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ASTM D6794 (2019) - Engine Filter Ability
ASTM D6794 (2019) - Engine Filter Ability
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6794 − 19
INTRODUCTION
Portions of this test method are written for use by laboratories that make use of ASTM Test
Monitoring Center (TMC)2 services (see Annex A1).
The TMC provides reference oils, and engineering and statistical services to laboratories that desire
to produce test results that are statistically similar to those produced by laboratories previously
calibrated by the TMC.
In general, the Test Purchaser decides if a calibrated test stand is to be used. Organizations such as
the American Chemistry Council require that a laboratory utilize the TMC services as part of their test
registration process. In addition, the American Petroleum Institute and the Gear Lubricant Review
Committee of the Lubricant Review Institute (SAE International) require that a laboratory use the
TMC services in seeking qualification of oils against their specifications.
The advantage of using the TMC services to calibrate test stands is that the test laboratory (and
hence the Test Purchaser) has an assurance that the test stand was operating at the proper level of test
severity. It should also be borne in mind that results obtained in a non-calibrated test stand may not
be the same as those obtained in a test stand participating in the ASTM TMC services process.
Laboratories that choose not to use the TMC services may simply disregard these portions.
ASTM International policy is to encourage the development of test procedures based on generic
equipment. It is recognized that there are occasions where critical/sole-source equipment has been
approved by the technical committee (surveillance panel/task force) and is required by the test
procedure. The technical committee that oversees the test procedure is encouraged to clearly identify
if the part is considered critical in the test procedure. If a part is deemed to be critical, ASTM
encourages alternative suppliers to be given the opportunity for consideration of supplying the critical
part/component providing they meet the approval process set forth by the technical committee.
An alternative supplier can start the process by initiating contact with the technical committee
(current chairs shown on ASTM TMC website). The supplier should advise on the details of the part
that is intended to be supplied. The technical committee will review the request and determine
feasibility of an alternative supplier for the requested replacement critical part. In the event that a
replacement critical part has been identified and proven equivalent, the sole-source supplier footnote
shall be removed from the test procedure.
For other information, refer to the research report of this test method.3
2
ASTM Test Monitoring Center, 6555 Penn Ave., Pittsburgh, PA 152006-4489.
This test method is supplemented by Information Letters and Memoranda issued by
1
This test method is under the jurisdiction of ASTM Committee D02 on the ASTM Test Monitoring Center. This edition includes all information letters
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of through No. 19-1. Users of this test method can contact the ASTM Test Monitoring
Subcommittee D02.B0 on Automotive Lubricants. Center to obtain the most recent of these.
3
Current edition approved July 1, 2019. Published July 2019. Originally approved Supporting data have been filed at ASTM International Headquarters and may
in 2002. Last previous edition approved in 2014 as D6794 – 14. DOI: 10.1520/ be obtained by requesting Research Report RR:D02-1492. Contact ASTM Customer
D6794-19. Service at service@astm.org.
examples. the same treatments such that the loss of filterability can be
3.1.4 engine oil, n—a liquid that reduces friction or wear, or determined.
both, between the moving parts within an engine; removes
5.5 Reference oils, on which the data obtained by this test
method is known, are available.
4
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 5.6 This test method requires that a reference oil also be
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM tested and results reported. Two oils are available, one known
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
to give a low and one known to give a high data value for this
5
The last approved version of this historical standard is referenced on test method.
www.astm.org. NOTE 1—When the new oil test results are to be offered as candidate oil
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D6794 − 19
test results for a specification, such as Specification D4485, the specifi- 6.3 Timer, capable of timing 30 s 6 1 s.
cation will state maximum allowable loss of filterability (flow reduction)
of the test oil as compared to the new oil. 6.4 Container, 250 mL, with blade compatible with the
blender.
6. Apparatus
6.5 Syringe, 1000 µL.
6.1 The apparatus consists of a 25 mL burette, a filter holder
with 25 µm automotive oil filter paper, and a source of 69 kPa 6.6 Glass Jars, 60 mL, wide-mouth with inert lined lids.
6 2 kPa air pressure. Discs of filter paper are cut to fit the
NOTE 2—Paperbacked lids may detach from lid and are not suggested
holder and installed (see Fig. 1). for use.
6.1.1 Burette (glass or plastic), 25 mL, with polytetrafluo-
roethylene (PTFE) stopcock and (1.8 6 0.1) mm burette tip 6.7 Mechanical Convection Oven, capable of maintaining
opening. 70 °C 6 1 °C.
6.1.2 Air Regulator, capable of regulating air to a pressure 6.8 Sensors (or equivalent timing devices), capable of mea-
of (69 6 2) kPa. suring sequential events to 1 s resolution.
6.1.3 Filter Holder, with effective filter area approximately
0.8 cm2. 6.9 Tubing, inert tubing used to connect to burette.
6.1.4 Automotive Oil Filter Paper, 25 µm porosity.6 6.9.1 Air Regulator Tubing, flexible tubing to prevent air
6.2 Blender, capable of 18 000 r/min 610 % without the from leaking from the air supply to the burette.
container. 6.9.2 Filter Holder Tubing, flexible tubing used to connect
burette tip to filter holder.
6
The sole source of supply of the automotive oil filter paper known to the 7. Reagents
committee at this time is The Central Parts Distributor, OH Technologies Inc., P.O.
Box 5039, Mentor, OH 44061-5039. If you are aware of alternative suppliers, please 7.1 Purity of Reagents—Use reagent grade chemicals in all
provide this information to ASTM International Headquarters. Your comments will tests. Unless otherwise indicated, it is intended that all reagents
receive careful consideration at a meeting of the responsible technical committee,1 shall conform to the specifications of the Committee on
which you may attend.
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NOTE 1—Filter holder has approximate area of 0.8 cm2. It contains automotive oil filter paper (25 µm porosity).
FIG. 1 Apparatus To Measure Engine Oil Filterability
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D6794 − 19
Analytical Reagents of the American Chemical Society,7 where Disconnect the air line and fill the burette with a well-mixed
such specifications are available. Other grades may be used, sample of test oil to a level 1 cm to 2 cm above the 0 mark.
provided it is first ascertained that the reagent is of sufficiently Pressurize the system to 69 kPa 6 2 kPa, open the stopcock,
high purity to permit its use without lessening the accuracy of and measure the flow time for each successive 5 mL of oil
the determination. between the 0 mL and 25 mL graduations.
7.2 Purity of Water—Unless otherwise indicated, references 10.4 Run each non-reference and reference oil in duplicate;
to water shall be understood to mean Test Method D1193 Type repeat Section 9 and 10.1 to 10.4 for each non-reference and
III deionized water or water of equivalent purity. each reference oil.
7.3 TMC Reference Oils—These are available from the Test 10.5 For TMC-monitored tests, run the TMC reference oil
Monitoring Center. on the same day as the non-reference oil.
8. Sampling 10.6 For tests not monitored by the TMC, an in-house
8.1 Take samples in accordance with the instructions in quality assurance oil can be used in place of the TMC
Practice D4057. reference.
new oil are first determined. Using the same filter disc, filter for a blind reference-testing program to protect against the
holder, and burette, reduce the new oil level in the burette to the possibility of bias in the results.
lowest level that allows no air bubbles below the stopcock. 12.1.1.1 The testing laboratory tacitly agrees to use the
TMC reference oils exclusively in accordance with the TMC’s
7
published Policies for Use and Analysis of ASTM Reference
Reagent Chemicals, American Chemical Society Specifications , American
Chemical Society, Washington, DC. For suggestions on the testing of reagents not Oils, and to run and report the reference oil test according to
listed by the American Chemical Society, see Analar Standards for Laboratory TMC guidelines.
Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville, NOTE 4—Policies for the Use and Analysis of ASTM Reference Oils are
MD. available from the TMC.
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12.1.2 Request a reference oil assignment from the TMC for test method and good laboratory practice. Following this
this test method. The TMC determines the specific reference oil recheck, the TMC assigns another TMC reference oil for
to be tested by the laboratory. Assignments are made by the testing.
unique identifying codes on the reference oil container labels. 12.1.6 Status of Non-Reference Oil Tests Relative to TMC
12.1.3 Run the TMC reference oil test according to the test Reference Oil Tests—The batch of non-reference tests is
method and in the same manner as the non-reference oil test(s). considered valid only if the results of the TMC reference oil
Run the reference oil simultaneously with, and in the same test meet the predetermined acceptance specifications for the
batch as, the non-reference oils. Reference oils and non- particular reference oil tested.
reference oils in the same batch shall be run within the same
13. Report
4 h time frame.
12.1.4 Reporting of Reference Oil Test Results—Report the 13.1 Report the following information:
results of all reference oil tests to the TMC according to the 13.1.1 Non-reference or reference oil identification.
following directives: 13.1.2 Porosity of filter used (25 µm).
12.1.4.1 The data report forms are available from the TMC 13.1.3 Percent change in final flow rate for each test.
for reporting all TMC reference oil test data to the TMC. 13.1.4 Average percent change in final flow rate for the
Report only the reference oil results to the TMC. Do not duplicate tests.
include any non-reference test data. Complete all of the 13.1.5 For TMC-monitored tests, contact the TMC for
required blank fields on the forms. reporting requirements.
12.1.4.2 Transmit reference test data to the TMC by elec- 13.1.6 For tests not monitored by the TMC, an in-house
tronic means or by telephone facsimile immediately upon quality assurance sample can be used to evaluate test accept-
completion of the test analysis. Include all of the reporting ability.
forms in the transmission. 14. Precision and Bias
NOTE 5—Specific protocols for the electronic transmission of test data 14.1 The following criteria should be used for judging the
to the TMC are available from the TMC. acceptability of 25 µm filter results:
12.1.5 Evaluation of Reference Test Oil Results—Upon 14.1.1 Repeatability—The difference between successive
receipt of the transmitted reference oil test results, the TMC test results, obtained by the same operator with the same
reviews the test for operational adherence to the published test apparatus under constant operating conditions on identical test
method. If the test is found to be operationally valid, the material, would in the long run, in the normal and correct
reference oil results are evaluated using acceptance criteria operation of the test method, exceed the following value only
established by the governing surveillance panel. The reference in one case in twenty:
oil acceptance criteria are subject to change at the discretion of 11.1 %
the surveillance panel.
12.1.5.1 If the transmitted test is found to be both opera- 14.1.2 Reproducibility—The difference between two single
tionally valid and statistically acceptable, the testing laboratory and independent results, obtained by different operators work-
is notified of the acceptable status of the reference test. The ing in different laboratories on identical test material, would in
uncoded TMC reference oil identification is also disclosed to the long run, in the normal and correct operation of the test
the testing laboratory. method, exceed the following value only in one case in twenty:
12.1.5.2 In the event that a TMC reference oil test is found 25.4 %
to be unacceptable, an explanation of the problem relating to 14.2 Bias—Since there is no accepted reference material
the failure is provided to the testing laboratory. If there is an suitable for determining the bias for this test method, bias
obvious operational reason for the failed test, the problem shall cannot be determined.
be corrected before requesting another TMC reference oil
assignment. If the reason for failure is not obvious, all 15. Keywords
test-related equipment shall be rechecked for compliance to the 15.1 engine lubricating oil; filterability; storage
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ANNEX
(Mandatory Information)
A1. ROLE OF THE ASTM TEST MONITORING CENTER AND THE CALIBRATION PROGRAM
A1.1 Nature and Functions of the TMC—The TMC is a tests needed to enable the TMC to recommend proper industry
nonprofit organization located in Pittsburgh, PA, USA. The performance and precision targets and performance acceptance
TMC is staffed to administer technical studies; conduct labo- limits. These donated tests will be run as required by ASTM
ratory visits; perform statistical analyses of reference oil test D02.B0.07 Engine Oil Water Tolerance Surveillance Panel to
data; blend, store, and ship reference oils; and provide associ- establish these targets and acceptance limits for new oils.
ated administrative functions to maintain the referencing cali-
bration program for various lubricant tests as directed by A1.7 TMC Information Letters:
ASTM Subcommittee D02.B0 and the Test Monitoring Board. A1.7.1 Occasionally it might become necessary to change
The TMC coordinates its activities with the test sponsors, the the test method, and notify the test laboratories of the change,
test developers, the surveillance panels, and the testing labo- prior to consideration of the change by either ASTM Subcom-
ratories through a consensus process. mittee D02.B0 on Automotive Lubricants, or ASTM Commit-
A1.2 Rules of Operation of the TMC—The TMC operates in tee D02 on Petroleum Products and Lubricants. In such a case,
accordance with the ASTM Charter, the ASTM Bylaws, the the TMC issues an Information Letter. Subsequently, prior to
Regulations Governing ASTM Technical Committees, the each semiannual ASTM Committee D02 meeting, the accumu-
Bylaws Governing ASTM Committee D02, and the Rules and lated Information Letters are balloted by ASTM Subcommittee
Regulations Governing the ASTM Test Monitoring System. D02.B0. Following this action, the approved Information
Letters are used to revise the affected standards, and these are
A1.3 Management of the TMC—The management of the balloted in the main committee, and finally, the Society. By this
Test Monitoring System is vested in the Test Monitoring Board means, the Society’s due process procedures are applied to
(TMB) elected by ASTM Subcommittee D02.B0. The TMB these Information Letters.
selects the TMC Administrator, who is responsible for direct-
A1.7.2 The review of an Information Letter prior to its
ing the activities of the TMC staff.
original issue might differ according to its nature. In the case of
A1.4 Operating Income of the TMC—The TMC’s operating an Information Letter concerning a part number change that
income is obtained from fees levied on the reference oils does not affect test results, the TMC is authorized to issue such
supplied and on the calibration tests conducted. Fee schedules a letter. Long-term studies by the Surveillance Panel to
are established and reviewed by ASTM Subcommittee D02.B0. improve test procedures through improved operation and
hardware control may result in a recommendation to issue an
A1.5 Conducting a Reference Oil Test—For those laborato- Information Letter. If obvious procedural items affecting test
ries choosing to utilize the services of the TMC in maintaining results need immediate attention, the test sponsor and the TMC
the calibration of test methods and apparatus, calibration issue an Information Letter and present the background and
testing is conducted at regular intervals as determined by data to the Surveillance Panel for approval prior to the
ASTM D02.B0.07 Engine Oil Filterability Surveillance Panel. semiannual ASTM Subcommittee D02.B0 meeting.
These tests are conducted using coded reference oils supplied
by the TMC as outlined in 11.1 of this test method. It is the A1.7.3 The ASTM Committee on Technical Committee
laboratories’ responsibility to maintain the calibration in ac- Operations (COTCO) in 1984 gave authority for the issuance
cordance with this test method. It is also the laboratories’ of Information Letters, as follows: “COTCO recognizes that
responsibility to keep an on-site reference oil inventory at or D-2 has a unique and complex situation. The use of Informa-
above the minimum level specified by the TMC test represen- tion Letters is approved providing each letter contains a
tative. disclaimer to the effect that such has not obtained ASTM
consensus. These Information Letters should be moved to such
A1.6 New Laboratories: consensus as rapidly as possible.”
A1.6.1 Laboratories wishing to participate in the ASTM A1.8 TMC Memoranda—In addition to the Information
Monitoring System will be requested to conduct reference oil
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SUMMARY OF CHANGES
Subcommittee D02.B0 has identified the location of selected changes to this standard since the last issue
(D6794 – 14) that may impact the use of this standard. (Approved July 1, 2019.)
ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should
make your views known to the ASTM Committee on Standards, at the address shown below.
This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,
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