2. Machine constant (y - axis)
_______________
Formulae:
d 4 L dT
Polar Moment of Inertia, J = mm 4 Rigidity Modulus, G = N / mm 2
32 J dq slope
Tmax d 2
Shear Strength, max = N / mm 2
J
32
Dept. of Mechanical Engg., BMSCE MT Lab Observation Book
Worksheet
33