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  • Muestra Silvita@edxelem

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    Fabio Jurado
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    This document summarizes the results of an EDX analysis of a sample. The sample was measured under vacuum conditions using an EDX-800HS instrument with a 10mm collimator and mylar sample cup. Qualitative analysis identified the elements Si, Cl, K, Rh, and S in the sample. Quantitative analysis found the sample contains 50.816% K, 44.547% Cl, 4.099% Si, and 0.539% S. Peak identification and intensities are provided for the Ti-U and C-Sc spectra.

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    muestra_silvita@edxelem

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    This document summarizes the results of an EDX analysis of a sample. The sample was measured under vacuum conditions using an EDX-800HS instrument with a 10mm collimator and mylar sample cup. Qualitative analysis identified the elements Si, Cl, K, Rh, and S in the sample. Quantitative analysis found the sample contains 50.816% K, 44.547% Cl, 4.099% Si, and 0.539% S. Peak identification and intensities are provided for the Ti-U and C-Sc spectra.

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    © All Rights Reserved
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    17 views2 pages

    Muestra Silvita@edxelem

    Uploaded by

    Fabio Jurado
    This document summarizes the results of an EDX analysis of a sample. The sample was measured under vacuum conditions using an EDX-800HS instrument with a 10mm collimator and mylar sample cup. Qualitative analysis identified the elements Si, Cl, K, Rh, and S in the sample. Quantitative analysis found the sample contains 50.816% K, 44.547% Cl, 4.099% Si, and 0.539% S. Peak identification and intensities are provided for the Ti-U and C-Sc spectra.

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    of 2

    Sample : MUESTRA_silvita@edx

    Operator:
    Comment : Comment
    Group : 10_vacio_mylar_kevin
    Date : 2023-08-22 21:31:04

    Measurement Condition
    ------------------------------------------------------------------------------------
    Instrument: EDX-800HS Atmosphere: Vac. Collimator: 10(mm) Sample Cup:Mylar
    ------------------------------------------------------------------------------------
    Analyte TG kV uA FI Acq.(keV) Anal.(keV) Time(sec) DT(%)
    ------------------------------------------------------------------------------------
    Ti-U Rh 50 23-Auto ---- 0 - 40 0.00-40.00 Live- 100 25
    C-Sc Rh 15 133-Auto ---- 0 - 20 0.00- 4.40 Live- 100 26

    Qualitative Result
    ------------------------------------------------------------------------------------
    Element: Si, Cl, K , Rh, S

    Peak List
    ------------------------------------------------------------------------------------
    Channel Line keV Net Int.(cps/uA)
    ------------------------------------------------------------------------------------
    Ti-U SiKa 1.74 2.9919
    ClKa 2.62 82.1436
    K Ka 3.30 49.7979
    K Kb 3.58 7.0263
    RhKaC 19.18 6.5831
    RhKa 20.18 12.8377
    RhKbC 21.42 1.6081
    RhKb 22.74 2.2080
    ------------------------------------------------------------------------------------
    C-Sc ClKaESC 0.88 0.5442
    ClKbESC 1.08 0.0566
    K KaESC 1.56 0.1742
    SiKa 1.74 1.4057 QF
    S Ka 2.36 0.9287 QF
    ClKa 2.62 34.8058 QF
    ClKb 2.82 3.0160
    K Ka 3.32 17.9870 QF
    K Kb 3.58 2.5290
    ------------------------------------------------------------------------------------

    Quantitative Result
    ------------------------------------------------------------------------------------
    Analyte Result [3-sigma] Proc.-Calc. Line Int.(cps/uA)
    ------------------------------------------------------------------------------------
    K 50.816 % [ 0.310] Quan-FP K Ka 17.9870
    Cl 44.547 % [ 0.195] Quan-FP ClKa 34.8058
    Si 4.099 % [ 0.084] Quan-FP SiKa 1.4057
    S 0.539 % [ 0.023] Quan-FP S Ka 0.9287
    Sample : MUESTRA_silvita@edx Group : 10_vacio_mylar_kevin Date : 2023-08-22 21:31:04
    Operator: Comment : Comment 01/01
    [cps/uA] Ti-U

    ClKa
    10.0
    K Ka

    5.0

    RhKa
    RhKaC
    K Kb

    RhKbC
    SiKa

    RhKb
    0.0
    0.0 10.0 20.0 30.0
    [keV]
    [cps/uA] C-Sc
    ClKa

    3.00

    2.00
    K Ka

    1.00
    ClKa ESC

    K Ka ESC
    ClKb ESC

    ClKb

    K Kb
    SiKa

    S Ka

    0.00
    0.0 2.0 4.0
    [keV]

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