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Jsa Jis z2371-2015 English
Jsa Jis z2371-2015 English
INDUSTRIAL
STANDARD
JIS Z 23 71 = 2015
(SFJ/JSA)
Methods of salt spray testing
ICS 77.060
Date o f E stablishment: 1 9 5 5 - 1 2 - 1 6
Date o f Revision : 20 15-06-22
Date of Public Notice in Official Gazette : 2 0 15-06-22
Investigated by: Japanese Industrial Standards Committee
Standards Board for ISO area
Technical Committee on Basic E ngineering
© JSA 2015
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or
utilized in any form or by any means, electronic or mechanical, including photocopying and
microfilm, without permission in writing from the publisher.
Printed in Japan
HT/AT
Contents
Page
Introduction························································································································· 1
1 Scope···························································································································· 1
5 Apparatus ··················································································································· 4
10 Duration of tests······································································································ 14
14 Test report················································································································ 1 6
(i)
Annex JC (normative) Rating number method ········ ···· ···· ···· ···· ···· ····························· 30
(ii)
Foreword
This translation has been made based on the original Japanese Industrial Standard
revised by the Minister of Economy, Trade and Industry, through deliberations at the
Japanese Industrial Standards Committee as the result of proposal for revision of
Japanese Industrial Standard submitted by The Surface Finishing Society of Japan
( SFJ)/Japanese Standards Association (JSA) with the draft being attached, based on
the provision of Article 12 Clause 1 of the Industrial Standardization Law applicable
to the case of revision by the provision of Article 14.
Consequently, JIS Z 2371 : 2000 is replaced with this Standard.
This JIS document is protected by the Copyright Law.
Attention is drawn to the possibility that some parts of this Standard may conflict with
patent rights, applications for a patent after opening to the public or utility model rights.
',!'he relevant Minister and the Japanese Industrial Standards C ommittee are not
r esponsible for identifying any of such patent rights , applications for a patent after
opening to the public or utility model rights .
(iii)
Introduction
This Japanese Industrial Standard has been prepared based on the third edition of
ISO 9227 published in 2012 with some modifications of the technical contents.
The portions given sidelines or dotted underlines are the matters in which the con
tents of the corresponding International Standard have been modified. A list of modi
fications with the explanations is given in Annex JD .
1 Scope
This Standard specifies the salt solutions, the apparatus, and the procedure (includ
ing evaluation of cabinet reproducibility related to corrosivity, test specimens, test con
ditions, and evaluation of test results) to be used in conducting the neutral salt spray
test, acetic acid salt spray test and copper-accelerated acetic acid salt spray (CASS) tests
for assessment of the corrosion resistance of metallic materials, with or without electro
plating, or inorganic film or organic coating such as painted coat.
WARNING Persons carrying out tests based on this Standard should be familiar
with normal laboratory practice. This Standard does not purport to
address all of the safety problems, if any, associated with its use. It
is the responsibility of the user of this Standard to establish appro
priate safety and health practices.
NOTE : The International Standard corresponding to this Standard and the sym
bol of degree of correspondence are as follows .
I S O 9227 : 2012 Corrosion tests i n artificial atmospheres-Salt spray tests
(MOD)
In addition, symbols which denote the degree of correspondence in the
contents between the relevant International Standard and JIS are IDT
(identical), MOD (modified), and NEQ (not equivalent) according to ISO/
IEC Guide 21-1.
2 Normative references
The following standards contain provisions which, through reference in this text,
constitute provisions of this Standard. The most recent editions of the standards
(including amendments) indicated below shall be applied.
JIS G 3 14 1 Cold-reduced carbon steel sheet and strip
JIS K 5600- 1-4 Testing methods for paints-Part 1: General rule-Section 4: Stan
dard panels for testing
NOTE : Corresponding International Standard: ISO 1514 : 2004 Paints and var
nishes-Standard panels for testing (MOD)
NOTE : Corresponding International Standard: ISO 2808 : 2007 Paints and var
nishes-Determination of film thickness (MOD)
:!-��--�-���_Q ____�'?.<!:(lf.1!1:__�!1:-�'?.':_�c/:�_(�����'.1:-t)
JIS K 8180 Hydrochloric acid (Reagent)
--------------------------------------------------------------------------
:!-��--�-���-f?---���-���-?:-�t4._(��0_��'.1:�)
JIS K 8576 Sodium hydroxide (Reagent)
--------------------------------------------------------------------------
b) Water used shall be deionized or distilled water with a conductivity not higher than
20 µSiem at 25 °C ± 2 °C.
a) Add --------
1 ml of acetic acid -----------------------------------------------------------------------------------------------------------
of special grade specified in JIS K 8355 per litre of salt so-
lution prepared in 4.1, agitate well, and measure the pH.
d) Check that the pH of samples of the sprayed solution collected in the test cabinet
at 25 °C ± 2 °C is between 3 . 1 and 3 . 3 .
��--�-�8:11 _ }:)�-��-�_l:1
_ _ !��--�?-�-�--�?-�--�-�-��-- s<?_ �-�Y��-!o_r _ _t� ��-i-��--i_s_ _ fi:e�_ _ _ fr:� �--�-��-r_�-��-��--����-�!
r_r:�_<:>!_�?__�_P.1:8:Y.��-�-·---�X_�!��i:-�-���-?-��?--����-���-<:>?__�-��P.��-�-�-�--��-��-�-r:__i_�--�-�m__�l>��-!:r_�-�-'--t}-.���i:
the solution by using filter paper or the like. If considered necessary, filter the solution
-------------------------------------------------------------------------------
before placing it in the salt solution reservoir of the apparatus, to remove any solid
matter which might block the apertures of the mist dispersion tower or atomizer nozzle.
5 Apparatus
5.1 General
b) The mist dispersion tower and the atomizer nozzle shall be made of inert material
such as plastics, and shall be capable of spraying the solution uniformly over the
test specimens from upper part of the spray cabinet (see Annex A).
c) The spraying shall be performed by free circulation of sprayed solution, and the
direction of the mist dispersion tower or the atomizer nozzle shall be adjusted so
that the sprayed solution does not directly fall on the test specimen. The mist dis
persion tower is suitable for this purpose. The upper parts of the cabinet shall be
designed so that drops of the sprayed solution formed on its surface do not fall on
the specimens being tested.
d) The sprayed solution and temperature inside the spray cabinet shall not be affected
by the open air.
e) The test specimen supports shall be capable of holding the test specimens at the
specified angle ll.
Note l) The test specimen supports shall be made of, or coated with, inert mate
rials such as plastics, and shall support the test specimen at the bottom
or side surfaces of the specimen. -------------------------------------------------------------------
Instead of using such supports, test
specimens may be hung with a glass hook or vinyl string as long as they
---------------------------------------------------------------------------------------------------------------------------------
���--��-_l:i-�-��--�-�--�11-�--�p��-����--P.����-���!--��--����11--�-�-�-�-'--�-��:r-�11-�P--�-�--�-�p_-_
ported at the bottom surfaces if necessary.
b) In order to prevent the evaporation of water from the sprayed droplets, the com
pressed air shall be humidified before entering the mist dispersion tower or atom
izer nozzle by passing through �--J:l:�:r??--���-���- or an air saturator. 'r?_�--�?-�P.!��-�-�-�
air supplied to the mist dispersion tower or atomizer nozzle shall be heated so that
----------------------------------------------------------------------------------------------------------------------------------------------------
�-�--�-?-�-�--���-���-�-�--�-1?:�--��-�P.�!���!�__i_J!�-��-�--�?-�--�P.!:�Y--�-l'.l-�-��-��-��--����-����--��Y�!:�}y
when mixed with the salt solution. An air saturator should be used to control the
humidity and temperature of the compressed air. Table 1 shows the guiding val-
------------------------------------------------------------------------------------------
ues that are given for the hot-water temperature in the air saturator at different
pressures.
c) The water used for ---------------------------
the humidifier or the air saturator for humidifying the com-
pressed air supplied to the mist dispersion tower or atomizer nozzle shall be ��
specified in 4.1 b).
NOTE : H igh silica concentrations in water may affect the performance of the
------------------------------------------------------------------------------------------------------------------------------------------------
heater and the water level sensor.
d) The salt solution to be supplied to the mist dispersion tower or the atomizer nozzle
------------------------------------------------------------------------------------------------------------------------------------------------------------
shall be maintained to be continuous and uniform spray mist. For a stable spray-
----------------------------------------------------------------------------------------------------------------------------------------------------
ing , the level of the salt solution in the salt solution reservoir, or flow of the salt
----------------------------------------------------------------------------------------------------------------------------------------------------
��!�����--��-I?P!���-�?.-�?-�--����--�-��J?_�t���!?---�����--?-�-��?-��-��!:-����-��-�-1?:�!�__?_�--��!?--�!:?_�!��:
70 45 61
84 46 63
98 47
---- -
63-
--
112 49 66
126 50 67
140 52 69
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6.1 General
To check the reproducibility and repeatability of the test results for one piece of
apparatus, or for similar items of apparatus in different laboratories, it is necessary to
verify the apparatus at regular intervals as described in 6.2 to 6.4.
NOTE : During permanent operation, a reasonable time period between two
checks of the corrosivity of the apparatus is generally considered to be 3
months.
To determine the corrosivity of the tests, reference-metal specimens made of steel
shall be used. As a complement to the reference-metal specimens made of steel, high
purity zinc reference-metal specimens may also be exposed in the tests in order to de
termine the corrosivity against this metal (see Annex B).
a) Use four or six reference specimens, depending on the size of the spray cabinet, that
are of 1 mm ± 0 . 2 mm thickness and 150 mm x 70 mm size, cut from -----------------------
SPCE-grade
cold rolled sheets or strips -��- ���-?-��-�-��-�--�-���--���- g -���-�- with an essentially fault
less surface and a matt finish (arithmetical mean deviation of the profile Ra = 0.8 µm
± 0 . 3 µm).
b) Clean the reference specimens carefully to eliminate all traces of dirt, oil or other
foreign matter that could influence the test results with an organic solvent such as
ethanol by means of a clean soft brush or an ultrasonic bath. Carry out the clean
ing in a vessel full of organic solvent such as ethanol. After cleaning, rinse the
reference specimens with fresh organic solvent such as ethanol, and then dry them.
d) Protect one face of the reference specimens with a removable coating, for example
an adhesive plastic film. The edges of the reference test specimens may be protected
by the adhesive tape as well.
a) Position four steel reference specimens in four quadrants (if six specimens are avail
able, place them in six different positions including the four quadrants) in the zone
of the spray cabinet where the test specimens are placed, with the unprotected face
upwards and at an angle of 20° ± 5° from the vertical.
b) The support for the reference specimens shall be made of, or coated with, inert
materials such as plastics. The lower edge of the reference specimens shall be level
with the top of the fog collector.
c) The parts of the test specimen support where the reference specimens are not placed
shall be filled with dummy specimens of inert materials such as plastics or glass
during the verification procedure.
�>-----�-�-��!.�-�-?:-�r_??__������11__�li-�--���-�-������-J?.��-�����-��-��-�-r��-���11-�_?:_a.:r._��-P.��-�-�-�--?_11_�_l?:�
supports in the spray cabinet instead of the dummy specimens of inert materials
----------------------------------------------------------------------------------------------------------------------------------------------------
like plastics or glass, and the test may be---------------------
--------------------------------------------------------------------------- performed---on both specimens
----------------- simulta-
--------------------- -----------
11_�_?.t:1:�-�:r.: ___�?-�-��--�li_i_�--���-?��11--�-1:1:�--�-a.�-�_,--��--�-���_1__?�.!��-�-���-?:-�?--�-��-�-�-��-!.�.r�!.�:-
�9��--: _ _ _ _ q _ a_ _r�_ � li a_ 1_ _�-?�_ ta_ .���-�li ��-�?_e_ ����-
_ r�11c_ �-� r��-�� �11s_ _ a_ 11_ �_ t_e�_ � _ sr_ ��j-��11�-��
not affect the test results of their counterparts.
e) Perform the test for 48 h under the test conditions shown in table 2.
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b) Clean the reference specimens carefully to eliminate all traces of dirt, oil or other
foreign matter that could influence the test results with an organic solvent such as
ethanol by means of a clean soft brush or an ultrasonic bath. Carry out the clean
ing in a vessel full of organic solvent such as ethanol. After cleaning, rinse the
reference specimens with fresh organic solvent such as ethanol, and then dry them.
c) Determine the mass of the reference specimens to ± 1 mg.
d) Protect one face of the reference specimens with a removable coating, for example
an adhesive plastic film. The edges of the reference test specimens may be protected
by the adhesive tape as well.
ports in the spray cabinet instead of the dummy specimens of inert materials like
----------------------------------------------------------------------------------------------------------------------------------------------------
p_l_��-����--()t_����-�l--���--���-���-�-!!.1.':lX.��-P.�!f�!:���--<?!.1..�?.��--�-(>-�-��-1:1:1:���--�-��-1?:��-':l.1?:�()-��}Y.:
Where this has been the case, it shall be reflected in the test report.
NOTE : Care shall be taken so that the reference specimens and test specimens
------------------------------------------------------------------------------------------------------------------------------------------------
do not affect the test results of their counterparts.
e) Perform the test for 24 h under the test conditions shown in table 2 .
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d) Protect one face of the reference specimens with a removable coating, for example
an adhesive plastic film. The edges of the reference test specimens may be protected
by the adhesive tape as well.
supports in the spray cabinet instead of the dummy specimens of inert materials
----------------------------------------------------------------------------------------------------------------------------------------------------
�-���-p_���-��-�-�--?-�__g}��-�-'--�!1-�-���--���-�--� ��--��-P.-�!f.?!!!1_�-�--��--���!1: -�P.���!!1-�-1?:�--��!!1-_l_l:��-��
?_�_?_l_l:�-�Y.: ___�?-�-��--���-�--���-�-��!1__ �?:�--�-��-�-'--��-�-��g-��-!�n�-���-�-�!1:-�-��--�-�-��-!.�r��-�:-
NoTE : Care shall be taken so that the reference specimens and test specimens
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ---- - - - - - - - - - - - - - - - ------ - - - - - - - - - - ---------- - - - - - - - - - - - ---------- - - - - - - - - - - - - - - -
do not affect the test results of their counterparts.
e) Perform the test for 24 h under the test conditions shown in table 2.
The solution used for chemical cleaning may be that prepared by mixing 500 ml
of hydrochloric acid specified in JIS K 8180 and 500 ml of water in 4.1 b) and add
-- - -
ing as a corrosion inhlbitcir 3.Kg ofhexamethylene tetramine (C6H12N4) specified
------- in ----- --- ------
drying.
c) Weigh the reference specimens to the nearest 1 mg. Divide the determined mass
loss by the area of the exposed surface area of the reference specimen in order to
assess the metal mass loss per square metre (g/m2) of the reference specimen. r_��--
-
form this removal procedure several more times until variation in the mass loss is
----------------------------------------------------------------------------------------------------------------------------------------------------
hardly observed, and determine the mass loss.
------------------------------
NOTE : It is recommended to use freshly prepared solution during every proce
dure for removal of corrosion products.
7 Test specimens
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e) In the case of using test specimens with organic coating such as painted coat, unless
otherwise agreed between the interested parties, preparation of test specimens shall
be in accordance with Annex C.
a) The specimens shall be placed in the cabinet facing upwards at an angle as close as
possible to 20° to the vertical, this angle, in all cases, being within the limits of 15°
to 25°. However, in the case of components cut from a product, they shall be placed
with the exposed surfaces adhering to these limits as closely as possible.
�f_-�_$"_����--�P�!?---������!?---�?-�-_�!?--���-�-���� _p_�-����� � _ ��-���- _�!?-�_l_ � __��>-'--�� _�-���-·_
b) The specimens shall be placed in the cabinet so that the surfaces to be tested are
exposed to free circulation of sprayed solution, and so that they are not in the di
rect line of travel of the spray from the mist dispersion tower or atomizer nozzle.
c) The specimens shall be placed so that they do not come into contact with anything
other than test specimens supports.
d) The positions of and intervals between specimens shall be such that no specimen
blocks free circulation of sprayed solution on other test specimens.
e) The sprayed solution on specimens shall not drip on other specimens.
f) For tests with a total duration exceeding 96 h, location permutation of specimens
is permitted. Where this has been performed, it shall be reflected in the test re
port.
If agreed upon between the interested parties, instead of location permutation of
------------------------------------------------------------------------------------------------------------------------------------------------
specimens, a device which rotates specimens around the mist dispersion tower may
----------------------------------------------------------------------------------------------------------------------------------------------------
be used.
9 Test conditions
The test conditions shall be as follows.
a) Prior to the test, check the test conditions given in table 2 by filling the test speci
men supports in the spray cabinet with dummy specimens made of inert materials
such as plastics or glass.
b) After it has been confirmed that the test conditions are within a specified range,
stop spraying the salt solution, remove the inert dummy test specimens from the
test specimen supports, mount the test specimens on the supports and start the test.
c) The sprayed solution collected in each of the fog collectors ( 5.6) shall have a sodium
chloride concentration and a pH value within the ranges given in table 2.
�9!.� :
_______ �:r_i- -�-1:1: �-���� -�r-��-� -���-�'--�r-�?-�--�.r�-�-��-�--�-��-".-��Y.--���-� �-���--�Y.- -�--��!?--�!-�Y.
Il1_e_t�r_-��--�it_lii11__t}ie_ __r13.11g
_ e__ o_f_ �:()_2_�__ t()__l_._()3_�_/3_�-��- 0_g_�-�--�q,_ _ t?:e_ _sa
_ lt
_ __C:()ll_-_
��Il��-�-���!?-__?X.�.1:1:�- �p��Y.��--�()��-��()!?-_ _��--����-�-�--�()- �()llf?_�Ill__�_C?__�?�--��q�-��-�---
ment.
d) The average rate of collection of sprayed solution in each fog collector shall be mea
sured over a minimum period of 24 h of continuous spraying.
e) The salt solution which has been sprayed shall not be re-used.
f) During operation, the salt solution should be free from dust and should be isolated
from ambient air to prevent the concentration of sodium chloride and the pH from
fluctuating.
47 CC ± 2 cc a)
--------------------- 47 CC ± 2 c c a)
--------------------- 63 cc ± 2 c a c )
---------------------
-- -- -- -- -- -- -- --
bl
-70- -kPa
- - -to
- - 170
- - - kPa
-- --
�?-��-� __a!___ _'�I)_l!l_I?_�!'_i:t_�'.1:�-� _��_ �-1:1-�_ i::i:t_�E:'. _?X _���J?.�E:'.�-��-�-_i:t�_i: _I?.�-� �-��!:�-_<?f. �� -��� -�- -� � -���·-
�!____�l?:�__I?!:�-��-'.l:i:�-�?_<?�!�-��--1!1_1:l_i_i:i_�����-�--l:l� -�-�-�r_l:l_=!=: P�-���:-
10 Duration of tests
The period of test shall be as designated by the specification covering the material
or product being tested. �f..1?:()�-A��-��ll-�-� ��?--��--�-1:1:��-l--��- -�:t:i_?.j�����--�() __�?-�--����-�-��ll�-�-�--
�-��-�-1?: -�_1:1:�-�-1?:��!:��-� ��--P��-��-� �:
The recommended periods of exposure are 2 h, 6 h, 24 h, 48 h, 96 h, 168 h, 240 h,
480 h, 720 h and 1 000 h.
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b) If the end-point of the test depends on the appearance of the first sign of corrosion,
the test specimens shall be inspected frequently. For this reason, this type of speci
men should not be tested with other specimens requiring tests of predetermined
durations.
b) Mass loss The initial mass of the test specimens measured before testing is com-
------------------------------------------------------------------------------------------------------------------------------------------------------------
14 Test report
The test report shall contain the following information. -Some of the items listed may
- - - - --------------------- - - - - - ------ - - - - - - - - - - - - - -
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3) others.
Annex A (informative)
Example of apparatus with means for treating
fog exhaust and drain
A.1 General
Figure A. 1 shows an example of basic construction and design of the apparatus meet
ing the conditions required by the main body of this Standard.
purpose, the temperature of the air saturator shall be kept at 4 7 ° C ± 2 ° C when the
------------------------------------------------------------------------------------------------------------------------------------------------------------
supply- - -air
----------- pressure in the NSS test is 98 kPa ± 1 0 kPa. In addition, the water in the
- - - - -------------- - - - - - - - -------------- - - - - - - -------------- - - - - - - - -------------- - - - - - - - -------------- - - - - - - - -------------- - - - - - - - -------------
��t-����!:��-?-� -����-�-��-������-��-<:1: -��- -�p_�-��!!:��-�!?:��!:Y���-�?.-��--�-?- -���-?�-�- -��P.?.��-����-�?--��!::
The spray cabinet shall be designed with temperature retention considerations so
- - - - - -------------- - - - - - - - -------------- - - - - - - - -------------- - - - - - - - ------------- - - - - - - - -------------- - - - - - - - -------------- - - - - - - -------------- - - -----
that it is not affected by fluctuation of the open air temperature. Sensors for tempera-
------------------------------------------------------------------------------------------------------------------------------------------------------------
ture control and for indicating the temperature and humidity shall be placed at least
------------------------------------------------------------------------------------------------------------------------------------------------------------
-1- -00 mm from the walls of the spray cabinet, and their temperature and humidity indi-
- - - - - - - - ----------- - - - - - - - - - - ------- - - - - - - - - - - - - - - ------ - - - - - - - - - - - - - - ------- - - - - - - - - - - - - - - ------- - - - - - - - - - - - - - - ------- - - - - - - - - - - - - - - ------- - - - - - - - - - - - - -
cations shall be able to be read from outside.
A.3 Exhaust
The exhaust shall not be done forcibly and shall be protected from wind pressure of
------------------------------------------------ - -------------------- - ------------------- - - ------------------- - ------------------- - - ------------------
the open air.
Preference shall be given to apparatus that has a means for properly dealing with
fog after the test, prior to releasing it from the building for environmental conservation,
and for draining water prior to discharging it to the drainage system.
3 2
13
4
5 10
0
0
8
a) Front view
16
5
15
6
Exhaust
17 11
19
20
b) Side view
Figure A.1 Example of apparatus with means for treating fog exhaust
and drain
Annex B (informative)
Evaluation of cabinet reproducibility related to
corrosivity (using zinc reference specimens)
B.1 General
This Annex describes a method for evaluating cabinet reproducibility and repeatabil
ity in the NSS test, AASS test and CASS test, using steel reference specimens as well
as zinc reference specimens.
�-��-��!:��-�-�-���!:l_ _P�?-�-�-�-1:1:�-�-·-
If agreed upon between the interested parties, test specimens may be placed on the
------------------------------------------------------------------------------------------------------------------------------------------------------
supports in the spray cabinet instead of the dummy specimens of inert materials like
------------------------------------------------------------------------------------------------------------------------------------------------------------
plastics or glass, and the test may be performed on both specimens simultaneously.
------------------------------------------------------------------------------------------------------------------------------------------------------------
���!�-�-1::�-�--1?--��- -����--��-�--�-�-��!--��--�-1::���--��--��x!����1- -��--��-�--����- -�-�-J?-?_��'.-
NOTE : Care shall be taken so that the reference specimens and test specimens
----------------------------------------------------------------------------------------------------------------------------------------------------
do not affect the test results of their counterparts.
Perform the test according to table B. 1 under the test conditions shown in table 2 .
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Table B . 1 Test duration and allowed range o f mass loss o f the zinc
reference specimens
Test method Test duration Allowed range of mass loss of (Informative) Allowed range
the zinc reference specimen of mass loss of the steel
reference specimen
2 2
h g/m g/m
Annex C (normative)
Preparation of test panels with organic coating
such as painted coat
C.1 General
This Annex specifies the method for preparation of test panels with organic coating
such as painted coat.
and without exposing them to direct sunlight. The test procedure shall then be carried
out as soon as possible.
a) Make a straight scribe mark through the organic coating to the substrate.
b) To apply the scribe mark, use a scribing tool with a hard tip. The tool should give
uniform shaped scribe marks.
c) The scribe mark shall have either parallel sides or an upwards-broadening cross
section that shows a width of 0.2 mm to 1.0 mm of the metallic substrate.
e) Scribe marks shall b e made in accordance with the following method ( see
figure C . 1), but other method agreed between the interested parties may be used.
Japanese Standards Association PROTEC TED B IS.len ��Jnfll �lolli EPY OF STANDARDIZATION 9972181
Provided by IHS under license with JSA tfo t for'Re'Safe , ��;t1�S""�:40:48
No reproduction or networking permitted without license from IHS
23
z 2371 : 20 15
1) X-shape scribe marks shall be made all over the test specimen surface or in the
--------------------------------------------------------------------------------------------------------------------------------------------------------
0
N
20 20
a) Example of X-shape scribe marks that are diagonals crossing each other
�r
�1
b) Example of single-line scribe mark which is parallel to the longer edge
0
N
0
N
0
N
22... 22...
c) Example of T-shape scribe marks that are vertical to each other
Annex JA (informative)
Arrangement and positions of test specimens
Unit : mm
30 to 50 Mist dispersion
For specimen 150 x 70 x 1
tower
Fog collector
Test
specimen
Approx. ¢ 1 00
Test
specimen
support
Fog collector
Annex JB ( informative)
Removal of corrosion products
Anodic oxide Hydrochloric acid (JIS K 8180) 10 ml 1 min to 20 °C to Wash the film using
film of Distilled water to make 1 10 ml 5 min 25 °C nylon-brush or a similar
aluminium tool which has been
immersed in solution,
wash with water and then
dry by ventilation. When
the corrosion products
remain, repeat this
procedure.
Iron and Hydrochloric acid (JIS K 8180) 1 min to 20 °C to Solution should be vigor-
steel 1 000 ml 25 min 25 °C ously stirred or specimen
Antimony trioxide ( III) (JIS K 8407) should be brushed. An
20 g increased number of
pickling intervals or longer
Tin (II) chloride dihydrate
times may be required in
(JIS K 8136) 60 g
certain circumstances .
Magnesium Chromium oxide (VI) (Cr03) 100 g 1 min Boiling The silver chromate is
and Silver chromate (Ag2Cr04) 100 g presented to precipitate
magnesium chloride.
Distilled water to make 1 000 ml
alloy
Chromium oxide (VI) (Cr03) 200 g 1 min 20 °C to The barium nitrate i s
Silver nitrate (JIS K 8550) 1 0 g 25 °C presented to precipitate
sulphide.
Barium nitrate (JIS K 8565) 20 g
Distilled water to make 1 000 ml
Japanese Standards Association PROTEC TED B IS.len ��Jnfll �l-lll EPY OF STANDARDIZATION 9972181
Provided by IHS under license with JSA tfo t for'Re'Safe , ��;t1�S""�:40:48
No reproduction or networking permitted without license from IHS
27
z 2371 : 20 15
Potassium permanganate
(JIS K 8247) 30 g
Ammonium dihydrogen citrate 100 g
Distilled water to make 1 000 ml
Sodium hydroxide (JIS K 8576) 200 g 20 min Boiling Zinc powder, which may
Zinc powder (JIS K 8013) 50 g naturally ignite by contact
with air, shall be handled
Distilled water to make 1 000 ml
with caution.
Zinc and Ammonium solution (JIS K 8085) 5 min 20 °C to After treatment with
zinc alloy 150 ml 25 °C ammonia solution,
Distilled water to make 1 000 ml additional treatment with
chromium oxide (VI) is
Chromium oxide (VI) (Cr03) 50 g 15 s to Boiling carried out for removing
Silver nitrate (JIS K 8550) 10 g 20 s the corrosion products.
Distilled water to make 1 000 ml Silver nitrate is dissolved
in water, and boiling
chromium oxide solution i s
added t o prevent a n excess
of crystallization of silver
chromate.
In order to avoid the zinc
attack on the metallic
substrate, chromium oxide
should not contain
sulphate.
NOTE: Chemicals followed by parenthesized JIS numbers shall be in accordance with the JIS
standard of that number.
Japanese Standards Association PROTEC TED B IS.len ��Jnfll �l.lli EPY OF STANDARDIZATION 9972181
Provided by IHS under license with JSA tfo t for'Re'Safe , ��;t1�S""�:40:48
No reproduction or networking permitted without license from IHS
29
z 2371 : 20 15
Lead and Sulphuric acid (JIS K 8951) 28 ml 3 min 75 °C Cathodic treatment with
2
lead alloy Inhibitor ( diorthotolylthiourea, 2 000 A/m current density.
quinoline ethiodide, or Use a carbon or platinum
13-naphtholquinoline) 0.5 g anode.
Distilled water to make 1 000 ml
Copper and Potassium chloride (JIS K 8121) 1 min to 20 °C to Cathodic treatment with
copper alloy 7.5 g 3 min 25 °C 100 A/m2 current density.
Distilled water to make 1 000 ml Use a carbon or platinum
anode.
NOTE: Chemicals followed by parenthesized JIS numbers shall be in accordance with the JIS
standard of that number.
Annex JC (normative)
Rating number method
JC.1 General
This Annex specifies the rating number method used for evaluation of the test re
sults of the salt spray test methods.
Table JC.1 Relation between rating numbers and corrosion area ratios
10 0.00
0 Over 50.00
The relation between rating numbers (RN) and corrosion area ratios (A) is as follows.
RN = 3 (2 - log10A )
However, i f the rating number (RN) i s 9.3 to 9.8, the following equation shall b e used.
RN = 10 - AI 0 . 1
Unit : mm
� dge is covered
l.f)
N
Surface to be 0 0
0 l.f)
evaluated .- .....
Edge i s
covered �
�
�
l.f)
N
10 50 1 01
l
70
�
• •
•
•
• •
• •
• •
•
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• • •
•
•
8- 1 8-2 8-3
Japanese Standards Association PROTECTED B IS.len ��Jnfll �lJll EPY OF STANDARDIZATION 9972181
Provided by IHS under license with JSA tfo t for'Re'Safe , ��;t1�S""�:40:48
No reproduction or networking permitted without license from IHS
37
z 2371 20 15
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Japanese Standards Association PROTEC TED B IS.len ��Jnfll �lJll EPY OF STANDARDIZATION 9972181
Provided by IHS under license with JSA tfo t for'Re'Safe , ��;t1�S""�:40:48
No reproduction or networking permitted without license from IHS
41
z 2371 20 15
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2- 1 2-2
2-3 2-4
l-l l-2
Bibliography
JIS H 8679-1 Anodizing of aluminium and its alloys-Rating system for the evalu
ation of pitting corrosion-Part 1: Rating number method
ISO 8407 : 2009 Corrosion of metals and alloys-Removal of corrosion products from
corrosion test specimens
Japanese Standards Association PROTEC TED B IS.len ��Jnfll �lJll EPY OF STANDARDIZATION 9972181
Provided by IHS under license with JSA tfo t for'Re'Safe , ��;t1�S""�:40:48
No reproduction or networking permitted without license from IHS
45
z 2371 : 20 15
ISO 10289 : 1 999 Methods for corrosion testing of metallic and other inorganic coat
ings on metallic substrates-Rating of test specimens and manu
factured articles subjected to corrosion tests
ISO 17872 : 2007 Paints and varnishes-Guidelines for the introduction of scribe
marks through coatings on metallic panels for corrosion testing
Tokuzou Kanbe, Shigeru Suga, "Reports on the Revision of ISO 922 7 Salt Spray Test
and the Development of Cyclic Corrosion Tests", The Journal of the Surface Finishing
Society of Japan, Vol. 58, No. 9, p .526-537 (2007)
Shigeru Suga and Shigeo Suga, Report on the results from the ISO/TC 156/WG 7
International Round Robin Test Programme on ISO 9227 Salt spray tests; J. Surface
Finish. Soc. Japan; Vol. 56, p. 28 (2005)
Japanese Standards Association PROTEC TED B J¥en ��IVlllU l'\t:�Y OF STANDARDIZATION 9972181
Provided by IHS under license with JSA N'O t for"Res'ate , �ot�lt 1�5"�:40 :48
No reproduction or networking permitted without license from IHS
Annex JD (informative) N >J:>..
l'V 0)
c.o
Comparison table between JIS and corresponding International Standard ---:i
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l'V
JIS Z 2371 : 2015 Methods of salt spray testing ISO 9227 : 2012 Corrosion tests in artificial atmospheres-Salt spray tests 0
�
Q1
(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical deviation (V) Justification
national International Standard between JIS and the International Standard by for the technical
Standard clause deviation and
number future measures
No. and title of Content No. of Content Classifi- Detail of technical deviation
clause clause cation by
clause
4 Salt solu- 4 . 2 pH adj ustment 3.2 Almost identical Addition JIS adds citations of JIS K 8576, JIS -
tion for testing of salt solution for with JIS. K 8180 and JIS K 8355 as those for the
(concluded) testing reagents to be used, in relevant sub-
4 .2 . 1 NSS test clauses. JIS replaces the ISO specifica-
tion of "pH paper which can be read in
4 . 2 . 2 AASS test Deletion
increments of 0 . 3 pH units" for routine
'"ti 4 . 2 . 3 CASS test checks of salt solution pH for NSS test
� with the pH paper of 0.2 pH units,
0
>-3 which are available in Japanese mar-
trj
0 ket. JIS also deletes the ISO specifica-
>-3 tion of "pH paper which can be read in
trj
l:j increments of 0 . 1 pH units" for checking
to salt solution pH of AASS test and CASS
� test, since such pH papers are not in
0 circulation in Japanese market. This
0
constitutes no technical deviation.
�s 4.3 Filtration of 3.3 Almost identical Addition JIS adds specification that freedom -
5 Apparatus 5 . 1 General - -
Addition JIS adds general requirements regard- -
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5 Apparatus 5.3 Spray cabinet 4.2 Almost identical Addition JIS provides an additional note consid- Under deliberation
(concluded) 7.4 with JIS. ering the case of cabinet volume less at ISO.
than 0.4 m3. JIS moves the specifica-
tion regarding test specimen support
given in 7.4 in ISO to 5.3 e). This con-
stitutes no technical deviation.
'"ti -
::tJ 5.4 Temperature 4.3 Identical
0 controls
>--,3
trJ
(') 5.5 Spraying device 4.4 Almost identical Addition JIS adds descriptions of "humidifica- Under deliberation
>--,3
trJ with JIS. tion of compressed air by means of at ISO.
t;j humidifier", "heating of compressed air"
td and "control of the flow of salt solu-
><! tion", in relevant subclauses.
(')
0 Alteration JIS alters the ISO specifications of
�
::tJ
water temperature for compressed air
of 98 kPa in table 1 , 48 °C and 64 ° C , to
0 47 °C and 63 °C, respectively. This
::r: constitutes no technical deviation.
>--,3
5.6 Fog collectors 4.5 Identical -
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6 Evaluation 6.4 CASS test 5.4 Almost identical Addition JIS adds specification that simulta- Under deliberation
of cabinet re- 6 . 4 . l Reference with JIS. neous testing of reference specimens at ISO.
producibility specimens and test specimens is permitted if
related to agreed, and also adds citation of JIS
6.4.2 Arrangement
corrosivity reagent standards and specification of
and test of refer-
(concluded) temperature of running water used for
ence specimens
'"ti rinsing in relevant subclauses. This
::tJ 6.4.3 Determina- constitutes no technical deviation.
0
>--,3 tion of mass loss
trJ
(') 6.4.4 Checking of
>--,3
trJ apparatus operation
t;j
7 Test speci- 7 . 1 Handling of - - Addition JIS adds requirements regarding han- -
td
><! mens test specimens dling of test specimens. This consti-
tutes no technical deviation.
(')
0
7 .2 Size of test 6.1 Almost identical Deletion JIS deletes the ISO specification that -
�
::tJ specimens with JIS. unless otherwise specified, test panels
Alteration
0 with an organic coating such as painted
::r: coat shall be used, based on the domes-
>--,3
tic situation of usage. JIS also alters
the dimensional requirements of test
specimens. This constitutes no techni-
cal deviation.
8 Arrange- -
7.1 Addition JIS adds for arrangement of test speci- -
ment of test 7.2 mens that "If the specimens are compo-
specimens nents cut from a product, conditions
7.3
agreed between the interested parties
shall be used". This constitutes no
technical deviation.
'"ti
� 9 Test condi- -
8 Almost identical Addition JIS adds the conditions "water tern- -
�
of tests nated, it shall be subjected to the
0 agreement between the interested par-
0
�s
ties.". This constitutes no technical
deviation.
::r:
>-3 test operation 9.3 the case where spraying has to be inter-
rupted, as it was given in its previous
9.4
edition, while ISO does not permit in-
terruption of spraying at all.
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01 t--'
14 Test report - 12 Almost identical Addition JIS adds the provision which permits -
'"ti
::tJ with JIS. omission of some of the items listed.
0 This constitutes no technical deviation.
>--,3
trJ
(') Annex A -
>--,3
trJ (informative)
t;j
Annex B -
td
><! (informative)
(') Annex C Annex C Almost identical Addition JIS adds examples to "preparation of -
0
(normative) with JIS. scribe marks", deletes the description
�
::tJ
Deletion
regarding aluminium, and adds
0 figure C . 1 . This constitutes no techni-
::r: cal deviation.
>--,3
- Annex D - Deletion JIS deletes Annex D of the ISO Stan- -
dard, since in JIS, the contents are
given in clause 1 3 .
Annex JA -
(informative)
Annex JB -
(informative)
Annex JC Rating number - - Addition JIS adds the "rating number method" -
(normative) method to "evaluation of test results".
NOTE 1 Symbols in sub-columns of classification by clause in the above table indicate as follows :
Addition: Adds the specification item( s) or content(s) which are not included in International Standard.
Alteration: Alters the specification content(s) which are included in International Standard.
NOTE 2 Symbol in column of overall degree of correspondence between JIS and International Standard in the above table indicates as follows:
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0
>-3
trj
0
>-3
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to
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0
0
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>-3
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