Heat Stable Reactor Heater 1.5 KG - HR (9.24 MM ID Tube)

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Output Summary Page 1

Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
See Data Check Messages Report for Warning Messages.
See Runtime Message Report for Warning Messages.
Process Conditions Hot Annulus Cold Pipe
Fluid name hot oil LA +water
Total flow rate (kg/s) 0.0114 4.17e-4
Inlet/Outlet Y (Wt. frac vap.) 0.0000 0.0000 0.0000 0.0000
Inlet/Outlet T (Deg C) 210.00 200.00 30.00 200.00
Inlet P/Avg (kPa) 301.32 301.32 2101.3 2101.3
dP/Allow. (kPa) 6.27e-3 30.000 2.34e-3 20.000
Fouling (m2-K/W) 0.000176 0.000176
Exchanger Performance
Annulus h (W/m2-K) 41.26 Actual U (W/m2-K) 36.96
Pipe h (W/m2-K) 637.36 Required U (W/m2-K) 31.05
Hot regime (--) Sens. Liquid Total duty (MegaWatts) 2.93e-4
Cold regime (--) Sens. Liquid Eff. area (m2) 0.171
EMTD (Deg C) 55.2 Overdesign (%) 19.04
Jacket Geometry

Jacket ID (mm) 52.502


Series (--) 1
Parallel (--) 1
Orientation (deg) 0.00
Pipe Geometry Nozzles
Type (--) Plain Annulus In (mm) 15.799
Pipe OD (mm) 13.716 Annulus Out (mm) 15.799
Length (m) 4.000

Pipe In (mm) 9.246


Pipe Out (mm) 9.246

Thermal Resistance, % Velocities, m/s


Annulus 89.55 Min Max
Pipe 8.60 Inside Annulus 7.16e-3 7.21e-3
Fouling 1.62 Inside Pipe 5.97e-3 6.97e-3
Metal 0.23

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Final Results Page 2
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Process Data Hot Shellside Cold Tubeside
Fluid name hot oil LA +water
Fluid condition Sens. Liquid Sens. Liquid
Total flow rate (kg/s) 0.0114 4.17e-4
Weight fraction vapor, In/Out (--) 0.0000 0.0000 0.0000 0.0000
Temperature, In/Out (Deg C) 210.00 200.00 30.00 200.00
Skin temperature, Min/Max (Deg C) 58.46 200.58 55.59 200.41
Wall temperature, Min/Max (Deg C) 57.44 200.52 57.11 200.50
Pressure, In/Average (kPa) 301.32 301.32 2101.3 2101.3
Pressure drop, Total/Allowed (kPa) 6.27e-3 30.000 2.34e-3 20.000
Velocity, Mid/Max allow (m/s) 7.20e-3 6.67e-3
Mole fraction inert (--)
Average film coef. (W/m2-K) 41.26 637.36
Heat transfer safety factor (--) 1.0000 1.0000
Fouling resistance (m2-K/W) 0.000176 0.000176
Overall Performance Data
Overall coef., Reqd/Clean/Actual (W/m2-K) 31.05 / 37.56 / 36.96
Heat duty, Calculated/Specified (MegaWatts) 2.93e-4 /
Effective overall temperature difference (Deg C) 55.2

See Runtime Messages Report for


warnings.

Exchanger Fluid Volumes


Approximate annulus (L) 8.1
Approximate pipe (L) 4.50e-1
Exchanger Construction Information
Jacket ID (mm) 52.502
Exchangers in Series 1 Parallel 1 Total area (m2) 0.172
Eff. area (m2/exch) 0.171
Exchanger orientation angle 0.00

Weight estimation Wet/Dry/Pipe 65.14 / 56.61 / 3.03 (kg/exch)

Pipe Information
Type Plain
Overall length (m) 4.000
Effective length (m) 3.968 Outside diameter (mm) 13.716
Total tubesheet (mm) 31.750 Wall thickness (mm) 2.235
Area ratio (out/in) 1.4835
Pipe metal SA-214 Tube (W) K01807

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Final Results Page 3
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

Annulus Heat Transfer Corrections


Total Fin
1.000 1.000
Pressure Drops (Percent of Total)
Annulus Ends Nozzle Annulus Pipe
13.03 1.77 Inlet 42.64 0.74
MOMENTUM 0.00 Outlet 42.55 0.45
Two-Phase Parameters
Method Inlet Center Outlet Mix F

H. T. Parameters Annulus Pipe


Overall wall correction 0.927 1.000
Midpoint Prandtl no. 17.05 1.58
Midpoint Reynolds no. 1505 328
Entrance Reynolds no. 1525 79
Exit Reynolds no. 1396 395
Fouling layer (mm)
Thermal Resistance, %
Annulus Pipe Fouling Metal Over Des
89.55 8.60 1.62 0.23 19.04
Total fouling resistance (m2-K/W) 4.37e-4
Differential resistance (m2-K/W) 0.0052
Annulus Nozzles

Inlet Outlet

Diameter (mm) 15.799 15.799


Velocity (m/s) 7.42e-2 7.36e-2
Pressure drop (kPa) 2.67e-3 2.67e-3

Nozzle R-V-SQ (kg/m-s2) 4.32 4.29


Shell ent. (kg/m-s2)

Inlet Outlet
Pipe Nozzles
Diameter (mm) 9.246 9.246
Velocity (m/s) 5.94e-3 6.98e-3
Pressure drop (kPa) 1.73e-5 1.05e-5
Nozzle R-V-SQ (kg/m-s2) 3.68e-2 4.33e-2

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Supplementary Results Page 4
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Externally Enhanced Pipe Geometry Internally Enhanced Pipe Geometry
Type Plain Type None
Fin density (fin/meter) Thickness (mm)
Fin height (mm) Pitch (L/D)
Fin thickness (mm)
Root diameter (mm)
Area/length (m2/m)

Mean Metal Temperatures


Mean jacket temperature 207.22 (C)
Tubesheet temperature 237.78 (C)
Mean pipe metal temperature, (C)
Inside Outside Radial
158.47 158.59 158.54

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Annulus Incremental Monitor Page 5
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

Point number (--) 1 2 3 4 5 6

Length from tube inlet (mm) 3968.3 3869.0 3670.6 3472.2 3273.8 3075.4
Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 210.00 209.96 209.87 209.77 209.65 209.52
Skin temperature (C) 200.58 199.33 197.90 196.23 194.23
Wall metal temperature (C) 200.52 199.26 197.82 196.14 194.13
MTD (C) 10.6 11.9 13.4 15.1 17.2
Superheat for Onset of Nucleate Boiling (C)
Delta MTD correction (--) 1.0000 1.0000 1.0000 1.0000 1.0000
Pressure (kPa) 301.32 301.32 301.32 301.32 301.32 301.32
Pressure drop (kPa) 2.67e-3 3.18e-5 3.25e-5 3.32e-5 3.40e-5 3.50e-5
Friction loss (kPa) 3.18e-5 3.25e-5 3.32e-5 3.40e-5 3.50e-5
Static head loss (kPa) 0.000 0.000 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000 0.000 0.000
Crossflow velocity (m/s)
Longitudinal velocity (m/s) 7.21e-3 7.21e-3 7.21e-3 7.21e-3 7.21e-3
Shear stress at tube wall
Crossflow (Pa) 0.00 0.00 0.00 0.00 0.00
Longitudinal flow (Pa) 1.96e-3 2.00e-3 2.05e-3 2.10e-3 2.16e-3
Area (m2) 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 8.55e-3 0.017 0.026 0.034 0.043
Duty (MegaWatts) 2.42e-6 2.76e-6 3.17e-6 3.66e-6 4.24e-6
Cumulative duty (MegaWatts) 2.42e-6 5.18e-6 8.36e-6 1.20e-5 1.63e-5
Heat flux (W/m2) 282.59 323.40 371.32 427.98 496.40
Calculated heat flux (W/m2) 339.86 388.91 446.24 513.67 594.75
Critical heat flux (W/m2)
Overall U (W/m2-K) 32.07 32.67 33.28 33.92 34.66
Shellside h (W/m2-K) 36.29 36.95 37.62 38.32 38.96
Sensible liquid h (W/m2-K) 36.29 36.95 37.62 38.32 38.96
Sensible vapor h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Local Reynolds (--) 1525.5 1525.6 1524.4 1523.0 1521.5 1519.7
Vapor Reynolds (--)
Liquid Reynolds (--) 1525.5 1525.6 1524.4 1523.0 1521.5 1519.7
Vapor Prandtl (--)
Liquid Prandtl (--) 16.891 16.888 16.898 16.908 16.921 16.935
Grashof number (--) 5.943e+8 6.670e+8 7.504e+8 8.464e+8 9.425e+8
Richardson number (--) 255.35 287.01 323.48 365.64 408.11
Flow regime param. (--) 0.0000 0.0000 0.0000 0.0000 0.0000
Condensate regime (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq
Boiling flow regime (--)
Boiling mechanism (--)

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Annulus Incremental Monitor Page 6
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

Point number (--) 7 8 9 10 11 12

Length from tube inlet (mm) 2877.0 2678.6 2480.2 2281.7 2083.3 1884.9
Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 209.37 209.18 208.97 208.72 208.43 208.08
Skin temperature (C) 191.97 189.32 186.09 182.41 177.98 172.68
Wall metal temperature (C) 191.85 189.18 185.92 182.21 177.75 172.41
MTD (C) 19.5 22.3 25.5 29.4 34.0 39.4
Superheat for Onset of Nucleate Boiling (C)
Delta MTD correction (--) 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000
Pressure (kPa) 301.32 301.32 301.32 301.32 301.32 301.32
Pressure drop (kPa) 3.59e-5 3.70e-5 3.83e-5 3.96e-5 4.11e-5 4.28e-5
Friction loss (kPa) 3.59e-5 3.70e-5 3.83e-5 3.96e-5 4.11e-5 4.28e-5
Static head loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Crossflow velocity (m/s)
Longitudinal velocity (m/s) 7.20e-3 7.20e-3 7.20e-3 7.20e-3 7.20e-3 7.20e-3
Shear stress at tube wall
Crossflow (Pa) 0.00 0.00 0.00 0.00 0.00 0.00
Longitudinal flow (Pa) 2.22e-3 2.28e-3 2.36e-3 2.44e-3 2.53e-3 2.64e-3
Area (m2) 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 0.051 0.060 0.068 0.077 0.085 0.094
Duty (MegaWatts) 4.93e-6 5.76e-6 6.77e-6 7.97e-6 9.40e-6 1.10e-5
Cumulative duty (MegaWatts) 2.12e-5 2.70e-5 3.37e-5 4.17e-5 5.11e-5 6.21e-5
Heat flux (W/m2) 577.06 673.88 791.86 932.00 1099.5 1290.4
Calculated heat flux (W/m2) 689.85 803.48 941.63 1105.0 1300.0 1522.2
Critical heat flux (W/m2)
Overall U (W/m2-K) 35.35 36.07 36.88 37.60 38.27 38.61
Shellside h (W/m2-K) 39.72 40.50 41.22 42.07 42.77 43.09
Sensible liquid h (W/m2-K) 39.72 40.50 41.22 42.07 42.77 43.09
Sensible vapor h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Local Reynolds (--) 1517.6 1515.2 1512.3 1509.0 1505.1 1500.5
Vapor Reynolds (--)
Liquid Reynolds (--) 1517.6 1515.2 1512.3 1509.0 1505.1 1500.5
Vapor Prandtl (--)
Liquid Prandtl (--) 16.952 16.972 16.994 17.021 17.053 17.091
Grashof number (--) 1.070e+9 1.218e+9 1.369e+9 1.571e+9 1.822e+9 2.107e+9
Richardson number (--) 464.47 530.63 598.59 689.74 804.50 935.68
Flow regime param. (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Condensate regime (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq
Boiling flow regime (--)
Boiling mechanism (--)

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Annulus Incremental Monitor Page 7
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

Point number (--) 13 14 15 16 17 18

Length from tube inlet (mm) 1686.5 1488.1 1289.7 1091.3 892.86 694.44
Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 207.67 207.19 206.63 205.96 205.19 204.28
Skin temperature (C) 166.39 158.90 150.04 139.40 127.32 113.59
Wall metal temperature (C) 166.07 158.54 149.60 138.88 126.73 112.90
MTD (C) 45.9 53.6 62.7 73.6 85.9 99.9
Superheat for Onset of Nucleate Boiling (C)
Delta MTD correction (--) 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000
Pressure (kPa) 301.32 301.32 301.32 301.32 301.32 301.32
Pressure drop (kPa) 4.48e-5 4.70e-5 4.96e-5 5.27e-5 5.62e-5 6.04e-5
Friction loss (kPa) 4.48e-5 4.70e-5 4.96e-5 5.27e-5 5.62e-5 6.04e-5
Static head loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Crossflow velocity (m/s)
Longitudinal velocity (m/s) 7.20e-3 7.19e-3 7.19e-3 7.19e-3 7.18e-3 7.18e-3
Shear stress at tube wall
Crossflow (Pa) 0.00 0.00 0.00 0.00 0.00 0.00
Longitudinal flow (Pa) 2.76e-3 2.90e-3 3.06e-3 3.25e-3 3.47e-3 3.72e-3
Area (m2) 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 0.103 0.111 0.120 0.128 0.137 0.145
Duty (MegaWatts) 1.29e-5 1.52e-5 1.79e-5 2.10e-5 2.45e-5 2.83e-5
Cumulative duty (MegaWatts) 7.51e-5 9.03e-5 1.08e-4 1.29e-4 1.54e-4 1.82e-4
Heat flux (W/m2) 1513.5 1779.0 2092.9 2461.9 2868.9 3314.2
Calculated heat flux (W/m2) 1782.2 2092.9 2462.6 2902.8 3395.1 3938.2
Critical heat flux (W/m2)
Overall U (W/m2-K) 38.84 39.08 39.27 39.47 39.52 39.42
Shellside h (W/m2-K) 43.26 43.43 43.61 43.70 43.69 43.51
Sensible liquid h (W/m2-K) 43.26 43.43 43.61 43.70 43.69 43.51
Sensible vapor h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Local Reynolds (--) 1495.1 1488.8 1481.5 1472.9 1462.9 1451.3
Vapor Reynolds (--)
Liquid Reynolds (--) 1495.1 1488.8 1481.5 1472.9 1462.9 1451.3
Vapor Prandtl (--)
Liquid Prandtl (--) 17.135 17.187 17.248 17.321 17.406 17.505
Grashof number (--) 2.441e+9 2.833e+9 3.304e+9 3.825e+9 4.418e+9 5.071e+9
Richardson number (--) 1092.0 1278.1 1505.4 1763.0 2064.3 2407.5
Flow regime param. (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Condensate regime (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq
Boiling flow regime (--)
Boiling mechanism (--)

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Annulus Incremental Monitor Page 8
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

Point number (--) 19 20 21 22

Length from tube inlet (mm) 496.03 297.62 99.206 0.000


Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 203.24 202.05 200.71 200.00
Skin temperature (C) 97.48 78.61 58.46
Wall metal temperature (C) 96.68 77.69 57.44
MTD (C) 116.3 135.6 157.9
Superheat for Onset of Nucleate Boiling (C)
Delta MTD correction (--) 1.0000 1.0000 1.0000
Pressure (kPa) 301.32 301.32 301.32 301.32
Pressure drop (kPa) 6.55e-5 7.19e-5 7.93e-5 2.67e-3
Friction loss (kPa) 6.55e-5 7.19e-5 7.93e-5
Static head loss (kPa) 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000
Crossflow velocity (m/s)
Longitudinal velocity (m/s) 7.17e-3 7.17e-3 7.16e-3
Shear stress at tube wall
Crossflow (Pa) 0.00 0.00 0.00
Longitudinal flow (Pa) 4.04e-3 4.43e-3 4.89e-3
Area (m2) 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 0.154 0.162 0.171
Duty (MegaWatts) 3.26e-5 3.71e-5 4.11e-5
Cumulative duty (MegaWatts) 2.15e-4 2.52e-4 2.93e-4
Heat flux (W/m2) 3808.8 4335.1 4806.9
Calculated heat flux (W/m2) 4547.1 5203.7 5798.1
Critical heat flux (W/m2)
Overall U (W/m2-K) 39.09 38.37 36.73
Shellside h (W/m2-K) 43.08 42.24 40.84
Sensible liquid h (W/m2-K) 43.08 42.24 40.84
Sensible vapor h (W/m2-K) 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00
Local Reynolds (--) 1438.1 1422.9 1405.8 1396.3
Vapor Reynolds (--)
Liquid Reynolds (--) 1438.1 1422.9 1405.8 1396.3
Vapor Prandtl (--)
Liquid Prandtl (--) 17.621 17.757 17.913 18.003
Grashof number (--) 5.815e+9 6.654e+9 7.506e+9
Richardson number (--) 2811.5 3286.6 3798.1
Flow regime param. (--) 0.0000 0.0000 0.0000
Condensate regime (--) Sens Liq Sens Liq Sens Liq
Boiling flow regime (--)
Boiling mechanism (--)

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Pipe Incremental Monitor Page 9
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Point number (--) 1 2 3 4 5 6

Length from tube inlet (mm) 0.000 99.206 297.62 496.03 694.44 892.86
Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 30.00 42.61 66.22 86.76 104.25 118.97
Skin temperature (C) 55.59 76.03 95.23 111.64 125.64
Wall metal temperature (C) 57.11 77.39 96.42 112.67 126.53
MTD (C) 157.9 135.6 116.3 99.9 85.9
Superheat for Onset of Nucleate Boiling (C)
Pressure (kPa) 2101.3 2101.3 2101.3 2101.3 2101.3 2101.3
Pressure drop (kPa) 1.73e-5 3.08e-4 2.18e-4 1.72e-4 1.46e-4 1.29e-4
Enhanced pressure drop mult (--)
Friction loss (kPa) 3.08e-4 2.18e-4 1.72e-4 1.46e-4 1.29e-4
Static head loss (kPa) 0.000 0.000 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000 0.000 0.000
Maximum velocity (m/s) 5.97e-3 6.06e-3 6.14e-3 6.23e-3 6.32e-3
Average velocity (m/s) 5.97e-3 6.06e-3 6.14e-3 6.23e-3 6.32e-3
Shear stress at tube wall (Pa) 3.32e-3 2.54e-3 2.01e-3 1.70e-3 1.51e-3
Area (m2) 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 8.55e-3 0.017 0.026 0.034 0.043
Duty (MegaWatts) 4.11e-5 3.71e-5 3.26e-5 2.83e-5 2.45e-5
Cumulative duty (MegaWatts) 0.0000 4.11e-5 7.82e-5 1.11e-4 1.39e-4 1.64e-4
Heat flux (W/m2) 4806.9 4335.1 3808.8 3314.2 2868.9
Calculated heat flux (W/m2) 5798.1 5203.7 4547.1 3938.2 3395.1
Critical heat flux (W/m2) 0.00 0.00 0.00 0.00 0.00
Overall U (W/m2-K) 36.73 38.37 39.09 39.42 39.52
Tubeside h (W/m2-K) 660.52 783.27 791.75 786.42 773.26
Enhanced heat transfer mult (--)
Sensible liquid h (W/m2-K) 660.52 783.27 791.75 786.42 773.26
Sensible vapor h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00 0.00 0.00
Local Reynolds (--) 79.396 79.429 119.78 158.69 193.66 224.28
Vapor Reynolds (--)
Liquid Reynolds (--) 64.506 79.429 119.78 158.69 193.66 224.28
Vapor Prandtl (--)
Liquid Prandtl (--) 7.0783 5.6888 3.7346 2.8422 2.3742 2.1005
Grashof (--) 201564 343006 504522 635318 725466
Richardson (--) 31.949 23.906 20.035 16.940 14.423
Flow regime param. (--) 0.0000 0.0000 0.0000 0.0000 0.0000
Condensate regime (--)
Boiling flow regime (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq
Boiling mechanism (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Pipe Incremental Monitor Page 10
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Point number (--) 7 8 9 10 11 12

Length from tube inlet (mm) 1091.3 1289.7 1488.1 1686.5 1884.9 2083.3
Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 132.21 143.81 153.54 161.71 168.59 174.40
Skin temperature (C) 137.96 148.82 157.87 165.50 171.93 177.33
Wall metal temperature (C) 138.72 149.46 158.42 165.97 172.33 177.67
MTD (C) 73.6 62.7 53.6 45.9 39.4 34.0
Superheat for Onset of Nucleate Boiling (C)
Pressure (kPa) 2101.3 2101.3 2101.3 2101.3 2101.3 2101.3
Pressure drop (kPa) 1.17e-4 1.08e-4 1.02e-4 9.69e-5 9.29e-5 8.97e-5
Enhanced pressure drop mult (--)
Friction loss (kPa) 1.17e-4 1.08e-4 1.02e-4 9.69e-5 9.29e-5 8.97e-5
Static head loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Maximum velocity (m/s) 6.41e-3 6.48e-3 6.55e-3 6.62e-3 6.67e-3 6.72e-3
Average velocity (m/s) 6.41e-3 6.48e-3 6.55e-3 6.62e-3 6.67e-3 6.72e-3
Shear stress at tube wall (Pa) 1.37e-3 1.26e-3 1.19e-3 1.13e-3 1.08e-3 1.05e-3
Area (m2) 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 0.051 0.060 0.068 0.077 0.085 0.094
Duty (MegaWatts) 2.10e-5 1.79e-5 1.52e-5 1.29e-5 1.10e-5 9.40e-6
Cumulative duty (MegaWatts) 1.85e-4 2.03e-4 2.18e-4 2.31e-4 2.42e-4 2.51e-4
Heat flux (W/m2) 2461.9 2092.9 1779.0 1513.5 1290.4 1099.5
Calculated heat flux (W/m2) 2902.8 2462.6 2092.9 1782.2 1522.2 1300.0
Critical heat flux (W/m2) 0.00 0.00 0.00 0.00 0.00 0.00
Overall U (W/m2-K) 39.47 39.27 39.08 38.84 38.61 38.27
Tubeside h (W/m2-K) 756.67 728.26 716.29 696.23 676.35 656.56
Enhanced heat transfer mult (--)
Sensible liquid h (W/m2-K) 756.67 728.26 716.29 696.23 676.35 656.56
Sensible vapor h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Local Reynolds (--) 251.52 275.80 296.38 313.67 328.29 340.74
Vapor Reynolds (--)
Liquid Reynolds (--) 251.52 275.80 296.38 313.67 328.29 340.74
Vapor Prandtl (--)
Liquid Prandtl (--) 1.9152 1.7802 1.6874 1.6228 1.5763 1.5418
Grashof (--) 775808 749614 770411 741171 701314 654467
Richardson (--) 12.263 9.8546 8.7705 7.5328 6.5073 5.6370
Flow regime param. (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Condensate regime (--)
Boiling flow regime (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq
Boiling mechanism (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Pipe Incremental Monitor Page 11
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Point number (--) 13 14 15 16 17 18

Length from tube inlet (mm) 2281.7 2480.2 2678.6 2877.0 3075.4 3273.8
Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 179.29 183.40 186.88 189.82 192.34 194.49
Skin temperature (C) 181.86 185.62 188.92 191.63 193.94 195.98
Wall metal temperature (C) 182.15 185.87 189.13 191.81 194.10 196.11
MTD (C) 29.4 25.5 22.3 19.5 17.2 15.1
Superheat for Onset of Nucleate Boiling (C)
Pressure (kPa) 2101.3 2101.3 2101.3 2101.3 2101.3 2101.3
Pressure drop (kPa) 8.72e-5 8.56e-5 8.27e-5 8.13e-5 8.01e-5 7.82e-5
Enhanced pressure drop mult (--)
Friction loss (kPa) 8.72e-5 8.56e-5 8.27e-5 8.13e-5 8.01e-5 7.82e-5
Static head loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000 0.000 0.000 0.000
Maximum velocity (m/s) 6.77e-3 6.81e-3 6.84e-3 6.87e-3 6.89e-3 6.92e-3
Average velocity (m/s) 6.77e-3 6.81e-3 6.84e-3 6.87e-3 6.89e-3 6.92e-3
Shear stress at tube wall (Pa) 1.02e-3 9.97e-4 9.64e-4 9.47e-4 9.33e-4 9.11e-4
Area (m2) 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 0.103 0.111 0.120 0.128 0.137 0.145
Duty (MegaWatts) 7.97e-6 6.77e-6 5.76e-6 4.93e-6 4.24e-6 3.66e-6
Cumulative duty (MegaWatts) 2.59e-4 2.66e-4 2.72e-4 2.77e-4 2.81e-4 2.84e-4
Heat flux (W/m2) 932.00 791.86 673.88 577.06 496.40 427.98
Calculated heat flux (W/m2) 1105.0 941.63 803.48 689.85 594.75 513.67
Critical heat flux (W/m2) 0.00 0.00 0.00 0.00 0.00 0.00
Overall U (W/m2-K) 37.60 36.88 36.07 35.35 34.66 33.92
Tubeside h (W/m2-K) 636.51 628.86 583.78 566.83 550.80 512.05
Enhanced heat transfer mult (--)
Sensible liquid h (W/m2-K) 636.51 628.86 583.78 566.83 550.80 512.05
Sensible vapor h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00 0.00 0.00 0.00
Local Reynolds (--) 351.23 360.06 367.58 373.94 379.39 384.13
Vapor Reynolds (--)
Liquid Reynolds (--) 351.23 360.06 367.58 373.94 379.39 384.13
Vapor Prandtl (--)
Liquid Prandtl (--) 1.5163 1.4971 1.4823 1.4709 1.4619 1.4546
Grashof (--) 602033 593484 450948 409463 371470 279425
Richardson (--) 4.8803 4.5778 3.3375 2.9283 2.5807 1.8937
Flow regime param. (--) 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Condensate regime (--)
Boiling flow regime (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq
Boiling mechanism (--) Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq Sens Liq

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Pipe Incremental Monitor Page 12
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Point number (--) 19 20 21 22

Length from tube inlet (mm) 3472.2 3670.6 3869.0 3968.3


Mass fraction vapor (--) 0.0000 0.0000 0.0000 0.0000
Bulk temperature (C) 196.35 197.95 199.35 200.00
Skin temperature (C) 197.67 199.14 200.41
Wall metal temperature (C) 197.79 199.24 200.50
MTD (C) 13.4 11.9 10.6
Superheat for Onset of Nucleate Boiling (C)
Pressure (kPa) 2101.3 2101.3 2101.3 2101.3
Pressure drop (kPa) 7.74e-5 7.67e-5 8.21e-5 1.05e-5
Enhanced pressure drop mult (--)
Friction loss (kPa) 7.74e-5 7.67e-5 8.21e-5
Static head loss (kPa) 0.000 0.000 0.000
Momentum loss (kPa) 0.000 0.000 0.000
Maximum velocity (m/s) 6.94e-3 6.95e-3 6.97e-3
Average velocity (m/s) 6.94e-3 6.95e-3 6.97e-3
Shear stress at tube wall (Pa) 9.01e-4 8.93e-4 8.86e-4
Area (m2) 8.55e-3 8.55e-3 8.55e-3
Cumulative area (m2) 0.154 0.162 0.171
Duty (MegaWatts) 3.17e-6 2.76e-6 2.42e-6
Cumulative duty (MegaWatts) 2.88e-4 2.90e-4 2.93e-4
Heat flux (W/m2) 371.32 323.40 282.59
Calculated heat flux (W/m2) 446.24 388.91 339.86
Critical heat flux (W/m2) 0.00 0.00 0.00
Overall U (W/m2-K) 33.28 32.67 32.07
Tubeside h (W/m2-K) 498.61 485.84 473.66
Enhanced heat transfer mult (--)
Sensible liquid h (W/m2-K) 498.61 485.84 473.66
Sensible vapor h (W/m2-K) 0.00 0.00 0.00
Condensate film h (W/m2-K) 0.00 0.00 0.00
Vapor phase h (W/m2-K) 0.00 0.00 0.00
Nucleate boiling h (W/m2-K) 0.00 0.00 0.00
Conv. boiling h (W/m2-K) 0.00 0.00 0.00
Film boiling h (W/m2-K) 0.00 0.00 0.00
Boiling thin film h (W/m2-K) 0.00 0.00 0.00
Natural convective h (W/m2-K) 0.00 0.00 0.00
Local Reynolds (--) 388.19 391.68 394.72 394.55
Vapor Reynolds (--)
Liquid Reynolds (--) 388.19 391.68 394.72 395.98
Vapor Prandtl (--)
Liquid Prandtl (--) 1.4487 1.4441 1.4403 1.4385
Grashof (--) 253961 230818 209823
Richardson (--) 1.6853 1.5046 1.3467
Flow regime param. (--) 0.0000 0.0000 0.0000
Condensate regime (--)
Boiling flow regime (--) Sens Liq Sens Liq Sens Liq
Boiling mechanism (--) Sens Liq Sens Liq Sens Liq

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
API 660 Shell-And-Tube Heat Exchanger Specification Sheet Page 13
Released to the following HTRI Member Company: SI Units

1 Client Location
2 Process unit heat stable reactor Item No.
3 Job No. Fabricator
4 Service of Unit Number of unit
5 Size 52.502 x 4000 mm Type
Jacketed Pipe Horizontal Connected In 1 Parallel 1 Series
6 Effective surface per unit (plain/finned) 0.171 m2 Shell/Unit 1 Effective surface per shell 0.171 m2
7 PERFORMANCE OF ONE UNIT Shell Side Tube Side
8 Inlet Outlet Inlet Outlet
9 Fluid Name hot oil LA +water
10 Fluid Quantity, Total kg/hr 41.150 1.5000
11 Vapor (relative molecular mass)
12 Liquid 41.150 41.150 1.5000 1.5000
13 Steam
14 Water 1.0500 1.0500
15 Noncondensables (relative molecular mass)
16 Temperature C 210.00 200.00 30.00 200.00
17 Density (Vapor/Liquid) kg/m3 786.13 792.02 1045.5 889.68
18 Viscosity (Vapor/Liquid) mN-s/m2 0.6953 0.7596 0.8892 0.1448
19 Specific Heat (Vapor/Liquid) kJ/kg-C 2.5785 2.5434 3.7291 4.4642
20 Thermal Conductivity (Vapor/Liquid) W/m-C 0.1062 0.1074 0.4689 0.4500
21 Specific latent heat kJ/kg @ C @ 210.00 @ 200.00 @ 30.00 @ 200.00
22 Inlet Pressure kPa 301.32 2101.3
23 Velocity m/s 7.20e-3 6.67e-3
24 Pressure Drop, Allow/Calc kPa 30.000 6.27e-3 20.000 2.34e-3
25 Fouling Resistance (min) m2-K/W 0.000176 0.000176
26 Average Film Coefficient W/m2-K 41.26 637.36
27 Heat Exchanged 292.80 W MTD (Corrected) 55.2 C
28 Transfer Rate W/m2-K Required 31.05 Fouled 36.96 Clean 37.56
29 Rho-V2 kg/m-s2 Inlet Nozzle 4.32 Bundle Entrance Bundle Exit
30 Hydrogen Service Tube Side (Y/N) Shell Side (Y/N) Sour Service Tube Side (Y/N) Shell Side (Y/N) Cyclic Service (Y/N)
31 CONSTRUCTION OF ONE SHELL
32 Tube No. 1 OD mm 13.716 NOZZLES - Number, Size and Rating
33 Tube Wall Thickness mm 2.235 minimum wall / average wall Shell Side Tube Side
34 Tube Pitch mm 17.145 Tube layout 30 Inlet mm 1 @ 15.799 1 @ 9.246
35 Tube Length m 4.000 Tube Type Plain Outlet 1 @ 15.799 1 @ 9.246
36 Tube-Tubesheet Joint Expanded (2 grooves) Intermediate @ @
37 Shell diameter mm (ID/OD) 52.502 / 57.264 Vent @ @
38 Cross Baffle Type Drain @ @
39 Baffle Spacing(c/c) mm 3968.3 No. of Crosspasses 1 Pressure Relief @ @
40 Baffle cut % Design pressure kPaG 517.11 2206.3
41 Tube support type None Vacuum kPa
42 Longitudinal baffle seal type None esign temp. (Max/MDMT) C 237.78 / 200.52 232.22 / 200.50
43 Bypass Seal Arrangement 1 pairs seal strips No Passes per Shell 1 1
44 Impingement Protection Type None Corrosion Allowance mm 0.000 0.000
45 MATERIALS OF CONSTRUCTION
46 Shell SA-516 70 Pl. K02700 Tube SA-214 Tube (W) K01807 Gaskets
47 Shell Cover Shell Side Mach. Mtl. (Kammprofile\Flex. Face)
48 Channel or Bonnet SA-516 70 Pl. K02700 Tube Side Mach. Mtl. (Kammprofile\Flex. Face)
49 Channel Cover SA-516 70 Pl. K02700 Floating Head
50 Floating Head Cover Spare Gaskets Reqd
51 Tubesheet-Stationary SA-105 Forgings K03504 Tubesheet-Floating Test Ring Reqd. (Y/N)
52 Baffles-Cross Baffles-Long Insulation-shell mm
53 Tube Support Material Insulation-channel mm inlet/outlet
54 Expansion Joint Type None Expansion joint material
55 Pressure design code Stamp Calculate MAWP Y/N TEMA Class non-TEMA
56 Remarks:
57
58
Reprinted with Permission

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
HEAT EXCHANGER RATING DATA SHEET Page 14
Released to the following HTRI Member Company: SI Units

Service of Unit Item No.


Type Jacketed Pipe Orientation Horizontal Connected In 1 Parallel 1 Series
Surf/Unit (Gross/Eff) 0.172 / 0.171 m2 Shell/Unit 1 Surf/Shell (Gross/Eff) 0.172 / 0.171 m2
PERFORMANCE OF ONE UNIT
Fluid Allocation Shell Side Tube Side
Fluid Name hot oil LA +water
Fluid Quantity, Total kg/s 0.0114 4.17e-4
Vapor (In/Out) wt% 0.00 0.00 0.00 0.00
Liquid wt% 100.00 100.00 100.00 100.00
Temperature (In/Out) C 210.00 200.00 30.00 200.00
Density kg/m3 786.13 792.02 1045.5 889.68
Viscosity mN-s/m2 0.6953 0.7596 0.8892 0.1448
Specific Heat kJ/kg-C 2.5785 2.5434 3.7291 4.4642
Thermal Conductivity W/m-C 0.1062 0.1074 0.4689 0.4500
Critical Pressure kPa
Inlet Pressure kPa 301.32 2101.3
Velocity m/s 7.20e-3 6.67e-3
Pressure Drop, Allow/Calc kPa 30.000 6.27e-3 20.000 2.34e-3
Average Film Coefficient W/m2-K 41.26 637.36
Fouling Resistance (min) m2-K/W 0.000176 0.000176
Heat Exchanged 2.93e-4 MegaWatts MTD (Corrected) 55.2 C Overdesign 19.04 %
Transfer Rate, Service 31.05 W/m2-K Calculated 36.96 W/m2-K Clean 37.56 W/m2-K
CONSTRUCTION OF ONE SHELL Sketch (Bundle/Nozzle Orientation)
Shell Side Tube Side
Design Pressure kPaG 517.11 2206.3
Design Temperature C 237.78 232.22
No Passes per Shell 1 1
Flow Direction Downward
Connections In mm 1 @ 15.799 1 @ 9.246
Size & Out mm 1 @ 15.799 1 @ 9.246
Rating Liq. Out mm @ 1 @
Tube No. 1.0000 OD 13.716 mm Thk(Avg) 2.235 mm Length 4.000 m Pitch 17.145 mm Tube pattern 30
Tube Type Plain Material SA-214 Tube (W) K01807 Pairs seal strips 1
Shell ID 52.502 mm Kettle ID mm Passlane Seal Rod No. 0
Cross Baffle Type None %Cut (Diam Impingement Plate None
Spacing(c/c) 3968.3 mm Inlet mm No. of Crosspasses 1
Rho-V2-Inlet Nozzle 4.32 kg/m-s2 Shell Entrance kg/m-s2 Shell Exit kg/m-s2
Bundle Entrance kg/m-s2 Bundle Exit kg/m-s2
Weight/Shell 56.61 kg Filled with Water 65.14 kg Bundle 3.03 kg
Notes: Thermal Resistance, % Velocities, m/s Flow Fractions
Shell 89.55 Shellside 7.20e-3 A
Tube 8.60 Tubeside 6.67e-3 B 1.000
Fouling 1.62 Crossflow 0.00 C 0.000
Metal 0.23 Window 7.20e-3 E
F

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
HEAT EXCHANGER SPECIFICATION SHEET Page 15
Released to the following HTRI Member Company: SI Units

Job No.
Customer Reference No.
Address Proposal No.
Plant Location Date 11-12-2023 Rev
Service of Unit Item No.
Size 52.502 x 4000 mm Type
Jacketed Pipe Horizontal Connected In 1 Parallel 1 Series
Surf/Unit (Gross/Eff) 0.172 / 0.171 m2 Shell/Unit 1 Surf/Shell (Gross/Eff) 0.172 / 0.171 m2
PERFORMANCE OF ONE UNIT
Fluid Allocation Shell Side Tube Side
Fluid Name hot oil LA +water
Fluid Quantity, Total kg/hr 41.150 1.5000
Vapor (In/Out)
Liquid 41.150 41.150 1.5000 1.5000
Steam
Water 1.0500 1.0500
Noncondensables
Temperature (In/Out) C 210.00 200.00 30.00 200.00
Specific Gravity 0.7865 0.7924 1.0460 0.8901
Viscosity mN-s/m2 0.6953 0.7596 0.8892 0.1448
Molecular Weight 320.00 320.00 23.70 23.70
Molecular Weight, Noncondensables
Specific Heat kJ/kg-C 2.5785 2.5434 3.7291 4.4642
Thermal Conductivity W/m-C 0.1062 0.1074 0.4689 0.4500
Latent Heat kJ/kg
Inlet Pressure kPa 301.32 2101.3
Velocity m/s 7.20e-3 6.67e-3
Pressure Drop, Allow/Calc kPa 30.000 6.27e-3 20.000 2.34e-3
Fouling Resistance (min) m2-K/W 0.000176 0.000176
Heat Exchanged 292.80 W MTD (Corrected) 55.2 C
Transfer Rate, Service 31.05 W/m2-K Clean 37.56 W/m2-K Actual 36.96 W/m2-K
CONSTRUCTION OF ONE SHELL Sketch (Bundle/Nozzle Orientation)
Shell Side Tube Side
Design/Test Pressure kPaG 517.11 / 2206.3 /
Design Temperature C 237.78 232.22
No Passes per Shell 1 1
Corrosion Allowance mm 0.000 0.000
Connections In mm 1 @ 15.799 1 @ 9.246
Size & Out mm 1 @ 15.799 1 @ 9.246
Rating Intermediate @ @
Tube No. 1 OD 13.716 mm Thk(Avg) 2.235 mm Length 4.000 m Pitch 17.145 mm
Tube Type Plain Material SA-214 Tube (W) K01807 Tube patter 30
Shell SA-516 70 Pl. K02700 ID 52.502 OD 57.264 mm Shell Cover
Channel or Bonnet SA-516 70 Pl. K02700 Channel Cover SA-516 70 Pl. K02700
Tubesheet-Stationary SA-105 Forgings K03504 Tubesheet-Floating
Floating Head Cover Impingement Plate None
Baffles-Cross Type None %Cut (Diam) Spacing(c/c) 3968.3 Inlet mm
Baffles-Long Seal Type None
Supports-Tube U-Bend Type None
Bypass Seal Arrangement 1 pairs seal strips Tube-Tubesheet Joint Expanded (2 grooves)
Expansion Joint Type None
Rho-V2-Inlet Nozzle 4.32 kg/m-s2 Bundle Entrance Bundle Exit kg/m-s2
Gaskets-Shell Side Mach. Mtl. (Kammprofile\Flex. Face) Tube Side Mach. Mtl. (Kammprofile\Flex. Face)
- Floating Head
Code Requirements TEMA Class non-TEMA
Weight/Shell 56.61 kg Filled with Water 65.14 kg Bundle 3.03 kg
Remarks:

Reprinted with Permission

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 16
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Hot Annulus (hot oil)
Property package VMGThermo
Reference pressure, (kPa) (P1= 271.32) (P2= 301.32)
(P) 1 2 3 4 5 6 7 8 9 10
Temperature, (C) 1 250.00 243.47 236.88 230.23 223.53 216.76 209.93 203.04 196.08 189.05
2 250.00 243.47 236.88 230.23 223.52 216.76 209.93 203.04 196.08 189.05
Enthalpy, (kJ/kg) 1 512.96 495.27 477.58 459.89 442.20 424.52 406.83 389.14 371.45 353.76
2 512.98 495.29 477.60 459.92 442.23 424.54 406.85 389.17 371.48 353.79
Weight fraction vapor 1 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
2 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Liquid Properties
Density, (kg/m3) 1 760.16 764.66 769.08 773.44 777.72 781.94 786.10 790.18 794.21 798.18
2 760.26 764.75 769.18 773.53 777.81 782.02 786.17 790.26 794.28 798.24
Viscosity, (mN-s/m2) 1 0.4944 0.5228 0.5529 0.5849 0.6191 0.6559 0.6957 0.7391 0.7869 0.8397
2 0.4944 0.5228 0.5529 0.5849 0.6191 0.6559 0.6957 0.7391 0.7869 0.8397
Thermal conductivity, (W/m-C) 1 0.1015 0.1023 0.1031 0.1039 0.1047 0.1055 0.1063 0.1071 0.1079 0.1087
2 0.1015 0.1023 0.1031 0.1039 0.1047 0.1055 0.1063 0.1071 0.1079 0.1087
Enthalpy, (kJ/kg) 1 0.0000 -17.69 -35.38 -53.06 -70.75 -88.44 -106.1 -123.8 -141.5 -159.2
2 0.0000 -17.69 -35.38 -53.06 -70.75 -88.44 -106.1 -123.8 -141.5 -159.2
Specific heat, (kJ/kg-C) 1 2.7189 2.6959 2.6728 2.6495 2.6260 2.6023 2.5783 2.5542 2.5297 2.5051
2 2.7187 2.6958 2.6727 2.6494 2.6259 2.6022 2.5783 2.5541 2.5297 2.5050
Surface tension, (mN/m) 1 12.839 13.221 13.608 14.000 14.397 14.800 15.208 15.622 16.041 16.467
2 12.839 13.221 13.608 14.000 14.397 14.800 15.208 15.622 16.041 16.467
Critical temperature, (C) 1 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00
2 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00
Critical pressure, (kPa) 1 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9
2 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9
Molecular weight, (--) 1 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00
2 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 17
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Hot Annulus (hot oil)
Property package VMGThermo
Reference pressure, (kPa) (P1= 271.32) (P2= 301.32)
(P) 11 12 13 14 15 16 17 18 19 20
Temperature, (C) 1 181.96 174.79 167.55 160.23 152.83 145.35 137.78 130.13 122.38 114.54
2 181.96 174.79 167.54 160.22 152.83 145.34 137.78 130.13 122.38 114.54
Enthalpy, (kJ/kg) 1 336.08 318.39 300.70 283.01 265.32 247.63 229.95 212.26 194.57 176.88
2 336.10 318.41 300.73 283.04 265.35 247.66 229.98 212.29 194.60 176.91
Weight fraction vapor 1 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
2 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Liquid Properties
Density, (kg/m3) 1 802.08 805.93 809.73 813.47 817.15 820.78 824.36 827.89 831.37 834.81
2 802.15 805.99 809.78 813.52 817.20 820.83 824.41 827.93 831.41 834.84
Viscosity, (mN-s/m2) 1 0.8989 0.9656 1.0417 1.1295 1.2317 1.3522 1.4960 1.6699 1.8832 2.1487
2 0.8989 0.9656 1.0417 1.1295 1.2317 1.3522 1.4960 1.6700 1.8832 2.1488
Thermal conductivity, (W/m-C) 1 0.1095 0.1104 0.1112 0.1121 0.1130 0.1138 0.1147 0.1156 0.1165 0.1174
2 0.1095 0.1104 0.1112 0.1121 0.1130 0.1138 0.1147 0.1156 0.1165 0.1174
Enthalpy, (kJ/kg) 1 -176.9 -194.6 -212.3 -229.9 -247.6 -265.3 -283.0 -300.7 -318.4 -336.1
2 -176.9 -194.6 -212.3 -229.9 -247.6 -265.3 -283.0 -300.7 -318.4 -336.1
Specific heat, (kJ/kg-C) 1 2.4801 2.4549 2.4294 2.4037 2.3776 2.3513 2.3246 2.2976 2.2702 2.2425
2 2.4801 2.4549 2.4294 2.4036 2.3776 2.3512 2.3245 2.2975 2.2701 2.2424
Surface tension, (mN/m) 1 16.898 17.336 17.780 18.230 18.688 19.152 19.623 20.101 20.587 21.081
2 16.898 17.336 17.780 18.230 18.688 19.152 19.623 20.101 20.587 21.081
Critical temperature, (C) 1 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00
2 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00
Critical pressure, (kPa) 1 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9
2 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9
Molecular weight, (--) 1 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00
2 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 18
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Hot Annulus (hot oil)
Property package VMGThermo
Reference pressure, (kPa) (P1= 271.32) (P2= 301.32)
(P) 21 22 23 24 25 26 27 28 29 30
Temperature, (C) 1 106.60 98.56 90.42 82.16 73.79 65.30 56.68 47.93 39.04 30.00
2 106.60 98.56 90.42 82.16 73.79 65.30 56.68 47.93 39.04 30.00
Enthalpy, (kJ/kg) 1 159.19 141.51 123.82 106.13 88.441 70.753 53.065 35.376 17.688 0.0000
2 159.22 141.54 123.85 106.16 88.473 70.785 53.098 35.410 17.722 0.0344
Weight fraction vapor 1 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
2 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Liquid Properties
Density, (kg/m3) 1 838.19 841.53 844.83 848.08 851.28 854.45 857.57 860.65 863.70 866.70
2 838.23 841.56 844.86 848.11 851.31 854.47 857.60 860.68 863.72 866.72
Viscosity, (mN-s/m2) 1 2.4847 2.9176 3.4864 4.2505 5.3024 6.7909 8.9642 12.251 17.429 25.972
2 2.4847 2.9176 3.4865 4.2506 5.3025 6.7910 8.9643 12.252 17.429 25.972
Thermal conductivity, (W/m-C) 1 0.1184 0.1193 0.1202 0.1212 0.1222 0.1232 0.1242 0.1252 0.1262 0.1273
2 0.1184 0.1193 0.1202 0.1212 0.1222 0.1232 0.1242 0.1252 0.1262 0.1273
Enthalpy, (kJ/kg) 1 -353.8 -371.5 -389.1 -406.8 -424.5 -442.2 -459.9 -477.6 -495.3 -513.0
2 -353.8 -371.4 -389.1 -406.8 -424.5 -442.2 -459.9 -477.6 -495.3 -512.9
Specific heat, (kJ/kg-C) 1 2.2144 2.1859 2.1570 2.1276 2.0978 2.0676 2.0368 2.0055 1.9737 1.9412
2 2.2143 2.1858 2.1569 2.1276 2.0978 2.0675 2.0368 2.0055 1.9736 1.9412
Surface tension, (mN/m) 1 21.583 22.093 22.612 23.140 23.677 24.224 24.782 25.349 25.928 26.519
2 21.583 22.093 22.612 23.140 23.677 24.225 24.782 25.349 25.928 26.519
Critical temperature, (C) 1 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00
2 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00 512.00
Critical pressure, (kPa) 1 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9
2 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9 1316.9
Molecular weight, (--) 1 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00
2 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00 320.00

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 19
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 1 2 3 4 5 6 7 8 9 10
Temperature, (C) 1 250.00 224.13 198.26 172.38 146.51 120.64 118.44 116.08 113.58 110.98
2 250.00 232.56 215.12 197.68 180.24 162.80 145.36 143.00 140.64 138.39
3 250.00 234.91 219.83 204.74 189.65 174.57 159.48 156.51 153.90 151.94
4 250.00 236.65 223.31 209.96 196.61 183.26 169.92 167.42 165.38 163.95
5 250.00 235.68 221.36 207.03 192.71 178.39 175.69 173.89 172.92 172.43
6 250.00 237.12 224.25 211.37 198.50 185.62 182.89 181.46 180.83 180.54
7 250.00 238.40 226.80 215.20 203.60 192.00 189.72 188.57 188.05 187.79
8 250.00 239.54 229.09 218.63 208.18 197.72 195.62 194.71 194.31 194.11
9 250.00 238.24 226.47 214.71 202.95 200.99 200.26 199.96 199.80 199.70
10 250.00 239.44 228.89 218.33 207.77 205.79 205.25 205.04 204.93 204.85
11 250.00 237.42 224.84 212.26 210.58 210.10 209.90 209.79 209.72 209.67
12 250.00 238.82 227.64 216.46 214.93 214.53 214.36 214.26 214.20 214.15
Enthalpy, (kJ/kg) 1 2348.0 2299.5 2251.6 2204.3 2157.7 2111.6 2071.0 2030.4 1989.7 1949.1
2 2344.1 2311.1 2278.4 2245.9 2213.7 2181.7 2150.0 2101.8 2053.7 2005.5
3 2340.2 2311.4 2282.8 2254.4 2226.2 2198.1 2170.2 2100.1 2029.9 1959.8
4 2336.1 2310.5 2285.0 2259.6 2234.3 2209.2 2184.2 2115.6 2047.0 1978.4
5 2332.1 2304.4 2276.8 2249.3 2222.0 2194.8 2105.1 2015.4 1925.7 1836.0
6 2328.0 2302.9 2277.8 2252.9 2228.0 2203.3 2089.9 1976.5 1863.2 1749.8
7 2323.8 2301.0 2278.2 2255.6 2232.9 2210.3 2098.7 1987.1 1875.5 1763.8
8 2319.6 2298.9 2278.2 2257.5 2236.9 2216.3 2087.9 1959.5 1831.2 1702.8
9 2315.3 2291.8 2268.3 2244.8 2221.4 2069.4 1917.4 1765.5 1613.5 1461.5
10 2311.0 2289.7 2268.4 2247.1 2225.8 2011.5 1797.1 1582.8 1368.4 1154.1
11 2306.6 2281.0 2255.3 2229.7 2018.0 1806.2 1594.5 1382.7 1171.0 959.24
12 2302.1 2279.1 2256.1 2233.1 1989.0 1744.8 1500.7 1256.6 1012.4 768.30
Weight fraction vapor 1 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.9547 0.9114 0.8703 0.8319
2 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.9478 0.8990 0.8540
3 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.9268 0.8616 0.8050
4 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.9298 0.8675 0.8130
5 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.9115 0.8364 0.7719 0.7136
6 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.8925 0.8042 0.7276 0.6564
7 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.8957 0.8090 0.7325 0.6609
8 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 0.8834 0.7870 0.7004 0.6181
9 1.0000 1.0000 1.0000 1.0000 1.0000 0.8660 0.7552 0.6539 0.5566 0.4615
10 1.0000 1.0000 1.0000 1.0000 1.0000 0.8198 0.6710 0.5315 0.3960 0.2627
11 1.0000 1.0000 1.0000 1.0000 0.8226 0.6736 0.5335 0.3974 0.2636 0.1313
12 1.0000 1.0000 1.0000 1.0000 0.7991 0.6285 0.4667 0.3090 0.1537 0.0000

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 20
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 11 12 13 14 15 16 17 18 19 20
Temperature, (C) 1 108.40 106.01 103.98 102.44 101.38 100.64 100.25 100.25 100.25 100.25
2 136.40 134.79 133.63 132.86 132.38 132.09 131.78 131.73 131.72 131.72
3 150.70 150.02 149.66 149.47 149.37 149.27 149.22 149.19 149.17 149.14
4 163.06 162.56 162.28 162.11 162.01 161.87 161.79 161.74 161.70 161.67
5 172.18 172.04 171.88 171.79 171.74 171.69 171.66 171.63 159.83 148.03
6 180.38 180.29 180.22 180.13 180.08 180.04 180.00 168.46 156.93 145.39
7 187.64 187.55 187.48 187.37 187.30 187.26 176.03 164.79 153.56 142.33
8 193.99 193.91 193.80 193.73 193.69 182.78 171.86 160.95 150.04 139.13
9 199.59 199.53 199.48 189.51 179.54 169.57 159.60 149.63 139.66 129.69
10 204.80 204.76 195.06 185.35 175.64 165.93 156.22 146.51 136.80 127.09
11 209.63 200.18 190.72 181.27 171.82 162.36 152.91 143.45 134.00 124.54
12 204.95 195.74 186.53 177.32 168.12 158.91 149.70 140.49 131.28 122.08
Enthalpy, (kJ/kg) 1 1908.4 1867.8 1827.2 1786.5 1745.9 1700.2 1563.0 1471.6 1070.8 1009.7
2 1957.3 1909.2 1861.0 1812.8 1764.7 1716.5 1572.0 1427.5 1283.0 1138.5
3 1889.6 1819.5 1749.3 1679.2 1609.0 1468.7 1328.4 1188.1 1047.8 860.73
4 1909.9 1841.3 1772.7 1704.2 1635.6 1452.7 1269.9 1087.0 904.19 721.34
5 1746.3 1656.7 1477.3 1297.9 1118.6 939.20 759.84 580.47 531.02 482.43
6 1636.5 1523.1 1409.7 1211.4 1013.0 814.60 616.22 567.20 519.09 471.78
7 1652.2 1540.6 1429.0 1168.5 908.08 647.63 599.28 551.88 505.31 459.46
8 1574.4 1446.1 1189.3 932.58 675.85 628.27 581.68 535.95 490.96 446.62
9 1208.2 954.88 701.58 657.56 614.43 572.09 530.44 489.40 448.91 408.89
10 939.70 725.35 681.96 639.50 597.84 556.88 516.54 476.76 437.48 398.63
11 747.50 704.76 662.96 621.98 581.71 542.08 503.01 464.45 426.33 388.56
12 726.21 685.06 644.75 605.16 566.21 527.84 489.98 452.58 415.59 377.87
Weight fraction vapor 1 0.7966 0.7647 0.7362 0.7105 0.6870 0.6624 0.5965 0.5539 0.3807 0.2632
2 0.8132 0.7765 0.7435 0.7133 0.6851 0.6583 0.5821 0.5083 0.4353 0.3625
3 0.7556 0.7114 0.6702 0.6307 0.5922 0.5166 0.4420 0.3678 0.2938 0.1956
4 0.7647 0.7205 0.6790 0.6389 0.5997 0.4974 0.3967 0.2968 0.1974 0.0985
5 0.6588 0.6056 0.5020 0.4001 0.2992 0.1989 0.0993 0.0000 0.0000 0.0000
6 0.5878 0.5206 0.4541 0.3392 0.2254 0.1124 0.0000 0.0000 0.0000 0.0000
7 0.5917 0.5239 0.4569 0.3028 0.1508 0.0000 0.0000 0.0000 0.0000 0.0000
8 0.5380 0.4593 0.3043 0.1515 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
9 0.3057 0.1521 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
10 0.1308 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
11 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
12 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 21
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 21 22 23 24 25 26 27 28 29 30
Temperature, (C) 1 100.24 100.24 76.83 53.41 30.00 -- -- -- -- --
2 131.72 131.71 131.70 131.69 131.68 111.35 91.01 70.67 50.34 30.00
3 149.11 149.09 134.20 119.32 104.43 89.55 74.66 59.77 44.89 30.00
4 161.64 147.02 132.39 117.76 103.14 88.51 73.88 59.25 44.63 30.00
5 136.22 124.42 112.62 100.82 89.01 77.21 65.41 53.61 41.80 30.00
6 133.85 122.31 110.77 99.23 87.69 76.15 64.62 53.08 41.54 30.00
7 131.09 119.86 108.63 97.40 86.16 74.93 63.70 52.47 41.23 30.00
8 128.21 117.30 106.39 95.48 84.56 73.65 62.74 51.83 40.91 30.00
9 119.72 109.76 99.79 89.82 79.85 69.88 59.91 49.94 39.97 30.00
10 117.38 107.67 97.96 88.25 78.55 68.84 59.13 49.42 39.71 30.00
11 115.09 105.64 96.18 86.73 77.27 67.82 58.36 48.91 39.45 30.00
12 112.87 103.66 94.45 85.25 76.04 66.83 57.62 48.42 39.21 30.00
Enthalpy, (kJ/kg) 1 465.81 282.94 186.05 91.993 0.0000 -- -- -- -- --
2 994.03 849.53 705.03 560.54 416.04 330.26 244.48 161.23 79.949 0.1537
3 673.66 486.59 426.27 364.82 300.90 238.54 177.52 117.60 58.586 0.3074
4 538.49 478.22 419.10 358.17 295.53 234.38 174.50 115.67 57.715 0.4612
5 434.60 387.36 336.07 285.86 236.60 188.17 140.45 93.341 46.760 0.6149
6 425.17 378.21 328.27 279.33 231.28 184.01 137.41 91.395 45.875 0.7687
7 414.25 367.64 319.23 271.76 225.11 179.18 133.87 89.117 44.824 0.9225
8 402.86 356.63 309.81 263.85 218.65 174.12 130.17 86.727 43.719 1.0763
9 367.27 324.28 282.04 240.46 199.47 159.01 119.01 79.413 40.171 1.2301
10 357.22 315.52 274.52 234.13 194.30 154.95 116.04 77.504 39.302 1.3839
11 347.42 306.99 267.19 227.96 189.25 150.99 113.14 75.640 38.455 1.5377
12 337.98 298.75 260.11 222.00 184.37 147.16 110.33 73.841 37.640 1.6916
Weight fraction vapor 1 0.0852 0.0000 0.0000 0.0000 0.0000 -- -- -- -- --
2 0.2898 0.2172 0.1447 0.0723 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
3 0.0976 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
4 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
5 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
6 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
7 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
8 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
9 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
10 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
11 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
12 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 22
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 1 2 3 4 5 6 7 8 9 10
Liquid Properties
Density, (kg/m3) 1 1109.6 1109.6 1109.6 1109.6 1109.6 1109.6 1109.3 1108.6 1107.4 1105.3
2 1065.7 1065.7 1065.7 1065.7 1065.7 1065.7 1065.7 1063.6 1060.6 1056.4
3 1036.2 1036.2 1036.2 1036.2 1036.2 1036.2 1036.2 1031.3 1024.2 1015.4
4 1012.6 1012.6 1012.6 1012.6 1012.6 1012.6 1012.6 1006.8 999.36 991.03
5 992.42 992.42 992.42 992.42 992.42 992.42 983.83 973.74 964.20 956.38
6 974.65 974.65 974.65 974.65 974.65 974.65 963.32 951.78 942.67 936.11
7 958.71 958.71 958.71 958.71 958.71 958.71 947.81 937.60 929.84 924.28
8 944.25 944.25 944.25 944.25 944.25 944.25 932.37 922.59 915.85 911.24
9 931.04 931.04 931.04 931.04 931.04 918.19 909.07 903.33 899.52 896.82
10 918.88 918.88 918.88 918.88 918.88 903.51 895.09 890.41 887.44 885.37
11 907.66 907.66 907.66 907.66 894.07 886.79 882.68 880.03 878.15 876.74
12 897.26 897.26 897.26 897.26 883.97 877.60 874.08 871.81 870.21 869.00
Viscosity, (mN-s/m2) 1 0.5129 0.5129 0.5129 0.5129 0.5129 0.5129 0.5123 0.5104 0.5066 0.5003
2 0.3606 0.3606 0.3606 0.3606 0.3606 0.3606 0.3606 0.3546 0.3468 0.3371
3 0.2972 0.2972 0.2972 0.2972 0.2972 0.2972 0.2972 0.2869 0.2743 0.2609
4 0.2589 0.2589 0.2589 0.2589 0.2589 0.2589 0.2589 0.2492 0.2385 0.2279
5 0.2324 0.2324 0.2324 0.2324 0.2324 0.2324 0.2206 0.2089 0.1993 0.1923
6 0.2126 0.2126 0.2126 0.2126 0.2126 0.2126 0.1993 0.1880 0.1803 0.1753
7 0.1972 0.1972 0.1972 0.1972 0.1972 0.1972 0.1857 0.1766 0.1704 0.1664
8 0.1848 0.1848 0.1848 0.1848 0.1848 0.1848 0.1735 0.1656 0.1607 0.1576
9 0.1746 0.1746 0.1746 0.1746 0.1746 0.1634 0.1566 0.1528 0.1504 0.1488
10 0.1660 0.1660 0.1660 0.1660 0.1660 0.1537 0.1481 0.1453 0.1436 0.1424
11 0.1588 0.1588 0.1588 0.1588 0.1484 0.1436 0.1412 0.1397 0.1387 0.1379
12 0.1525 0.1525 0.1525 0.1525 0.1428 0.1389 0.1368 0.1356 0.1348 0.1342
Thermal conductivity, (W/m-C) 1 0.1505 0.1505 0.1505 0.1505 0.1505 0.1505 0.1532 0.1565 0.1607 0.1659
2 0.1568 0.1568 0.1568 0.1568 0.1568 0.1568 0.1568 0.1627 0.1702 0.1797
3 0.1647 0.1647 0.1647 0.1647 0.1647 0.1647 0.1647 0.1773 0.1944 0.2165
4 0.1733 0.1733 0.1733 0.1733 0.1733 0.1733 0.1733 0.1886 0.2085 0.2323
5 0.1824 0.1824 0.1824 0.1824 0.1824 0.1824 0.2070 0.2381 0.2714 0.3023
6 0.1920 0.1920 0.1920 0.1920 0.1920 0.1920 0.2278 0.2696 0.3080 0.3392
7 0.2018 0.2018 0.2018 0.2018 0.2018 0.2018 0.2397 0.2806 0.3163 0.3449
8 0.2118 0.2118 0.2118 0.2118 0.2118 0.2118 0.2576 0.3021 0.3373 0.3638
9 0.2218 0.2218 0.2218 0.2218 0.2218 0.2769 0.3238 0.3575 0.3818 0.4001
10 0.2317 0.2317 0.2317 0.2317 0.2317 0.3062 0.3566 0.3881 0.4095 0.4251
11 0.2415 0.2415 0.2415 0.2415 0.3128 0.3592 0.3884 0.4084 0.4231 0.4344
12 0.2509 0.2509 0.2509 0.2509 0.3272 0.3716 0.3985 0.4168 0.4301 0.4404

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 23
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 11 12 13 14 15 16 17 18 19 20
Liquid Properties
Density, (kg/m3) 1 1102.1 1097.5 1091.6 1084.8 1077.6 1069.7 1051.2 1042.4 1133.2 1131.5
2 1050.9 1044.3 1037.2 1030.1 1023.4 1017.4 1003.3 993.62 986.83 981.81
3 1006.1 997.45 990.08 983.97 978.95 971.34 965.92 961.88 958.76 955.53
4 982.90 975.72 969.69 964.72 960.64 952.75 947.57 943.90 941.16 939.01
5 950.32 945.64 939.03 934.63 931.47 929.08 927.20 925.68 939.44 952.33
6 931.37 927.83 925.10 921.55 918.98 917.03 915.48 929.56 942.78 955.19
7 920.23 917.19 914.81 910.86 908.21 906.27 920.55 933.97 946.58 958.43
8 907.93 905.45 901.95 899.57 897.83 912.20 925.73 938.47 950.46 961.75
9 893.70 891.56 889.97 903.56 916.41 928.57 940.08 950.98 961.29 971.04
10 883.82 882.60 896.24 909.14 921.37 932.96 943.94 954.36 964.23 973.57
11 875.63 889.28 902.21 914.47 926.11 937.16 947.65 957.61 967.05 976.02
12 882.64 895.58 907.86 919.52 930.61 941.15 951.18 960.70 969.75 978.58
Viscosity, (mN-s/m2) 1 0.4908 0.4776 0.4614 0.4439 0.4266 0.4091 0.3702 0.3549 0.6598 0.6484
2 0.3257 0.3135 0.3016 0.2907 0.2814 0.2736 0.2573 0.2478 0.2417 0.2376
3 0.2484 0.2383 0.2304 0.2244 0.2198 0.2134 0.2092 0.2063 0.2042 0.2020
4 0.2188 0.2116 0.2059 0.2016 0.1983 0.1924 0.1888 0.1864 0.1847 0.1835
5 0.1873 0.1838 0.1791 0.1762 0.1743 0.1729 0.1718 0.1710 0.1848 0.2009
6 0.1720 0.1696 0.1679 0.1657 0.1643 0.1632 0.1623 0.1745 0.1886 0.2049
7 0.1637 0.1618 0.1603 0.1580 0.1565 0.1555 0.1664 0.1788 0.1931 0.2098
8 0.1556 0.1541 0.1521 0.1508 0.1499 0.1597 0.1708 0.1835 0.1981 0.2151
9 0.1471 0.1459 0.1451 0.1535 0.1629 0.1734 0.1853 0.1987 0.2142 0.2322
10 0.1416 0.1410 0.1488 0.1574 0.1669 0.1776 0.1897 0.2034 0.2191 0.2374
11 0.1374 0.1446 0.1526 0.1613 0.1710 0.1819 0.1942 0.2082 0.2242 0.2427
12 0.1409 0.1483 0.1564 0.1653 0.1752 0.1863 0.1988 0.2130 0.2293 0.2481
Thermal conductivity, (W/m-C) 1 0.1728 0.1815 0.1924 0.2051 0.2192 0.2358 0.2913 0.3224 0.1537 0.1551
2 0.1918 0.2063 0.2229 0.2406 0.2585 0.2761 0.3226 0.3593 0.3879 0.4105
3 0.2420 0.2681 0.2929 0.3153 0.3352 0.3679 0.3933 0.4134 0.4296 0.4471
4 0.2579 0.2828 0.3058 0.3262 0.3442 0.3818 0.4089 0.4293 0.4451 0.4579
5 0.3288 0.3510 0.3851 0.4097 0.4283 0.4429 0.4547 0.4645 0.4692 0.4730
6 0.3639 0.3835 0.3994 0.4211 0.4374 0.4502 0.4606 0.4659 0.4703 0.4738
7 0.3674 0.3854 0.4000 0.4255 0.4434 0.4569 0.4626 0.4675 0.4715 0.4746
8 0.3842 0.4002 0.4239 0.4407 0.4534 0.4594 0.4646 0.4690 0.4726 0.4754
9 0.4221 0.4380 0.4500 0.4559 0.4611 0.4657 0.4696 0.4728 0.4753 0.4772
10 0.4371 0.4467 0.4528 0.4582 0.4630 0.4672 0.4708 0.4737 0.4760 0.4776
11 0.4435 0.4497 0.4554 0.4604 0.4648 0.4687 0.4719 0.4746 0.4766 0.4781
12 0.4468 0.4526 0.4578 0.4624 0.4665 0.4700 0.4730 0.4754 0.4772 0.4793

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 24
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 21 22 23 24 25 26 27 28 29 30
Liquid Properties
Density, (kg/m3) 1 1001.5 998.37 1017.2 1032.8 1045.2 -- -- -- -- --
2 977.97 974.92 972.43 970.36 968.61 988.34 1006.2 1021.7 1034.6 1045.2
3 953.03 951.02 966.23 980.70 994.77 1007.5 1018.9 1029.0 1037.7 1045.3
4 937.28 953.31 968.08 982.30 995.99 1008.4 1019.5 1029.3 1037.9 1045.3
5 964.40 975.71 987.33 998.10 1008.0 1017.1 1025.4 1032.8 1039.5 1045.3
6 966.81 977.92 989.14 999.54 1009.1 1017.9 1025.9 1033.2 1039.7 1045.4
7 969.55 980.44 991.19 1001.2 1010.4 1018.9 1026.6 1033.6 1039.8 1045.4
8 972.37 983.03 993.31 1002.9 1011.7 1019.8 1027.3 1034.0 1040.0 1045.4
9 980.72 990.28 999.23 1007.6 1015.3 1022.5 1029.1 1035.1 1040.6 1045.4
10 983.09 992.26 1000.9 1008.9 1016.4 1023.3 1029.6 1035.5 1040.7 1045.5
11 985.37 994.18 1002.4 1010.2 1017.4 1024.0 1030.2 1035.8 1040.9 1045.5
12 987.55 996.01 1003.9 1011.4 1018.3 1024.7 1030.7 1036.1 1041.1 1045.5
Viscosity, (mN-s/m2) 1 0.3087 0.3062 0.4037 0.5699 0.8893 -- -- -- -- --
2 0.2346 0.2324 0.2306 0.2292 0.2280 0.2736 0.3392 0.4387 0.6002 0.8893
3 0.2005 0.1992 0.2234 0.2539 0.2932 0.3451 0.4156 0.5148 0.6609 0.8893
4 0.1825 0.2024 0.2268 0.2576 0.2972 0.3494 0.4200 0.5190 0.6641 0.8893
5 0.2199 0.2427 0.2704 0.3046 0.3473 0.4019 0.4730 0.5682 0.6998 0.8893
6 0.2242 0.2473 0.2753 0.3098 0.3528 0.4075 0.4786 0.5733 0.7033 0.8893
7 0.2294 0.2528 0.2812 0.3161 0.3594 0.4142 0.4852 0.5792 0.7074 0.8892
8 0.2350 0.2589 0.2877 0.3228 0.3665 0.4215 0.4922 0.5855 0.7118 0.8892
9 0.2532 0.2782 0.3081 0.3443 0.3887 0.4439 0.5140 0.6046 0.7248 0.8892
10 0.2588 0.2841 0.3143 0.3507 0.3952 0.4505 0.5203 0.6101 0.7284 0.8892
11 0.2644 0.2900 0.3205 0.3572 0.4019 0.4571 0.5265 0.6155 0.7321 0.8892
12 0.2701 0.2960 0.3267 0.3636 0.4084 0.4637 0.5328 0.6208 0.7356 0.8892
Thermal conductivity, (W/m-C) 1 0.4736 0.4859 0.4872 0.4815 0.4682 -- -- -- -- --
2 0.4287 0.4438 0.4564 0.4671 0.4764 0.4829 0.4873 0.4865 0.4803 0.4683
3 0.4610 0.4725 0.4761 0.4799 0.4850 0.4875 0.4871 0.4839 0.4777 0.4683
4 0.4684 0.4732 0.4764 0.4807 0.4854 0.4876 0.4871 0.4838 0.4776 0.4684
5 0.4758 0.4777 0.4827 0.4860 0.4876 0.4875 0.4856 0.4818 0.4762 0.4685
6 0.4763 0.4788 0.4834 0.4864 0.4878 0.4875 0.4855 0.4817 0.4761 0.4685
7 0.4769 0.4800 0.4841 0.4868 0.4879 0.4874 0.4853 0.4815 0.4760 0.4686
8 0.4774 0.4811 0.4849 0.4872 0.4880 0.4873 0.4851 0.4813 0.4758 0.4686
9 0.4802 0.4839 0.4865 0.4878 0.4880 0.4868 0.4843 0.4805 0.4754 0.4687
10 0.4812 0.4846 0.4869 0.4880 0.4879 0.4867 0.4842 0.4804 0.4753 0.4688
11 0.4822 0.4853 0.4873 0.4881 0.4879 0.4865 0.4840 0.4802 0.4752 0.4688
12 0.4831 0.4858 0.4876 0.4883 0.4879 0.4864 0.4838 0.4800 0.4751 0.4689

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 25
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 1 2 3 4 5 6 7 8 9 10
Liquid Properties
Enthalpy, (kJ/kg) 1 0.0000 -74.39 -148.8 -223.2 -297.6 -372.0 -378.3 -385.1 -392.4 -399.9
2 0.0000 -53.44 -106.9 -160.3 -213.8 -267.2 -320.6 -327.9 -335.2 -342.3
3 0.0000 -48.39 -96.78 -145.2 -193.6 -241.9 -290.3 -299.9 -308.5 -315.1
4 0.0000 -44.50 -89.00 -133.5 -178.0 -222.5 -267.0 -275.4 -282.4 -287.4
5 0.0000 -49.44 -98.88 -148.3 -197.8 -247.2 -256.6 -263.1 -266.7 -268.6
6 0.0000 -45.89 -91.78 -137.7 -183.6 -229.5 -239.4 -244.8 -247.2 -248.4
7 0.0000 -42.60 -85.21 -127.8 -170.4 -213.0 -221.5 -226.0 -228.0 -229.1
8 0.0000 -39.49 -78.99 -118.5 -158.0 -197.5 -205.6 -209.2 -210.8 -211.7
9 0.0000 -45.63 -91.26 -136.9 -182.5 -190.3 -193.3 -194.6 -195.3 -195.7
10 0.0000 -42.00 -84.00 -126.0 -168.0 -176.1 -178.4 -179.3 -179.8 -180.1
11 0.0000 -51.26 -102.5 -153.8 -160.8 -162.8 -163.7 -164.2 -164.6 -164.8
12 0.0000 -46.60 -93.19 -139.8 -146.3 -148.1 -148.9 -149.3 -149.6 -149.8
Specific heat, (kJ/kg-C) 1 2.8753 2.8753 2.8753 2.8753 2.8753 2.8753 2.8823 2.8921 2.9059 2.9255
2 3.0642 3.0642 3.0642 3.0642 3.0642 3.0642 3.0642 3.0856 3.1144 3.1523
3 3.2074 3.2074 3.2074 3.2074 3.2074 3.2074 3.2074 3.2561 3.3230 3.4057
4 3.3341 3.3341 3.3341 3.3341 3.3341 3.3341 3.3341 3.3933 3.4681 3.5525
5 3.4520 3.4520 3.4520 3.4520 3.4520 3.4520 3.5442 3.6532 3.7592 3.8490
6 3.5643 3.5643 3.5643 3.5643 3.5643 3.5643 3.6933 3.8280 3.9384 4.0204
7 3.6725 3.6725 3.6725 3.6725 3.6725 3.6725 3.8041 3.9309 4.0305 4.1038
8 3.7773 3.7773 3.7773 3.7773 3.7773 3.7773 3.9297 4.0592 4.1513 4.2158
9 3.8791 3.8791 3.8791 3.8791 3.8791 4.0537 4.1821 4.2653 4.3214 4.3617
10 3.9781 3.9781 3.9781 3.9781 3.9781 4.1998 4.3261 4.3979 4.4440 4.4765
11 4.0743 4.0743 4.0743 4.0743 4.2802 4.3943 4.4600 4.5028 4.5331 4.5560
12 4.1677 4.1677 4.1677 4.1677 4.3794 4.4840 4.5426 4.5805 4.6074 4.6277
Surface tension, (mN/m) 1 32.583 32.583 32.583 32.583 32.583 32.583 33.535 34.641 35.930 37.426
2 32.504 32.504 32.504 32.504 32.504 32.504 32.504 33.838 35.337 36.977
3 32.399 32.399 32.399 32.399 32.399 32.399 32.399 34.390 36.525 38.583
4 32.200 32.200 32.200 32.200 32.200 32.200 32.200 34.054 35.914 37.593
5 31.927 31.927 31.927 31.927 31.927 31.927 34.176 36.188 37.723 38.799
6 31.598 31.598 31.598 31.598 31.598 31.598 34.144 36.091 37.352 38.152
7 31.225 31.225 31.225 31.225 31.225 31.225 33.474 35.109 36.157 36.830
8 30.818 30.818 30.818 30.818 30.818 30.818 33.067 34.514 35.373 35.909
9 30.383 30.383 30.383 30.383 30.383 32.645 33.909 34.608 35.037 35.327
10 29.926 29.926 29.926 29.926 29.926 32.435 33.507 34.040 34.359 34.572
11 29.451 29.451 29.451 29.451 31.620 32.552 33.028 33.317 33.514 33.657
12 28.962 28.962 28.962 28.962 31.021 31.823 32.226 32.472 32.640 32.763

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 26
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 11 12 13 14 15 16 17 18 19 20
Liquid Properties
Enthalpy, (kJ/kg) 1 -407.5 -414.6 -420.7 -425.4 -428.7 -431.1 -432.4 -432.4 -432.4 -432.4
2 -348.6 -353.8 -357.6 -360.2 -361.8 -362.8 -363.9 -364.1 -364.1 -364.1
3 -319.4 -321.8 -323.1 -323.8 -324.2 -324.5 -324.7 -324.9 -325.0 -325.1
4 -290.6 -292.4 -293.5 -294.1 -294.5 -295.1 -295.4 -295.6 -295.8 -295.9
5 -269.5 -270.1 -270.7 -271.1 -271.3 -271.5 -271.7 -271.8 -321.2 -369.8
6 -249.0 -249.4 -249.7 -250.0 -250.3 -250.4 -250.6 -299.6 -347.7 -395.0
7 -229.7 -230.1 -230.4 -230.9 -231.1 -231.3 -279.7 -327.1 -373.7 -419.6
8 -212.2 -212.6 -213.0 -213.3 -213.5 -261.1 -307.7 -353.4 -398.4 -442.8
9 -196.2 -196.4 -196.6 -240.7 -283.8 -326.2 -367.8 -408.9 -449.4 -489.4
10 -180.4 -180.5 -223.9 -266.4 -308.1 -349.0 -389.4 -429.2 -468.5 -507.3
11 -165.0 -207.7 -249.5 -290.5 -330.8 -370.4 -409.5 -448.1 -486.2 -523.9
12 -191.9 -233.1 -273.4 -313.0 -351.9 -390.3 -428.2 -465.6 -502.6 -539.2
Specific heat, (kJ/kg-C) 1 2.9526 2.9889 3.0346 3.0875 3.1440 3.2078 3.3686 3.4496 2.6357 2.6854
2 3.2001 3.2568 3.3188 3.3819 3.4425 3.4987 3.6358 3.7337 3.8052 3.8589
3 3.4949 3.5798 3.6548 3.7186 3.7722 3.8557 3.9167 3.9630 3.9993 4.0372
4 3.6369 3.7137 3.7798 3.8355 3.8822 3.9745 4.0368 4.0817 4.1156 4.1424
5 3.9207 3.9773 4.0590 4.1148 4.1552 4.1861 4.2106 4.2306 4.1516 4.0832
6 4.0811 4.1272 4.1632 4.2106 4.2451 4.2716 4.2928 4.2070 4.1328 4.0684
7 4.1582 4.1997 4.2325 4.2874 4.3247 4.3521 4.2604 4.1811 4.1121 4.0519
8 4.2627 4.2983 4.3490 4.3837 4.4093 4.3123 4.2284 4.1553 4.0914 4.0354
9 4.4086 4.4411 4.4652 4.3687 4.2847 4.2110 4.1459 4.0883 4.0372 3.9917
10 4.5009 4.5200 4.4188 4.3307 4.2533 4.1851 4.1246 4.0708 4.0228 3.9801
11 4.5741 4.4683 4.3763 4.2955 4.2242 4.1609 4.1046 4.0542 4.0092 3.9689
12 4.5175 4.4216 4.3376 4.2633 4.1974 4.1385 4.0859 4.0388 3.9965 3.9567
Surface tension, (mN/m) 1 39.132 41.000 42.921 44.755 46.392 47.945 51.047 52.271 34.478 34.976
2 38.690 40.365 41.893 43.207 44.295 45.182 46.987 48.042 48.720 49.191
3 40.337 41.703 42.727 43.495 44.080 44.900 45.442 45.826 46.112 46.399
4 38.965 40.020 40.816 41.420 41.888 42.724 43.234 43.578 43.827 44.017
5 39.548 40.083 40.786 41.225 41.526 41.746 41.916 42.051 44.549 47.005
6 38.685 39.062 39.342 39.691 39.934 40.115 40.255 42.725 45.157 47.547
7 37.287 37.614 37.861 38.253 38.506 38.685 41.111 43.503 45.858 48.174
8 36.272 36.534 36.887 37.118 37.283 39.657 42.001 44.313 46.589 48.827
9 35.647 35.859 36.012 38.195 40.355 42.489 44.596 46.673 48.717 50.727
10 34.728 34.846 36.983 39.100 41.194 43.263 45.304 47.317 49.298 51.246
11 33.768 35.858 37.930 39.982 42.011 44.016 45.994 47.944 49.864 51.752
12 34.806 36.833 38.843 40.832 42.799 44.742 46.659 48.548 50.409 52.239

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 27
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 21 22 23 24 25 26 27 28 29 30
Liquid Properties
Enthalpy, (kJ/kg) 1 -432.4 -432.4 -522.3 -610.9 -698.6 -- -- -- -- --
2 -364.2 -364.2 -364.2 -364.3 -364.3 -444.8 -523.8 -601.4 -678.1 -754.2
3 -325.2 -325.3 -385.6 -444.9 -503.2 -560.8 -617.6 -674.0 -729.9 -785.6
4 -296.0 -356.3 -415.4 -473.6 -530.8 -587.3 -643.1 -698.4 -753.4 -808.0
5 -417.7 -464.9 -511.4 -557.4 -603.0 -648.1 -692.8 -737.3 -781.5 -825.6
6 -441.7 -487.7 -533.1 -578.0 -622.4 -666.5 -710.2 -753.7 -796.9 -840.0
7 -464.8 -509.4 -553.5 -597.1 -640.3 -683.2 -725.7 -768.0 -810.1 -852.1
8 -486.5 -529.8 -572.5 -614.8 -656.7 -698.3 -739.5 -780.6 -821.5 -862.3
9 -529.0 -568.1 -606.9 -645.3 -683.4 -721.3 -758.9 -796.4 -833.8 -871.0
10 -545.7 -583.8 -621.4 -658.8 -695.9 -732.7 -769.4 -805.9 -842.2 -878.5
11 -561.2 -598.2 -634.8 -671.1 -707.2 -743.0 -778.7 -814.2 -849.6 -884.9
12 -575.4 -611.3 -646.9 -682.3 -717.4 -752.3 -787.0 -821.6 -856.0 -890.4
Specific heat, (kJ/kg-C) 1 3.8430 3.8749 3.8057 3.7588 3.7314 -- -- -- -- --
2 3.9009 3.9346 3.9623 3.9856 4.0054 3.9162 3.8442 3.7910 3.7539 3.7312
3 4.0669 4.0908 4.0161 3.9498 3.8889 3.8394 3.7998 3.7689 3.7462 3.7310
4 4.1641 4.0787 4.0071 3.9422 3.8837 3.8359 3.7976 3.7677 3.7456 3.7308
5 4.0239 3.9723 3.9197 3.8749 3.8370 3.8052 3.7790 3.7580 3.7420 3.7306
6 4.0122 3.9616 3.9117 3.8690 3.8327 3.8023 3.7771 3.7569 3.7414 3.7303
7 3.9992 3.9497 3.9027 3.8623 3.8280 3.7990 3.7750 3.7557 3.7408 3.7301
8 3.9861 3.9378 3.8936 3.8556 3.8231 3.7957 3.7729 3.7545 3.7402 3.7299
9 3.9479 3.9060 3.8694 3.8377 3.8103 3.7870 3.7674 3.7515 3.7390 3.7297
10 3.9369 3.8974 3.8628 3.8327 3.8067 3.7844 3.7658 3.7505 3.7384 3.7295
11 3.9266 3.8893 3.8565 3.8279 3.8032 3.7820 3.7642 3.7495 3.7379 3.7293
12 3.9168 3.8816 3.8506 3.8234 3.7999 3.7797 3.7626 3.7486 3.7374 3.7291
Surface tension, (mN/m) 1 56.223 56.449 60.745 64.794 68.582 -- -- -- -- --
2 49.537 49.802 50.013 50.186 50.329 54.331 58.171 61.834 65.308 68.582
3 46.615 46.785 49.822 52.781 55.656 58.441 61.130 63.720 66.205 68.582
4 44.167 47.212 50.187 53.086 55.902 58.631 61.268 63.808 66.247 68.582
5 49.415 51.776 54.086 56.341 58.538 60.676 62.752 64.762 66.707 68.582
6 49.894 52.193 54.443 56.639 58.781 60.864 62.889 64.851 66.749 68.582
7 50.447 52.675 54.854 56.983 59.060 61.082 63.047 64.953 66.799 68.582
8 51.023 53.176 55.283 57.343 59.352 61.309 63.212 65.060 66.850 68.582
9 52.702 54.638 56.535 58.391 60.204 61.973 63.697 65.374 67.002 68.582
10 53.160 55.038 56.877 58.678 60.437 62.155 63.830 65.460 67.044 68.582
11 53.607 55.427 57.211 58.957 60.665 62.333 63.960 65.544 67.085 68.582
12 54.037 55.802 57.533 59.227 60.885 62.505 64.085 65.626 67.125 68.582

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 28
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 1 2 3 4 5 6 7 8 9 10
Liquid Properties
Critical temperature, (C) 1 350.37 350.37 350.37 350.37 350.37 350.37 351.03 351.81 352.76 353.89
2 354.51 354.51 354.51 354.51 354.51 354.51 354.51 355.58 356.82 358.22
3 357.09 357.09 357.09 357.09 357.09 357.09 357.09 358.83 360.78 362.75
4 359.02 359.02 359.02 359.02 359.02 359.02 359.02 360.74 362.53 364.23
5 360.57 360.57 360.57 360.57 360.57 360.57 362.77 364.84 366.51 367.72
6 361.85 361.85 361.85 361.85 361.85 361.85 364.47 366.60 368.05 368.99
7 362.95 362.95 362.95 362.95 362.95 362.95 365.35 367.20 368.43 369.24
8 363.89 363.89 363.89 363.89 363.89 363.89 366.38 368.09 369.13 369.80
9 364.70 364.70 364.70 364.70 364.70 367.31 368.85 369.73 370.27 370.64
10 365.42 365.42 365.42 365.42 365.42 368.42 369.78 370.47 370.88 371.16
11 366.04 366.04 366.04 366.04 368.70 369.91 370.54 370.92 371.18 371.37
12 366.59 366.59 366.59 366.59 369.19 370.25 370.79 371.13 371.35 371.52
Critical pressure, (kPa) 1 9854.3 9854.3 9854.3 9854.3 9854.3 9854.3 10193 10598 11086 11672
2 11992 11992 11992 11992 11992 11992 11992 12545 13186 13910
3 13326 13326 13326 13326 13326 13326 13326 14226 15232 16249
4 14324 14324 14324 14324 14324 14324 14324 15211 16139 17014
5 15123 15123 15123 15123 15123 15123 16260 17333 18194 18819
6 15787 15787 15787 15787 15787 15787 17139 18242 18990 19477
7 16351 16351 16351 16351 16351 16351 17592 18549 19187 19607
8 16838 16838 16838 16838 16838 16838 18128 19008 19549 19893
9 17260 17260 17260 17260 17260 18606 19403 19857 20139 20330
10 17629 17629 17629 17629 17629 19180 19883 20240 20454 20599
11 17953 17953 17953 17953 19328 19951 20275 20473 20609 20708
12 18237 18237 18237 18237 19578 20127 20407 20580 20698 20785
Molecular weight, (--) 1 72.659 72.659 72.659 72.659 72.659 72.659 71.143 69.328 67.143 64.517
2 63.084 63.084 63.084 63.084 63.084 63.084 63.084 60.607 57.738 54.496
3 57.108 57.108 57.108 57.108 57.108 57.108 57.108 53.081 48.572 44.018
4 52.640 52.640 52.640 52.640 52.640 52.640 52.640 48.669 44.512 40.593
5 49.062 49.062 49.062 49.062 49.062 49.062 43.970 39.162 35.310 32.510
6 46.086 46.086 46.086 46.086 46.086 46.086 40.031 35.094 31.745 29.562
7 43.560 43.560 43.560 43.560 43.560 43.560 38.004 33.719 30.860 28.980
8 41.382 41.382 41.382 41.382 41.382 41.382 35.605 31.660 29.238 27.697
9 39.491 39.491 39.491 39.491 39.491 33.464 29.892 27.861 26.599 25.741
10 37.838 37.838 37.838 37.838 37.838 30.894 27.743 26.145 25.184 24.536
11 36.388 36.388 36.388 36.388 30.230 27.440 25.989 25.100 24.493 24.047
12 35.115 35.115 35.115 35.115 29.107 26.650 25.394 24.623 24.094 23.704

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 29
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 11 12 13 14 15 16 17 18 19 20
Liquid Properties
Critical temperature, (C) 1 355.23 356.76 358.39 360.00 361.49 362.94 366.03 367.27 349.18 349.68
2 359.73 361.27 362.72 364.00 365.09 366.00 367.90 369.04 369.78 370.29
3 364.50 365.92 367.01 367.85 368.49 369.41 370.02 370.45 370.77 371.09
4 365.67 366.81 367.69 368.37 368.90 369.86 370.45 370.85 371.13 371.35
5 368.58 369.20 370.03 370.55 370.90 371.16 371.36 371.52 371.52 371.52
6 369.63 370.08 370.42 370.84 371.14 371.35 371.52 371.52 371.52 371.52
7 369.80 370.20 370.51 370.99 371.30 371.52 371.52 371.52 371.52 371.52
8 370.25 370.58 371.02 371.31 371.52 371.52 371.52 371.52 371.52 371.52
9 371.05 371.33 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
10 371.37 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
11 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
12 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
Critical pressure, (kPa) 1 12366 13155 13998 14831 15599 16350 17945 18588 9234.7 9496.6
2 14692 15485 16233 16896 17461 17931 18914 19502 19883 20148
3 17155 17888 18454 18886 19220 19693 20007 20230 20397 20563
4 17757 18348 18803 19155 19430 19926 20230 20435 20583 20696
5 19264 19586 20014 20281 20465 20599 20703 20785 20785 20785
6 19806 20040 20215 20433 20585 20697 20785 20785 20785 20785
7 19895 20102 20259 20510 20671 20785 20785 20785 20785 20785
8 20128 20297 20527 20678 20785 20785 20785 20785 20785 20785
9 20543 20683 20785 20785 20785 20785 20785 20785 20785 20785
10 20704 20785 20785 20785 20785 20785 20785 20785 20785 20785
11 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
12 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
Molecular weight, (--) 1 61.411 57.877 54.103 50.369 46.928 43.565 36.424 33.542 75.434 74.261
2 50.992 47.440 44.089 41.119 38.592 36.486 32.084 29.450 27.742 26.556
3 39.960 36.677 34.145 32.208 30.713 28.594 27.186 26.187 25.443 24.700
4 37.263 34.620 32.579 31.005 29.774 27.550 26.188 25.270 24.607 24.103
5 30.517 29.072 27.158 25.960 25.137 24.535 24.072 23.704 23.704 23.704
6 28.087 27.039 26.257 25.280 24.600 24.096 23.704 23.704 23.704 23.704
7 27.691 26.760 26.058 24.937 24.215 23.704 23.704 23.704 23.704 23.704
8 26.648 25.888 24.858 24.185 23.704 23.704 23.704 23.704 23.704 23.704
9 24.789 24.158 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
10 24.065 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
11 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
12 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Properties Profile Monitor Page 30
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Physical Properties Profile: Cold Pipe (LA +water)
Property package VMGThermo
Reference pressure, (kPa) (P1= 101.33) (P2= 283.14) (P3= 464.96) (P4= 646.78) (P5= 828.60) (P6= 1010.4)
(P7= 1192.2) (P8= 1374.1) (P9= 1555.9) (P10= 1737.7) (P11= 1919.5) (P12= 2101.3)
(P) 21 22 23 24 25 26 27 28 29 30
Liquid Properties
Critical temperature, (C) 1 371.29 371.52 371.52 371.52 371.52 -- -- -- -- --
2 370.67 370.95 371.18 371.37 371.52 371.52 371.52 371.52 371.52 371.52
3 371.33 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
4 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
5 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
6 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
7 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
8 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
9 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
10 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
11 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
12 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52 371.52
Critical pressure, (kPa) 1 20666 20785 20785 20785 20785 -- -- -- -- --
2 20342 20491 20609 20705 20785 20785 20785 20785 20785 20785
3 20687 20785 20785 20785 20785 20785 20785 20785 20785 20785
4 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
5 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
6 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
7 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
8 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
9 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
10 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
11 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
12 20785 20785 20785 20785 20785 20785 20785 20785 20785 20785
Molecular weight, (--) 1 24.238 23.704 23.704 23.704 23.704 -- -- -- -- --
2 25.686 25.019 24.491 24.061 23.704 23.704 23.704 23.704 23.704 23.704
3 24.141 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
4 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
5 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
6 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
7 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
8 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
9 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
10 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
11 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704
12 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704 23.704

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Stream Properties Page 31
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Hot Annulus Fluid Inlet Outlet
Fluid name hot oil
Flow (kg/s) 0.0114
Temperature (C) 210.00 200.00
Pressure (kPa) 301.32 301.32
Weight fraction vapor (--) 0.0000 0.0000
Vapor Properties
Flow (kg/s) -- --
Density (kg/m3) -- --
Viscosity (mN-s/m2) -- --
Conductivity (W/m-C) -- --
Heat capacity (kJ/kg-C) -- --
Molecular weight (--) -- --
Liquid Properties
Flow (kg/s) 0.0114 0.0114
Density (kg/m3) 786.13 792.02
Viscosity (mN-s/m2) 0.6953 0.7596
Conductivity (W/m-C) 0.1062 0.1074
Heat capacity (kJ/kg-C) 2.5785 2.5434
Molecular weight (--) 320.00 320.00
Latent heat (kJ/kg) -- --
Surface tension (mN/m) 15.204 15.805
Molar Composition Vapor Liquid K-Value Vapor Liquid K-Value

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Stream Properties Page 32
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Cold Pipe Fluid Inlet Outlet
Fluid name LA +water
Flow (kg/s) 4.17e-4
Temperature (C) 30.00 200.00
Pressure (kPa) 2101.3 2101.3
Weight fraction vapor (--) 0.0000 0.0000
Vapor Properties
Flow (kg/s) -- --
Density (kg/m3) -- --
Viscosity (mN-s/m2) -- --
Conductivity (W/m-C) -- --
Heat capacity (kJ/kg-C) -- --
Molecular weight (--) -- --
Liquid Properties
Flow (kg/s) 4.17e-4 4.17e-4
Density (kg/m3) 1045.5 889.68
Viscosity (mN-s/m2) 0.8892 0.1448
Conductivity (W/m-C) 0.4689 0.4500
Heat capacity (kJ/kg-C) 3.7291 4.4642
Molecular weight (--) 23.704 23.704
Latent heat (kJ/kg) -- --
Surface tension (mN/m) 68.582 35.897
Molar Composition MW Vapor Liquid K-Value Vapor Liquid K-Value
1 LACTIC ACID 90.08 0.0000 0.0790 -- 0.0000 0.0790 --
2 WATER 18.02 0.0000 0.9211 -- 0.0000 0.9211 --
Mass Composition Vapor Liquid Vapor Liquid
1 LACTIC ACID 0.0000 0.3000 0.0000 0.3000
2 WATER 0.0000 0.7000 0.0000 0.7000

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Drawings Page 33
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

53
mm

4
m

Unit heat stable reactor Total tube inlet nozzles 1 Stream ID Shellside Tubeside
TEMA typeJacketed Pipe Total tube outlet nozzles 1 Stream name hot oil LA +water
Shell diameter 52.502 mm Total shell inlet nozzles 1 Flow (total), kg/s 0.0114 4.17e-4
Tube length 4 m Total shell outlet nozzles 1 Pressure drop, kPa 6.27e-3 2.34e-3
Dry weight 57 kg/shell Temperature, C 210.00 200.00 30.00 200.00
Wet weight 65 kg/shell Wt. fraction vapor 0.0000 0.0000 0.0000 0.0000
Bundle weight 3 kg/shell Pressure, kPa 301.32 301.32 2101.3 2101.3

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Drawings Page 34
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Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe

Unit heat stable reactor


Exchanger typeJacketed-Pipe
15.799 mm Jacket ID 52.502 mm
Pipe OD 13.716 mm
Nozzles
-Shell Inlet ID 15.799 mm
-Shell Outlet ID 15.799 mm

15.799 mm

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Input Reprint Page 35
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Jacket Data
Run mode Rating
Hot fluid location Annulus
Exchanger angle 0.00 deg
Number of exchangers in series 1
Number of exchangers in parallel 1
Jacket inside diameter 52.502 mm
Flow in exchanger Countercurrent
Train flow direction Countercurrent
Shellside vacuum pressure None
Tubeside vacuum pressure None
Shellside radiography None
Tubeside radiography None
Shellside corrosion allowance 0.000 mm
Tubeside corrosion allowance 0.000 mm
TEMA class non-TEMA
Design temperature inside pipe 232.22 C
Design pressure inside pipe 2206.3 kPaG
Design temperature inside annulus 237.78 C
Design pressure inside annulus 517.11 kPaG
Tubesheet design temperature 237.78 C

Pipe Data
Type Plain
Pipe outside diameter 13.716 mm
Wall thickness 2.235 mm
Pipe length 4.000 m
Pipe material SA-214 Tube (W) K01807

Nozzle Data
Radial position of annulus inlet nozzle Program decides
Longitudinal position of annulus inlet nozzle At rear head
Radial position of annulus outlet nozzle Program decides
Annulus Inlet ID 15.799 mm
Annulus Outlet ID 15.799 mm
Pipe Inlet ID 9.246 mm
Pipe Outlet ID 9.246 mm

Process Conditions Data Hot Fluid Cold Fluid


Phase condition Sensible liquid Sensible liquid
Flow rate -- 4.17e-4 kg/s
Inlet vapor fraction 0.0000 0.0000
Outlet vapor fraction 0.0000 0.0000
Inlet temperature 210.00 30.00 C
Outlet temperature 200.00 200.00 C
Inlet pressure 301.32 2101.3 kPa
Allowable pressure drop 30.000 20.000 kPa
Duty multiplier 1.0000

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Input Reprint Page 36
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Process Fouling Data Hot Fluid Cold Fluid
Fouling resistance 0.0002 0.0002 m2-K/W

Hot Fluid Property Data


Fluid name hot oil
Physical property method Property generator
Temperature interpolation option Program
Flash type Integral
Critical point composition basis Local liquid phase
Critical point calculation method Pseudo critical
Quantity units Weight
Number of components 1
Property package VMGThermo

Hot Fluid Component Data


Component number 1
Component name Therminol 55
Comp. bank name Therminol 55
Component bank VMGThermo
Component code 19895
Component phase Mixed
Component quantity 1.0000

Hot Fluid User-Specified Conditions for Property Generation


Point option Defined P and T ranges
Starting pressure 301.32 kPa
Ending pressure 271.32 kPa
Starting temperature 250.00 C
Ending temperature 30.00 C
Vapor fraction / enthalpy basis Mole/mole fraction
Increment option Equal Enthalpy
Pressure sets Auto
Temperature points Auto
Minimum number of 2-phase points Auto
Logic for regenerating properties If associated input changes
Regenerate properties on next run No
Supercritical phase Liquid
Insert bubble point Yes
Insert dew point Yes
Create 2-phase zones Yes
Adjust calculated points Yes
Generate latent heat No

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Input Reprint Page 37
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Cold Fluid Property Data
Fluid name LA +water
Physical property method Property generator
Temperature interpolation option Program
Flash type Integral
Critical point composition basis Local liquid phase
Critical point calculation method Pseudo critical
Quantity units Weight
Number of components 2
Property package VMGThermo

Cold Fluid Component Data


Component number 1 2
Component name LACTIC ACID WATER
Comp. bank name LACTIC ACID WATER
Component bank VMGThermo VMGThermo
Component code 348 5101
Component phase Mixed Mixed
Component quantity 0.3000 0.7000

Cold Fluid User-Specified Conditions for Property Generation


Point option Defined P and T ranges
Starting pressure 2101.3 kPa
Ending pressure 101.33 kPa
Starting temperature 30.00 C
Ending temperature 250.00 C
Vapor fraction / enthalpy basis Mole/mole fraction
Increment option Equal Enthalpy
Pressure sets Auto
Temperature points Auto
Minimum number of 2-phase points Auto
Logic for regenerating properties If associated input changes
Regenerate properties on next run No
Supercritical phase Liquid
Insert bubble point Yes
Insert dew point Yes
Create 2-phase zones Yes
Adjust calculated points Yes
Generate latent heat No

Control Name Data


Problem name heat stable reactor for 30% LA

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri
Input Reprint Page 38
Released to the following HTRI Member Company:

Xjpe 9 (64 bit) 11-12-2023 11:59 SN: 00342-945981152 SI Units


heat stable reactor for 30% LA
heat stable reactor
Rating - Horizontal Countercurrent Flow Jacketed Pipe
Control Methods Data
Annulus friction factor method Commercial
Pipe friction factor method Commercial
Pure component condensation No
Condensing correlation HTRI Proration
Mole fraction inerts 0.0000
Momentum exclusion 0.0000 %
Perform shellside subcooling calculations No
Pure component boiling No
Check film boiling Yes
Nucleate boiling method Physical property/theoretical boiling range
Component boiling method Nucleate and convective
Reduced pressure calculation method Program decides

Control User-Defined Methods Data


Add non-nucleate boiling Yes

Unit: heat stable reactor D:\Ongoing Projects\LA_PLA\Heat Stable Reactor\heat stable 1.5 Kg_hr.htri

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