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AATCC TM115-2000e(2011)e

Test Method for Electrostatic Clinging of Fabrics: Fabric-to-Metal


Developed in 1965 by AATCC Commit- for information purposes only. The pre- × 300 plate must have a No. 4 finish (see
tee RA32; revised 1969, 1973, 2000; cautions are ancillary to the testing proce- 12.3.1) on the included angle side, and
editorially revised 1974, 1976, 1977, dures and are not intended to be all inclu- should be kept clean and smooth at all
1978, 1991, 1999, 2008, 2019; reaf- sive. It is the user’s responsibility to use times. A fine line is indented across the
firmed 1977, 1980, 1989, 2005, 2011; safe and proper techniques in handling test plate surface 230 mm from the top of
editorially revised and reaffirmed 1986, materials in this test method. Manufac- the plate and this is used to position the
1995. turers MUST be consulted for specific lower edge of the specimen (see 12.3).
details such as material safety data sheets 6.1.2 Variable Angle Experimental
and other manufacturer’s recommenda- Test Plate—The sensitivity of this test de-
1. Purpose and Scope tions. All OSHA standards and rules pends on the included angle of the metal
must also be consulted and followed. plate and can be diminished by decreas-
1.1 This test method evaluates the rela- 4.1 Good laboratory practices should ing the included angle or vice versa. A
tive clinging tendency of certain fabrics be followed. Wear safety glasses in all more versatile version of the test plate,
due to electrostatic charge generation. laboratory areas. suitable for research work, which allows
The test integrates the effect of fabric 4.2 The radioactive bar emits alpha ra- facile change of the sensitivity, uses a 25
weight, stiffness, construction, surface diation which is externally harmless to × 100 × 100 mm aluminum base with
character, finish application and other the human body. The radioactive isotope several slots machined into the base at
fabric parameters which affect the ten- polonium 210 is toxic and precaution different angles (e.g., 0.017, 0.087, 0.175,
dency of fabrics to cling. should be exercised to prevent ingestion 0.35, 0.52, 0.70, 0.87, 1.05 RAD) from
or inhalation of the solid material. Do not the vertical axis into which a 100 × 360
2. Principle take the radioactive bar apart or touch the mm stainless steel plate fits.
radioactive strip under the grid. If the 6.2 Grounding Plate—This is a 200 ×
2.1 Clinging of positively or negatively strip is touched or handled, wash hands 360 mm, flat, 18 gauge Type 304 stain-
charged fabrics to the human body occurs thoroughly at once. Return the device to less steel plate, attached to a ground, such
due to instantaneous induction of an the manufacturer when it loses its effec- as a water pipe, with wire (e.g., No. 18
equal and opposite charge on the surface tiveness as a static eliminator for reacti- stranded, plastic-covered electronic
of the body when the charged fabric is vation when tested in accordance with wire). One such grounding plate is re-
brought close to it. A basic law of physics 12.3.1 or for disposal if use is to be dis- quired for each test plate.
states that oppositely charged materials continued. Do not discard as scrap. 6.3 Radioactive bar (see 12.4).
attract each other. A metal plate exhibits
6.4 Rubbing blocks, white pine, ap-
a similar phenomenon of instantaneous
prox. 20 × 50 × 150 mm adjusted to
charge induction as would the human 5. Uses and Limitations
weigh 65 g and with strips of 20 mm
body when placed in the field of a
5.1 This test method is not intended for wide, double-faced tape on the ends of
charged material. Therefore, a metal plate
use in determining the suitability of fab- each block to attach ends of the rubbing
can be used to simulate the problems of
ric for use in hazardous areas where the fabric.
clinging observed between charged gar-
ments and the human body. Some indi- electrostatic generation of sparks might 6.5 Polyurethane foam, 25 × 100 × 300
viduals are more prone to electrostatic result in fires or explosions. mm non-rigid, having a density of 21 kg/m3
clinging than others, and a given individ- 5.1.1 Certain fabrics, particularly those and an ILD (Identification Load Deflec-
ual may be more prone at one time than at of heavy construction, which do not ex- tion) firmness of 6.8 kg when tested
another time. Therefore, fabric-to-metal hibit a clinging propensity by this method (see 12.3) as directed in ASTM D3574.
cling times cannot be related directly to might cling under some conditions of 6.6 Clamps, metal (e.g., No. 3 Bulldog
fabric-to-body clinging for different indi- use. Clamp or Di-acro Toggle Clamp, see
viduals. 5.1.2 This test method is primarily use- 12.4), with 70 mm edges covered with 20
2.2 In this test method, the time (td) is ful for determining clinging properties of mm electrical tape to prevent scratching
lightweight apparel fabrics, such as those of the surface of the test plates.
measured for the charge on a fabric speci-
men to decay to a level where the electri- intended for use in lingerie. 6.7 Stopwatch, with 0.01 min or one of
cal attractive forces between the speci- equivalent precision marked in other
men and the metal plate are over- units.
6. Apparatus and Materials (see 12.2)
balanced by the gravitational forces of 6.8 Forceps or tweezers, non-conduct-
the specimen acting to pull the specimen 6.1 Test plates. ing, ivory-tipped, forceps used with ana-
away from the plate (see 12.1). 6.1.1 Standard Test Plate—A test plate lytical balances.
(see 12.3) is made by bending 100 × 450 6.9 Oven, forced-draft type, capable of
mm strips of 18 gauge Type 304 stainless maintaining a temperature of 105 ± 2°C
3. Terminology
steel across the width 150 mm from one (221 ± 5°F).
3.1 electrostatic clinging, n.—adher- end so that an included angle of 1.22 ± 6.10 Conditioning chamber, capable of
ence of one substance to another caused 0.04 RAD is formed between the 100 × providing relative humidity control of
by an electrical charge on one or both 150 mm base and the 100 × 300 upright 40 ± 2% and temperature at 24 ± 1°C (75
surfaces. plate. The grain of the finish should be ± 2°F) with circulating air.
such that the 450 direction of the test 6.10.1 If tests are to be conducted at
4. Safety Precautions plate corresponds to the length or grain relative humidities or temperatures other
direction of the stainless steel sheets from than 40 ± 2% RH and 24 ± 1°C (75 ±
NOTE: These safety precautions are which they are made. The face of the 100 2°F), the conditioning test chamber should

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM115-2000e(2011)e 207
Copyright © 2020 American Association of Textile Chemists and Colorists
be capable of providing the necessary Table I—Safe Ironing Temperature Guide
range of test conditions (such as 20-65 ±
2% RH and from 10-30 ± 1°C [50-86 ± Class 0 Class IV
2°F). Class I Class II Class III 204°C and
6.11 Rubbing fabrics. Below 121°C 121-135°C 149-163°C 177-191°C Above
6.11.1 Nylon rubbing fabric—100% Modacrylic 93-121°C Acetate Nylon 6,6 Cotton
spun nylon 6,6. Olefin (Polyethylene) 79-121°C Olefin (Poly- Acrylic Polyester Fluorocarbon
6.11.2 Polyester rubbing fabric— 100% propylene) Azlon
spun polyester. Nylon 6 Glass
Hemp, Jute,
6.12 Fabric iron, domestic hand type, Ramie
with appropriate settings (see Table I). Rubber 82-93°C Silk Spandex Linen
6.13 Cleaning solvent: halogenated hy- Wool Rayon,
drocarbon metal-cleaning solvent herein- Viscose
after called HH Solvent. Saran 66-93°C Triacetate
(heatset)
7. Test and Rubbing Specimens Vinyon 54°C

7.1 Test fabrics—Twelve 75 × 230 mm


test specimens are required. Using die or
scissors, cut six specimens with the ing, state the temperatures used in the re- the 1.22 RAD included angle side with a
longer dimension parallel to the warp, or port. For any humidity or temperature metal bulldog or toggle clamp with the
wale, direction and six with the longer di- test conditions that are to be used, the test face of the test specimen out. Position the
mension parallel to the fill, or course, di- and rubbing specimens should be condi- lower edge of the test specimen even with
rection. (Do not cut fabric specimens tioned for at least 16 h (see 12.8). the indented line on the metal plate.
with a hot soldering iron or heated wire 9.5 Attach the metal grounding plate
since the edges can cause localized static 9. Procedure with the wire to a suitable ground and
problems due to heat degradation of the place it horizontally in the controlled hu-
fibers and antistatic agents.) 9.1 Clean the metal test plate before midity chamber and lay the polyurethane
7.2 Rubbing fabrics—Both nylon and testing every different lot of fabric. To foam on top.
polyester rubbing fabrics are required. clean, swab with a facial tissue saturated 9.6 Place the metal test plate with at-
Using die or scissors, cut six nylon and with HH Solvent (wear protective tached test specimen in a horizontal posi-
six polyester rubbing fabrics, each 75 × gloves). Allow the plate to dry at least 5 tion on the polyurethane foam in such a
230 mm, with the longer dimension par- min in the conditioning test chamber be- way that the long arm of the plate com-
allel to the warp, or wale, direction of the fore using. Make sure that HH Solvent pletely rests on the polyurethane foam
fabric. does not accumulate in the conditioning with the short arm of the test plate closest
7.3 Do not contaminate the test speci- test chamber as a result of cleaning the to the operator and pointing upward. The
mens or the rubbing fabric by unnecessary metal test plate. If the No. 4 finish on the clamp should extend over the edge of the
handling or by allowing them to come in surface of the test plate is changed notice- supporting foam so that the back of the
contact with transferable materials. ably due to use, replace the test plate with plate is completely supported.
7.4 If either the test or rubbing fabric a new one. 9.7 Place the rubbing block with at-
specimens do not lay completely flat, 9.2 Handle the fabric test specimens tached rubbing fabric at the top of the
press them free of creases or wrinkles and rubbing fabrics at only one marked plate so that the long axis of the rubbing
with a dry, clean iron at the appropriate corner to minimize transfer of impurities fabric and the long axis of the test speci-
setting as directed in Table I. Do not use to the remainder of the fabric. men are at right angles (see Fig. 1, Step
test specimens with curled edges.
9.3 Adhere double-faced adhesive tape B). The side of the rubbing block that
around all four 20 mm thick sides of the does not expose the cut edge of the rub-
8. Conditioning bing fabric should be down. Keep the test
rubbing block. Completely discharge the
8.1 Since equilibration of a test speci- rubbing fabric on both sides with the ra- plate and rubbing block perfectly flat on
men from the dry versus the wet condi- dioactive bar (Caution, see 4.2). Place a their facing surfaces to ensure complete
tion relative to the humidity of the test 50 × 150 mm side of wood block on the contact between test and rubbing fabrics
chamber may show hysteresis, precondi- rubbing fabric in such a way that the 150 during charge generation.
tion the specimens from the dry side rela- mm dimension of the block parallels the 9.8 Place the middle fingers on the
tive to the humidity in the test chamber. 230 mm dimension of the rubbing fabric back edge of the rubbing block and pull
To accomplish this, place the test and and the block is centered on the fabric. the rubbing assembly the full length of
rubbing specimens in the forced-draft Bring up the protruding edges of the fab- the test specimen (see Fig. 1, Step C).
oven at 105 ± 2°C (221 ± 4°F) for 30 ric so that they adhere tightly to the dou- Grasp the lock between the thumbs and
min. Transfer them immediately to the ble-faced tape on all four sides of the middle fingers at the ends of the block,
controlled humidity chamber allowing no rubbing block. Take care that the double- lift the assembly from the test specimen
more than 15 s for the transfer. faced tape does not extend to the area be- and return the rubbing assembly to its
8.2 Condition and test the test and tween the rubbing surface of fabric and original position at the top of the test
rubbing specimens at 40 ± 2% RH and 24 the block. specimen. Repeat this rubbing sequence
± 1°C (75 ± 2°F) in the controlled humid- 9.4 Grasp a test specimen at one corner 12 times at a cycle of approx. 1 rubbing
ity chamber for at least 16 h. If the test is and allow it to hang free. Discharge both cycle per second. The total 12 rubbing cy-
conducted at lower humidities (such as sides of the test specimen using the radio- cles should be completed in no more than
30 ± 2% or at 20 ± 2%), or at higher hu- active bar, holding the bar not over 25 15 s. For constant rubbing pressure, take
midities (such as 65 ± 2%), keep the tem- mm away from the fabric as it moves up care that the only downward pressure on
perature at 24 ± 1°C (75 ± 2°F) for stan- or down (Caution, see Section 4 and Fig. the test specimen comes from the weight
dard testing. If other temperature 1, Step A). Fasten the test specimen at the of the rubbing block and fabric.
conditions are used for nonstandard test- top of the long arm of the metal plate on 9.9 Quickly place the assembly in an

208 AATCC TM115-2000e(2011)e AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists
upright position on a grounded plate. watch immediately (see Fig. 1, Step F). the condition without assigning cling time
Grasp the lower right corner of the test 9.10 After every 30 ± 2 s, grasp the (see 12.9).
specimen with the nonconducting twee- lower corner of the test specimen with 9.12 Test three specimens in both warp
zers (see Fig. 1, Step D), pull the nonconducting tweezers, pull the test (or wale) and filling (or course) direc-
unclamped part of the test specimen com- specimen completely away from the tions against both nylon and polyester
pletely away from the metal plate to a metal plate to a point where the test spec- rubbing fabrics, using fresh test speci-
point where the test specimen is posi- imen is positioned vertically for 1 ± 0.5 s, mens and fresh rubbing fabric surfaces
tioned vertically for ± 0.5 s (see Fig. 1, and then release the test specimen from for each determination (see 12.10).
Step E), and then release the test speci- the tweezers.
men from the tweezers. Start the stop- 9.11 Record the time, to the nearest 0.1
min, for the fabric to decling of its own 10. Report
accord (see Fig. 1, Step G). Disregard
any tendency for the test specimen to 10.1 Report the time (td) to the nearest
continue clinging within 25 mm of the 0.1 min required for a test specimen to
bottom of the holding clamp. decling from the metal plate as specified
9.11.1 If the time is greater than 10 in 9.9 and 9.11.2. Report the three indi-
min, discontinue the test and report td as vidual values of tests in both warp (or
>10 min (greater than 10 min). In some wale) and filling (or course) directions as
cases, a different “maximum cling time” well as an average of each of the three
period may be chosen. In this case, report determinations, reporting separately the
the actual maximum cling time used for times (td) obtained with both nylon and
the testing. polyester rubbing fabrics.
9.11.2 If the test specimen declings 10.1.1 If the td value of two of a set of
almost completely but persists in clinging three test specimens is less than the se-
in a small localized area in addition to the lected maximum cling time selected from
area within 25 mm of the bottom of the 9.11.1 but the td value of the third test
holding clamp, discard and test an addi- specimen is greater than the selected
tional specimen. If this condition is ob- maximum cling time, report the average
served in all test specimens, note and report of the two determinations which are less
A

B C D

E F G

Fig. 1—Principal steps in conducting test.

AATCC Manual of International Test Methods and Procedures/2021 AATCC TM115-2000e(2011)e 209
Copyright © 2020 American Association of Textile Chemists and Colorists
than the selected maximum cling time experimental error (see 12.7). 12.5 The clinging behavior by this method
and disregard the td value of the third test 11.3 Bias. Electrostatic clinging can be of test of clean, finish-free 100% cotton fab-
specimen. Report that the third specimen defined only in terms of a test method. rics can be used as a reference point for anti-
exceeded the maximum cling time. static behavior of test fabrics of similar
There is no independent method for de- construction and weights. Garments made
10.1.2 If the td value of two of a set of termining the true value. As a means of from such clean, finish-free 100% cotton fab-
three test specimens is greater than the estimating this property, the method has rics are generally considered to be free of
selected maximum cling time, report the no known bias. clinging problems under use conditions.
td value as greater than the selected maxi- 12.6 Gayler, J., R. E. Wiggins, and J. B.
mum cling time and disregard the td value Arthur, Department of Textile Technology,
of the third test specimen. 12. Notes and References
School of Textiles, North Carolina State Uni-
10.2 Report the percent relative humid- 12.1 For details, see American Dyestuff Re- versity, “Static Electricity Generation, Mea-
ity and the temperature at which the spec- porter, Vol. 56, 1967, pp345-350. surement, and Its Effect on Textiles,” May
imens were tested. 12.2 For potential equipment information 1965, pp11-12.
pertaining to this test method, please visit 12.7 The statistical analyses and related
the online AATCC Buyer’s Guide at www. data are on file at AATCC, P.O. Box 12215, Re-
11. Precision and Bias search Triangle Park NC 27709; tel: +1.919.
aatcc.org/bg. AATCC provides the possibility
of listing equipment and materials sold by its 549.8141; fax: +1.919.549.8933; e-mail:
11.1 Precision. Extensive interlabora- ordering@aatcc.org; web site: www.aatcc.org.
tory evaluations run in 1955 on woven Corporate members, but AATCC does not
qualify, or in any way approve, endorse or cer- 12.8 At a given temperature, accumulation
fabrics indicated that, for the fabrics tify that any of the listed equipment or of static electricity generally is greater the
tested, the 95% confidence limits of this materials meets the requirements in its test lower the relative humidity (and vice versa).
test are ± 0.5 min (see 12.1). methods. For example, fabrics which show a low degree
11.2 An interlaboratory test on tricot 12.3 Available from AATCC, P.O. Box of static accumulation at 40% RH and 24°C
fabrics was run in 1975 which involved 12215, Research Triangle Park NC 27709; tel: (75°F) may exhibit severe static accumulation
the following variables: +1.919.549.8141; fax: +1.919.549.8933; e-mail: at 25% RH and 24°C (75°F) while fabrics
5 laboratories ordering@aatcc.org; web site: www.aatcc.org. which exhibit static problems at 40% RH and
12.3.1 The specified No. 4 finish on the 24°C (75°F) may exhibit a low degree of static
4 fabrics accumulation at 65% RH and 24°C (75°F).
2 levels of laundering standard test plate shall be as specified in the
ASTM Metals Handbook, Vol. 2, 8th Edition, The relationship between the tendency for
2 fabric directions 1964, p599, which states: “Following initial static accumulation and relative humidity var-
2 relative humidities grinding with coarser abrasives, sheets are fi- ies with the specific antistatic agent, fiber, fab-
2 types of nylon and 2 types of polyester nally finished with lubricated 120-150 mesh ric construction, surface charger, etc.
rubbing fabrics abrasive belts.” The resultant No. 4 finish sur- Therefore, although 40% RH and 24°C (75°F)
Based on the results of this study, the 95% face roughness expressed in micro-inches is are the standard conditions for the test, signifi-
45 maximum. cant information as to the probable antistatic
confidence limits for the average decling performance properties of a fabric may require
time of a set of three observations, none of 12.4 Since the polonium in this radioactive
element has a limited half life (approx. 6 that tests be run also at a lower relative humid-
which exceeds the maximum cling time of ity, such as 20%, and 24°C (75°F), an atmo-
months), the radioactive bar must be checked
10 min, is ± 2.0 min for tests at 20% RH periodically to be sure that it is sufficiently ac- spheric condition not unusual in modern
and ± 1.7 min for tests at 40% RH. tive for complete removal of charge. The ra- heated and air conditioned buildings. Com-
Some of the fabrics tested did not cling dioactive bar may be checked by testing a plete evaluation may also require tests at the
at all (0 min) while others clung more specimen known to exhibit a cling time of at upper level of 65% RH and 24°C (75°F).
than the maximum 10 min, at which point least 10 min when tested as directed in Section 12.9 Clinging in a small localized area can
testing is discontinued. In this interlabo- 6. A jersey stitch nonantistatic heatset 40 be indicative of the presence of foreign mate-
ratory test, 576 different test conditions denier nylon tricot fabric free of finish or rial or some irregularity and may not be char-
scoured and in the range of 50-100 g/m2 is acteristic of the clinging properties of the
were listed which involved 1,728 individ- fabric lot from which the test specimens were
satisfactory for this purpose. The fabric
ual decling measurements. Of the 576 should be charged as directed and then deion- taken.
test conditions, 469 contain at least one 0 ized with the radioactive bar. If the test speci- 12.10 Since several determinations some-
or 10 value. Only 109 contain no 0 or 10. men shows zero cling time, the radioactive bar times can be run concurrently, time can be
Any set of these replicates containing a 0 is sufficiently active for complete removal of saved by having several test plates and
or 10 cannot give a valid estimate of the charge. grounding plates available.

210 AATCC TM115-2000e(2011)e AATCC Manual of International Test Methods and Procedures/2021
Copyright © 2020 American Association of Textile Chemists and Colorists

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