1.

Secondary Mixed Standard Calculation:

Conc. in ampule Actual Conc. Final vol. of
Item# Analyte Catalog No.: (ug/mL) (ug/mL) methanol (mL)
1 Benzene 30249 2000 20 25
2 Carbon Tetrachloride 30259 2000 10 25
3 1,2-Dichlorobenzene 31442 1000 10 25
4 1,4-Dichlorobenzene 31444 1000 10 25
5 1,2-Dichloroethane 30277 2000 10 25
6 cis-1,2-Dichloroethene 30279 2000 10 25
7 trans-1,2-Dichloroethene 30280 2000 10 25
8 Dichloromethane 30401 2000 10 25
9 Ethylbenzene 30290 2000 10 25
10 Styrene 30410 2000 10 25
11 Tetrachloroethene 30413 2000 10 25
12 Toluene 30415 2000 10 25
13 Vinyl Chloride 30089 2000 10 25
14 o-Xylenes 30425 2000 10 25
15 p-Xylenes 30426 2000 10 25
16 m-Xylenes 30424 2000 10 25
17 1,2-Dibromo-3-chloropropan 30270 2000 10 25
18 Dibromoethane 30272 2000 10 25

2. Calibration Standards
Initial vol.
Final volume of cal. Conc. Of mixed from mixed
Level Cal. Conc. (ug/L) (mL) (ug/mL) (mL)
1 0.25 25 10 0.000625
2 1 25 10 0.0025
3 2.5 25 10 0.00625
4 5 25 10 0.0125
5 10 25 10 0.025
6 25 25 10 0.0625
7 50 25 10 0.125

3. Secondary Internal Standard

Secondary conc. Vol. of methanol Initial vol.
Conc. In ampule (µg/mL) (µg/mL) (mL) (mL)
2000 25 10 0.125

4. Working internal standard

Required conc. Initial vol.
Conc. Of secondary (µg/mL) Final vol. (mL) (µg/L) (mL)
10 25 40 0.1
Initial vol. of In. Vol of
analyte (mL) Density (kg/m3) Density (g/mL) Analyte (g)
0.25 876 0.876 0.2190
0.125 1594 1.594 0.1993
0.25 1300 1.3 0.3250
0.25 1250 1.25 0.3125
0.125 1250 1.25 0.1563
0.125 1.284 0.1605
0.125 1.257 0.1571
0.125 1.33 0.1663
0.125 866 0.866 0.1083
0.125 0.909 0.1136
0.125 0.0000
0.125 867 0.867 0.1084
0.125 911 0.911 0.1139
0.125 0.876 0.1095
0.125 861 0.861 0.1076
0.125 860 0.860 0.1075
0.125 2.05 0.2563
0.125 2.17 0.2713
2.625