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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles

for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Designation: D6794 − 19

Standard Test Method for


Measuring the Effect on Filterability of Engine Oils After
Treatment with Various Amounts of Water and a Long (6 h)
Heating Time1
This standard is issued under the fixed designation D6794; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.

INTRODUCTION

Portions of this test method are written for use by laboratories that make use of ASTM Test
Monitoring Center (TMC)2 services (see Annex A1).
The TMC provides reference oils, and engineering and statistical services to laboratories that desire
to produce test results that are statistically similar to those produced by laboratories previously
calibrated by the TMC.
In general, the Test Purchaser decides if a calibrated test stand is to be used. Organizations such as
the American Chemistry Council require that a laboratory utilize the TMC services as part of their test
registration process. In addition, the American Petroleum Institute and the Gear Lubricant Review
Committee of the Lubricant Review Institute (SAE International) require that a laboratory use the
TMC services in seeking qualification of oils against their specifications.
The advantage of using the TMC services to calibrate test stands is that the test laboratory (and
hence the Test Purchaser) has an assurance that the test stand was operating at the proper level of test
severity. It should also be borne in mind that results obtained in a non-calibrated test stand may not
be the same as those obtained in a test stand participating in the ASTM TMC services process.
Laboratories that choose not to use the TMC services may simply disregard these portions.
ASTM International policy is to encourage the development of test procedures based on generic
equipment. It is recognized that there are occasions where critical/sole-source equipment has been
approved by the technical committee (surveillance panel/task force) and is required by the test
procedure. The technical committee that oversees the test procedure is encouraged to clearly identify
if the part is considered critical in the test procedure. If a part is deemed to be critical, ASTM
encourages alternative suppliers to be given the opportunity for consideration of supplying the critical
part/component providing they meet the approval process set forth by the technical committee.
An alternative supplier can start the process by initiating contact with the technical committee
(current chairs shown on ASTM TMC website). The supplier should advise on the details of the part
that is intended to be supplied. The technical committee will review the request and determine
feasibility of an alternative supplier for the requested replacement critical part. In the event that a
replacement critical part has been identified and proven equivalent, the sole-source supplier footnote
shall be removed from the test procedure.
For other information, refer to the research report of this test method.3

1. Scope* It simulates a problem that may be encountered in a new engine


1.1 This test method covers the determination of the ten-
dency of an oil to form a precipitate that can plug an oil filter.
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2
ASTM Test Monitoring Center, 6555 Penn Ave., Pittsburgh, PA 152006-4489.
This test method is supplemented by Information Letters and Memoranda issued by
1
This test method is under the jurisdiction of ASTM Committee D02 on the ASTM Test Monitoring Center. This edition includes all information letters
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of through No. 19-1. Users of this test method can contact the ASTM Test Monitoring
Subcommittee D02.B0 on Automotive Lubricants. Center to obtain the most recent of these.
3
Current edition approved July 1, 2019. Published July 2019. Originally approved Supporting data have been filed at ASTM International Headquarters and may
in 2002. Last previous edition approved in 2014 as D6794 – 14. DOI: 10.1520/ be obtained by requesting Research Report RR:D02-1492. Contact ASTM Customer
D6794-19. Service at service@astm.org.

*A Summary of Changes section appears at the end of this standard


Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
Copyright by ASTM Int'l (all rights reserved); Wed Dec 4 07:20:46 EST 2019
1
D6794 − 19
run for a short period of time, followed by a long period of heat, particularly from the underside of pistons; and serves as
storage with some water in the oil. a combustion gas sealant for the piston rings.
1.2 The values stated in SI units are to be regarded as 3.1.4.1 Discussion—It may contain additives to enhance
standard. No other units of measurement are included in this certain properties. Inhibition of engine rusting, deposit
standard. formation, valve train wear, oil oxidation, and foaming are
examples. D5862
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 3.1.5 non-reference oil, n—any oil other than a reference
responsibility of the user of this standard to establish appro- oil–such as a research formulation, commercial oil, or candi-
priate safety, health, and environmental practices and deter- date oil.
mine the applicability of regulatory limitations prior to use. 3.1.5.1 Discussion—Reference oils are used to calibrate
1.4 This international standard was developed in accor- testing facilities, to compare the performance of other oils, or
dance with internationally recognized principles on standard- to evaluate other materials (such as seals) that interact with
ization established in the Decision on Principles for the oils.
Development of International Standards, Guides and Recom- 3.1.6 reference oil, n—an oil of known performance
mendations issued by the World Trade Organization Technical characteristics, used as a basis for comparison.
Barriers to Trade (TBT) Committee. 3.1.6.1 Discussion—Reference oils are used to calibrate
testing facilities, to compare the performance of other oils, or
2. Referenced Documents to evaluate other materials (such as seals) that interact with
2.1 ASTM Standards:4 oils. D5844
D1193 Specification for Reagent Water 3.2 Definitions of Terms Specific to This Standard:
D4057 Practice for Manual Sampling of Petroleum and 3.2.1 effective filter area, n—that surface of a test filter that
Petroleum Products can receive the material to be filtered.
D4485 Specification for Performance of Active API Service
Category Engine Oils 3.2.2 new oil, n—an unused oil having the identical formu-
D5844 Test Method for Evaluation of Automotive Engine lation and base stock as the test oil.
Oils for Inhibition of Rusting (Sequence IID) (Withdrawn 3.2.3 test oil, n—the new oil with various amounts of water
2003)5 added.
D5862 Test Method for Evaluation of Engine Oils in Two- 3.2.3.1 Discussion—A potential precipitate in the test oil is
Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine induced by heating the oil and aging.
(Withdrawn 2009)5
4. Summary of Test Method
3. Terminology 4.1 Add deionized water to the test oil for a final solution of
3.1 Definitions: 0.6 %, 1.0 %, 2.0 %, and 3.0 % water in oil. The sample is
3.1.1 calibrate, v—to determine the indication or output of a heated to 70 °C for 6 h, followed by storage at room tempera-
device (e.g., thermometer, manometer, engine) with respect to ture. The sample is filtered and the flow rate is calculated
that of a standard. determining the engine oil filterability characteristics.
3.1.2 calibration test, n—a test, using a coded oil, conducted
5. Significance and Use
as specified in the test method.
3.1.2.1 Discussion—The test result is used to determine the 5.1 It is normal for some of the combustion products of an
suitability of the testing facility/laboratory to conduct such internal combustion engine to penetrate into the engine lubri-
tests on non-reference oils. cant and be retained in it.
3.1.3 candidate oil, n—an oil that is intended to have the 5.2 When an engine is run for a period of time and then
performance characteristics necessary to satisfy a specification stored over a long period of time, the by-products of combus-
and is tested against that specification. tion might be retained in the oil in a liquefied state.
3.1.3.1 Discussion—It may contain additives to enhance 5.3 Under these circumstances, precipitates can form that
certain properties. Inhibition of engine rusting, deposit impair the filterability of the oil the next time the engine is run.
formation, valve train wear, oil oxidation, and foaming are 5.4 This test method subjects the test oil and the new oil to
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examples. the same treatments such that the loss of filterability can be
3.1.4 engine oil, n—a liquid that reduces friction or wear, or determined.
both, between the moving parts within an engine; removes
5.5 Reference oils, on which the data obtained by this test
method is known, are available.
4
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 5.6 This test method requires that a reference oil also be
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM tested and results reported. Two oils are available, one known
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
to give a low and one known to give a high data value for this
5
The last approved version of this historical standard is referenced on test method.
www.astm.org. NOTE 1—When the new oil test results are to be offered as candidate oil

Copyright by ASTM Int'l (all rights reserved); Wed Dec 4 07:20:46 EST 2019
2
D6794 − 19
test results for a specification, such as Specification D4485, the specifi- 6.3 Timer, capable of timing 30 s 6 1 s.
cation will state maximum allowable loss of filterability (flow reduction)
of the test oil as compared to the new oil. 6.4 Container, 250 mL, with blade compatible with the
blender.
6. Apparatus
6.5 Syringe, 1000 µL.
6.1 The apparatus consists of a 25 mL burette, a filter holder
with 25 µm automotive oil filter paper, and a source of 69 kPa 6.6 Glass Jars, 60 mL, wide-mouth with inert lined lids.
6 2 kPa air pressure. Discs of filter paper are cut to fit the
NOTE 2—Paperbacked lids may detach from lid and are not suggested
holder and installed (see Fig. 1). for use.
6.1.1 Burette (glass or plastic), 25 mL, with polytetrafluo-
roethylene (PTFE) stopcock and (1.8 6 0.1) mm burette tip 6.7 Mechanical Convection Oven, capable of maintaining
opening. 70 °C 6 1 °C.
6.1.2 Air Regulator, capable of regulating air to a pressure 6.8 Sensors (or equivalent timing devices), capable of mea-
of (69 6 2) kPa. suring sequential events to 1 s resolution.
6.1.3 Filter Holder, with effective filter area approximately
0.8 cm2. 6.9 Tubing, inert tubing used to connect to burette.
6.1.4 Automotive Oil Filter Paper, 25 µm porosity.6 6.9.1 Air Regulator Tubing, flexible tubing to prevent air
6.2 Blender, capable of 18 000 r/min 610 % without the from leaking from the air supply to the burette.
container. 6.9.2 Filter Holder Tubing, flexible tubing used to connect
burette tip to filter holder.

6
The sole source of supply of the automotive oil filter paper known to the 7. Reagents
committee at this time is The Central Parts Distributor, OH Technologies Inc., P.O.
Box 5039, Mentor, OH 44061-5039. If you are aware of alternative suppliers, please 7.1 Purity of Reagents—Use reagent grade chemicals in all
provide this information to ASTM International Headquarters. Your comments will tests. Unless otherwise indicated, it is intended that all reagents
receive careful consideration at a meeting of the responsible technical committee,1 shall conform to the specifications of the Committee on
which you may attend.
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NOTE 1—Filter holder has approximate area of 0.8 cm2. It contains automotive oil filter paper (25 µm porosity).
FIG. 1 Apparatus To Measure Engine Oil Filterability

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D6794 − 19
Analytical Reagents of the American Chemical Society,7 where Disconnect the air line and fill the burette with a well-mixed
such specifications are available. Other grades may be used, sample of test oil to a level 1 cm to 2 cm above the 0 mark.
provided it is first ascertained that the reagent is of sufficiently Pressurize the system to 69 kPa 6 2 kPa, open the stopcock,
high purity to permit its use without lessening the accuracy of and measure the flow time for each successive 5 mL of oil
the determination. between the 0 mL and 25 mL graduations.
7.2 Purity of Water—Unless otherwise indicated, references 10.4 Run each non-reference and reference oil in duplicate;
to water shall be understood to mean Test Method D1193 Type repeat Section 9 and 10.1 to 10.4 for each non-reference and
III deionized water or water of equivalent purity. each reference oil.
7.3 TMC Reference Oils—These are available from the Test 10.5 For TMC-monitored tests, run the TMC reference oil
Monitoring Center. on the same day as the non-reference oil.
8. Sampling 10.6 For tests not monitored by the TMC, an in-house
8.1 Take samples in accordance with the instructions in quality assurance oil can be used in place of the TMC
Practice D4057. reference.

9. Preparation of Test Oil Sample and Filter 11. Calculation


9.1 Add 49.7 g 6 0.1 g of test oil, 0.3 g 6 0.05 g of 11.1 Calculate the flow rate for the new oil and the test oil
deionized water using the 1000 µL syringe to the blender, and for each 5 mL portion of oil using Eq 1:
mix for 30 s 6 1 s at 18 000 r ⁄min 610 %. FR 5 A⁄B (1)
9.2 Repeat 9.1 with 49.5 g 6 0.1 g of test oil and
where:
0.5 g 6 0.05 g water for 1 % water, 49.0 g 6 0.1 g of test oil
and 1.0 g 6 0.05 g water for 2 % water, and 48.5 g 6 0.1 g of FR = the flow rate of oil, mL/s,
A = volume of oil, mL, and
test oil and 1.5 g 6 0.05 g water for 3 % water.
B = flow time, s.
9.3 Transfer the sample to a 60 mL wide-mouth glass jar
and place the loosely capped (1⁄4 turn) jar in an oven at 70.0 °C 11.2 Calculate the percent change in flow rate of the test oil
6 1.0 °C for 6 h 610 min. Remove from the oven, tighten cap, relative to the new oil with the final oil flow rates (between
and allow to cool to room temperature 20 °C to 24 °C. 20 mL and 25 mL measured with the same filter disc) using Eq
2:
9.4 Store the sample in the dark at room temperature 20 °C
∆FR 5 100~ E 2 D ! ⁄D (2)
to 24 °C.
9.5 Within 48 h 6 2 h of removing the sample from the where:
oven, determine the filterability (see 10.2) of the sample. ∆FR = change in flow rate, %,
E = final test oil flow rate, mL/s, and
9.6 Dry filters in an oven at 70 °C 6 2 °C for 30 min 6
D = final new oil flow rate, mL/s.
2 min and store in a desiccator until used.

10. Procedure 12. TMC Reference Oil Testing


10.1 Assemble apparatus as shown in Fig. 1 with filter 12.1 Test a TMC-coded reference oil along with each batch
installed in proper orientation (25 µm smooth side up). of non-reference oil tests. Run the reference oil simultaneously
with, and in the same batch as, the non-reference oils.
10.2 Determine the new oil flow rate by placing a sample of
the new oil in the burette. Pressurize the system and force at NOTE 3—Annex A1 discusses the involvement of the ASTM TMC with
least 10 mL of oil through the filter to saturate the filter with oil respect to the reference test-monitoring program.
and remove any air bubbles. Disconnect the air line and fill the 12.1.1 Prior to conducting a reference oil test, procure a
burette with new oil to a level 1 cm to 2 cm above the 0 mark. supply of reference oils directly from the TMC. These oils have
Pressurize the system to 69 kPa 6 2 kPa, open the stopcock, been formulated or selected to represent specific chemistry
and measure the flow time for each successive 5 mL of oil types, or performance levels, or both. Each reference oil
between the 0 mL and 25 mL graduations. sample is identified using a unique set of identification codes
10.3 To determine the test oil flow rate, the flow times of the on the container labels. The coded reference samples provide
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new oil are first determined. Using the same filter disc, filter for a blind reference-testing program to protect against the
holder, and burette, reduce the new oil level in the burette to the possibility of bias in the results.
lowest level that allows no air bubbles below the stopcock. 12.1.1.1 The testing laboratory tacitly agrees to use the
TMC reference oils exclusively in accordance with the TMC’s
7
published Policies for Use and Analysis of ASTM Reference
Reagent Chemicals, American Chemical Society Specifications , American
Chemical Society, Washington, DC. For suggestions on the testing of reagents not Oils, and to run and report the reference oil test according to
listed by the American Chemical Society, see Analar Standards for Laboratory TMC guidelines.
Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville, NOTE 4—Policies for the Use and Analysis of ASTM Reference Oils are
MD. available from the TMC.

Copyright by ASTM Int'l (all rights reserved); Wed Dec 4 07:20:46 EST 2019
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D6794 − 19
12.1.2 Request a reference oil assignment from the TMC for test method and good laboratory practice. Following this
this test method. The TMC determines the specific reference oil recheck, the TMC assigns another TMC reference oil for
to be tested by the laboratory. Assignments are made by the testing.
unique identifying codes on the reference oil container labels. 12.1.6 Status of Non-Reference Oil Tests Relative to TMC
12.1.3 Run the TMC reference oil test according to the test Reference Oil Tests—The batch of non-reference tests is
method and in the same manner as the non-reference oil test(s). considered valid only if the results of the TMC reference oil
Run the reference oil simultaneously with, and in the same test meet the predetermined acceptance specifications for the
batch as, the non-reference oils. Reference oils and non- particular reference oil tested.
reference oils in the same batch shall be run within the same
13. Report
4 h time frame.
12.1.4 Reporting of Reference Oil Test Results—Report the 13.1 Report the following information:
results of all reference oil tests to the TMC according to the 13.1.1 Non-reference or reference oil identification.
following directives: 13.1.2 Porosity of filter used (25 µm).
12.1.4.1 The data report forms are available from the TMC 13.1.3 Percent change in final flow rate for each test.
for reporting all TMC reference oil test data to the TMC. 13.1.4 Average percent change in final flow rate for the
Report only the reference oil results to the TMC. Do not duplicate tests.
include any non-reference test data. Complete all of the 13.1.5 For TMC-monitored tests, contact the TMC for
required blank fields on the forms. reporting requirements.
12.1.4.2 Transmit reference test data to the TMC by elec- 13.1.6 For tests not monitored by the TMC, an in-house
tronic means or by telephone facsimile immediately upon quality assurance sample can be used to evaluate test accept-
completion of the test analysis. Include all of the reporting ability.
forms in the transmission. 14. Precision and Bias
NOTE 5—Specific protocols for the electronic transmission of test data 14.1 The following criteria should be used for judging the
to the TMC are available from the TMC. acceptability of 25 µm filter results:
12.1.5 Evaluation of Reference Test Oil Results—Upon 14.1.1 Repeatability—The difference between successive
receipt of the transmitted reference oil test results, the TMC test results, obtained by the same operator with the same
reviews the test for operational adherence to the published test apparatus under constant operating conditions on identical test
method. If the test is found to be operationally valid, the material, would in the long run, in the normal and correct
reference oil results are evaluated using acceptance criteria operation of the test method, exceed the following value only
established by the governing surveillance panel. The reference in one case in twenty:
oil acceptance criteria are subject to change at the discretion of 11.1 %
the surveillance panel.
12.1.5.1 If the transmitted test is found to be both opera- 14.1.2 Reproducibility—The difference between two single
tionally valid and statistically acceptable, the testing laboratory and independent results, obtained by different operators work-
is notified of the acceptable status of the reference test. The ing in different laboratories on identical test material, would in
uncoded TMC reference oil identification is also disclosed to the long run, in the normal and correct operation of the test
the testing laboratory. method, exceed the following value only in one case in twenty:
12.1.5.2 In the event that a TMC reference oil test is found 25.4 %
to be unacceptable, an explanation of the problem relating to 14.2 Bias—Since there is no accepted reference material
the failure is provided to the testing laboratory. If there is an suitable for determining the bias for this test method, bias
obvious operational reason for the failed test, the problem shall cannot be determined.
be corrected before requesting another TMC reference oil
assignment. If the reason for failure is not obvious, all 15. Keywords
test-related equipment shall be rechecked for compliance to the 15.1 engine lubricating oil; filterability; storage
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D6794 − 19
ANNEX

(Mandatory Information)

A1. ROLE OF THE ASTM TEST MONITORING CENTER AND THE CALIBRATION PROGRAM

A1.1 Nature and Functions of the TMC—The TMC is a tests needed to enable the TMC to recommend proper industry
nonprofit organization located in Pittsburgh, PA, USA. The performance and precision targets and performance acceptance
TMC is staffed to administer technical studies; conduct labo- limits. These donated tests will be run as required by ASTM
ratory visits; perform statistical analyses of reference oil test D02.B0.07 Engine Oil Water Tolerance Surveillance Panel to
data; blend, store, and ship reference oils; and provide associ- establish these targets and acceptance limits for new oils.
ated administrative functions to maintain the referencing cali-
bration program for various lubricant tests as directed by A1.7 TMC Information Letters:
ASTM Subcommittee D02.B0 and the Test Monitoring Board. A1.7.1 Occasionally it might become necessary to change
The TMC coordinates its activities with the test sponsors, the the test method, and notify the test laboratories of the change,
test developers, the surveillance panels, and the testing labo- prior to consideration of the change by either ASTM Subcom-
ratories through a consensus process. mittee D02.B0 on Automotive Lubricants, or ASTM Commit-
A1.2 Rules of Operation of the TMC—The TMC operates in tee D02 on Petroleum Products and Lubricants. In such a case,
accordance with the ASTM Charter, the ASTM Bylaws, the the TMC issues an Information Letter. Subsequently, prior to
Regulations Governing ASTM Technical Committees, the each semiannual ASTM Committee D02 meeting, the accumu-
Bylaws Governing ASTM Committee D02, and the Rules and lated Information Letters are balloted by ASTM Subcommittee
Regulations Governing the ASTM Test Monitoring System. D02.B0. Following this action, the approved Information
Letters are used to revise the affected standards, and these are
A1.3 Management of the TMC—The management of the balloted in the main committee, and finally, the Society. By this
Test Monitoring System is vested in the Test Monitoring Board means, the Society’s due process procedures are applied to
(TMB) elected by ASTM Subcommittee D02.B0. The TMB these Information Letters.
selects the TMC Administrator, who is responsible for direct-
A1.7.2 The review of an Information Letter prior to its
ing the activities of the TMC staff.
original issue might differ according to its nature. In the case of
A1.4 Operating Income of the TMC—The TMC’s operating an Information Letter concerning a part number change that
income is obtained from fees levied on the reference oils does not affect test results, the TMC is authorized to issue such
supplied and on the calibration tests conducted. Fee schedules a letter. Long-term studies by the Surveillance Panel to
are established and reviewed by ASTM Subcommittee D02.B0. improve test procedures through improved operation and
hardware control may result in a recommendation to issue an
A1.5 Conducting a Reference Oil Test—For those laborato- Information Letter. If obvious procedural items affecting test
ries choosing to utilize the services of the TMC in maintaining results need immediate attention, the test sponsor and the TMC
the calibration of test methods and apparatus, calibration issue an Information Letter and present the background and
testing is conducted at regular intervals as determined by data to the Surveillance Panel for approval prior to the
ASTM D02.B0.07 Engine Oil Filterability Surveillance Panel. semiannual ASTM Subcommittee D02.B0 meeting.
These tests are conducted using coded reference oils supplied
by the TMC as outlined in 11.1 of this test method. It is the A1.7.3 The ASTM Committee on Technical Committee
laboratories’ responsibility to maintain the calibration in ac- Operations (COTCO) in 1984 gave authority for the issuance
cordance with this test method. It is also the laboratories’ of Information Letters, as follows: “COTCO recognizes that
responsibility to keep an on-site reference oil inventory at or D-2 has a unique and complex situation. The use of Informa-
above the minimum level specified by the TMC test represen- tion Letters is approved providing each letter contains a
tative. disclaimer to the effect that such has not obtained ASTM
consensus. These Information Letters should be moved to such
A1.6 New Laboratories: consensus as rapidly as possible.”
A1.6.1 Laboratories wishing to participate in the ASTM A1.8 TMC Memoranda—In addition to the Information
Monitoring System will be requested to conduct reference oil
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Letters discussed under A1.7, supplementary memoranda may


tests to ensure that the laboratory is using the proper testing be issued by the TMC. These memoranda are developed by the
techniques. Information concerning fees, laboratory TMC, often under the guidance of the surveillance panel, and
inspections, reagents, testing practices, appropriate committee to participating laboratories. The memoranda convey such
membership, and rater training can be obtained by contacting information as approval for test parts or materials, clarification
the TMC Administrator. of the test procedure, notes and suggestions of the collection
A1.6.2 The calibrating reference oils produce various filter- and analysis of special data that the TMC may request, or for
ability characteristics. When new reference oils are selected, any other pertinent matters having no direct affect on test
member laboratories will be requested to run their share of the performance, results, and precision and bias.

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D6794 − 19
SUMMARY OF CHANGES

Subcommittee D02.B0 has identified the location of selected changes to this standard since the last issue
(D6794 – 14) that may impact the use of this standard. (Approved July 1, 2019.)

(1) Revised Introduction, Sections 6, 9, and 11, and subsections


3.1.3, 3.1.5, and 4.1.

ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
of infringement of such rights, are entirely their own responsibility.

This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should
make your views known to the ASTM Committee on Standards, at the address shown below.

This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,
United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above
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