Determination of Ductility: Detailed Information

1. Introduction:
Ductility in bitumen refers to its ability to elongate without cracking under the load of traffic, especially
in road construction. Temperature fluctuations can cause bitumen to expand and contract, and
insufficient ductility may result in cracking. This chapter outlines the method for determining the
ductility of various bituminous products, including distillation residue, cutback bitumen, and blown-type
bitumen.

3. Apparatus:

Mould: Made of brass, with specific dimensions forming a briquette specimen.

Water Bath: Preferably with a thermostat for temperature control.

Testing Machine: Used for pulling the briquette apart continuously immersed in water.

Thermometer: Conforming to specified requirements.

4. Procedure:

Sample Preparation:

Melt bituminous material to 75-100°C above the softening point.

Assemble the mould, coat surfaces to prevent sticking, and fill with molten bitumen.

Cool, cut off excess bitumen, and place in a water bath at the specified temperature.

Testing:

After 85-95 minutes, remove the briquette and test immediately.

Pull the clips apart horizontally at a uniform speed until rupture occurs.

Measure the distance for rupture.

5. Report:

Normal Test:

Average of three normal tests is reported as ductility, provided they are within ±5 percent of their mean
value.

If the two higher values are within ±5 percent, report the mean of those two.

Abnormal Test:

If bituminous material contacts water or the bath bottom, adjust water properties.

If normal tests are unobtainable on three successive attempts, report ductility as unobtainable.

6. Precision:
Test results shall not differ by more than 10 percent of the mean for repeatability and reproducibility.

7. Precautions:

Ensure the flatness and levelness of the plate where the mould is placed.

Exercise care during filling to avoid distortion and air pockets in the moulded sample