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Perkin Elmer Elan DRC II ICP-MS Spectrometer
Perkin Elmer Elan DRC II ICP-MS Spectrometer
Perkin Elmer Elan DRC II ICP-MS Spectrometer
PerkinElmer SCIEX ICP-MS ■ For SEMI S2-0200 installations, a In addition, the instrument should
instruments are complete systems minimum of 300 Lux illumination be located in an area that is:
P R E P A R A T I O N
with the exception of the following is required at the floor level around
items which must be provided the ELAN® DRC II instrument. ■ Free of smoke and
by the customer: electrical power, corrosive fumes
exhaust vents, argon gas supplies In order to minimize contamination ■ Not prone to excessive vibration
with approved regulator, DRC gas problems, a dust-free environment
is necessary. For ultra-trace
■ Out of direct sunlight
supply, and coolant system. The
items shown in the following techniques, environmental ■ Away from heat radiators
checklist need to be considered contamination becomes a limiting
factor in the determination. PerkinElmer SCIEX ICP-MS
when preparing the laboratory for
To quantitate ubiquitous elements instruments have been designed
the instrument.
such as Fe, Ca, K, Na, etc. below for indoor use. The ELAN DRC II
■ Environmental conditions 1 ppb (µg/L), a class 1000 can be installed into a mobile
environment is necessary for laboratory if vibration is isolated.
■ Electrical requirements
sample preparation and analysis.
■ Space requirements This is not an indication of WARNING:
w w w. p e r k i n e l m e r. c o m
■ Exhaust ventilation the performance limitations of the Do not use the instrument in an area
■ Coolant requirements instrument, but a recommendation where explosion hazards may exist.
for an ultra-clean environment.
■ Argon gas requirements
■ DRC (dynamic reaction cell)
gas requirements
Environmental Conditions
The environment in which the
instrument is installed should meet
the following conditions.
System Layout
There should be sufficient space The drain vessel should be placed
The ICP-MS system consists of the near the spectrometer for the various to the right of the instrument. The
main instrument, the computer accessories (autosampler, FIAS, laser, drain vessel should NOT be stored in
controller assembly, and a printer. electrothermal vaporizer, etc.). It is an enclosed storage area. The drain
The dimensions of the instrument recommended that the accessories be system should be checked regularly
are given in Figure 1. Table I lists the placed on a movable cart or table to and replaced when necessary. Should
dimensions of the instrument and allow for easy servicing access. it become necessary to replace the
the computer. Table II lists the drain vessel, it should be made from
dimensions of the accessories. The system computer may be a material not likely to be attacked
placed on a bench or a separate by samples being analyzed. Glass or
The ELAN can be positioned in either computer table. other brittle materials must not be used.
a linear or an L-shaped configuration.
In the L-shaped configuration, the Drain Vessels Liquid waste should always be
computer and printer are positioned segregated and clearly labeled. Never
on one leg of the L. The instrument A 15-liter drain vessel is supplied mix organic and inorganic liquids in
and an accessory table make up the with the ELAN DRC II ICP-MS. The the same drain vessel. Organic and
other leg. A recommended workstation vessel is made of HDPE (high density inorganic drain vessels should never
layout is shown in Figure 2. polyethylene) and is used to collect be stored in the same area.
the effluent from the ICP sample
introduction system.
Safe Handling of Gas Facilities Requirements and options. If the power line is
Cylinders unstable, fluctuates or is subject to
Table III provides information on surges, additional control of the
Notice: The permanent installation the gas and liquid services required incoming power may be required. A
of gas supplies is the responsibility for the ELAN DRC II. Tables IV and V means of electrically grounding the
of the user and should conform show the electrical supply requirements instrument must be available.
to local safety and building codes. and approximate power consumption
of the ELAN DRC II and its 60-Hertz-Operation Connections
■ Fasten all gas cylinders securely major accessories. The instrument is shipped with
to an immovable bulkhead or a two 400 cm line cord cables. The
permanent wall. installation kit includes two Hubbell
Electrical Requirements No. 2621 plugs and two Hubbell No.
■ When gas cylinders are stored in
Power to the ELAN DRC II is to be 2620 receptacles for use with two 60
confined areas, such as a room,
delivered from two 30 A single-phase Hz single phase outlets. The instru-
ventilation should be adequate to
200-240 V dedicated electrical branch ment is wired for power at the time
prevent toxic or explosive accumu-
circuits according to the power of installation.
lations. Move or store gas cylinders
only in a vertical position with the specifications in Table IV. Table V
50-Hertz-Operation Connections
valve cap in place. provides the electrical supply
The instrument is shipped with two
requirements and approximate power
■ Locate gas cylinders away from 400 cm line cord cables. It is up to
consumption of the major accessories
heat or ignition sources, including the service person installing the
heat lamps. Cylinders have a pressure-
relief device that will release the Table III. Services Required for the ELAN DRC II
contents of the cylinder if the
Gases ■ Argon, 414 ± 7 kPa (60 ± 1 psi) at 20 L/minute flow
temperature exceeds 52 °C (125 °F).
■ Ammonia (99.999%), 48 ± 14 kPa (7 ± 2 psi) operating, 103.4 kPa
■ When storing cylinders external (15 psi) maximum
to a building, the cylinders should Cooling Coolant circulation of at least 3.8 L/min (1.0 gpm) at an operating
be stored so that they are protected pressure of 344 ± 14 kPa (50 ± 2 psi).
against temperature extremes Table IV. ELAN DRC II Power Specifications
(including the direct rays of the
sun) and should be stored above Power Consumption
ground on a suitable floor. Maximum Volt Amperes (total, both circuits) 6000 VA
■ Mark gas cylinders clearly to Maximum Continuous Current (per circuit) 20 A
identify the contents and status Voltage Amplitude Specification
(full, empty, etc.).
Operating Voltage 200 - 240 V
■ Do not attempt to refill gas Maximum Allowable Percent Sag 5%
cylinders yourself. Maximum Allowable Percent Swell 5%
Phase (single or three) Single phase or three phase
■ Use only approved regulators and
Frequency Specification
hose connectors. Left-hand thread
fittings are used for fuel gas tank Operating Frequency 50 or 60 Hz
connections whereas right-hand Allowable Frequency Variance ± 1 Hz
fittings are used for oxidant and Waveform Specification
support gas connections.
Maximum Supply Voltage Total Distortion 5%
■ Arrange gas hoses where they will Maximum Supply Voltage Distortion by Single Harmonic 3%
not be damaged or stepped on and
Table V. Electrical Requirements of ELAN Accessories
where things will not be dropped
on them. Equipment Voltage (AC) Power
■ Perform periodic gas leak tests Computer Depends on Model Depends on Model
by applying a soap solution to all Printer: HP LaserJet 4200 100-127 V/220-240 V, 50/60 Hz 580 W
joints and seals. Cooling System:
■ It is strongly recommended that Heat Exchanger 208-240 V, 50/60 Hz, 2.75 A 660 W
DRC gases be installed in a gas (PolyScience 3370) 120V, 60HZ, 5.5A
cabinet with adequate ventilation.
© 2003 PerkinElmer, Inc. All rights reserved. PerkinElmer is a registered trademark and FIAS, DRC and Dynamic Reaction Cell are
trademarks of PerkinElmer, Inc. SCIEX and ELAN are registered trademarks of MDS SCIEX, a division of MDS, Inc. All trademarks
depicted are the property of their respective holders and owners. PerkinElmer reserves the right to change this document at any time
and disclaims liability for editorial, pictorial, or typographical errors.
006040D 040300 Printed in USA