Chem 242 Lab 4 Qualitative Unknown

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Fw per Nowe fotes (glee), aA @ pert HO NIA \ OA18 SL Saini bicowtnate (NAAC,] Writont S40 Blo IM Naot Coast ratory 134.917 | | 23 tm tel Conrhiee item — | 36.46 10% YAPROMA (olubiliby) haglitho| gers) sboxid , imatemt He peor UA) iettant cosine |1AT eprepino | (altel) annalle oc amittint | Go. | ¢ Leraatdehyhe (oldelyho) — |Mamwnable dexic arnt | (06.124 |__| U3 deers Unto (DP) " 1) [tong (eet a DNR A ap ope earl \ ToL t AS To ethanol CECH) |Fermas'e, toric, orth, WH Yb OF | fvininal | PLekone (etre) | flarmae, toric iting | 98-07 Lebnkerre | (Alia) |fommnaila does miter [Af rs ee Garner (Cerium) xi ao vite wept [fei 7 nlite rie S48-Uo 0.5 ml | a dioxane female, ae oniveg,| 86-UI Low | \eakano | (hat) | flunmaste, tery © |\5023) | \deoy \ F | Jeoorg @ pumphthel | Lthenel) erik amt Bet | bey ‘Signaiure et Date jinessiTa Pp 1 | "THE HAYDEN-MeNEIL STUDENT LAB NOTEBOOK Note: Insert Divider Under Gopy Sheet Before Writing a Exp, No. Experiment Subject Date Lage 4 Name ]iab Parner oe Causes | Gwo [ e TZ. Reudure (vayl) CD Sceabinety Tekh Comp) Ae-Smal wears Cemboal, acidic, basic) & acidic bane Weely Hoyo ladle ernai| Melin Gy weet Tre Px Se Bens eos 7m D FEE compounds (Lenephthal, beritsicacid, n-propiinel, sensaldeyle ), and umtrowm Solid , add 2-3 deo py (Lipuds) o S-257 Golids) het tnse wl Umb solvent ond. o.ctogs) 1) Vetpar® 4 tere tubes wi labely ¢ DU Emb pure tho Dime 7M Nao 3) tme S% Nato, Hime (M HUI 3) Fe e/ tere mrpoand » pct U-Bdeeps mw .0lg in TH (—F q) kepeat Ge eh tee Cmpoend, men ol emwigtlas EAE mien A tangs omypeats (solids) short be- washed 5) Gwe ting war ae C) iF compound idrolves ih pure Ho , chetesetl + yor Can Lbs 1 # (obrpund witl be disselvabe at all pis —F tums @ idm & —bares | low MW tums @ ttm P- acd | oerine litmas wubaryed —Apteo( llewm (A?) ee mw )] Date winess7TA a [Date Signature ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK ‘Note: insert Divider Under Copy Sheet Before Wnting ate 3 ae + [iccmuuaas “pine eererner Be, eae F_Oesewnins /eetales_(DegI) | + Unknown solid > VU SPEC. Un Pann = = Petal set geld ~deay Uke to GSlov > Seago Yellon Mt dindeliva mergeen ly act bette an werting Ruy = 136 os Be 139, Z mete: D dolusility Tere ou 5-546 lame . ? 1) Lewaphthel Coat pherel ) OO a Br expect T ies, S Cwaots), CE)/s? ( NattCo; ) 1M ot U 5 he Noo\s Haw 3 Im el ? © l LY) bewwit acd (sored CR) Nw —rexput EZ (Wyo), ¢ vaorr), 5 (HaHCo;) U U U J 4, wwe pe Sco, hy 3 ean A afk) = on oe s eas ) Un lors Agen a Os paper = |) \ (enpusk rental fem 4Ul Za bry yellow to gr wowhle7, Sei Na aut a bate esata Date Signature ‘THE HAYDEN-MeNEIL STUDENT LAB NOTEBOOK Note: Insert Divider Under Copy Sheet Before Writing Expermen/Subject “BNO lakieial ED [ite [Seciinte. ——_| 4) benaaldehyde Cepud SB) cr eget THY, Yi hay, Tcua) Rack U U oc whe wusot) WU patio, 7 nenown. Fes WP TASALble TSH he agolable Aabe Joe elle qk Yet ne (2 we ink se ep 0 Naot, palo, HCl ae Wey functional ree! Ad, tore aleokd, Clee @® onr tet (rekloonge veazont ) 6 2K wed = rH WW byiy Y) dretore Cuiymid (atone? dew ange yellow precipitate, Sho Fell) 2) U-batemel CLamid allel) eye Spengect he rae A Light ry Vet 3) benrzogharere (5atich ety ow epee PRA: petite oa LJ noes ee toe Leh gr YJ “a er pie veto yee) tat som (ee peapeote ) _ | ignature ate “Hl hk 5 A ‘we ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK “ee geen = wo eo eee e @D Grime test (yellev env) 7 r alee) AXA, UJ (Hasna) ? ae ae 1) u L) (Hg, D) r-nwphdbo\ éatrd ise) Darah ol oe ard) oo LU U Case) 3) beneeie acid (slid lege CA.) co Ar FPeHPE ne sae ae preeytene ) Unenonr Qawey cos beh dow pecig Pt) DW. rowdure (NMED (ur dioxane) brow oa ” Fal POM dom Fond aristable sdeed ) Jorcin roy | y wigs chloide Co) - if sludic, use OC, e yu iF Solutle , 2 DO 3) oMSo LUimetylsntfoxide) We sluie, de DMSO-—dy D Atone —ifsolwle , we Acdtvre —de ie pour net poluse it ay hunk » ask TA! ~ ob L sob g sek ae Ta tertonre, dissolv Uml solvent wi) 0,022 4 colth enero $ To ppt NIKE tnhe) woe Fo - = Fo mg solid (0.0754) ond Deb mb MME solvent, — HH TR SIF HO¢go [EL Un ne dire pid ont - dm Bay KW kbs om Re? e Sonate Date WinessiT& Date _ | THE HAYDEN-MeNEIL STUDENT LAB NOTEBOOK Note: Inert Divider Under Copy Sheet Batore Witing 4 Fixes er a Sperlee Cousek CHEM) | Ta a aoe Toa ewe [ Deco. __[Sectentior 242 180 & zr. Safety Hagerdy Coney A Ube Gann bumverd are ont, nettudont ir allowed omy 8 Flomimable —vaatenalys | 1 P Bunsen kumer flame hold be wrpact £ slug (nutlage £ yellow) + By Balstein, hold Compornd te ee eisremds! 2 + be Corti ‘of het wetall Chet spatula) DO feactinn Table Cou yD: Crate | Meer [Stole emt fel Unto (belsteih’ pz ) ; Gem Bie Arid (CAL) | daiteurt , comese 222 - Bromebenzene (Kihe}] Menmalle vntert |15% 01 L Un {ignttine) [-octetenc| (nbshel) D. Rroedune (Pag 2) eet) cel Pee 1) Betseein hale 2 RUITVE TST = ary haleyon! @€ 0 ; (bed grt pare) 1D Abjath bensen lawman Rome yr ith LYE | 2) bend ond of copper wire te form email clered los 2) beat fre lop until it pled bay Ny Cremona whey) a) ek vive val a x) Pip wre ety info umbvaun bang (& if solrk ound venlt siete te Copper) aoe ¥ > paw inal Sinai of warternanan orbs wuitetle 9 lal epee Taek copper wire with 2 the a BS Place wre rte wise Untnrowes Le (solid shontel adhere) Wee Flume (Lompeund vill burn at frag) = Yellan , sesty =) ee » a Oy pose TET = TOR wax a J Face smatl amount of umpora on srectala sre ke Hare & Biseme Sootj ness Crot ened isl) ¥ y Raw wire we Eves 2) ‘Flanne = (ow H = libely (Srseina es ello sorb (smobay) lamre ie iS e blee , Clean’ ame = hiyh H = bles not bengere Date TT wiinessrin Date [Sionatore Note Ingen Didar Under Copy Sheet Before Wrting E ‘JHE HAYDEN-MeNEIL STUDENT LAB NOTEBOOK ea TZ tepaits ond vssemations (Page)? nother 1) Belytemn esp | | Secton No € Genzeit Acid Fromobensene Unter troudor ite oS) 1 2 why Hare 4 expect no vly O eagect greets glstein x Tynan Tex Bemeit Aid boctadecane | Uae 2> g> € ext yellow, expect ble, sorty fama Chew Mame 7 ea) ? Qunive?) DME \ D watylere dhlerde pam .- Le GM too eral e Dale winess7TA Date Signature (te: Insert Dwider Under Copy Sheet Before Writing ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK ‘Note: Insert vider Under Copy ewe : ae Sate (Seite. € ~ palm PoC for Solid & Aird tn trouns | Nitro Groups Lseumdany £0) WE Srog MISCO um AND ~I3Sbum”) + Eewons Hydroxide, Tere Positive = ved brown precipitate Qed \) Su test ata tube , add ve wgtcene Sel o- x : ms Lomb Sh meee LP win Balla 2 Mix well! pce Ldrep 2M salient ai Hz Im UM pete Wan Lenk EM pete Sine iy Liaise ro 6) Cap ube 2 shake vigorously | BD) Look fr ved-bown precipita Tet Lompound 2 2~ nit votoluenc, xz. Safety & teartinn Table € eNO, + Felel), —> P-NH, + FeloWy Chemical Safety Nees | Bu Amounts fame oe Nana. | ety [Selon | | an Bn, og Slo femous ammonium galfateles)) iwitarrt 342, Me LS Wh UM satis ach (H,30y) | comosive Ut stan) vitor] (deg 2M Folbin methane! — [flammable , worst, [nt tox Tenitrotlvene (Lipeil) Axis | Baiinaynil AST S dives Lome CAS Slo GRNYSD, laa — s, pr? 10 gare Sos Pemons nats ) ‘ pe eee we y se 54 Fry can wate sullee a 3s iO “tt 5; e (ye depart 2 19 fat [Senate Date WinessTa = 1 : eee THE WAVDENLNGNEIL STUDENT LAB NOTEBOOK I ¥en On Saw Co oon veg Tab Parner = RINo Desk [Secton No, Amives (Day 3) Nitros Avid Tes = PHIM for 7 2* MleyLamines ; (Sanilinas, possity wittig Be ° HN 3 Gatley | array ? (Palka ammes SD diazninn don, ™ ° wo, Nz when cold ved L UF 2274 (amines diatonivons fom OS ate dye oe pwning eye mee wt wg > rere eer aa me = yel fo empoenal Ca | Salery Nokes | nw |r ma plone!) | Gv} Une 5 7 contented Satie il So, eeesbey iy Sere [0% 04. sedis witvite NWO oid Brg, kone ated] / Bomaphctive |, iL Write, Coro / (Won (0.1) lol. aq. Naot Loose URL f aniline. (I" yt) ic, er eit, cord 10 drwes | / |] woretinslaniline (v'arj|) | Aemmmetle toric — | 10 dvwps Wcey loving (171k) [fowmemate oxic natant to dveps ! Ro cedure _ lege 1) Add (00 J gelid ov 10 devps liquid +e ter4oube. 2) paselve z 5 ZAC Dio 6 dikes ununtratad salient avik (5%) 3 ‘Tou nti FER ammonin swlface pitta ATP sof add ~4rmel DI bo +o vedissolve sare as much as posstole D COOL soln, W eo bat POST peepee 426k ube with Zmb 0% 04, NANO, Csudinm nitvite) Fe DET cots Oe eed ek iy, ) pete sevond 4004 tube wath 109 my (0-1 ) prnaphthel dirreh ik Lenk lore MeOH and one Dt se eae veel Signature Date wiiness/Ta = | ‘Note: Insert Divider Under Copy Sheet Before Writing ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK Name Tab Partner Locker € (HM,) _ 67 Add GIA) sodium nitrite NANO, PLOPUISE -to Geoled) soln. of Amie RE Luntnown) while shaving eee abe T AP Lok Be bubbles of Mz (dente enfuse with brown nitregen onic gas’) HIE nabstantial bubbles (gas) at O°C —P_I? alg! onming K Fivmsstion of yellow oil /y eller solid Ldomprmd > 2? ber 3°) dimire # if (tle /mo Mz gas at 0°C > HAL HALE sol “Cumrmoun) 9 take BALE soln (unten TT) tetttue Ts (ee) amd norm te OT and add duepwite Ate (td 6 -naplcthel soln. +000 IN jwbath! (0%) tate ees aw dye = (° ary) C frceyn ete. Aine sk oun ds 2 Nine ({Parglamine ) ant , ani (aninire ea edness ae boty | ne CI? alrgt Disposal wr pesidyne fiom hitww acid 425 ite ae vale Xai unl 6M Hl = loK for Me as baile —bayslas 2 Pay r Amare Signature Date Witness/TA ~ Date 7 "THE HAYDEN-MeNEIL STUDENT LAB NOTEBOOK Note: Insert Dwvider Under Copy Sheet Before Writing Exp. No. Experiment Subject CAB 4 “Bare peated Beskno Eooee od € | Obiewatt Nitreu Aud Test “Unto TT Vata TT Lefers MaNOr ater NaNOz Pa ae HOE ore EE A paeN* Y ko) Ne ells! gow) d +e OT ater adding Prrapithe| /MLolL solh. ey ight anspor veer elo hs, ems ‘ate en i i NS a A een aud +eb+ > Ue engl sein Ce C € 7 Sionaiure Date Wiiness/T& Dae ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK Note: inser Dwvider Under Copy Sheet Before Wting ne £ Tara aay ———|fausoa —— _ Dako |Sectonno. e Corbrorey |" aids Sodiwin bicarbonate erp Aremni Ll ( safer: fu | Prmananky ( ho Ulivi) on ann Kar te | jvritent BH OF | | odinon bi aan ' Sh y.s Chatto, wer Prue TD Dissolve small among compoind (0.0.97) th S% Sedo bitartonate ea eoncod abhles Coratts (0b servactitn, LZ pun Geanbente payed yellay om test a wo Tonle Saale Date Wiiness/Ta Date ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK Note: Insert Dwvider Under Copy Sheet Before Waiting — —_— Sa hey — * ___ [es Eas Potential Amires J 1,4 -diams bon tena PyPBine -2~ Grteylie accel AN SS ( 2 ott x Y " X OH \ xX wr “nveth Y } T—methory-¢ “nik voanil re » edie lim tic ecrel Nu \ Ox at io a \ ae Y PR: Heo HEC | ) Acetmide mf DNso (53°C | vA eo" Gensamabo Ms / 7 {ore | tonitroaniline oy? Mur 46 Ved “C SG Aroternidlesf 2 USC pemaamide Ye (11°C po Wt anda= 135-84 quctamid, (atone 1) Signature Date ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK WitnassrTA Tae Tote: inser Divider Under Copy Sheet Before Writing a i Acetamids (Arning deviate) Procedunt, shins ctd £7 Hey we Tab L D Mae au ve a sy eaten aces. sens amd Om L acetic an de 2 wet 4 < asieg A men v ix rates \FT mixture 2 he 5 CA REX reeip tote. produc} a 1 ne preewaods Guns, Seratol re of Alase 8) Collect Lepr _, Sttratim cor ash podwet Ce a) reer in allize fom Som ethane! /4_0 a * 2a Amine» gon mage wing Arlee iepern gate mte aes conden ter aa (fetter, guetlnak nf Sut Sh aiey mip aud wens: re ne et tes | fr fee ! peel oF as uel nal Iydnde Soon ae: a tye bine! Gols SIFT SIT Reflng —we fe ft “Aker ote ea le Cinaee id? er ton) shile = Wh for decimntina 4 He + mA yale rentirte ' ej W NUR? wee aan we (No “dba the/pes Wife daolight (eemsps neorYe [Sionstore Ee Witness/TA Tose 5 ‘THE HAYDEN MCNEIL STUDENT LAB NOTEBOOK a . J Note: Insert Divider Under Copy Sheet Betore Wing e NBO a Berzamide Ro D Mx oe emis, pen omd Iml 10% Mactt ih » Ao pats a5 Ss! 3) lap ond Firate Abe ee ain ngorngy SEF s 9) adpye pit > me HEL of Pa bH i > ee [pitocte ca cal aint revatio Loalhcoldk Wo 6) Recrgstallite Kor SOD rretuse of ethane! / Hp? Reedy, & YD ln small RGE, disdve 0.25 amd Zisr me olene D AA 0.15 mE chloide ook amine In Emme py ning PY 3) efx fr © lool row and pour if inte TO me Hye ese tee (real tate product SD Blker and nhie cp tate. and it shold Se safer yea == wie firth ane Imo se Os 4 benny ce ORF Tay = OAL \. (Bain Signature Date Twiness7TA Date ‘THE HAYDEN-McNEIL STUDENT LAB NOTEBOOK Tote: Insert Divider Under Copy Shest Sefore Writing mans of Alar pore = o.ttlg FR mass = OOF = FP+ ode = a ae We yale der Io e Ae yx tee DY Cusv°e) Prater Mp beremide | mf acetamide (153 C) peta ce $3A- 40 -\ 1382-342, ~007 — Bereumide 5 - SW/so wetane | (th, 0 MP Ceeryztallieed Dome >? [Sint wethane J 84 Smee 0 Lee 152.3 = 0.0: clans ate Oy K Lobes pe vealed = 0.464 9 ating iN aauonrt dint fom cet, res golatiltty teres, DUE, pelted ipiitimy morstond frevant Lumengal Unerni 4 Sy y allow 1 Rather cyptta\ tats, Wlataimide anvetie, OFX ig gha 2 NM, cond LE, the Dato (pli) 0. 407 Worsitparc tts) yi lietly U—Wrethocy—Enitvoaniiine , os reogptal\t do TAa Wn fort vepulEed Wh A Fale poyilve, arnde = ost as pected oF ary anes, “Takveg ete ” my duet Atwowmrt HY WME, MY, onda ter c “ forthe specbeivspy igus) unworn plant TS \ieely TLhlvobourartabye, [Sinatre Date [wiiness/TA z I Date ; ‘THE HAYDEN-MeNEIL STUDENT LAB NOTEBOOK Note: Insert Divider Under Copy Sheet Before Writing spe ene

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