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Journal of Magnetism and Magnetic Materials 157/158 (1996) 440-441

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Three-axis cryogenic Hall sensor


J. Kvitkovi~ *, M. Majoro~
Institute of Electrical Engineering, Slovak Academy of Sciences, D{tbravsk5 cesta 9, 842 39 Bratislava, Slovak Republic

Abstract
Magnetic field measurements are very important for magnetic and superconducting material research. Hall sensors have
many advantages for these measurements. They can also be used for magnetic field profile measurements, which provide
information about material homogeneity. We have developed a three-axis Hall system which consists of three perpendicular
InSb Hall sensors for operation at room as well as cryogenic temperatures. The active area of each sensor is 50 × 50 bcm2. It
is located at the comer edge of the substrate and is suitable for detecting the spatial field profile within a cube of
225 × 225 × 225 /zm 3. The sensitivity of the sensor is of the order of 20 m V / T and the offset voltage is < 50 /zV for a
nominal control current of 10 mA. The problems of detecting the 3D field components using planar Hall sensors and the
oscillatory signal behaviour due to quantum effects are discussed.

Keywords: Hall sensor; Magnetic field; Superconductor

1. I n t r o d u c t i o n ceramics substrate to its lower left corner. By this proce-


dure and by reduction of the thickness of substrate edges it
The investigation of the trapped magnetic field near the is possible to place the active area of the elementary Hall
surface of superconducting or magnetic samples by a Hall sensor within a space of dimensions 225 × 225 × 225
probe is the most straightforward method for characteriz- /xm 3. This enables us to measure the tangential field
ing their granularity and homogeneity in a quick and components at a distance of 250 /xm from the sample
simple way. Local magnetic properties can be measured surface. The InSb plate was thinned by grinding and
without limitation from sample dimensions. Profile mea-
surements are more advantageous than magnetic investiga-
tions using pick-up coil based methods such as vibrating-
sample or SQUID magnetometers. In particular, the mea- 29
surement of both axial and tangential magnetic field com-
ponents offers complementary information about the num-
ber of grains, their dimensions and locations [1-3]. In the
present paper we report on the development and testing of 28.5 T=4.2 K
a sensor for the measurement of all three vector magnetic
field components.
%0.:.° , . • . .

2. D e s c r i p t i o n o f t h e H a l l s e n s o r z8

y
• ~ q [ b O • °11~0 • $ 0 ~ 0 • ° • • D4DID• • • • ~°OLD|

The elementary Hall sensor is fabricated from


monocrystalline InSb which is glued to the supporting
ceramics. We have designed the geometry of the active 27.5
sensor area in the shape as shown in the insert of Fig. 1.
The active area was reduced to dimensions of 50 /xm × 50
/zm and its position was shifted from the center of the
27 I , I F t

i 2 3 4
B [w]
* Corresponding author. Fax: +42-7-375-816; email: Fig. 1. Magnetic field dependence of the sensitivity and the
elekkvit @savba.sk. photolithographical mask of the Hall sensor.

0304-8853/96/$15.00 Copyright © 1996 Elsevier Science B.V. All rights reserved.


SSDI 0 3 0 4 - 8 8 5 3 ( 9 5 ) 0 1 2 2 1 - 4
J. Kvitkovi{, M. Majoro~/ Journal of Magnetism and Magnetic Materials 157/158 (1996) 440-441 441

polishing. The Hall sensor was patterned by photolitho- the quantum oscillations. To fulfil the condition /xB < 1
graphical methods. After etching, the Hall and current one must reduce the mobility /L ~ 1/n by appropriate
contacts were soldered by indium to copper wires. The doping n with scattering cross section c~,. The m o b i l i t y / z
Hall sensor for 3D field measurements consists of three only indirectly depends on concentration n (it scales with
independent Hall sensors whose active area centers are the dopant concentration by ionized impurity scattering at
placed in three mutually perpendicular planes. All three low temperatures). On the other hand, an increase of the
Hall sensors are supplied by a single constant current concentration n of carders reduces the Hall constant, i.e.
source of 10 m A with 10 -5 stability. the sensitivity of the Hall sensor is diminished [4,5]. W e
chose a doping level of n = 2 X 1017 cm 3 as a compromise
3. Properties and experimental results between avoidance of quantum oscillations and loss of
sensitivity. It is known that the Hall sensor is sensitive
The sensitivity of each elementary sensor is in the only to components of the magnetic field perpendicular to
range 2 0 - 3 5 m V / T and the offset voltage is < 5 0 / z V for its surface, ff the magnetic induction B is not perpendicu-
a nominal control current of 10 mA. The linearity error l o t t o the sample surface the output voltage is proportional
(nonlinear magnetic field dependence of sensitivity C) was to the projection of the magnetic induction B N o n t o the
measured in a superconducting magnet in the magnetic perpendicular axis of the sensor [6]:
field range 0 - 5 T at a temperature of 4.2 K (Fig. 1). It can
be seen that the maximum linearity error in this magnetic UH =RHZBN/t= (RralBcos 6 ) / t ,
field range is < 1%. At 4.2 K and in magnetic fields where R H is the Hall constant, I the control current, t the
higher than 2 T quantum oscillations of the Hall voltage thickness of the semiconductor, and 3 the angle between
appear which are caused by the de H a a s - S h u b n i k o v effect. B and the surface normal. W e placed the Hall sensor in a
Oscillations are observed if an electron performs more plane perpendicular to the external magnetic field and
than one cyclotron motion between subsequent collisions, rotated this plane by angle 6 from - 9 0 ° to + 90 °. The
i.e. wc~-> 1 or /zB > 1, where T is the mean collision measurement was performed in magnetic fields up to 0.4 T
time, ~ the carrier mobility, and B the magnetic induction at a temperature of 77 K (Fig. 2).
[4]. An additional criterion is ho~c > 2~rkT, where oJ° =
eB/m* is the cyclotron frequency, m* the effective mass
4. Summary
of charge carriers, e the electron charge, k the Boltzman
constant, T the temperature, and h Planck's constant. W e
have optimized the material parameters in order to reduce We have developed a three-axis cryogenic Hall sensor
for measurement of all three field components in the
temperature interval from 4.2 up to 350 K. The sensor has
T:77 K IHp:10 mA a rather small linearity error of < 1% in magnetic fields
15
up to 5 T and reduced quantum oscillations. In the case of
• • II
our selected InSb material the error caused by the planar
• ", • B=0.1 T
Hall effect is less than 0.8% at a magnetic field of 1 T.
12 • • B=0.2 T
Acknowledgement: The authors would like to acknowl-
* B=0.3 T
• • B=0.4 T
edge support for this work by the Slovak Grant Agency,
grant No. 2 / 1 0 8 6 .
> 9


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References
• • • A AA' " • • A • •
6 a• • A • •
+ • AA ~ [1] F. Frangi, L. Jan~.k, M. Majoro~ and S. Zannella, Physica C
224 (1994) 20.

0
-I00
i•
ioi

.~'°,
~
• A oo o°

......
-50
g o Oo
ooOOO 1

0
....... . .i:::i:.:,
50 tO0
[2] M. PolAk, M. Majoro~ and J. Kvitkovi~, Cryogenics 34 (ICEC
Suppl.) (1994) 805.
[3] M. MajoroL M. Pol~k, J. Kvitkovi~, D. Suchofi, L. Martini,
V. Ottoboni and S. Zannella, in: Proc. Magnet Technology '95
Conf., Tampere, Finland, in press.
[4] R. Boll and K.J. Overshott, in: Magnetic Sensors (VCH,
[o] Cambridge, 1989)p. 1.
[5] M. Polfik, Electrotechnical J. 25 (1974) 456.
Fig. 2. Angular dependence of the Hall voltage for various [6] H.H. Wieder, Hall Generators and Magnetoresistors (Pion,
magnetic fields. London, 1971).

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