State of New Jersey Department of Environmental Protection Certifies That ELEMENT ONE INC Laboratory Certification ID #NC009 is hereby approved as a Nationally Accredited Environmental Laboratory to perform the analyses as indicated on the Annual Certified Parameter List which must accompany shis certificate to be valid having duly met the requirements of the Regulations Governing the Certification of Laboratories and Environmental Measurements N.J.A.C. 7:18 et. seq. and having been found compliant with the 2016 TNI Standard approved by the The NELAC Institute Expires June 30, 2024 @& Michele M, Teck Manager NJDEP is a NELAP Recagnized Accreditation Body ‘This cefeate i fo be cosscucutycplayed athe arson wi the anval eed prareert na cation on he promises Walle oe pul. Corsuners are uted vey De abowlays axren exresatin tvs with the Ste Na NELAP,New Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6'30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09 Activity ID: NLC 230002 (6319-0 CAROLINA BEACH RD WILMINGTON NC 28412 Category: AE01 ~Inorganics « Non-Metals Anal reais i cect aera © Repel code Param Sree PMR cen cseanaie ae ss = a cunfed Yes ———-AEOL DON eenctwocr cenfes —Yee—=—=—«AED1.0080 Brana bn Chontonapy ePa2e "1 caries Yer_—=—=—«AEOH.00E0 Brine bn Chonstonspy PAA ss canfet —Yer—Ae04.080 cha vn cheney eras ‘1 conte: Yes—=—=AO1.0000 Cham tm Crontopapy eazea "1 cried Yes_—=—=—AEOL004—_ chrome iereer pases "1 cored Yes_—=—-EOOD.-—_chomlzn weer EPA: caro —Yen—=—EOLOEED. Fare SADNS cots erate ws cafe Yen === A000 Fare Souci on Ect era ws canied Yen AEOLOOTID.—_Hydogen oie tn Gromer era " cunfed Yeu AEOLOOTED.—_Hyogen brie tn chromaoraty EPA284 Wu canfed Yeu AEDLEORID.-—_—Hytogen cro tn Cromarty Pas " cantad —Yor———AEDL.ORSO. ‘Hyon cre be Cros py PAA " canted Yen_——=—AEDL.ONEO.—_‘Hytoan oe tn Chromiogary era " cares Ye———«EDHOTOCO—_Hyropen te tn chomaogty EAA " cored Yws—=—=—«DHOTBC0 Pare ater ciovinete ear? " cere Yes. =—=—=—«AEDHOTEEO. Paro ater ceovinotc ePazot cere Yen—=—=AEDHOTEEO. Parco ater ceovietc EPA ZA " carat Yon=—=—«AEDLOTBSD. Prien Naer cenit eraa02 ws Catiled —Yen—=—=AEDL.Y800. Prat Matar. cei pas ™ cetited Yeu —=—=—AEDL.OBSO._—Prlat at. cron EPASA wu cried Yen_—=—=—=AEOLOLND Prise Hater ceavintc eens ' cated Yor_—=—=—«CAOLOYED.-—_—Prista Mater ceavnte eens ' cated Yen—=—=AEOLGQOND_—_—Priso Mater ceavintic cease ' crt feo1520s) Part Mate covet erase centey —You=—=—=EOLCRNID.—Paiuat atr vrai ease caled—Yes=—=—AEOLO21#D.—_ Paka Mater Seva Pas w ir and Emicsions, BT = Biological Tissue, DW: inking Water, NPW = Non- Potable Water, SC old and Chemica Materials Page tofNew Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NC009 Activity 1D: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON NC 28412 Category: AEO1 ~Inorganics - Non-Metals Analysis, Techniqu ‘AEO1.02960 Partculate Matter Gavimotric, ‘Other NJ Alr Test Method + Centos ‘AE01,02500 Sulfur Dioxide ‘Bvium-Thorin Titration EPAS No Ceres Yee ‘AE01.02550 Sulfur Dioxide Gravimetric EPAGA Ny Centied Yes ‘AE01.02600 —_Sullur Dioxide Govimotrc PAGS Na Centies Yes ‘AE01.02650 —_SullurDixide ‘Barium-Thorin Titration EPA Na Ceres No ‘AE01,02700 Sulfur Dioxide {en Chromatography EPAB Ny Coniied No ‘AED1.02750 Sulfur Tondo len Chromatography EPA Na Contied Yes ‘AED1.02800 ‘Sulfur, Total Reduced ‘Baium-Thorin Titration EPA 164 na ented Yes ‘AED1.02850 Sulfur, Total Reduced ‘Baium-Thorn Ttraton EPA 16A Ny Conted Yes ‘AED1.02600 Sulfur acld Barium-ThorinTiaion EPAS Na Contted No ‘AE01.02050 Sulfur acid len Chromatography EPA Na Category: AE02 ~Inorganics - Metals Analysis Mercury (Etemental, Oxcized, Partcte- ‘ASTM 06786 Bound and Total) Conted Yes ‘AE0200100 Metals EPAGO Ns Contes Yes ‘AE02.00150 Chromium (vt) EPA.GO6t nN Cortes Yes 1AE02.00250 Mercury EPA 101A, N Cortog Yes 'AE02,00500 Beryllium ePmis EPA 103, wy Contod Yes ‘AE02,00700 Brym ops EPA104 wy Contes Yes ‘AE02.00750 Mercury 'AA, Cold Vapor EPA 105 Ny Contes Yes 1AE02.00850 Arsenie eps EPA 108, Ny Contiod Yos ‘AE02.00850 Arsenio ePnas EPA 1084, Nu Contiied Yes ‘AE02.01050 Arsenic icPms EPA 1088, NJ KEY: AE = Airand Emissions, BT = Blloglal Tissues, DW = Drinking Water, MPW» Non-Potable Water, SCM= Sold and Chemica! Mates Page 2019New Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09 Activity 1D: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON NC 28412 Category: AE02 -Inorganles - Metals Analysis ‘Yoo ‘Ac02.01200 Lead iePaas Nu Yes A0201250 Mercury ‘AA, Cold Vapor Nu Yes ‘AE02.04250 Aluminum ops Nu Yes ‘AE02.04300 Antimony ops Nu Yes 0204350 Arsenic ‘cPinas Nu Yes 'A02.04400 Barium Pinas uu Yes ‘AE02.04450 Beryllium opis Nu Yes ‘AE02.04500 Cadmium 1oPms No Yes ‘A&0204860 Chromium ops No Yee ‘AE0204600 Cobalt eps Nu Yes ‘AE02.04850 Copper eps Nu ‘AE02.04750 Lead pias. Na ‘AE02.04800 -Manganose eps. Na ‘AE02.04850 —-Molybdanum opm, EPA29 Na ‘AE02,04900 Nichol rePias PAZ Na ‘AE02.04950 Phosphorus eps, EPA20 Na Cartiied 'AE02.05000 Selenium ropns EPA29 NI Centied AE02.05050 iver 1oPms EPA29 NI Cortes ‘AE02.05100 Thallium iopms EPA 20 NI Cortes ‘AE0205150 Tia opus EPA 29 NI Certiied .A02.05200 Vanadium ops EPA 20 Nu Certiies ‘A02,05250 Zine ops EPA 28 Ny Certiied .AE02.05400 Chromium PIMs EPA 308 Ny certiiea ‘AE0205550 Chromium PIMs EPA 306A, Ny Caries ‘A02.08600 Mercury (Total Vapor Phase) Sorbent Trap /Entract Tharmal Dosoption AA EPA 308 Na = Aland Emistlons, ST = Bologeal Tesues, DW = Drinking Water, NPW= Non-Potable Water, SC Solid and Cheria! Matai Page 3 ofWILMINGTON NC 28412 Category: NPW03-Inorganic Parameters Centies Cortes Caries Ceriied Corie’ Ceoriied Ceres coniied Coniied Cottiod Contes Cortes ap moe Yes Yes Yes Yee Code ‘NPwo3.02400 NPwo8.03550 NPwos.04000 ‘Newos.08500 NPwo3.11050 NPwO3.13650 NPwoa,15550 NPwos.t7850 NPw0s.18000 Newoa.t8190 NPwi03.18300 NPwio3.18850 Npwoa.2t110 NPwoa.21450 New Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NC009 Activity ID: NLC 230002 6319-D CAROLINA BEACH RD Parameter Bromide (Chemical oxygen demand Chloride Fluoride Nitrate Nite Orthophosphate Residue - Mterable (TOS) Residue -ronfiterable (TSS) Residue Wola Residue voatte Sulfate otal organic carbon (TOC) Total organic carbon (TOC) Category: NPWO6--Metals - NPW Preparation Methods ‘status Cortes Cortog Contos Category: NPWO7~Metals Biigibie Roport NJ Data Yes Yee Yes Code. 'NPW06.00060 NPwios.00100 NP wos.00250 Parametor Metals Metals Metals, Tota ‘Technique len Chromatography Spectrophotometrc Manual/Auto len Chromatography len Chromatography len Chromatography len Chromatography len Chromatography Cravimetic, 180 Degrees C Gravimetic, 103-105 Degrees C, Post Wrashing Gravimette, 103-105 Doge Cravimatie, 550 Degrees len Chromatography Combustion Infrared Spectromety or FID Technique TSLP, Toxicly Procedure, Shaker ‘Sytetic PPT Leachate Procedure ‘Acid Digestion/Aqueous Samples KEY: AE = Alrand Emissions, BT = Biological Tissues, BW = Drinking Water, NPW = Non-Potable Water, SCM = Sold and Chena! Materials Approved Methods EPA3000 (ther HACH 8000 (1979) EPA3000 EPA3000 EPA2000 EPA3000 EPA300.0 ‘SM 2540 6-415 ‘SM 2540 0-15 ‘SM 2540 £18 EPA 300.0 sMsa10 14 ‘8-846 90608 Approved Methods SW-846 1911 sw-see 1312 SSW-846 30100, Page 409 a) Na Na Na na Primary Nu Ny NyNew Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6'30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09 Activity 1D: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON NC 28412 Centied ‘NPWO7.03200 Chromium (VI) (45u Fler, lon Chromatography EPA2IB6 ND Cetiied NPwo7.03350 Mercury Manual Cold Vapor EPA 245.1 Nu certiied NPWo7.12100 Chromium (Vi) bn Chromatography ‘sw846 7198 Ny Certied NPWO7.12150 Mercury liquid waste ‘AA, Manual Cold Vapor ‘SW848 7470A Nu Category: NPWO8~Metals - ICP, ICP/MS and DCP Cartes Yes NPWO8.05650 Aluminum tion, CPIM. EPA 2008 Centiea Yes INPW08.05700 Antimony tion, CPIM. EPA 2008 Ny Certied Yes NPW08.05750 Arsenic Digestion, cps EPA 2008 Na Ceoniied Yes NPW08.05800 Barium Digestion, Cems EPA 2008 NI Centiied Yes NPW06.05850Berylium Digestion, CPMS EPA 2008 Nu Centiied Yes NPW08.05950 Cadmium Digestion, ICPIMS EPA 2008 NI Contiied NPwoe.06000 Calcium Digestion, ICPIMS EPA 2008 NI Cortied NPWw06.08050 Chromium Digestion, ICP”MS EPA 2008 NI Cortied NPWw0e.06100 Cobalt Digestion, ICP”MS EPA 2008 _ Contiod NPWw08.06150 Copper Digestion, ICP”MS EPA 2008 Nu Certs NPwO8.06250 Iron Digestion, ICP”MS EPA 2008 NI Contes NPwos.06s00 Lead Digestion, ICPMS EPA 2008 No Cortes [NPWO8.06350 Magnesium Digestion, CPS EPA 2008 Na Certited NPWO8.06400 Manganese Digestion, cPnas EPA 2008 Na Certited |NPWO8.06450 Molybdenum Digestion, cPmMs EPA 2008 Na Certiied INPWO8.06500 Nickel Digestion, cps EPA 2008 Na Certied Yes NPWO8.06550 Potassium Digestion, ICPMS EPA 2008 Nu Cetiied Yes NPW08.06600 Selenium Digestion, IOPIMS EPA 2008 No Coniied Yes NPW08.08700 Sliver Digestion, ICPIMS EPA 2008 N KEY: AE Alrand Emissions, BT = Blologlea Tissues, OW = Drinking Wate, NPW = Non-Potable Water, SCM= Soli and Chemiea!Matorile Page sofNew Jersey Department of Environment Protection, Environmental Laboratory Certificat on Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09 Activity 1D: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON Nc 28412 Category: NPWO8—Metals IcP, ICPIMS and DCP ible ray. Status Report WJ Code Parameter Technique ‘Approved Methods can Cerf Yes -—-—NPWOB.06750 Sodium Digestion IPMS " EPA2008 Na Contioa Yes NPWO0B.06859 Thallium Digestion, ICPIMS EPA 2008 na Contes Yes NPW08.06050 Tin Digestion, CPIMS EPA 2008 Na Ceniied Yes NPWo8.07000 Titanium Digestion, ICPIMS EPA2008 Ny Ceoniied Yos NPWOB.07150 Vanadium Dgostion, CPIM EPA 2008 Na Coxtted Yes \NPwo8.07200 Zine Dgostion, CPs EPA 2008 Nu Contned Yes ‘NPW08.14400 Aluminum rpms sw-846 60208, Na Cored Yos NP WO8.14450 Antimony crm ‘Sv¥-845 60208 Nu Corton Yes NPW08.14500 Arsenic IcPms ssw-846 60208, Na Contion Yes NPW08.14550 Barium IcPms sw.s46 60208, Ny Corts Yor NPW08.14600 Benya IcPms 811-848 60208 Ng Contos Yes NP W08.14650 Boren crs ‘sw-s4s 60208, Ny Contd Yes NPW08.14700 Cadmium IcPms ssw-846 80208, Ny Ceres Yes NPWos.14750 Calcium IcPms ssw.s46 60208, Nu Contes Yos NPW08.14600 Chromium cris swi-846 60208, No Cerified Yes NPW08.14850 Cobalt Ices ssw-846 60208 Ny Corte Yes NPW08.14800 Copper IcPms ssw-846 60208, N Contiod NPWw08.14950 Iron rerims sw-846 60208 Ns Contig NPW08.15000 Lead crs ‘swi-sas 60208, Ny Contiog Yos 'NPW708.15050 Magnesium \cPms sw-s46 60208 ws Ceontiog Yes INPW08.15100 Mongenese (cps sw-846 60208 uN Certo Yes NPW08.15150 Molybdenum IcPms ‘8-846 60208 Ny Certied Yes NPW08.15200 Nickel crs ‘sw-846 60208 Ny Cortiied Yes INPWo08.15250 Potassium IcPms ‘sw-046 60208 Ny Ceti Yes NPW0s.15300 Selenium IcPms ‘8W-846 60208 Na Certied Yes NPW09.15350 Silcon crm, ‘SW-846 60208 Na Cotiied Yes NPWo8.15400—Siver IcPmis ‘sw-846 60208 Ny KEY: AE= Alrand Emissions, BT = Biologcal Tissues, OW: [PW = Non-Potabe Water, SCM = Sold and Chena! Material Page 6 ofNew Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09 Activity ID: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON NC 28412 Category: NPWO8—Metals - ICP, ICP/MS and DCP ‘SW-846 60208 NI Certified NPWOS.15450 Sodium cPns Cortiied NPW08.18600 Strontium eps ‘SW-646 60208 No Centied NPWO8.15550 —Thallum cPms ‘sW-646 60208 NI Contes NPWO8.15650 Tin PMs ‘sw-846 60208 NI Contes NPWO8.15700 Titanium pms ‘sw846 60208 No Centied ‘NPwO8.15850 Vanadium pms 'SW-848 60208 N Centiied ‘NPwo8.15800 Zine rPns ‘sw-846 60208 N Category: SCMO2-Charactoristics of Hazardous Waste Certified Yos ‘SCM02.00800 pH sol and waste {Use with Wator oF Calcium Chlorides ‘8-646 90450, Category: SCMO03~Inorganic Paramoters and Preparation Certified Yes 'SCMO3.05000 ola fixed, and volatile sli (SQAR) Gravimetic, 500 Degrees C ‘SM 2540 G SM 18h Ed, NI Category: SCM05~-Metals - SCM Preparation Methods ND ‘eid Digestion, Soll Sediment & Sludge ‘SW-848 30508 KEY: AE Aland Emissions, BT = ological Tissues, DW = Drinking Water, NPW = Non-Potable Water, SCM= Soll and Chemical Matai Page of 9New Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09. Activity ID: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON Nc 28412 Category: SCM05~Metals - SCM Preparation Methods Cook arameter Pechnique ented ‘SCMO5.00100 Mais. (Chromium VI Digestion ‘SVi-846 30608 Ceniied ‘SCMo5.00300 Metals. Merowave Ald Digest Slceout & Org Matix vi-646 9052 Nu Ceriied SCMO5.00350 Mais. Meromave Acid Digest: Soll Seciment & 8VV-846 30518 Nu ‘Sudge cantied Yes ‘SCM05.00500 Metals ‘Shake, Extraction with Water ‘ASTM D9967-12 Nu Ceriied Yes ‘SCM05.00650 Metals Synthetic PPT Leachate Procedure svi-e4s 1912 Na Cortied Yes 'SCM05.00600Motais ‘TSLP, Toxelty Procedure, Shaker svi-o46 1911 Nu Category: SCMO6--Metals Contes Yos ‘SCM05.02750 Chromium (VI) len Chromatography SWi-B46 7198 Contiog Yes ‘SCMO6.02800 Mercury - solid waste ‘AA, Manvel Cold Vapor syi-846 74718 No Contied Yes ‘SCMO6.02850 Mercury - sod waste 'AA, Thermal Decomposition, Amalgamation swi-ese 7473 NI Category: SCMO7—Metals - ICP, ICP/MS and DCP. Centied Yes ‘SCMO7.01600 Aluminum Nw Centied Yos ‘SCMO7.01650 Antimony opis ‘sw-046 60208 ws Certied Yes SCMa7.01700 Arsenic eps ‘sW-646 60208 uN Certiied Yes ‘SCMa7.01750 Barium oPmas ‘sw-846 60208 uu Certiied Yes ‘SCMO7.01800 Beryllium crams ‘Sw-946 60208 Ny Cote’ Yes 'SCMO7.01850 Boron reps ‘SW-846 60208 Na KEY: AE = Alrand Emissions BT = Biologics Tiesu DW = Drinking Water, NPW = Non-Potabe Water, SCM = Soll and Chemical MaterNew Jersey Department of Environment Protection Environmental Laboratory Certification Program Annual Certified Parameter List and Current Status Effective as of 7/17/2023 until 6/30/2024 Laboratory Name: ELEMENT ONE INC Laboratory Number: NCO09 Activity 1D: NLC 230002 6319-D CAROLINA BEACH RD WILMINGTON NC 28412 Category: SCMO7--Metals -ICP, ICP/MS and DCP Eiigibie to ] Status Reports code Prometer Technique Approved Methods ae ‘Coriied Yes ‘SCMG7.01900 Cadmium i GPM a set © $W846.60208 uN Cored Yee ScMO7.01950 Calcium rats 846 60208, ws Cerited Yee SCM07,02000 Chromium cents s94s 60208, wy cers Yow ScMo7.02050 Cobat cents 3-948 60208, wy Coriied Yon SCMOT.02100 Copper cents 3846 60208, wy Ceriied Yes SoMO7.02150 on cents 948 60208, wy Cerifed Yes cMo7.02200 Lead cents 846 60208, Nu Corifed Yes ScMO7.02250 Magnesium cents 3-846 60208, a Cored Yes SOMOT.02900 Manganese cents 846 60208, wy Cored Yee SCMO7.02950 Mobionum coms sua%e 20208 nu cenied ——Yos SCMO7.02400 Neko! cents s.84s 60208, wy Corites Yee SCMO7.02450 Potassium cents 849 60208, w Cored Yes SCMOT.02500 Selenium cms 848 60208, w Cerited Yes ScMOT.02550 Sion coms 5-848 60208, i Corifed Yes Scl07.02500 _Siver coms 5.846 60208, Ny Cored Yes Sc}H07 02650 Sodium coms 5-845 60208, Ny Cones Yes S0}07.02700 Stent coms 1.946 60208, wy Corited Yes ScM07.02750 Thalia coms 7.845 90208, Nu conte Yoo scMo7.02950 Tin cons s.a46 60208, wy cones Yee Sc¥07.02900 Tau coms s.849 60208, a Contes Yon ‘SCMO7.09050 Vanadium coms sw.846 60208, wy Cconited Yow sscMor.0a100 Zine coms v.84 60208, oy Michele M. Potter, Mana KEY: AE = Air and Emisslons, BT = Blological Tissues, OW = inking Water, NPW: Potable Water, SC old and Chemica Materials Page ot