Professional Documents
Culture Documents
2000 GC Manual
2000 GC Manual
2000 GC Manual
ABB
NOTICE
ABB Inc.
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
A1 February 2000
A2 August 2000
B1 January 2001
B2 March 2001
B3 August 2001
B4 November 2001
B5 January 2002
C1 August 2002
All C1
The revision status is noted at the bottom of each page of this manual.
2000-OSM, C1 i
For further information or assistance contact:
ABB Inc.
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
ii 2000-OSM, C1
TABLE OF CONTENTS
Title Page
SECTION 1. INTRODUCTION
2000-OSM, C1 iii
TABLE OF CONTENTS (continued)
Title Page
SECTION 3. OPERATION
iv 2000-OSM, C1
TABLE OF CONTENTS (continued)
Title Page
2000-OSM, C1 v
TABLE OF CONTENTS (continued)
Title Page
SECTION 5. MAINTENANCE
vi 2000-OSM, C1
TABLE OF CONTENTS (continued)
Title Page
SECTION 6. TROUBLESHOOTING
2000-OSM, C1 vii
TABLE OF CONTENTS (continued)
Title Page
viii 2000-OSM, C1
TABLE OF CONTENTS (continued)
Title Page
SECTION 8. REPAIR
2000-OSM, C1 ix
TABLE OF CONTENTS (continued)
Title Page
x 2000-OSM, C1
TABLE OF CONTENTS (continued)
Title Page
2000-OSM, C1 xi
TABLE OF CONTENTS (continued)
Title Page
xii 2000-OSM, C1
TABLE OF CONTENTS (continued)
Title Page
2000-OSM, C1 xiii
TABLE OF CONTENTS (continued)
Title Page
xiv 2000-OSM, C1
TABLE OF CONTENTS (continued)
Title Page
2000-OSM, C1 xv
TABLE OF CONTENTS (continued)
Title Page
xvi 2000-OSM, C1
ILLUSTRATIONS
Figure Title Page
2000-OSM, C1 xvii
ILLUSTRATIONS (continued)
xviii 2000-OSM, C1
ILLUSTRATIONS (continued)
2000-OSM, C1 xix
ILLUSTRATIONS (continued)
xx 2000-OSM, C1
ILLUSTRATIONS (continued)
10-1 Chroma I/O Board, Showing UG1 and UH1 .......................................................................... 10-30
10-2 Background Screen .............................................................................................................. 10-46
10-3 Report, Basic I/O and Options Screen .................................................................................. 10-47
10-4 Real Time BASIC Status Screen ........................................................................................... 10-47
10-5 BASIC COMMON! Area Edit Screen ..................................................................................... 10-48
2000-OSM, C1 xxi
For further information or assistance contact:
ABB Inc.
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
xxii 2000-OSM, C1
GLOSSARY
Auto Zero procedure bringing the detector signal as close to electrical zero as
possible; brings the signal into the most sensitive area of the A/D
baseline reference point from which peak height or peak area is measured on a
chromatogram; detector signal level at which no components are detected
calibration run analysis that involves injecting a standard sample consisting of specific
components whose concentrations and elution sequences are known
CE Mark certification process and marking which denote that analyzer complies
with applicable new approach directives within the European Union
Chroma I/O Chromatographic Input/Output PCB; provides the interface between the
analog domain of the gas chromatographic analyzer and the digital
domain of the controller
components peaks, parameters or ratios that are being measured or calculated from a
chromatographic analysis
CPU Central Processing Unit; controls the analyzer and collects and
manipulates the data
cursor keys front panel control keys marked with directional arrows
default values assigned parameters the controller will assume unless the operator
redefines the values
2000-OSM, C1 G-1
GLOSSARY (continued)
Digital I/O Digital Input/Output PCB; enables the use of additional stream valves and/
or alarm sensors
DIP switch PCB switch that is used to set values through hardware instead of
software
drift the variances from the baseline or the norm; generally associated with
uncontrolled or unwanted changes in pressure or temperature
elution time the amount of time from the start of analysis that it takes for a peak to be
fully detected
EPROM Erasable, Programmable, Read Only Memory; program software that can
be erased and reprogrammed a limited number of times
E2PROM Electrically Erasable Programmable Read Only Memory; used for the safe
storage of tables (sometimes written E2PROM or EEPROM)
field highlighted area on display screen where data entry and modification are
allowed; data entry is ended (terminated) by filling the field with characters
or by pressing ENTER or any soft key or cursor key
Gate On/Off the time-coded function command which turns on and off the collection of
data from the detector
GC Gas Chromatagraph
Help key front panel control key used to access information pertaining to the current
screen display content
highway address numbers from one to 32 that uniquely identify remote GCC’s
G-2 2000-OSM, C1
GLOSSARY (continued)
host link serial communications link which allows the transmitting of analysis results
to the host computer
I/O Input/Output
LO COMM Local Communication Module PCB; optional PCB in the GCC that makes
the analyzer communications network possible (sometimes written
LOCOM)
LSV Liquid Sample Valve; used to inject small amounts of liquid into the
sample column
method table operator-entered data specifying the name, retention time, key
designation, response factor, low and high limits, and calibration
concentrations of the various elements of an analysis; also specifies
when, how, and under what conditions the method of data collection is to
proceed
microprocessor the semiconductor circuit containing the central processing unit functions
noise any unwanted signal superimposed upon a useful signal which tends to
obscure the desired information
“Panic” key nickname for F1 key directly under the screen (soft key); pressing this key
will return the display to the Background screen without changing any
current values in memory; may need press it several times consecutively,
depending on where the current screen relative to the Background screen
peak area method of measurement in which total peak area beneath the peak
envelope is used to calculate the concentration
peak discrimination the non-linear unequal dilution of hydrocarbons in the column train
2000-OSM, C1 G-3
GLOSSARY (continued)
Post Analysis the portion of the controller program that calculates the value for the
routine components from the collected data, after completion of the analysis
redundant the means by which a remote GCC can be connected to one or two
highways central devices by two separate, but equivalent, data highways
retention time the time, from the start of analysis, that a peak maximum elutes from the
column
selection field horizontal screen display; Right and Left cursor keys move through
options printed on screen; make selection by leaving field with Up or
Down cursor key
Soft Keys four front panel control keys directly under the screen
stream purging the procedure allowing the next stream sample to be analyzed to flow
continuously through the sample loop of the injection valve in preparation
for the next sample injection and analysis cycle
G-4 2000-OSM, C1
GLOSSARY (continued)
stream step TCF command that permits the next stream sample to purge the sample
loop during the remainder of the present cycle
text field field that accepts data entered with all non-terminating keys
watchdog timer hardware circuit alarm that indicates when the software fails to cycle
through its entire task structure within a set period of time
2000-OSM, C1 G-5
CAUTION
Beginning in January 1996, all analyzers bearing the CE Mark imprint on their nameplates have
EMC shielding that meets the requirements for CE Mark. When working with one of these analyz-
ers, you must handle it carefully to avoid damaging the shielding. If any shielding becomes
damaged or is removed from the analyzer, new shielding must be installed to maintain the CE
mark certification.
ABB Lewisburg has designed “Total Envelope Protection” into its analyzers. The basic enclosure
itself (which is fabricated from sheet steel with all seams welded), when properly “grounded” or
“earthed”, becomes the first barrier of protection from emissions that could radiate from the unit.
In addition, the enclosure also provides a high level of immunity from electromagnetic interference
(EMI) which could affect the performance of the analyzer.
In order for the analyzers produced by ABB Lewisburg to maintain their tested integrity, the instal-
lation methods employed are of equal importance. The grounded enclosure produces a Faraday
Shield around the electronic components, detection systems, and other sensitive components
which could generate EMI or be affected by EMI. An extension of this Faraday shield must be
carried throughout the installation scheme.
If the analyzer is used in a manner not specified by ABB Inc., the protection provided by the
analyzer may be impaired.
NOTE
Special conditions of Certificate of Conformity LCIE 97.D6074 X apply to the electrical equipment
for its safe use. Special conditions for electrical and purge and pressurization are included on the
nameplate of the analyzer. Special conditions for Ex components, which are described in the
individual subsections of Section 8 (“REPAIR”) of this manual, apply to the following certified
components:
Ex Component Certificate
G-6 2000-OSM, C1
SECTION 1. INTRODUCTION
EQUIPMENT DESCRIPTION
The Process Gas Chromatograph PGC2000 separates and measures the individual
components of gas or liquid samples. It automatically samples and analyzes process
streams, using the analyzer's Gas Chromatographic Controller (GCC) to control analytical
functions. The analyzer (see Figure 1-1) may be mounted on a wall, a rack, or a floor stand.
It includes an insulated, air-heated Oven Compartment, a Gas Chromatograph Controller, a
purge air panel, and a pressure control panel.
Gas
Chromatographic
Controller
(GCC)
Pressure
Purge Air Control
Panel Panel
Oven
Compartment
Nameplate
(on side
or front)
The Oven Compartment houses an isothermal oven which contains the analytical columns,
the detectors, and the sample valves.
The Gas Chromatograph Controller (GCC) contains the card cage with PCBs, the
Temperature Controller, and one or more of the following detector amplifiers: flame ionization
(FID), thermal conductivity (TCD), and flame photometric (FPD). The front panel has a liquid
crystal display (LCD), keyboard, and controller board. The FPD assembly itself is located in
a special cabinet mounted on the left side of the analyzer.
2000-OSM, C1 1-1
Below the GCC are the Purge Air Panel and the Pressure Control Panel. The Purge Air
Panel contains the heater air and purge air gauges and regulators. The Pressure Control
Panel contains the Electronic Pressure Controller (EPC) or a group of mechanical regulators
and gauges. When the EPC is installed the Pressure Control Panel has a blank front panel.
Each analyzer has a temperature code (T-Rating) listed on the nameplate. This T-Rating
indicates the temperature classification of the area in which the analyzer has been designed
to operate. T-Ratings and area classifications for analyzer locations are determined and
supplied by the customer.
A package titled “Important Papers” comes with the analyzer. Included in this package are
data sheets and installation drawings needed to support installation and setup of the
analyzer. This manual refers to these data sheets and drawings as the “Data Package.”
When the analyzer has a flame photometric detector (FPD), a panel attached to the left side
of the analyzer contains the detector, the detector amplifier, and the high-voltage transformer
that provides the spark to ignite the FPD (see Figure 1-2).
Transformer
0 0
FPD Electrometer
Assembly
Detector
1-2 2000-OSM, C1
AIR PURGE SYSTEMS
If the analyzer will be in a Class I hazardous location, an air purging system must be installed
to reduce the risk of explosion. Class I locations are those in which flammable gases or
vapors are or may be present in the air in quantities sufficient to produce explosive or
ignitable mixtures.
SYSTEM VARIATIONS
This manual supports the PGC2000 basic analyzer. An appendix to the main manual
presents additional instructions for special applications such as PGC2002 (simulated
distillation), PGC2003 (PNA), PGC2005 (temperature programmed GC), PGC2007 (fuel
sulfur), PGC2008 (olefins), and PGC2030 (Sparging Sample Conditioning System).
SPECIFICATIONS
Physical
Environmental (Enclosure): Protected from weather: IP 52, (NEMA Type 12) Equivalent
Mounting:
Wall: 32 mm (1.3 in.) from wall with brackets
Floor: Optional wheeled dolly
Sample Entries:
Gas: Bottom
Liquid: Right Side
2000-OSM, C1 1-3
CENELEC: Eex pde [ib] ib IIB+H2 T4 to T2 (LCIE 97.D6074 X)
Power
Instrument Air
Analytical Detectors
1-4 2000-OSM, C1
Columns: 1/16, 1/8, 3/16 inch, Packed Stainless or Fused Silica
Capillary
Setpoint Resolution: 1° C
Temperature Stability:
Steady Ambient: ±0.1° C
Ambient Range: ±1.0° C
Inlet Pressure:
Minimum: Setpoint + 130 kPa (20 psig)
Maximum: 1380 kPa (200 psig)
NOTE: Supply pressure less than or equal to 1380 kPa (200 psig) and 345
kPa (50 psig) higher than max output required; e.g., supply to a 700 kPa
(100 psig) regulator should not exceed 1034 kPa (150 psig).
Regulation: 0.1 kPa (0.01 psi) outlet / 10.0 kPa (1.0 psi) inlet
Accuracy: N/A
Repeatability: N/A
Quality: GC Grade
2000-OSM, C1 1-5
Gas Control (Digital)
Number of Zones: 1 to 5
Inlet Pressure:
Minimum: Setpoint + 69 kPa (10 psig)
Maximum: 1034 kPa (150 psig)
Accuracy:
0-50 psig: 1.7%
50-100 psig: 2.7%
Quality: GC Grade
1-6 2000-OSM, C1
SECTION 2. INSTALLATION AND START-UP
Locate the analyzer as close as practical to the stream to be sampled. Analyzer location and
area classification are the customer's responsibility.
When determining where to install the analyzer, include the following location criteria:
The following tools and equipment are required to install and check out the system.
Plumbing Installation
All plumbing connections enter at the right side of the cabinet. Be careful to avoid damaging
fittings and to ensure tight connections. Refer to the Data Package for specific plumbing
information.
For brass and stainless steel pipe fittings, wrap the threads with Teflon tape or a suitable
thread sealant. Make all connections and then tighten them appropriately. Leak check each
connection as described in the "Leak Check" paragraph.
2000-OSM, C1 2-1
Gas Requirements
• Burner Air: ISA Hydrocarbon Free Grade with hydrocarbon content less than 1 ppm and
dew point less than -40° C.
• Carrier Gases: varies with the application; the lower the levels of components being
measured, the higher the necessary carrier gas purity.
• TCD: for percent level measurements, gases of 99.99% purity; for ppm measurement
ranges, 99.995% purity.
• FID: for measurements down to 5 ppm, gases of 99.995% purity; lower ranges require
higher levels of purity (refer to the Data Package for specifics).
• FPD: varies with the application; refer to the Data Package for specifics.
Calibration Sample
A primary factor in determining the accuracy of the analyzer's calibration is the quality and
precision of the calibration sample. Regardless of the sample composition or number of
complete analysis components, generally only measured components are in the calibration
sample.
The analyzer contains circuits that detect the loss of purge air to the analyzer and generate
alarm signals to the operator. The customer has the responsibility to connect the purge
alarm to a visual or audible annunciator located in a constantly monitored area, as required
by NFPA 496 (1993).
You must take extreme care to avoid having the sample lines exert force on the sample
connections of the Liquid Sample Valve. For example, if stiff 1/4-inch tubing or heat-traced
lines are bent into position and attached to the valve, the force will cause premature failure of
the valve stem and seals, resulting in leakage. A loop of 1/8-inch tubing or a flex hose is
recommended between the valve and the sample line (this may be insulated if necessary).
Figure 2-1 illustrates the incorrect and correct connection methods.
It is also important to use two wrenches when tightening the sample line connections to the
sample chamber. One wrench must be used to back up the force applied to tighten the fitting
(direct wrench force will bend the stem).
2-2 2000-OSM, C1
Putting a loop in the tubing or using flexible hose reduces
any sideways force at the connection.
INCORRECT CORRECT
EQUIPMENT MOUNTING
WARNING
Unpack the analyzer near the installation site and move it with a transportation machine.
Handle the analyzer carefully so that it does not fall. For floor-mounted units, secure the
Analyzer with anchor bolts. Secure wall-mounted units appropriately. Refer to the Outline
and Mounting Dimensions drawing in the Data Package for specific mounting information.
CONNECTIONS
Tubing
Refer to the applicable drawings in your Data Package for specific tubing and connection
information while you perform the following steps.
1. Do not remove the tube caps, provided at the analyzer tubing ports to prevent
deterioration of the columns, until immediately before making each connection.
3. To ensure using proper size tubing and pipe, refer to the Outline and Mounting
Dimensions Diagram contained in the Data Package.
2000-OSM, C1 2-3
4. Use lines and fittings free of interior contamination from grease, oil or other substances.
Before connecting these lines, completely air-purge their interiors.
5. Carefully connect the lines so that there are no leaks from the connections. Leak check
each connection as described in the "Leak Check" paragraph.
Analyzer Air
Carrier Gas
Sample
The methods used for transporting the sample from the process stream to the analyzer or
from the calibration sample to the analyzer are critical to the operation of the analyzer. Refer
to the system drawings in the Data Package for specific sample system connections.
Hydrogen Gas
WARNING
The analyzer uses hydrogen gas as a burner fuel with flame cell detectors (FID and FPD)
and sometimes uses it as a carrier gas. Verify that the hydrogen gas meets the criteria
stated in the "Gas Requirements" paragraph. Refer to the Data Package for specific
connection information.
Vent
Typical analyzer vents are: Cell Vents, Backflush Vent, Sample Vent, and Housing Vent. All
vents must be at atmospheric pressure unless otherwise specified in the Data Package. The
vent lines should slope down from the analyzer so that condensation will not collect in the
analyzer or cause backpressure in the external tubing. Refer to the Data Package for
specific connection information.
Electrical
The analyzer must be installed according to all applicable codes. If it will be in a hazardous
area, the wiring method must conform to the applicable explosion proof requirements.
Install the signal wiring and power wiring in separate conduit pipes or cable trays to reduce
noise and crosstalk. If a grounding (earthing) connection is required, connect the
appropriate size grounding wire to the Earthing Connection on the right side of the oven
compartment.
The following wiring is required, though the amount of wiring varies with the installation.
• Power wiring for heater, power circuits, electronics, and grounding circuit (circuit breaker
protection must be provided by the customer)
2-4 2000-OSM, C1
• Signal wiring between the GCC and the VistaNET
• Contact output Error alarms, timing signal, status signal, and annunciator
Refer to the applicable drawings in your Data Package for specific interconnection wiring
information.
The following instructions assume that all equipment has been properly installed and
checked, that the analyzer has been application engineered, and that temperature
controllers, alarm switches and other adjustments have been properly set.
CAUTION
Precautions
1. Refer to the Data Package for correct values and settings before adjusting pressure,
flow, temperature, etc.
2. Review all data on alarms and corrective action before operating the analyzer.
4. Observe and take note of all caution tags attached to the analyzer; make all adjustments
using the specific data sheets for this analyzer.
5. Ensure all air, gas and sample supply lines coming into the analyzer are properly
connected and turned OFF at the external flow shutoff valves (these shutoff valves are
normally associated with analyzer installation and are not a part of the analyzer itself).
2000-OSM, C1 2-5
6. Ensure the power supply line is properly connected and turned OFF at the circuit
breaker outside the analyzer (this circuit breaker is associated with analyzer installation
and is not part of the analyzer itself).
Verify that the sample system has been leak and flow checked and is known to be operating
correctly.
GCC Pre-Checks
CAUTION
Before opening any analyzer doors, ensure the area is safe and hazard-
free and will remain so the entire time the analyzer is open.
1. Verify that the circuit breaker which supplies power to the analyzer is turned OFF.
2. Release the GCC front panel by turning the panel latches fully counterclockwise with a
5/16-inch (or 8 mm) hex key wrench.
5. Close the GCC front panel and hold the front panel shut while you tighten the panel
latches.
Analyzer Pre-Checks
The purge air and heater air pressures are set during factory checkout and calibration tests.
These settings should not be changed during installation setup and operation. They can be
verified at the gauges on the Purge Air Panel.
Analytical pressures are also set during factory checkout and calibration tests but these
settings may have to be adjusted for the installation environment. Once you have verified
proper operation of the analyzer, adjust the analytical pressures as necessary.
1. Visually inspect the analyzer for inoperative or damaged gauges, loose or damaged
connections, and overall condition.
2. If you have not completed the GCC pre-checks (previous paragraph), perform those
steps now.
4. Refer to the Data Package to ensure that air supply at the specified pressure is provided
to the INSTRUMENT AIR inlet.
5. Refer to Figure 2-2 (when EPC is installed, the Pressure Control Panel will be blank).
The purge air and heater air pressures should be as specified on the label below the
corresponding regulator.
2-6 2000-OSM, C1
Purge Air Panel Pressure Control Panel
7. Refer to the Data Package to ensure that the specified carrier gas is provided at the
specified pressure to each CARRIER inlet.
9. For EPC-equipped analyzers, refer to the Manual Pressure Control Mode screen. Verify
that carrier and gas pressures are the same as those specified in the Data Package. If
necessary, adjust each set point (SP) until it is the same as the Data Package value.
10. If the analyzer has mechanical regulators, verify from the Pressure Control Panel gauge
that carrier and pressures are the same as that specified in the Data Package. If
necessary, adjust each regulator until its gauge value is the same as the Data Package
value.
11. Verify any other gases in the same manner as Carrier #1.
12. If a leak occurs during start-up, perform the leak check described in "Leak Check"
paragraph.
13. Allow sufficient time for oven warm-up. The oven should stabilize at the temperature
indicated in the Data Package. If adjustments are required, adjust the Digital
Temperature Controller as described in "DIGITAL TEMPERATURE CONTROLLER" in
Section 4.
Leak Check
If a leak occurs during initial turn-on, perform a simple leak check on the analyzer section as
follows:
1. Plug all carrier gas vents and pressurize to 30 psig. Shut off the carrier supply.
2. Note pressure drop-off on the carrier supply and column pressure gauges. A visual
decline is excessive.
3. Starting at the inlet to the detector and working back to the carrier gas supply, plug the
exit of each valve or column to locate the leak.
4. Use “Snoop®“ or other suitable leak detection solution to check for leaks.
2000-OSM, C1 2-7
MATCHING COLUMN FLOWS
When you are matching column flows, refer to the Data Package for flow rates and valve
configurations. Although methods of matching column flows vary with valve configurations,
the following procedures apply to most configurations. Verify flows using a flow meter
connected to the point being checked (e.g., cell vent).
2. On the Manual Control Mode screen (see Figure 2-3), the first line (“Valves:”) indicates
which valves are ON. The cursor will be on the second line (“Enter Valve: 0”), which
enables you to turn valves on and off.
3. To turn Valve One ON, verify that the number “1” does not appear on the first line, then
press the “1” key on the keyboard. The number “1” appears momentarily on the second
line and then appears on the first line.
F1 F2 F3 F4
4. To turn Valve One OFF, verify that the number “1” appears on the first line (“Valves”).
Move the cursor to the second line and press the number “1” key. The number “1”
disappears from the first line of the screen.
5. Turn Valve Two and other valves on and off manually in the same manner.
2-8 2000-OSM, C1
Checking Total Column Flow
To check column flow using a 10-port sample valve and an 8-port selector valve, perform the
following steps (other valve configurations use similar procedures):
2. See Figure 2-4. To check total column flow, set Valves One and Two to ON.
3. Connect the flow-measuring device to the CELL VENT of the detector cell and measure
the flow rate. The total column flow should be as specified in the Data Package. s If
necessary, adjust the COLUMN PRESSURE regulator to obtain the specified flow rate.
CARRIER
IN
COLUMN
PRESSURE
ADJ
PI
SAMPLE
VENT
SELECTOR
1 6 FLOW ADJ 1 6
2 7 2 7 SELECTOR
SAMPLE
IN VENT
3 8 3 8
COLUMN
4 9 2 4 9
5 10 5 10
ANALYTICAL
FLOW ADJ COLUMN
3
COLUMN 1
BACKFLUSH
SAMPLE LOOP
VENT
CELL
DETECTOR
VENT
2000-OSM, C1 2-9
Checking Analytical Flow Adjust
1. Set Valve One to OFF; Valve Two remains ON (see Figure 2-5).
CARRIER
IN
COLUMN
PRESSURE
ADJ
PI
SAMPLE
VENT
SELECTOR
1 6 FLOW ADJ 1 6
2 7 2 7 SELECTOR
SAMPLE
IN VENT
3 8 3 8
COLUMN
4 9 2 4 9
5 10 5 10
ANALYTICAL
FLOW ADJ COLUMN
3
BACKFLUSH
VENT
COLUMN 1
SAMPLE LOOP
CELL
DETECTOR
VENT
2. To compensate for the pressure drop through Column 1, adjust the ANALYTICAL FLOW
ADJUST needle valve (accessed from the right side of the Oven Compartment) until the
flow rate at the cell vent of the detector cell is the same as the total column flow.
3. If the analyzer has several valves, first set the lowest-numbered valve ON and check
the flow rate. Then set the other valves on one at a time, checking the flow rate and
adjusting the corresponding restrictor (if necessary) after each valve is turned on.
1. Connect the flow-measuring device to the Backflush Vent and verify that Valves One
and Two are OFF (see Figure 2-6).
2-10 2000-OSM, C1
2. Adjust the Backflush Vent restrictor to the flow rate stated in the Data Package.
CARRIER
IN
COLUMN
PRESSURE
ADJ
PI
SAMPLE
VENT
SELECTOR
1 6 1 6
FLOW ADJ
2 7 2 7 SELECTOR
SAMPLE
IN 3 8 VENT
3 8
COLUMN
4 9 4 9
2
5 10 5 10
ANALYTICAL
FLOW ADJ COLUMN
3
BACKFLUSH
VENT
COLUMN 1
SAMPLE LOOP
CELL
DETECTOR
VENT
2000-OSM, C1 2-11
Checking Selector Flow Adjust
1. See Figure 2-7. Set Valve One to ON and Valve Two to OFF.
CARRIER
IN
COLUMN
PRESSURE
ADJ
PI
SAMPLE
VENT
SELECTOR
1 6 FLOW ADJ 1 6
2 7 2 7 SELECTOR
SAMPLE
VENT
3 8 IN 3 8
COLUMN
4 9 2 4 9
5 10
5 10
ANALYTICAL
FLOW ADJ COLUMN
3
COLUMN 1
BACKFLUSH
SAMPLE LOOP
VENT
CELL
DETECTOR
VENT
2. To compensate for the pressure drop through Columns 1 and 2, adjust the SELECTOR
FLOW ADJUST needle valve until the flow rate at the cell vent is the same as the total
column flow.
1. See Figure 2-7. Connect the flow-measuring device to the Selector Vent and verify that
Valve One is ON and Valve Two is OFF.
2. To compensate for the pressure drop through Column 3, adjust the Selector Vent
restrictor until the flow rate at the Selector Vent is the same as the total column flow.
2-12 2000-OSM, C1
EQUIPMENT STARTUP
CAUTION
Before opening any analyzer doors, ensure the area is safe and hazard-
free and will remain so the entire time the analyzer is open.
The following instructions assume that all equipment has been properly installed and
checked, that the analyzer has been application engineered, and that temperature
controllers, alarm switches and other adjustments have been properly set.
CAUTION
Initial Power On
For Y and Z purged analyzers, note the purge label on the analyzer and allow sufficient air
purge time before switching on the power source at the circuit breaker. Once the purge
requirements are met, turn power to the equipment ON at the supply breaker. The following
components receive power: oven heater system, optional heated devices (Liquid Sample
Valve vaporizer, Air Clean-up/Methanizer), detector power supply, and GC Controller (display
illuminates).
CAUTION
Verify that the X Purge is not in override (see "X Purge Override
Option" in Section 4).
For X Purged and CENELEC certified analyzers, you can turn the power supply ON at the
circuit breaker immediately after the air supply is turned ON. X Purge automatically controls
the purge time and applies power to the analyzer only after the purge cycle is completed.
Refer to the Data Package for specific purge cycle time. (There is an X Purge Override
operation that may be used during startup, if necessary. See "AIR PURGING" in Section 4
for detailed information.)
1. Turn ON carrier gas to purge the columns. Do this before the oven is heated to prevent
the columns from being damaged.
2. For FID and FPD only: if the Flameout LED on the GCC front panel is not illuminated,
turn off Burner Fuel at the Pressure Control Panel. The isothermal oven must be at
operating temperature before igniting the flame, to prevent damage to the detector.
3. Allow adequate time for the oven to heat to proper operating temperature before
continuing. Condensation damage may occur to the Methanizer/Air Clean-up unit if the
oven is not at operating temperature before Burner Air flow starts.
4. Check the oven temperature on the Temperature Control screen (see "Temperature
Control Table" in Section 4).
2000-OSM, C1 2-13
NOTE
The oven will begin to cycle and control temperature in about one hour.
However, total equilibrium may take 8 to 12 hours depending on the
analyzer configuration and ambient conditions. Baselines will continue
to drift until the system stabilizes.
5. Turn ON Burner Fuel and Burner Air at the flow shut off valves and observe the Actual
values shown on the Manual Pressure Control Mode screen. Ensure pressures are set
according to the Data Package and adjust set points (SP) as necessary. If the analyzer
has mechanical regulators, observe the gauges on the Pressure Control Panel and
adjust the regulators as necessary.
CAUTION
Ensure the area is safe and hazard free before opening the oven
compartment to leak check the hydrogen flow path inside the oven.
6. After the temperature stabilizes, recheck all purge air pressures at the gauges on the
Purge Air Panel. Adjust corresponding regulators, if needed, according to the Data
Package.
7. Check column pressure by examining the Actual values for Carrier #1 and Carrier #2
shown on the Manual Pressure Control Mode screen. Verify these values with the Data
Package specification and adjust the Carrier #1 and Carrier #2 set points as necessary.
8. If the analyzer has mechanical regulators, check column pressure by examining the
Carrier #1 and Carrier #2 gauges on the Pressure Control Panel and verify these values
with Data Package specifications. Adjust the Carrier #1 and Carrier #2 regulators as
necessary.
9. Turn ON Calibration Gas supply (may be called Standard Sample). The gauges and
regulators used to monitor the calibration gas are normally part of the Sample
Conditioning System. If necessary, adjust the appropriate controls on the Sample
Conditioning System to provide the analyzer with correct sample pressure and flow,
according to the Data Package.
10. On the Background screen press the F2 (Manual Control) soft key.
11. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
a. On the Chroma Board screen press the F3 (Manually Zero Baseline) soft key.
b. Add the values of the Hardware Zero reading and Software Zero reading.
c. Open the GCC front panel and locate the TCD Amplifier Board on the left side
wall of the GCC.
2-14 2000-OSM, C1
d. Adjust the TCD Zero Adjust on the TCD Amplifier Board until the Detector
Reading on the Chroma Board screen is equal to the sum of the Hardware and
Software Zero readings.
e. On the Chroma Board screen, press the F3 (Manually Zero Baseline) soft key.
The Detector Reading should now be 2.00 ± 0.05 mV and the Hardware Zero
should be 10% or less.
CAUTION
a. On the Chroma Board screen, observe the “Flame” line. If "Lit" is underlined the
flame should be on and the Flameout LED on the front panel should be off.
b. If the Flame is not lit and the Ignitor is Off, press the F4 (Manual Ignitor On) soft
key to light the cell flame. The ignitor coil remains powered for the specified
Timeout period. Once the flame lights the Flame Out LED will go off. The cell
flame burns as long as there is sufficient burner air and hydrogen fuel in the cell.
a. On the Chroma Board screen, observe the “Flame” line. If "Lit" is underlined the
flame should be on and the Flameout LED on the front panel should be off.
NOTE
With an FPD, if "Lit" in underlined on the Chroma Board screen and the
Flameout LED on the front panel is ON, verify the Flameout Alarm is set
to normally open (NO). See "SOFTWARE VERIFICATION" in Section 5
for instructions on checking the status of the Flameout Alarm.
2000-OSM, C1 2-15
b. On the Chroma Board screen, verify that the FPD Temp Zone is the same as
that specified in the Data Package (see Figure 2-8).
Manually Manual
Exit Graphics Zero Ignitor
Baseline On
F1 F2 F3 F4
c. On the Chroma Board screen, observe the "Ignitor" line. "Manual" should be
underlined.
e. On the Manual Control Mode Screen, press the F4 (Press. & Temp. Control) soft
key.
f. On the Pres and Temp Control screen, cursor to TEMP CONTROL and press the
F2 (Manual Temp Control) soft key.
g. On the Manual Temperature Control Mode screen (see Figure 2-9), verify that
the actual temperature for the FPD is at least 120 degrees.
2-16 2000-OSM, C1
**** Manual Temperature Control Mode ****
Zone Config Actual SP Rate
ISO-OVEN ISO 79.9 80.0 0.0
PROG. OVEN PROG/C 220.1 220.0 0.0
FPD ISO 120.2 125.0 0.0
LSV ISO 199.9 200.0 0.0
F1 F2 F3 F4
h. When the temperature is at least 120 degrees, press the F1 (Escape) soft key
two times to return to the Manual Control Mode screen.
i. On the Manual Control Mode screen, press the F2 (Detector and Graphics) soft
key.
j. On the Chroma Board screen, verify the flame is off and the Ignitor is Off.
k. Press the F4 (Manual Ignitor On) soft key to light the cell flame. The ignitor coil
remains powered for the specified Timeout period. Once the flame lights the
Flame Out LED will go off. The cell flame burns as long as there is sufficient
burner air and hydrogen fuel in the cell.
14. With Dual Detectors, perform steps 12 and 13 for each detector, as appropriate.
15. Again verify settings with the Data Package and adjust as needed. Check oven
temperature on the Temperature Control screen (see "Temperature Control Table" in
Section 4).
2000-OSM, C1 2-17
1. Verify that the Background screen is displayed (see Figure 2-10). If it is not displayed,
press the F1 soft key several times until the Background screen appears.
********** B A C K G R O U N D **********
ABB Analytical GCC Remote 0.1
803V029-1R (Std GCC) (C) 2001
**ALARM**
**ALARM** 20-JUN-2002 THU 08:16:01
**ALARM**
Analysis Time :00114 Peaks Found:00
Cycle Time :00000 State:Idle
F1 F2 F3 F4
5. On the Table Storage screen cursor down to RESTORE TABLES FROM E2PROM.
7. When “Are You Sure? Y/N” appears on the screen, press the “Y” key.
This restores to main memory the tables that were most recently saved to E2PROM.
If ABB Lewisburg provided Applications Engineering, verify all method tables by comparing
them to those in the Data Package. This is done most easily by printing the tables (if a
printer is connected to the analyzer). To print the method tables:
2-18 2000-OSM, C1
3. On the Commands screen cursor down to PRINTER.
4. Press the F2 (Test Printer) soft key. A string of characters should print. If characters
print go to step 5. If a string of characters does not print go to step 9.
7. Select a table to print. Repeat until you have printed all tables.
8. Verify that the printed tables are the same as those in the Data Package. If so, go to
"Calibration Run."
9. If a string of characters did not print when you selected Test Printer, cursor to TESTING/
SET UP.
11. On the Hardware Set Up screen, verify that the baud rate, parity, data bits, and stop bits
values match those set at the printer. Refer to the printer manual if necessary.
12. Press the F2 (Exit & Update) soft key and return to the Commands screen.
Calibration Run
If you have a calibration run specified for your analyzer, request a calibration and compare
the results with those in the Data Package. To do this perform the following steps (which will
enable you to perform a single calibration run):
2. On the Commands screen cursor to TABLE EDIT and then press the F2 (Methods) soft
key.
3. The Method Table #?? screen will appear. Use the number keys on the GCC front panel
to enter the number of the method to be calibrated. When the desired number appears
on the screen, press the F2 (Edit The Table) soft key.
4. The Cal Define & Cycle Time screen will appear. Note the calibration stream number
that appears on the Primary Cal Stream line.
6. When the next Method Table screen appears, press the F1 (Exit) soft key, then press
the F1 (Escape) soft key.
7. When the Commands screen appears, cursor to ANALYSIS CONTROL and then press
the F2 (Request Analysis) soft key.
2000-OSM, C1 2-19
8. On the Request Analysis screen (see Figure 2-11), select the method number for a
calibration run.
Accept Clear
Escape The All
Request Requests
F1 F2 F3 F4
9. Place the cursor on “Cal” and then press the F2 (Accept The Request) soft key.
10. Press the F1 (Escape) soft key to return to the Commands screen.
11. If the analyzer is running, go to step 14. If the analyzer is stopped, go to step 12.
12. On the Commands screen, press the F4 (Start/Stop Analysis) soft key.
13. On the Start/Stop Analysis screen, press the F2 (Start Analyzer) soft key. The controller
will perform the calibration as soon as it completes all other requests.
14. Press the F1 soft key as necessary to return to the Background screen.
15. Watch the screen to determine when the calibration stream (noted in step 4) has purged
and starts the calibration.
16. Press the F3 (Current Report, Basic I/O, and Options) soft key.
17. On the Report, Basic I/O and Options screen, cursor to CURRENT REPORT, if
necessary, and press the F2 (View Current Report) soft key. The desired report will
display at the end of the calibration.
18. When the report is complete, press the F1 soft key as necessary to return to the
Background screen. The analyzer will continue to run until the operator stops it.
19. To stop the analyzer, press the F1 (Exit to Commands) soft key.
2-20 2000-OSM, C1
20. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and press the
F4 (Start/Stop Analysis) soft key.
21. On the Start/Stop Analysis screen, cursor to “At End of Analysis?” and then press the F2
(Stop Analyzer) soft key.
22. Press the F1 soft key as necessary to return to the Background screen.
Checking Streams
To verify the operation of each stream, perform a single analysis on each one before going
into full operation.
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and then press
the F2 (Request Analysis) soft key.
3. On the Request Analysis screen (see Figure 2-11), select the stream to be analyzed.
4. Place the cursor on “Stream” and then press the F2 (Accept The Request) soft key.
7. On the Start/Stop Analysis screen, press the F2 (Start Analyzer) soft key. The controller
will start the analysis on this stream as soon as all other requests have been completed.
9. Watch the screen to determine when the desired stream has purged and starts the
analysis.
10. Press the F3 (Current Report, Basic I/O, and Options) soft key.
11. On the Report, Basic I/O and Options screen, cursor to CURRENT REPORT, if
necessary, and press the F2 (View Current Report) soft key. The desired report will
display at the end of the analysis.
12. When the report is complete, press the F1 soft key as necessary to return to the
Background screen.
13. To repeat the process for the remaining streams or to rerun this stream, repeat steps 1
through 12.
14. When checkout is complete, press the F1 soft key to return to the Background screen.
The Chroma I/O PCB, located in slot 2 of the GCC Card Cage, requires setting of switches
for network operation and local control options. Eight-position DIP Switch SW1 controls
these features.
2000-OSM, C1 2-21
Refer to the Data Package to see if a network identification (“Remote Number”) is assigned
to the analyzer. When you determine the Remote Number for this analyzer, set or verify this
identification using positions 1 through 5 of SW1, as follows.
NOTE
CAUTION
4. Locate Switch SW1 on the Chroma I/O PCB (see Figure 2-12).
1 0
1
2
3
4
5
6
7
8
ON OFF
SW1
5. Set the switch positions to the desired remote number, using Figure 2-13 as a guide.
6. Insert the Chroma I/O PCB into slot 2 of the Card Cage and make sure the PCB is
securely in place.
2-22 2000-OSM, C1
Switch No. Switch No.
5 4 3 2 1 5 4 3 2 1
1 1 1 1 1 #1 0 1 1 1 1 #17
1 1 1 1 0 #2 0 1 1 1 0 #18
1 1 1 0 1 #3 0 1 1 0 1 #19
1 1 1 0 0 #4 0 1 1 0 0 #20
1 1 0 1 1 #5 0 1 0 1 1 #21
1 1 0 1 0 #6 0 1 0 1 0 #22
1 1 0 0 1 #7 0 1 0 0 1 #23
1 1 0 0 0 #8 0 1 0 0 0 #24
1 0 1 1 1 #9 0 0 1 1 1 #25
1 0 1 1 0 #10 0 0 1 1 0 #26
1 0 1 0 1 #11 0 0 1 0 1 #27
1 0 1 0 0 #12 0 0 1 0 0 #28
1 0 0 1 1 #13 0 0 0 1 1 #29
1 0 0 1 0 #14 0 0 0 1 0 #30
1 0 0 0 1 #15 0 0 0 0 1 #31
1 0 0 0 0 #16 0 0 0 0 0 #32
Remote No.
The local control options are manual control, view only, and screen saver, using SW1
positions 6, 7, and 8 (SW1 positions 6 and 7 interact).
• Setting SW1-7 to OFF locks the screen in a “view only” mode; you cannot edit any
tables or functions. Setting SW1-7 to ON disables the “view only” function.
• SW1-6 provides manual control but does not let you update tables. Setting SW1-6 to
OFF enables manual control, but only when SW1-7 is in the ON position. When SW1-7
is set of OFF this overrides the setting of SW1-6.
• The screen saver option lets you blank the display screen when it is not being used.
SW1-8 OFF activates the screen saver, while SW1-8 ON disables this feature.
2000-OSM, C1 2-23
If the GCC has user nameable inputs option, you may insert names for up to five sensor
inputs (digital inputs on the Chroma I/O Board). To enter these names, perform the following
steps:
2. On the Commands screen, cursor down to NAMES and press the F2 (Name Sensors &
Basic) soft key.
3. On the Sensor And Basic Alarm Names screen, enter the desired names (up to ten
alpha-numeric characters each) and then press the F2 (Exit and Update) soft key to
save the names.
Analytical Operation
Once you have verified the calibration data and each stream’s data, you are ready to place
the analyzer into full operation. Display the Background screen and then perform the
following steps:
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and then press
the F4 (Start/Stop Analysis) soft key.
3. On the Start/Stop Analysis screen press the F2 (Start Analyzer) soft key.
The analyzer will run according to an already designated method table (usually #1). The
analyzer will continue to operate until you command it to stop (see "Stopping the Analyzer").
You can verify a chromatogram’s zero baseline in one of the following ways:
Recording a Chromatogram
2. On the Manual Control Mode screen (see Figure 2-14), cursor down to CHROMA, then
left to OFF.
4. Cursor to CHROMA and then press the ENTER key. The recorder turns on and will
record the chromatogram.
5. When the chromatogram is complete, press the F1 soft key as necessary to return to
the Background screen.
2-24 2000-OSM, C1
****** Manual Control Mode ******
Valves:- - - - - - - - Time:00000
Enter Valve: [0] Cycle Time:00000
RECORDER: Method Tbl: 000
Offset : 0 % Stream: 01
Attn : 5 Purging: 01
Off Chroma Bar Trend Peaks: 00
PURGE SELECT: :0 State: Idle
Start Crest End Peak
Time Time Time Area Type
Last: 52 55 73 18032 Val-Bas
38 43 51 15322 Bas-Val
F1 F2 F3 F4
Displaying a Chromatogram
2. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
4. On the Graphics Mode screen press the F2 (Display the Graphics) soft key. A
chromatogram will scroll up the screen as it happens. A baseline at mid-screen is good.
5. When you have completed the chromatogram display, press the F1 soft key as
necessary to return to the Background screen.
2. On the Manual Control Mode screen press the F3 (Manually Zero Baseline) soft key.
3. A message line appears above the soft key, similar to the following: “Zero Offset Used
004%.” A value less than 10% is good.
4. When you have completed the zero offset check, press the F1 soft key as necessary to
return to the Background screen.
2000-OSM, C1 2-25
Time Cycle Check
Perform a complete program cycle to verify that each stream and method is operating
according to the Data Package.
Verify Reports
Compare all reports in the Data Package to the corresponding reports in the analyzer by
printing the analyzer reports.
2. On the Commands screen, cursor down to NAMES and then press the F3 (Name
Headers) soft key.
3. On the Name Headers screen, enter a header (up to two lines) and then press the F2
(Exit and Update) soft key to save the headers.
3. Press the F2 (Printer Report Type) soft key to display the Printer Report Type screen
(see Figure 2-15). Highlighted or underlined items on this screen indicate the current
selections.
4. Cursor right or left to the report type you want to print: Raw Data, Regular, or Short (see
"OTHER TABLES AND REPORTS" in Section 4 for detailed examples of report types).
5. Cursor down to Print and then cursor right to Always to activate the printer.
6. Cursor down to Alarm Report and select No (or Yes to print an alarm report).
7. Cursor down to Frequency if you are changing how often you print this report.
“Frequency” in this screen means whether you will print the report each time it occurs
(“1”), only every other time it occurs (“2”), only every third report that occurs (“3”), etc.
8. When you have made and verified your selections, press the F2 (Exit and Update) soft
key to print the report.
2-26 2000-OSM, C1
****** Printer Report Type ******
GC Analysis Report:
Type: [Raw Data] Regular Short
Print: Never Always On Alarm
Alarm Reports: No Yes
Frequency: 1
Inhibit Cal/Bench Report: No Yes
Exit
Escape and
Update
F1 F2 F3 F4
Benchmark Run
Benchmarks are periodic tests used to ensure the analyzer is functioning properly. If you
perform a benchmark of each applicable method at the end of start-up, this will provide a
reference for later benchmarks. In order to do benchmarks, the benchmark concentrations
must be entered into the Component Definition screen and the benchmark stream must be
defined (see "Preparing a Method Table" in Section 4).
2. On the Commands screen cursor to TABLE EDIT and then press the F2 (Methods) soft
key.
3. The Method Table #?? screen will appear. Use the number keys on the GCC front panel
to enter the number of the method to benchmark. When the desired number appears
on the screen, press the F2 (Edit The Table) soft key.
4. The Cal Define & Cycle Time screen will appear. Note the benchmark stream number
that appears on the Benchmark Stream line.
6. When the next Method Table screen appears, press the F1 (Exit) soft key, then press
the F1 (Escape) soft key.
7. When the Commands screen appears, cursor to ANALYSIS CONTROL and then press
the F2 (Request Analysis) soft key.
2000-OSM, C1 2-27
8. On the Request Analysis screen select the method number to be benchmarked.
9. Place the cursor on “Bench” and then press the F2 (Accept The Request) soft key.
10. Press the F1 (Escape) soft key to return to the Commands screen.
11. If the analyzer is running, go to step 14. If the analyzer is stopped, go to step 12.
12. On the Commands screen press the F4 (Start/Stop Analysis) soft key.
13. On the Start/Stop Analysis screen press the F2 (Start Analyzer) soft key. The controller
will perform the benchmark as soon as all other requests have been completed.
14. Press the F1 soft key as necessary to return to the Background screen.
15. Watch the screen to determine when the benchmark stream (noted in step 4) has
purged and starts the benchmark.
16. Press the F3 (Current Report, Basic I/O, and Options) soft key.
17. On the Report, Basic I/O and Options screen, cursor to CURRENT REPORT, if
necessary, and press the F2 (View Current Report) soft key. The desired report will
display at the end of the benchmark run.
18. When the report is complete, press the F1 soft key as necessary to return to the
Background screen. The analyzer will continue to run as directed by the Stream
Assignment Table unless it is stopped by the operator.
19. To stop the analyzer press the F1 (Exit to Commands) soft key.
20. On the Commands screen, cursor to ANALYSIS CONTROL, if necessary, and press the
F4 (Start/Stop Analysis) soft key.
21. On the Start/Stop Analysis screen, cursor to “At End of Analysis?” and then press the F2
(Stop Analyzer) soft key.
22. Press the F1 soft key as necessary to return to the Background screen.
To adjust the Thermal Conductivity Detector (TCD) zero, perform the following steps:
2. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
3. On the Chroma Board screen press the F3 (Manually Zero Baseline) soft key. The
Detector Reading should change to a value of 2.00 mV ± 0.05 mV.
4. Note the readings (on the Chroma Board screen) for Hardware Zero, Software Zero,
and Detector Reading values.
2-28 2000-OSM, C1
6. Locate the TCD Amplifer PCB on the left side wall of the GCC and remove the plug
covering the Zero Adjust Potentiometer (see Figure 2-16).
Zero Adjust
Potentiometer
7. Adjust the Zero Adjust potentiometer until the Detector Reading is equal to the sum of
the Hardware Zero and Software zero values noted in step 4.
8. Press the F3 (Manually Zero Baseline) soft key and recheck the readings. The detector
is adequately zeroed when the Hardware Zero percentage is less than 10%.
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and then press
the F4 (Start/Stop Analysis) soft key.
3. On the Start/Stop Analysis screen, verify that the highlighted area is on "At End of
Analysis?" and press the F2 (Stop Analyzer) soft key. The analyzer will stop at the end
of the analysis.
If the analyzer is connected to ABB's VistaNET, you must connect the GCC to the VistaNET
PC as described in the VistaNET 2.0 Installation Guide (2300-IG). After the connections
have been completed and verified you must set up the GCC to work on this network. This
setup consists of several sets of front panel display entries.
Initial Setup
These steps set up the analyzer to work with VistaNET. The paragraphs that follow explain
specific additional information required for full VistaNET operation.
2000-OSM, C1 2-29
NOTE
Before changing VistaNET screens, verify all data with your Network
Administrator to ensure proper VistaNET connection and operation.
2. On the Commands screen, cursor to TESTING/SETUP and then press the F4 (Status
Display) soft key.
3. On the Controller Status screen, press the F2 (Clear Highway Stats) soft key to reset all
data to zero so you will know when VistaNET data is sent and received.
4. On the Commands screen, cursor to VISTANET and then press the F2 (VistaNET
Tables and Commands) soft key.
5. On the VN Menu screen (see Figure 2-17), cursor to STARTUP and then press the F2
(Essential Addresses) soft key.
TABLES
STARTUP
TESTING
F1 F2 F3 F4
6. On the VistaNET Essential Addresses screen (see Figure 2-18), enter the GCC's
identification on the Name line. This identifies the device type and location.
7. Cursor down to the Tag line and enter the GCC's tag number. This usually identifies the
tap in the process that connects to the analyzer.
8. Cursor to the Board Address line and enter the Communication Board's address.
9. Cursor to the Domain 1 line and enter your GCC's Domain 1 identification.
10. Cursor to the Domain 2 line and enter your GCC's Domain 2 identification.
2-30 2000-OSM, C1
******* VistaNET Essential Addresses *******
Name: [GCC10 ]
Tag: GCC10
Exit
Escape and
Update
F1 F2 F3 F4
11. Cursor to the VNSA Address line and enter the complete address of the VNSA serving
your GCC.
12. Cursor to the Router Address line and enter the complete address of the Router serving
your GCC.
13. When you have completed and verified your entries, press the F2 (Exit and Update) soft
key to save your entries.
Next you must enter the appropriate access level. There are three levels of remote access
(i.e., via VistaNET) granted by the analyzer:
You set the remote access level for an analyzer from the front panel as follows:
2000-OSM, C1 2-31
1. At the VN MENU screen, cursor to STARTUP and press the F3 (Access Level)
soft key (see Figure 2-19).
2. Select level desired from scroll list and select Exit and Update.
Exit
Escape and
Update
F1 F2 F3 F4
Subscriber List
Since you want the analyzer to automatically send analysis results and analyzer events to
the VistaREPORTER, the HIU, and VistaSTORAGE, you must enter their addresses and
associated time-outs in the Subscriber List. The time-out determines how long the analytical
device will wait for an appropriate response from the server before trying an alternate
domain or different server altogether.
Unlike the Essential Addresses and Access Level, the Subscriber List can be edited
remotely. This installation procedure will only cover editing the Subscriber List from the
device’s front panel.
2-32 2000-OSM, C1
**** VN Menu *****
TABLES
STARTUP
TESTING
Subscriber SQC
Escape List Config
Table
F1 F2 F3 F4
2. Press the F2 (Subscriber List) soft key to access the VistaNET Subscriber List (see
Figure 2-21).
Type: HIU
Primary Address: 0.1.0.100
Secondary Address: 0.2.0.100
Time Out: 7000 ms
F1 F2 F3 F4
2000-OSM, C1 2-33
3. Cursor to Type field and select server type: HIU, RD (VistaREPORTER), or SD
(VistaSTORAGE).
4. Cursor to Primary Address field and enter the full address of the server that the
analytical results or analyzer events will be sent to first.
5. Cursor to Secondary Address field and enter the full address of the server that is
contacted only when no proper response has been received from the Primary Address
within the time limit set in the Time Out field.
6. Cursor to the Time Out field and enter the time period before the analytical device will
switch to the Secondary Address for services. The time-out period must be entered in
milliseconds. Note: If the HIU time-out period is inadequate for HIU communications
with the DCS, the HIU will automatically modify the analytical device’s Subscriber List.
10. When you have completed all entries, press the F2 (Exit & Update) soft key.
When all entries have been completed and verified, you should perform the following steps
to ensure VistaNET is operating properly.
1. On the VN Menu screen with Startup highlighted, press the F4 (Refresh VNSA Tables)
soft key and then press the Escape soft key to return to the Commands screen.
2. On the Commands screen, cursor to TESTING/SETUP and then press the F4 (Status
Display) soft key.
3. On the Controller Status screen (see Figure 2-22), note that "Blocks Acked" and "Blocks
Received" both have numbers, indicating that your command to Refresh VNSA Tables
was sent and acknowledged. You are now connected to VistaNET.
2-34 2000-OSM, C1
***** Controller Status *****
Clear
Escape Highway
Stats
F1 F2 F3 F4
2000-OSM, C1 2-35
For further information or assistance contact:
ABB Inc.
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
2-36 2000-OSM, C1
SECTION 3. OPERATION
The GCC’s internal controls and indicators are as shown in Figure 3-1.
Reset Switch
(resets SBC PCB)
Halt
Time Out
Run
Highway 2 Transmit
Highway 2 Receive
Highway 1 Transmit
Highway 1 Receive
The GCC’s external controls and indicators are as shown in Figure 3-2.
Recorder Jacks
FLAME OUT 0 - 10 V
F1 F2 F3 F4 ENTER HELP
2000-OSM, C1 3-1
Regulator and Gauge Panels
The Purge Air Panel contains the pressure regulators and gauges for controlling the purge
air and heater air (see Figure 3-3).
If the analyzer has mechanical regulators and gauges, the Pressure Control Panel will have
the analytical regulators and gauges. (The application determines which specific regulators
and gauges are installed.) If the analyzer has EPC, the Pressure Control Panel has a blank
front panel.
Oven Compartment
On the right side of the oven compartment are located the column flow adjustments for
setting flows. These needle valves, located in the oven for thermal stability, allow flows to be
set using a screwdriver through the oven wall without disturbing the thermal integrity of the
analysis zone.
NORMAL OPERATION
When the analyzer is first installed or when it is being turned on for the first time after
maintenance or repair, you should verify that all installation and startup checks have been
completed (see Section 2 of this manual).
Display Screen
This analyzer operates from a series of menus and screens, using the display on the GCC.
The Background screen is the default screen, from which you can select the other screens.
Since all screens are divided into the same basic elements, you should understand this
screen structure before operating the analyzer (see Figure 3-4).
3-2 2000-OSM, C1
********** B A C K G R O U N D ********** Screen Title
ABB Analytical GCC Remote 0.1
803V029-1R (Std GCC) (C) 2001
**ALARM**
**ALARM** 20-JUN-2002 THU 08:16:01
**ALARM**
Analysis Time :00114 Peaks Found : 00 Data Display
Cycle Time :00000 State : Idle
Soft Keys
F1 F2 F3 F4
When the Background screen is not displayed, you can return to the Background screen by
repeatedly pressing the F1 soft key until the Background screen appears.
Before you start into full analytical operation, perform a calibration (if appropriate) and a
single analysis on each stream. These precautions enable you to verify the analyzer and the
process.
CAUTION
When you stop analytical operation, select “At End of Analysis” unless
an emergency occurs. Selecting “Now” stops an analysis immediately,
which can inadvertently damage the analyzer if it stops while an
analysis is in progress. Stopping during an analysis can trap sample in
a column or permit temperature or pressure ramps to continue without
adequate control.
Checking Calibration
If you have a calibration run specified for your analyzer, request a calibration run and
compare the results with those in the Data Package. To do this perform a single calibration
run:
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and then press
the F2 (Request Analysis) soft key.
2000-OSM, C1 3-3
3. On the Request Analysis screen (see Figure 3-5) select the method number to be
calibrated.
Accept Clear
Escape The All
Request Requests
F1 F2 F3 F4
4. Place the cursor on “Cal” and press the F2 (Accept The Request) soft key.
7. On the Start/Stop Analysis screen press the F2 (Start Analyzer) soft key. The controller
will run the calibration when all other requests have been completed.
8. When the calibration run is complete, verify that the Commands screen is displayed and
then press the F4 (Start/Stop Analysis) soft key.
9. On the Start/Stop Analysis screen, cursor to “At End of Analysis?” and then press the F2
(Stop Analyzer) soft key.
10. Press the F1 soft key as necessary to return to the Background screen.
11. On the Background screen press the F3 (Cur Report, Basic I/O & Options) soft key. The
screen will display the current report. The analyzer will run the calibration when it clears
other requests and the report will appear on the screen as it happens.
12. When you have completed the calibration test, press the F1 soft key to return to the
Background screen.
Checking Streams
To verify the operation of each stream, perform a single analysis on each one, as follows:
3-4 2000-OSM, C1
1. On the Background screen press the F1 (Exit to Commands) soft key.
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and then press
the F3 (Streams) soft key.
3. On the Stream Assignment screen, determine which streams are active. Then press the
F1 (Exit) soft key to return to the Commands screen.
5. On the Request Analysis screen (see Figure 3-5), select the stream number to be
analyzed.
6. Place the cursor on “Stream” and then press the F2 (Accept The Request) soft key.
9. On the Start/Stop Analysis screen press the F2 (Start Analyzer) soft key. The controller
will start the analysis on this stream when all other requests have been completed.
10. Press the F1 soft key as necessary to return to the Background screen.
11. Watch the screen to determine when the selected stream has purged and is starting its
analysis.
12. Press the F3 (Cur Report, Basic I/O, & Options) soft key.
13. On the Report, Basic I/O and Options screen, cursor to CURRENT REPORT, if
necessary, and press the F2 (View Current Report) soft key. The desired report will
display at the end of the analysis.
14. When the report is complete, press the F1 soft key as necessary to return to the
Background screen.
15. To repeat the process for the remaining streams or to rerun this stream, repeat steps 1
through 14.
16. When checkout is complete press the F1 soft key to return to the Background screen.
Analytical Operation
Once you have verified the calibration data and each stream’s data, you are ready to place
the analyzer into full analytical operation.
3. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and press the
F4 (Start/Stop Analysis) soft key.
2000-OSM, C1 3-5
4. On the Start/Stop Analysis screen press the F2 (Start Analyzer) soft key.
The analyzer will run the stream for which it is purging, according to the method designated
in the Stream Assignment screen. The analyzer will continue in analytical operation until you
command it to stop.
3. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and press the
F4 (Start/Stop Analysis) soft key.
4. On the Start/Stop Analysis screen cursor to At End of Analysis? and press the F2 (Stop
Analyzer) soft key.
ALARMS
The analyzer has different types and levels of alarms to help you resolve analyzer problems.
When an alarm signal appears on the Background Screen, press the F4 (Alarms) soft key to
display the ALARMS screen with the alarm message (see Figure 3-6).
When you finish with the alarm messages, press the F1 (Exit) soft key to return to the
Background screen without deleting the alarms, or press the F2 (Clear Alarms and Exit) soft
key to clear the alarms and return to the Background screen.
Clear
Exit Alarms
and Exit
F1 F2 F3 F4
3-6 2000-OSM, C1
Alarm messages are of two primary types: main alarms and subordinate alarms. Main
alarms identify a major alarm category. These alarms appear on the alarm screen at the left
margin (e.g., “Post Analysis Error:” in Figure 3-6). If a main alarm has subordinate alarms,
the main alarm title will include a colon (:). Subordinate alarms appear below the main
alarms, indented and preceded by an asterisk (*) to show their subordinate status (e.g.,
“*Valve Manually Switched” in Figure 3-6).
For more information on these alarms refer to "ALARMS" in Section 6, which describes each
alarm in detail.
CHROMATOGRAMS
Chromatograms can be displayed on the screen or recorded on a strip chart recorder while
the analysis is in progress. This can be useful when you suspect an analysis problem.
Displaying a Chromatogram
2. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
4. On the Graphics Mode screen, set % of Screen Offset to 0 and press the F2 (Display
The Graphics) soft key. The chromatogram will scroll up the screen as it happens.
5. If the chromatogram is too large for the screen or too small to read, press the right or left
cursor arrow key to change attenuation. The attenuation value appears at the bottom of
the Graphics screen, after the letter “R”, with higher numbers representing more
attenuation.
6. To change the speed at which the chromatogram scrolls, press the up (faster) or down
(slower) cursor arrow key. Speed appears at the bottom of the Graphics screen after
the letter “S”, with higher numbers representing faster speed.
7. On the Manual Control Mode screen, cursor down to the attenuation line (Attn:) and
change the attenuation value as necessary to obtain the desired chromatogram size.
The attenuation ranges from 0 to 12 (lower numbers provide more sensitivity).
8. After you have selected an attenuation value, press the F2 (Detector and Graphics) soft
key and then repeat steps 3 through 5.
Recording a Chromatogram
1. Connect the recorder to the red and black front panel jacks or to J104 terminals 2 (+)
and 1 (-) on the left side of the GCC. For a 0-100 mv recorder, install a 1000-ohm, 1/4
watt, 1% resistor across these terminals.
3. On the Manual Control Mode screen, cursor down to Chroma, then left to Off.
2000-OSM, C1 3-7
5. Cursor to Chroma and press ENTER. The recorder will turn on and record the
chromatogram.
6. If the chromatogram is too large for the recorder or too small to read, press the F1 soft
key as necessary to return to the Manual Control Mode screen.
7. On the Manual Control Mode screen, cursor down to the attenuation line (Attn:) and
change the attenuation value as necessary to obtain the desired chromatogram size.
Figure 3-7 correlates attenuation values with recorder ranges. These ranges exclude
any operator-entered ZERO OFFSET. (If you have entered a 5% ZERO OFFSET, the
recorder range for Attenuation 1 would become -0.244 to +4.636 mv.)
8. When you finish plotting chromatograms, go to the Manual Control Mode screen.
9. Cursor to Chroma, then to Off, and then press ENTER. The recorder will stop.
1 0 - 4.88 mv
2 0 - 9.75 mv
3 0 - 19.52 mv
4 0 - 39.02 mv
5 0 - 78.08 mv
6 0 - 156.16 mv
7 0 - 312.32 mv
8 0 - 624.64 mv
9 0 - 1.250 V
10 0 - 2.500 V
11 0 - 5.00 V
12 0 - 10.00 V
If it is necessary to turn off power to the analyzer for maintenance, perform the following
steps:
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and press the
F4 (Start/Stop Analysis) soft key.
3. On the Start/Stop Analysis screen, cursor to At End of Analysis? and press the F2 (Stop
Analyzer) soft key. The analyzer will stop at the end of the analysis.
c. Turn off remaining flows at their sources and plug all vents.
3-8 2000-OSM, C1
6. To return the analyzer to operational status, perform the normal turn-on and calibration
procedures.
COMMAND TREE
The menu system (command tree) branches out from general to specific topics, eventually
leading you to a screen that allows you to view or edit the desired parameters. The soft key
selections move you down the command tree one level at a time. Figure 3-8 shows the top
level of the command tree and the remaining levels of all branches other than Commands.
Figure 3-9 shows the tree structure under Commands.
BACKGROUND
TO FIGURE 3-9
"COMMANDS" MANUAL
BASIC INPUT TEMPERATURE
AND OUTPUT CONTROL
VIEW
START/STOP ALARMS
AND EDIT BASIC
OPTIONS MANUAL
PRESSURE
CONTROL
DETECTOR &
GRAPHICS TEMP CONTROL PRESSURE
CONFIG
PRES CONTROL
PRESS. & TEMP. ZONE CONFIG.
CONTROL
CONTROLLER
TYPE
2000-OSM, C1 3-9
FROM FIGURE 3-8
COMMANDS
REQUEST TREND TABLE
ANALYSIS
TEST PRINTER
CHROMA
PRINTER BOARD 1
SAVE OR
PRINT TABLES RESTORE TABLES
DIGITAL
BOARD 1
STORAGE UPDATE
& CONFIG. DIGITAL
CONFIG. DIGITAL
BOARD 2
DISPLAY SAVED
DATA GRAPHICS
TESTING/SETUP HARDWARE
SETUP
REPROCESS REPORT TO
STATUS SAVED DATA PRINTER
DISPLAY
3-10 2000-OSM, C1
SECTION 4. TECHNICAL DESCRIPTION
FUNCTIONAL DESCRIPTION
Figure 4-1 shows a typical analytical flow system, using the flame ionization detector for
illustration. Connections at the right side of the analyzer cabinet provide all gas and air
inputs. Sliding plate valves, liquid sample valves, or a combination of both, provide control
and measurement of the sample. Each analytical valve is air-actuated by an electrical
solenoid valve, which in turn is controlled by the Solenoid Driver PCB. An operational cycle
for the valves consists of three modes: sample purge, sample inject, and backflush. In the
sample purge mode, sample flows through the sample loop to vent. In the sample inject
mode, the sample valve switches, capturing a plug of sample which the the carrier then
sweeps through the column train to the detector. In the backflush mode, the carrier
backflushes Column 1 to vent.
SUPPLY
AIR SAMPLE
PURGE VENT
AIR ADJ SV SV
CARRIER
IN
SELECTOR
1 6 FLOW ADJ 1 6
2 7 2 7 SELECTOR
3 8 3 8 VENT
COLUMN 4 9 4 9
PRESSURE 5 10 5 10
ADJ
ANALYTICAL COLUMN
FLOW ADJ 2
COLUMN
1 COLUMN CELL
3 DETECTOR VENT
SAMPLE LOOP
SAMPLE
IN OVEN
BACKFLUSH
VENT
The sample valve captures a sample in the sample loop. When the valve switches, the
carrier gas sweeps a sample plug through the sample/backflush valve, through Column 1, to
Column 2 and into the detector cell, where it is converted to an electrical signal. Column 1
performs preliminary separation to remove the heavier non-measured components, which
are then backflushed to vent. Column 2 separates the components to be measured, which
elute sequentially. The electronic output signal from the detector represents the component
inputs proportionally.
2000-OSM, C1 4-1
The selector valve determines which components will be measured. The sample output from
Column 2 goes through Column 3 to the detector for measurement. When the valve
switches, the sample not being measured is flushed through the Selector Vent.
The carrier gas has three purposes: to purge the columns and cell prior to introducing a
sample, to sweep the sample into the detector cell, and to backflush the backflush column.
An externally mounted pressure regulator and gauge regulate the input flow.
The sample system, together with the GCC, controls the calibration sample input. The
sample system flow and pressure control depend on the sample system configuration.
DETECTORS
Introduction
Standard detectors are the Flame Ionization Detector (FID), the Thermal Conductivity
Detector (TCD), and the Flame Photometric Detector (FPD). These detectors may be used
separately, in combination, or as dual detectors. FID and TCD cell subassemblies are
located in the upper half of the oven chamber; the FPD is mounted in a panel on the left side
of the analyzer.
The Manual Control Mode screen provides access to detector information and adjustment,
as follows:
2. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
3. The Chroma Board screen (see Figure 4-2) shows the detector status and adjustments.
4. For FID and FPD equipped analyzers, operate the ignitor manually by pressing the F4
(Manual Ignitor On) soft key.
5. For TCD equipped analyzers, set the baseline by adjusting TCD Zero Adjust on the TCD
Amplifier Board (inside the GCC) while watching the Detector Reading on the screen.
Turn the adjustment screw until you reach the minimum value for the Detector Reading.
6. When you finish the detector adjustments and have verified them, press the F1 soft key
as necessary to return to the Background screen.
If an analyzer with an FPD has the FLAME OUT LED illuminated on the front panel, it can be
ignited either automatically or manually. When the Chroma Board screen has Auto or Auto
Timeout highlighted, the ignitor operates as follows:
1. If the temperature zone associated with the FPD is greater than 110 deg C (or the
temperature zone number is set to “0”), the ignitor is turned on for three seconds.
2. The analyzer waits 15 seconds, then checks the state of the flame. If the flame is lit the
ignition sequence is complete.
3. If the flame is not lit, the analyzer repeats steps 1 and 2 (up to six times).
4. If, after six attempts to light the flame, it still is not lit, the ignition sequence terminates
and the hyrdrogen is shut off.
4-2 2000-OSM, C1
***** Chroma Board *****
Detector: FID
Manually Manual
Exit Graphics Zero Ignitor
Baseline On
F1 F2 F3 F4
5. From the Chroma Board screen you can press the F4 (Manual Ignitor On) soft key to
request ignition. This automatically turns on the hydrogen supply.
If an analyzer with an FID has the Flameout LED illuminated on the front panel, it can be
ignited either automatically or manually. When the Chroma Board screen has Auto
highlighted, the ignitor will continuously try to ignite the flame. When Auto Timeout is
highlighted, the ignitor will attempt to ignite the flame for the time specified by Timeout on the
Chroma Board screen.
The FID cell (see Figure 4-3) reduces the physical sample to an electrical signal which an
interpretation device such as a recorder can condition and plot.
Breather Microdot
Adapter Connector
Thermocouple
Ignitor Polarizer
Jet
2000-OSM, C1 4-3
The cell consists of a polarized jet, a collector, and a chamber in which hydrogen fuel and
sample are burned in air. A current, whose magnitude is proportional to the concentration of
the sample, flows between the jet and the collector. This current goes to the FID Amplifier
Assembly.
The FID Amplifier Assembly provides ignition control for the FID cell and amplification of the
detector cell output signal prior to routing the signal to the control section for signal
processing. It consists of a power supply, ignitor assembly, electrometer amplifier, and
associated circuitry. The power supply provides the necessary dc voltages for the FID
Amplifier Assembly and FID.
The ignitor assembly provides control for the ignitor in the detector cell. In the event of a
flame-out, the thermocouple senses the flame-out, illuminates the Flame-Out LED, and
sends a message to the ignitor assembly, which re-ignites the flame. The electrometer
amplifier takes the FID cell’s output, amplifies it, and sends it to the control section for signal
processing.
Two types of thermal conductivity detector are used in this analyzer, a filament TCD and a
thermistor TCD (see Figure 4-4).
The filament TCD works on the principle that a heated body loses heat dependent on the
composition of the surrounding gas. Filaments sense the rate of heat loss so that any
change in filament current results in a bridge output proportional to the change. The TCD
contains a reference filament and a measurement filament. When the reference carrier gas
flows across both filaments, the two filaments have the same filament temperature and the
bridge has a zero output. During a measurement cycle a sample flows through the
measurement filament, changing thermal conductivity and the filament temperature, thereby
causing a corresponding change in electrical resistance. The bridge senses this change in
current and increases or decreases current flow through the bridge to compensate for the
temperature change. The change in current flow sensed by the bridge is proportional to the
component concentration in the sample being measured.
Cable
Reference Measure
Filament Filament Measure Reference
Thermistor Thermistor
Reference
Vent
Sample
In
Sample
Vent Measurement Reference
Vent Vent
Reference In
Measurement Reference
In In
4-4 2000-OSM, C1
The thermistor TCD works on the principle that thermistor resistance varies inversely with
temperature change. The TCD contains a reference thermistor and a measurement
thermistor, connected to a comparator circuit. When the reference carrier gas flows across
both thermistors, the two thermistors have the same resistance and the comparator circuit
generates a zero output. During a measurement cycle a sample flows across the
measurement thermistor, thereby creating a resistance difference between the two
thermistors. This resistance difference sensed by the comparator circuit creates an output
signal representing component concentration in the sample being measured.
Flame photometric detection works on the principle that when sulfur is burned in a hydrogen-
rich atmosphere, luminescence (light) characteristic to sulfur is produced. The FPD cell (see
Figure 4-5) consists of a teflon burner chamber equipped with a spark ignition system, and a
photomultiplier tube which is thermoelectrically temperature controlled. A narrow bandpass
filter optically connects the burner chamber and the photomultiplier tube. An exponential
amplifier conditions and amplifies the photomultiplier tube output to provide a linear output
over a wide dynamic range. Sulfur addition permits accurate measurement of low-level sulfur
compounds.
When a sulfur compound passes through the hydrogen-rich flame, strong luminescence
occurs between 320 and 460 nm. The narrow band-pass filter allows a sulfur spectra-
centered transmission at 394 nm ± 5 nm to achieve a specific ratio of sulfur to non-sulfur
compounds between 10,000 and 30,000:1. A photomultiplier tube views the filtered light and
outputs a voltage proportional to the intensity of the filtered luminescence. For maximum
sensitivity, the detector is optimized with respect to temperature, gas flow rates, and bias
voltage on the photomultiplier tube.
Because the amount of sulfur in the sample is very small, a sulfur addition module provides a
standard level of sulfur. This keeps the sulfur readings above the noise level within the
analyzer. When the analyzer processes a sulfur compound, the sulfur in the sample adds to
the standard sulfur, providing a level more easily measured by the photomultiplier tube.
Intercolumn Detector
The intercolumn detector measures the total sample elution profile before complete
component separation takes place in the analytical column, or as a part of a heart cut, or
backflush valve switch. It is generally used as a setup aid during installation or after rework.
While the exact location of the intercolumn detector is application dependent, it can be
connected between the sample valve and the column, between the column and the analytical
detector, or between the sample valve and the backflush valve.
2000-OSM, C1 4-5
Sequential Dual Detectors
Sequential dual detectors allow one analyzer to provide the detection output of two detectors
to meet speed or sensitivity requirements. Because these detectors function sequentially
using any two detectors, one Chroma I/O Board controls both detectors and their signal
output in series. Valve switching in the method tables determines which detector's data will
be processed by the Chroma I/O Board at any given time. Sample flow through the
detectors is application-specific; the details are shown in the Data Package.
Simultaneous dual detectors function in parallel using any two detectors. To accomplish this
simultaneous processing requires one Chroma I/O Board in the analyzer for each detector.
Chroma I/O Board #1 is in GCC Card Cage slot 2 and Chroma I/O Board #2 is in slot 1.
Stream assignments and method tables determine which detector processes each stream
and method. Since sample flow through the detectors is application-specific, refer to the
Data Package for this information.
NOTE
The same Method Table cannot be used for both Chroma I/O Boards.
Each Chroma I/O Board must have its own calibration stream.
Normalized analyses do not normalize across detectors.
• In the Master/Master mode each Chroma I/O Board controls a separate sample system,
which allows totally independent analyses to be run simultaneously.
• In the Master/Slave mode there is only one sampling system. The methods assigned to
the Master Chroma I/O (Chroma Bd #1) perform the stream stepping and control the
analysis time. The slave (Chroma Bd #2) starts its cycle simultaneously with the master,
but the slave’s cycle time is shorter than that of the master. When the slave completes
its analysis it waits until the beginning of the next master cycle to start another run.
All stream and valve outputs originate in Chroma I/O Board #1 (the total number of streams
and valves for any particular GCC configuration remains the same).
Alarm inputs generic to the GCC (e.g., purge air) connect to both Chroma I/O Boards.
Detector specific alarm inputs connect to the appropriate Chroma I/O Board.
Each Chroma I/O Board can have up to five user-defined sensors. However, you can assign
a total of only five sensor names, so the sensors for the two boards share sensor names
(i.e., Sensor #1 for Chroma I/O Board #2 may differ from Sensor #1 for Chroma I/O Board
#1, but they have the same sensor name).
When the Simultaneous Dual Detector option is installed, many screens and functions
change to support this option. The Background screen shows data for both Chroma I/O
Boards all the time (see Figure 4-6). While the Background screen provides information on
both detectors, other screens will show the data from only one of the two detectors at a time.
4-6 2000-OSM, C1
********** B A C K G R O U N D **********
ABB Anlaytical GCC Remote 0.1
803V031-1R (Sim Dual Det) (C) 2001
19-JUN-2002 WED 15:52:34
Chroma 1 Chroma 2
F1 F2 F3 F4
To select or change which detector’s data is viewed, press the F2 (Manual Control) soft key
on the Background screen. On the Manual Control Mode screen, press the F2 (Detector and
Graphics) soft key. When the Chroma Board screen appears (see Figure 4-7), the top line
identifies the board whose data is shown.
Chroma Board #: [ 1 ]
Select Select
Escape Chroma Bd Chroma Bd
and View and Exit
F1 F2 F3 F4
2000-OSM, C1 4-7
To view the data from the second Chroma I/O Board, enter "2" in the highlighted box on the
screen and then press the F2 (Select Chroma Bd and View) soft key. The Chroma Board #2
screen will appear (see Figure 4-8) and all screens showing Chroma I/O Board data will now
show the data from Chroma Board #2.
Detector: FID
Manually Manual
Exit Graphics Zero Ignitor
Baseline On
F1 F2 F3 F4
Pressing the F3 (Select Chroma Bd and Exit) soft key will also change the selected board,
but it will not display the Chroma I/O Board #2 screen.
The Control Parameters screen contains the entries for selecting whether Chroma I/O Board
#2 is run as a master or a slave. To view the Control Parameters screen, press the F1
(Commands) soft key on the Background Screen. On the Commands screen, cursor to
MISC. and press the F2 (Control Parameters) soft key. On the Control Parameters screen
(see Figure 4-9), cursor down the selections until "Detector 1 Mode" and "Detector 2 Mode"
appear. Select the desired mode for Detector 2 and then press the F2 (Exit and Update) soft
key to save this setting.
4-8 2000-OSM, C1
********** Control Parameters **********
Update Trends on Alarm: No Yes
Auto Update of RF: No Yes
Max RF Variation: 0.000000
Unknown Peak RF: 0.000000
Unknown Peak Units: % ppm
Slope Detect Tics: Never Last First
Detector 1 Mode: Master
Detector 2 Mode: Master Slave
Analyzer Name:
More Below
F1 F2 F3 F4
The Stream Assignment screen adds two columns to its standard screen (see Figure 4-10),
one to identify the detector used for each stream and method (Det), the other to identify the
link between master and slave (Link).
Exit
F1 F2 F3 F4
Since there is no dummy stream in Master/Master mode, all Link column entries are "00".
2000-OSM, C1 4-9
In Master/Slave mode, the Link column in the Stream Assignment screen shows which
stream the slave is using. Because only the Master detector controls the actual streams
used, this slave stream is a "dummy" stream. In Figure 4-10, stream 01 has "01" in the Det
column (Master) and "02" in the Link column. Stream 02 (which is the Link for stream 01)
has "02" in the Det column (Slave) and "00" in the Link column (no link).
Each Chroma I/O Board can send analog output to a recorder, using the terminal board
connections on the right side of the GCC. Chroma I/O Board #2 will always provide data
associated with its respective detector. Chroma I/O Board #1 can provide data associated
with either detector, depending on selections made on the Manual Control Mode screen. In
addition, Chroma Board #1's selected data is available at the front panel Recorder jacks.
The Manual Control Mode screen (see Figure 4-11) controls the recorder output locations for
Chroma I/O Board #1. The RECORDER field selects which detector's output Chroma I/O
Board #1 will send to the recorder outputs. The Mode field selects the type of output to be
sent to the recorder (chromatogram, bar graph, etc.). Press the left and right cursor keys to
scroll the selections.
F1 F2 F3 F4
Other screens and menus have minor changes to help identify which detector is being used
at any given time. Changes you may encounter are:
• Entries in the Random Streams screen must be streams running Master analyses. If a
stream is assigned to the Slave detector, the entry will be skipped.
• The Alarm screen is really two screens with Simultaneous Dual Detectors. When you
press the Alarms soft key, the first screen identifies alarms associated with Chroma I/O
Board 1. Pressing the Exit soft key accesses the second alarm screen, identifying
alarms associated with Chroma I/O Board 2.
4-10 2000-OSM, C1
• Vista Basic commands identify the detector by placing the Chroma I/O Board number
after the alarm name (e.g., CUR_STRM (1) or INTEGER = RAI (1,0), where the first
digit identifies the Chroma I/O Board).
Before starting an analysis, the GCC prompts for the Chroma I/O Board to use during the
analysis. The selected Chroma I/O Board must be in Master mode or the analysis will not
start. If the second Chroma I/O Board is running as Slave and it is linked to the Master
board, an analysis will start on it as well. If both boards are in Master mode, the analyses
can be synchronized by pressing the F4 (Start on Both Masters) soft key. This scheme
works only if the cycle times are the same length for the methods used.
CIRCUIT BOARDS
The Power Supply PCB, on the left side wall of the GCC Card Cage, converts the system
input power to provide voltages for the other boards and functions in the analyzer. Its
outputs include +5 Vdc for digital circuits, +15 Vdc and -15 Vdc for analog circuits, and 18
Vac for current modules on the Analog Output PCB. The Power Supply PCB also has alarm
LEDs to assist in isolating power problems.
The Chroma I/O PCB, in GCC Card Cage slot 2, uses the control information from the SBC
to switch valve and recorder output functions. During an analysis, the Chroma I/O Board
processes detector amplifier output to provide digital and analog outputs for post analysis
verification. When a second Chroma I/O PCB is used it is in GCC Card Cage slot 1.
The Single Board Computer PCB, in GCC Card Cage slot 3, provides all analyzer system
control functions. On the SBC reside E2PROM storage, computer memory, and the address
and data control circuits which coordinate internal and external data activities.
The DC Solenoid Driver PCB, at the bottom left of the GCC Card Cage, has ten solenoid
control circuits. It generates a +110 volt signal for energizing the solenoids controlling the
analyzer and sample system valves. When the controlling signal (common) from the control
section is applied to any of the inputs, a transistor completes the circuit to the appropriate
solenoid. If a second DC Solenoid Driver PCB is used, it is at the bottom right of the GCC
Card Cage.
The Front Panel PCB, on the inside of the GCC front panel, provides the interface for the
display, the instrinsically safe recorder jacks, and the keypad. This assembly is also the
platform for the optional LO COMM PCB.
2000-OSM, C1 4-11
FID Amplifier PCB
The FID Amplifier PCB, on the left side wall of the GCC, amplifies the flame ionization
detector output signal and applies it to the Chroma I/O Board for processing. This assembly
also accomplishes FID flame sensing and ignition. This PCB's gain configuration is set at
the factory.
The TCD Amplifier PCB, on the left side wall of the GCC, amplifies the thermal conductivity
detector output signal and provides it to the Chroma I/O Board for processing.
The FPD Amplifier PCB linearizes and amplifies the flame photometric detector output signal
and applies it to the Chroma I/O Board for processing. This assembly also contains circuitry
for control of thermoelectric coolers for the photomultiplier tube and for FPD flame sensing
and ignition, conditioned through the FPD Interface Assembly. It is located inside the FPD
panel at the left of the analyzer.
The DTC Backplane PCB, located on the GCC right-hand door, has two micro controller
chips, one to run the DTC Backplane PCB and the other to check continuously for over-
temperature conditions in the temperature controlled zones. If the temperature in any zone
exceeds the T-Rating limit, the DTC Backplane PCB shuts off power to the temperature
zones and aborts the analysis.
AC Conditioning PCB
The AC Conditioning PCBs, piggybacked on the DTC Backplane PCB, provide AC heater
voltage to the zone boards, power compensation and zero crossing signals to the DTC
Backplane PCB, and the coolant control output to the Coolant Control Solenoid.
The DTC Zone PCBs, piggybacked on the DTC Backplane PCB, provide individual zone
temperature sensing and power application to heaters for each zone of the digital
temperature controller.
The Electronic Pressure Control Multibus PCB, located in Card Cage slot 4, continuously
checks the pressure controlled zones. If any zone loses pressure control, the Electronic
Pressure Control Multibus PCB sends an alarm to the Single Board Computer PCB, which
aborts the analysis.
The EPC Control PCB, mounted in the EPC Module, provides the overall control for the
electronic pressure controller.
4-12 2000-OSM, C1
EPC Sensor PCB
The EPC Sensor PCBs, mounted on the pressure transducers in the EPC Module, provide
the individual zone pressure data to the EPC Module PCB.
The Local Communications Module (LO COMM) PCB, piggybacked on the Front Panel PCB,
provides remote access for the analyzer, so that this analyzer can operate with other Vista
GCC front panels. See 'REMOTE GC OPERATION OPTION" for a detailed explanation of
remote GC operation.
The Communications Board, in any open slot in the GCC Card Cage, provides a two-channel
interface between the GCC and the VistaNET. See "VISTANET OPTION" for a detailed
explanation of the VistaNET option.
The Analog Output (Trend) PCB has two configurations: a voltage board providing up to 48
outputs and a current board providing up to 16 outputs. Trend PCBs are in GCC Card Cage
slots 6 and 7. See ANALOG OUTPUT OPTION" for a detailed explanation of the Analog
Output option.
The Digital Input/Output PCB has two configurations: up to 48 outputs or up to 16 inputs and
32 outputs. Digital I/O PCBs are in GCC Card Cage slots 5 and 6. See DIGITAL I/O
OPTION" for a detailed explanation of the Digital Input/Output option.
METHOD TABLES
A method table is the program used to control an analyzer during an analysis. It contains all
the instructions and data required to identify each component of the sample and produce a
meaningful analysis report. The analyzer can have a maximum of eight method tables, each
supporting up to 62 components. In order for the analysis to be accurate, the analyzer must
be calibrated first.
Calibration provides a response factor which converts the individual component’s peak area
or peak height into an actual component concentration value. This response factor is
generated by one of three calibration methods performed prior to obtaining any valid analysis
results. These calibration methods are:
• External Standard, in which the controller calibrates the analyzer against an external
calibration standard of precisely known component concentration
External Standard calibration requires you to provide the calibration concentration (CC)
for each component to be analyzed. Each component must be contained in one of the
two calibration streams so that the detector response may be determined for each
component independent of all other components. The system performs an analysis of
2000-OSM, C1 4-13
the calibration stream, obtaining corrected values for the peak area (A) and peak height
(H) of each component contained in that stream. The controller then calculates the
response factor (RF) for each component as follows:
or
• Normalized, in which the controller calibrates the analyzer against the external standard,
then calculates the sum of all peak areas and determines the percent contribution of
each component peak
RFi = (Atot/Ai)CCi, where “Ai” is for individual component, “Atot” for total
Component concentration values are then obtained based on corrected peak area
values following an analysis:
As part of the calibration you can also select primary and secondary calibration streams,
benchmark stream, multiplier exponent, and K-factor:
• primary calibration stream has a default setting in the analyzer of stream 10. This does
not need to be set or changed (but it can be changed if desired).
• secondary calibration stream is necessary when all standard components are not
compatible in the same container.
NOTE
4-14 2000-OSM, C1
• multiplier exponent is an exponential value which allows the analyzer to present the
response factor as an easily identified number (e.g., if response factor is 0.000005,
analyzer might show response factor = 5 and multiplier exponent = 6).
• K-factor is used with the indirect external standard to provide a means of relating the
calibration standards of all components when only one component can be measured.
Once the relationship between the various components is established (at installation),
only the K-factor is changed during calibration.
This subsection explains how to prepare a method table by constructing a sample method
table. Figure 4-12 shows a chromatogram of the analysis to be controlled. This analysis is
90 seconds long and has three components to measure: A, B, and C. These components
elute at the following times (after the start of the analysis): component A, 30 seconds;
component B, 50 seconds; and component C, 70 seconds.
C
A
0 90
TIME (in seconds)
In order to construct a method table for this analysis, you need to know when to turn valves
on and off, how the components are defined, and how to measure the components. For this
2000-OSM, C1 4-15
analysis we shall use slope detection, which is described in detail in "PEAK DETECTION."
Figure 4-13 illustrates the data needed to construct a method table for this analysis.
2. On the Commands screen, cursor down to TABLE EDIT and then press the F2
(Methods) soft key.
3. The Method Table #?? screen will appear (see Figure 4-14). Use the number keys on
the GCC front panel to enter the number “1” for this method (which is the method
number given in Figure 4-13 data). When the correct number shows on the screen,
press the F2 (Edit the Table) soft key.
4-16 2000-OSM, C1
***** Method Table #?? *****
Edit
Escape The
Table
F1 F2 F3 F4
4. The Cal Define & Cycle Time screen will appear (see Figure 4-15). Set the analysis
cycle time for 90 seconds using the number keys.
Continue
F1 F2 F3 F4
2000-OSM, C1 4-17
5. Cursor to the Calibration Type line. The current choice is underlined. To change the
choice, cursor right or left to the desired type (in this case Ext Std) and then cursor to
the next line. Moving the cursor up or down sets the new choice.
6. Cursor to each line in turn and choose the appropriate term or value:
Analysis Normalization: No
Primary Cal Stream: 10
Secondary Cal Stream: 0
Benchmark Stream: 0
7. Review each line to ensure you have entered the correct data and then press the F1
(Continue) soft key.
8. The Method Table #01 screen will appear (see Figure 4-16), allowing you to enter the
time-related data from Figure 4-13.
F1 F2 F3 F4
9. Press the F2 (Insert Line) soft key and then enter “1” using the number keys.
10. Cursor to the Function column. The number you entered now changes to “0001.” In the
Function column, use the up and down arrow keys to scroll the function names until
“Valve On” appears, and then cursor to the right.
12. Press the F2 (Insert Line) soft key and repeat the insertion procedure for each line in the
Method Table down through “Valve Two Off.”
4-18 2000-OSM, C1
13. After you complete the “Valve Two Off” line, press the F2 (Insert Line) soft key.
14. Enter “30” for Component #1’s time and then cursor right to select “Component.” Since
this is the first component entered into the table, “Undefined” will appear in the Value
column.
15. Cursor right to the Value column. The Component Definition screen will appear (see
Figure 4-17), which will allow you to define this component. Cursor to each line in turn
and enter the appropriate data.
Name: [ ONE ]
Units: PPM % Calculated
Key Component: No Yes
Retention Time Dev: ± 5.0000000 secs
Response Factor: 1.0000000
Calibration Concentration: 100.00000
Benchmark Concentration: 100.00000
High Concentration Alarm: 100.00000
Low Concentration Alarm: 0.0000000
More Below
Continue
F1 F2 F3 F4
16. Review each line to ensure you have entered the correct data and then press the F1
(Continue) soft key.
17. When the Method Table #01 screen appears, enter the data for the remaining items in
the Method Table. Remember to name Component Two “B” and Component Three “C.”
18. When you have completed all lines in the Method Table, review the table to ensure all
data are correct and then press the F1 (Exit) soft key.
19. On the Method Table #01 screen, press the F2 (Exit and Update) soft key to save this
Method Table.
The procedure for editing a method table is the same as that for preparing a new table.
Follow the applicable steps in "Preparing a Method Table" to access the particular screen to
be changed and then insert the new information in place of the information already existing.
2000-OSM, C1 4-19
If the data to be revised exists in the time-related portion of the method table, perform the
following steps to edit the table:
2. In step 3 insert the desired method number and then proceed to step 4.
3. In steps 4 through 7, review the Cal Define & Cycle Time screen and make changes as
necessary.
4. When the Method Table #01 (or other number you have chosen) appears, locate the
specific line you want to change.
5. If necessary, cursor to the Time column, and then cursor down to the line you want to
edit.
6. If you want to change the time, use the number keys to insert the new time. If this
changes the place of this line in the table, it will automatically move to the correct place
when you leave the Time column.
7. If you want to change the function, cursor right to the Function column and scroll up or
down to display the new function.
8. If you want to change the value, cursor right to the Value column and make the
necessary changes.
9. When you have completed the changes, press the F1 (Exit) soft key.
10. On the Method Table #01, press the F2 (Exit and Update) soft key to save your changes
to the method table.
2. On the Commands screen, cursor down to PRINTER and then press the F2 (Print
Tables) soft key.
3. On the Print Tables screen (see Figure 4-18), cursor to METHOD TABLE and then press
the F2 (Select Table) soft key.
4-20 2000-OSM, C1
****** Print Tables ******
[METHOD TABLE]
TREND TABLE
TIME TABLE
DIGITAL TABLE
RANDOM TABLE
VISTA BASIC PROGRAM
STREAM TABLE
PRESS. & TEMP.
DIGITAL INS & OUTS
Print
Escape Selected
Table
F1 F2 F3 F4
2000-OSM, C1 4-21
4. On the second Print Tables screen, enter the Method Table number and then press the
F2 (Print Selected Table) soft key. The Method Table and Component Table will print
(see Figure 4-19).
4-22 2000-OSM, C1
5. When all the data have printed, press the F1 soft key as necessary to return to the
Background screen.
PEAK DETECTION
The analyzer measures peaks in two different ways: forced gating and slope detection. Both
methods can exist in the same analysis, but they cannot both measure peaks at the same
time. If the method has forced gating and slope detection on at the same time, the controller
uses the one turned on first, ignoring the second one and sending an alarm to tell you that
both peak detection methods were on.
Forced Gating
When a component's elution time is known, forced gating can measure the peak. You
specify the gating time on and off, which lets you measure only that amount of peak area you
desire. In the method table, forced gating has four commands associated with it.
On @ Base
Off @ Base
On @ Valley
Off @ Valley
“On @ Base” tells the controller it is at the base and to start measuring. The controller
continues to measure until it reads “Off @ Base” or “Off @ Valley” regardless of whether
there are no peaks, one peak, or multiple peaks. The other functions work similarly.
Slope detection determines a peak’s starting and ending points using the analyzer’s
computer. With slope detection active, the controller constantly checks the chromatographic
signal for changes which would indicate the start of a peak, a peak’s maximum, and the end
of a peak. Slope detection utilizes several other functions: noise calculation, peak lumping,
tangent skim, baseline definitions, peak width, and suspend end. In order to explain how
these functions interact, the chromatorgram in Figure 4-20 shows the basic functions, and
the following paragraphs describe the functions.
SLOPE SLOPE
NOISE DETECT DETECT
CALC ON NOW OFF NOW
ON
PEAK
NOISE WIDTH
CALC
OFF
T0 TIME T-END
2000-OSM, C1 4-23
Slope Detection: Basic Functions
The basic slope detection functions used in a method table are Noise Calculation, Peak
Width, and Slope Detect. Slope Detect On and Slope Detect Off must always appear in the
method table when you want to use slope detection. If noise calculation and peak width are
not specified, the controller will use its stored default values.
Noise calculation determines the noise level in the analysis during a period of inactivity.
Shortly after the start of the analysis, Noise Calc is turned on for at least two seconds, and
then turned off. This noise level measured by Noise Calc is used to decide when the slope
of the chromatogram indicates a peak change and not just random fluctuation due to noise.
Peak width is used to calculate the minimum slope of the start of a peak. A lower number
causes the system to respond more quickly to the start of a peak but is less sensitive to long
term change. A higher number causes the system to respond less quickly but is more
sensitive. For that reason the default is set at 8, a median value that provides both good
response and sensitivity for most applications. Peak width only has meaning when slope
detect is running.
Slope Detect On tells the method that slope detection will be used for this analysis. It should
appear in the method well before the first peak is expected to start. Slope Detect Off tells the
method that you are finished using slope detection. Slope detection has six commands
associated with it use:
On Now
Off Now
Off @ Base
Off @ Valley
Off @ Min
Neg Peak
“On Now” starts slope detection at the next peak. “Off Now” stops slope detection
immediately. “Off @ Base turns off slope detection at the next baseline condition. “Off @
Valley” turns off slope detection at the next valley. “Off @ Min” turns off slope detection at
the next minimum, whether it is a baseline or a valley. “Neg Peak” looks for a negative going
slope to trigger the slope detection algorithm. The negative peak search only works for one
peak. You must enter another “Neg Peak” to continue the search for a second negative
peak.
In addition to the basic functions, there are six supplemental slope detection functions which
may or may not be used: peak lumping, tangent skim, baseline definitions, suspend end,
end=crest plus, and area rejection. When and how the method uses them depends on the
specific application.
Peak lumping allows you to sum consecutive peaks into a single lumped peak for calculation.
It allows you to focus on the total area of several consecutive components rather than the
individual peak areas. To use peak lumping, turn Peak Lump On prior to the end of the first
peak in the series of peaks to be lumped together (see Figure 4-21). Turn Peak Lump Off
after the end of the last peak in the series. The lumped peak file will include all peaks which
end while the lumped peaks function is active (peaks 2, 3, 4, and 5 in Figure 4-21).
4-24 2000-OSM, C1
6
5
2
1
3 4
TIME
PEAK LUMP ON PEAK LUMP OFF
Tangent skim lets you analyze a smaller peak riding on the tail of a large peak. Tangent skim
directs the slope detection algorithm to look for this by identifying a tangent termination point
for the next peak which begins on a valley point (see Figure 4-22). Since the tangent skim
termination search operates only during a single peak, it is activated by setting Tangent Skim
at the proper time in the method table (no On/Off is required). To use tangent skim, choose a
time in the method table that occurs at a point before the peak in question and set Tangent
Skim. The search begins at the first valley point (point B in Figure 4-22) after the request
point (point A) and ends at the peak termination point. The controller determines it has found
a tangent termination point when the slope of the chromatogram being measured at point C
equals the slope of the line BC. The tangent point identifies this second peak as being a
small peak on the tail of a larger peak, rather than a separate peak.
1
B
2
C
A D
TIME
TANGENT SKIM
Baseline definitions override the normal slope detection definition of the peak topology. This
permits you to define how the baseline is drawn for a peak or series of peaks. In the method
table, the baseline function has five commands associated with it:
Pk End =Vly
Pk End =Base
Proj Forward
Proj Reverse
Proj Term
2000-OSM, C1 4-25
If a specific application is such that the slope detect algorithm has difficulty determining
whether a particular point at the end of a peak is a valley or a baseline, it can provide erratic
data. The algorithm sometimes calls the point a valley and sometimes it calls it a baseline,
thus providing different peak areas in adjacent analyses (see Figure 4-23). By selecting “Pk
End =Vly” you can force the routine to call it a valley each time it occurs, thus removing the
indecision and stabilizing the calculations. “Pk End =Base” is used the same way as “Pk
End =Vly.” Selecting “Pk End =Vly” or “Pk End=Base” forces the slope detect algorithm to
call the point a valley or a baseline every time, whichever provides the more accurate data.
The difference between the two is shown in Figure 4-23, where the area within triangle ABC
is not measured in “Pk End=Base.” It is important to measure these peaks the same way
every time, for consistency.
PEAK PEAK
END AREA END
AREA
MEASURED MEASURED
B
A C
TIME TIME
The remaining baseline commands allow you to project a horizontal baseline between two
defined points on the chromatogram. This projected baseline may be set forward (to
measure from the baseline before the peak) or reverse (to measure from the baseline after
the peak). The command to start a projection must be entered at a time before the slope
detect function senses the start of a peak, and the ending command must be entered at a
time before the slope detect routine senses an end of peak.
“Proj Forward” is a forward projection flag inserted before the start of a desired peak. This
sets the baseline as the start of the peak (see “HBF” in Figure 4-24). “Proj Term” is a flag to
end the projection, thereby identifying the peak or group of peaks to be measured. It is set
after “Proj Forward” and before the end of the peak (see “HBT” in Figure 4-24). Line AB in
Figure 4-24 represents the baseline.
C D
A B
TIME
HBF HBT
4-26 2000-OSM, C1
“Proj Reverse” is a reverse projection flag that identifies the end of a desired peak or group
of peaks. It is set in the baseline after the end of the peak (see “HBR” in Figure 4-25). With
reverse projection, “Proj Term” is set before the start of the peak—and before “Proj Reverse”
(see “HBT” in Figure 4-25). The system then measures the peak that occurs between HBT
and HBR. Line JK in Figure 4-25 represents the baseline.
H I
K J
BASELINE FOUND
BUT IGNORED
B
A C F
D
E
TIME
2000-OSM, C1 4-27
Another method for handling badly tailing peaks is “End=Crest+” (see Figure 4-27). This
code forces the end of the peak to be the crest time plus the time specified in the code,
providing a reproducible end to the peak even if the crest of the peak is moving. To use this
command, insert “End = Crest+” into the method together with a specified time after the
crest. The method allows times from 1 to 380 for the length of time after the crest.
END SPECIFIED BY
CREST END=CREST+
TIME
END=CREST+
Area rejection is used to separate smaller, unwanted, peaks from larger peaks. If several
small peaks are close to peaks of interest, area rejection allows you to define a minimum
area a peak has to reach to be retained. Slope detection still measures all the peaks, but at
the end of the analysis all peaks below the rejection area are disregarded. To use area
rejection, insert Reject Area into the method, together with the threshold area value which
tells the controller what minimum peak area is to be retained for analysis. The method
allows you to specify areas from 1.0 to 9,000,000 for the rejection area (corrected peak area
in the Raw Data Report).
This section discusses the time-coded functions that are not part of peak detection.
A method table will contain one or more of these functions when the particular application
requires it. The following sections describe each function.
Auto Zero
Auto zero supplies an offset which brings the raw baseline signal down to its most sensitive
range. It also supplies a software offset to bring the signal to 2.0 mV. The auto zero offset is
±100 mV with a resolution of 1.7 mV. Using all of the offset voltage generates an alarm.
The auto zero function occurs immediately when requested, except that it is ignored during
any of the following situations (which cause alarms):
4-28 2000-OSM, C1
NOTE
Stream Step
Stream Step begins the automatic sample purge of the next sample stream to be analyzed.
It must occur after completion of the sample inject for the stream currently being analyzed.
This is particularly important when the current stream being analyzed requires multiple
sample injections.
The analyzer samples the active streams in sequential order. However, you can change the
order by setting a random stream-stepping order (using the Random Stream Step table
accessed from the Commands screen).
You may request calibration, benchmark, or analysis of a specific stream at any time. The
GCC stacks and executes multiple stream analysis requests on a last in - first out basis
following the next stream step. The controller will step to any manually requested stream
regardless of its active/inactive status. Only after all requested stream analyses are
completed does the controller step to the next active stream in the routine sequence.
When the screen displays the desired method table, you can change the timing of the stream
step or add a stream step if the method table does not contain one.
NOTE
Each method table must contain a stream step in order for the
equipment to operate properly. If a method table does not have a
stream step, the controller will continue to process the last-identified
stream, repeating it until the purge stream is manually changed or a
stream step is inserted into the method table.
Valve On and Valve Off control the operation of a selected valve. Each method table should
contain the valve on and off sequences required for the selected stream. The time of the first
“Valve On” in a method table is used in all reports as the sample inject time. Occasionally
you may have to add a valve on-off sequence, delete a sequence, or change the timing of a
sequence.
To turn on a valve: access the method table, set the desired time to turn on the valve, and
then select “Valve On” and the valve number.
To turn off a valve: access the method table, set the desired time to turn off the valve, and
then select “Valve Off” and the valve number.
Tic Mark
This allows you to generate positive or negative event markers for the reconstructed
chromatogram. Tic marks identify a particular point in time on the chromatogram that you
select. A tic mark can go upward from the analysis line (positive) or downward (negative).
2000-OSM, C1 4-29
Skip Next TCF On Alarm
This allows you to skip the next time-coded function if any sensor alarm is active. This
allows you to bypass sample injection if the chromatographic sensors indicate that the
analyzer is not operating according to preset parameters, such as temperature.
This allows you to skip the next time-coded function when this stream value equals the
stream number entered in the method table. This function allows you to skip a TCF on a
particular stream, usually because that TCF does not apply to that stream.
This allows you to execute the next TCF in the method only if the stream value equals the
stream number entered in the method table. This function allows you to add a specific TCF
to a particular stream, but not to every stream.
Pressure Check
Pressure check, part of the optional Electronic Pressure Controller, lets you check for
pressure zone variances. A pressure value outside the zone limit causes an alarm. This
feature is described in detail in "ELECTRONIC PRESSURE CONTROL OPTION."
Pressure Control
Pressure control, a feature of the optional Electronic Pressure Controller, lets you review or
modify the pressure zone set point and ramp rate. This feature is described in detail in
"ELECTRONIC PRESSURE CONTROL OPTION."
Temperature Check
Temperature Check lets you check for temperature zone variances. A temperature value
outside the zone limit causes an alarm and, depending on the condition, aborts the analysis.
This feature is described in detail in "DIGITAL TEMPERATURE CONTROLLER."
Temperature Control
This lets you review or modify the temperature zone set point and ramp rate. This feature is
described in detail in "DIGITAL TEMPERATURE CONTROLLER."
This section discusses tables and reports that are not covered elsewhere.
Unless otherwise stated, perform the following steps to view or edit a table:
4-30 2000-OSM, C1
2. On the Commands screen, cursor down to TABLE EDIT and press the F3 (Other
Tables) soft key.
3. On the Edit Other Tables screen, cursor down to the desired table and then press the F2
Edit the Table) soft key.
4. View or edit the table, then press the F1 (Exit) soft key.
5. On the next screen, press the F2 (Exit and Update) soft key to save the new data, or
press the F1 (Escape) soft key to retain the original data.
Printing Tables
2. On the Commands screen, cursor down to PRINTER and then press the F2 (Print
Tables) soft key.
3. On the Print Tables screen, cursor to the desired table and then press the F2 (Print
Selected Table) soft key. The table will print.
Printing Reports
2. On the Commands screen, cursor down to REPORTS and then press the F2 (Printer
Report Type) soft key.
3. On the Printer Report Type screen, cursor to the Type line and select the type of report
print by highlighting it.
4. Cursor to the Print line and select No if you do not want to print a report, Yes if you want
to print each time the report is created, Alarm if you want to print only when an alarm
condition occurs, Change if you want to print only when an alarm condition changes, or
Freq if you want to set how often to print a report.
5. Cursor to the Alarm Reports line and select No or Yes. Selecting No or Yes in step 4
overrides any alarm selection.
6. Cursor to the Frequency line and select how often you want to print a report. In this
usage, “1” means the report will print every time the report occurs; “2” means it will print
every other time; “3” means it will print every third report. Selecting No or Yes in step 4
overrides any frequency value.
7. Cursor to the Inhibit Cal/Bench Report line and select No or Yes. This selection
determines whether calibration and benchmark reports print in addition to analysis
reports (Yes), or just the analysis reports (No) will print.
8. When you have completed all entries, review the screen to verify all data. Then press
the F2 (Exit and Update) soft key to save the changes, or press the F1 (Escape) soft
key to retain the original values. The printer will print the report as you have specified it.
2000-OSM, C1 4-31
Random Stream Stepping Table
The Random Stream Stepping Table establishes the sequence in which the various streams
are to be analyzed, up to a maximum of 50 entries. The table lists the streams in numerical
order unless the operator orders a different sequence. Figure 4-28 shows the Random
Streams screen and Figure 4-29 shows the printed table.
Stream
0001
0002
0001
0003
0004
0001
0005
0006
More Below
Insert Delete
Exit Line Line
F1 F2 F3 F4
4-32 2000-OSM, C1
Time Table
This table contains the schedules for automatic calibrations, benchmarks and stream
analyses (see Figure 4-30). The Time Table lists information by the day of the month and
time of day (using a 24-hour clock). If you enter “00” as the day, hour, or minute, the
specified event will occur every day, hour, or minute.
Insert Delete
Exit Line Line
F1 F2 F3 F4
2. On the Commands screen, cursor to TABLE EDIT and then press the F3 (Other Tables)
soft key.
3. On the Edit Other Tables screen, cursor to TIME TABLE and then press the F2 (Edit the
Table) soft key.
4. On the Time Table screen, cursor to the desired line and edit the table as described in
steps 6 through 10, as necessary.
5. If there are no entries in the Time Table, press the F2 (Insert Line) soft key.
6. Use the up and down cursor arrow keys to set the desired day.
7. Cursor right one column and set the desired hour with the up and down cursor arrow
keys.
8. Cursor right one column and set the desired minute with the up and down cursor arrow
keys.
2000-OSM, C1 4-33
9. Cursor right one column and select a function using the up and down cursor arrow keys.
The available selections are:
10. Cursor right one column and select the value for the desired function (method number,
valve number, Vista Basic program, etc.). Use the keyboard number keys to enter the
number and then press ENTER.
11. Add more lines by inserting lines and repeating steps 6 through 10 as needed.
12. When you have completed the Time Table, press the F1 (Exit) soft key.
13. On the next screen press the F2 (Exit And Update) soft key to save the Time Table
changes, or press the F1 (Escape) soft key to retain the original values.
14. Press the F1 soft key as necessary to return to the Background screen.
Stream Table
The Stream Table identifies the status of each stream. This identifies the active streams and
the method number and Vista BASIC program assigned to each stream. It also allows you to
edit the table. You access the Stream Table for printing the same way as other tables, but
you access it for viewing or editing differently from other tables.
3. On the Stream Assignment screen (see Figure 4-31) review the stream data and edit as
necessary. This table lists the active streams and the method number and Vista BASIC
program number assigned to each stream. When “00” is in the Vista BASIC column, no
Vista BASIC program is associated with that stream.
4. When you finish editing the stream data, press the F1 (Exit) soft key.
5. On the next screen, press the F2 (Exit and Update) soft key to save the new stream
data, or press the F1 (Escape) soft key to retain the original data.
4-34 2000-OSM, C1
****** Stream Assignment ******
Exit
F1 F2 F3 F4
This report (see Figure 4-32) provides analytical information on each component in a
particular method. The data includes retention time, concentration, uncorrected and
corrected peak heights and areas, slope sensitivity, peak width, start and end times, and
start and end amplitudes. This level of information is often useful to have when
troubleshooting the equipment.
2000-OSM, C1 4-35
Regular Report
This report (see Figure 4-33) summarizes the analytical information on each component in a
given method, providing only retention time and concentration data.
Short Report
This report (see Figure 4-34) gives basic information on the analysis, which you can use to
check analyzer operation periodically. It is a one-line report which provides the stream
number, injection time, and concentration for each component by number. The Short Report
comes in two forms:
• without alarm, which has only the analytical data (shown in Figure 4-34)
• with alarm, which identifies any active alarm (has two-line alarm message above the
report)
ST INJT 01 02 03 04 05 06 07 08 09
01 816 4.96 0.9680 0.5211 3.348 0.6100 0.9982 8876. 0.04273 8860.
This report (see Figure 4-35) automatically prints after each calibration run. Depending on
how you set the parameters, the calibration will update the response factors automatically,
leave them as previously set, or update only when the deviation does not exceed the level
you originally specified.
4-36 2000-OSM, C1
8:09:18 Fri 30 Sep 1988 Stream 10
AIR PURGING
When an area classification indicates combustible gases or particles are present in the air,
and you have an analyzer containing a possible source of ignition located in this
environment, the analyzer may have an air purging system to reduce the degree of risk. The
type of air purge used depends on the classification of the analyzer's environment; the
analyzer is labelled accordingly.
• Y Purge reduces the internal classification of the analyzer from Division I to Division II.
Y and Z Purge
The analyzer has a standard air purge system which will reduce the internal classification by
one level. For a Division I internal classification, this purge system, labeled Y Purge, reduces
the classification to Division II. For a Division II internal classification, this purge system,
labeled Z Purge, will reduce the classification to Nonhazardous/General Purpose. Since the
Y and Z Purge systems are identical except for nomenclature, the following explanation
applies to both.
The purge air enters the analyzer system through a pressure regulator, an orifice, and a
gauge used to set purge flow, and then into the electronics housing where purge air flow is
maintained until a fault condition exists.
1. Loss of purge air supply causes the gauge to indicate lower pressure.
2. Blockage of the first orifice causes the gauge to indicate lower pressure.
3. Blockage of the second orifice causes the gauge to indicate increased pressure.
2000-OSM, C1 4-37
When any of these conditions exists, the GCC will set an *** ALARM *** signal display on
the screen and cause a purge alarm contact to switch. A Y or Z Purge alarm alerts you to the
condition, but it does not turn off the analyzer.
NOTE
Purge time depends on the application. Refer to the analyzer label or Data Package for
specific analyzer purge time.
X Purge Operation
While X Purge (see Figure 4-36 for features and Figure 1-1 for location) is an optional
feature, installations specifying CENELEC certification require it. X Purge reduces risk by two
levels and turns off the analyzer when an alarm occurs.
GND 2 L1(H) 4 L2(N) 6
L2 (NEUT)
CUSTOMER
POWER L1 (HIGH)
CONNECTIONS
GND
When you turn the power ON, X Purge begins monitoring the electronics housing (GCC and
Purge Air Panel) air purge pressure. When the air purge pressure reaches the specified
level, the X Purge starts a timed cycle. If the air purge pressure remains at the specified
level during the timed cycle, X Purge will supply power to the equipment when it completes
the timed cycle. If the air purge pressure drops before the X Purge completes the timed
cycle, X Purge resets the timer and starts over. It continues to reset the timer until the
analyzer achieves and maintains the correct pressure for a complete timed cycle. The X
Purge will not supply power to the analyzer until it sucessfully completes the timed cycle.
The X Purge cycle time depends totally on the application, but it may vary with analyzer
configuration and condition. Refer to the analyzer label or Data Package for specific purge
specifications. Once X Purge applies power to the analyzer, power continues to the analyzer
as long as the electronics housing maintains air purge pressure.
X Purge removes power from the analyzer when the electronics housing air purge pressure
drops below specifications. It locks out power to the analyzer and activates an alarm. The
analyzer has connections available to the customer for connecting the purge alarm to a
visual or audible annunciator located in a constantly monitored area.
4-38 2000-OSM, C1
In order to re-start the analyzer after an X Purge alarm, you must first correct the cause of
the drop in pressure. Then turn the power OFF at the circuit breaker for at least ten seconds
and turn the power back ON. This starts a new X Purge timed cycle, which it must complete
before it will supply power to the analyzer. If you do not correct the cause and cannot
achieve and maintain pressure, the X Purge will not complete the cycle and will not supply
power to the analyzer.
When X Purge removes and locks out power to the analyzer after a drop in electronics
housing purge air pressure (or before pressure has initially attained the specified level), you
can use Override to provide power to the analyzer for troubleshooting or maintenance
purposes. Override does not cancel the X Purge power lockout but temporarily overrides it.
WARNING
CAUTION
Use the X Purge Override Option only for start up, troubleshooting, and maintenance. Do not
leave it on during regular operation of the analyzer. Override requires a well-lighted area to
function. A light sensor inside the X Purge housing allows you to enable Override after you
remove the X Purge housing cover. When you replace the cover, the light sensor cancels
Override.
2. Remove the X Purge housing cover and press the Override button (see Figure 4-36) to
apply power to the analyzer.
NOTE
CENELEC versions of the X Purge have a set screw in the lid that must
be removed before the housing cover can be removed.
4. When you have completed the maintenance and troubleshooting, replace the X Purge
housing cover (and the CENELEC set screw).
5. To cancel Override safely and properly and to reset X Purge, turn the supply power OFF
at the circuit breaker outside the analyzer (for at least ten seconds) and then turn power
ON again.
6. With X Purge reset, the air purge timed cycle begins in the electronics housing.
2000-OSM, C1 4-39
When you use Override during start-up, it overrides the X Purge control of power to the
analyzer, but the air purge timed cycle continues. Once the electronics housing has
pressurized and X Purge completes its timed purge cycle, the analyzer will have power from
the X Purge. If you replace the housing cover without turning the power off at the circuit
breaker, the analyzer will still have power because of X Purge.
If the electronics housing pressure drops during Override use and if the timed cycle is
complete, the X Purge will lock out its power to the analyzer. Since Override bypasses the X
Purge, the analyzer will still have power. If you cancel Override by replacing the housing
cover without turning off the power at the circuit breaker, the X Purge power lock out will
cause the analyzer to be without power. To restart X Purge, you must correct the cause of
the drop in pressure, then turn power OFF (for at least ten seconds), and then ON again.
The X Purge must complete its timed cycle before the analyzer will receive power.
NOTE
The X Purge housing has terminals for connecting a remote control override (see Figure 4-
36), except in CSA certified analyzers. The customer is solely responsible for connecting
and maintaining the remote control switch. This remote control is only to be used during
start-up, maintenance and troubleshooting. The customer must ensure the remotely
controlled override is removed when start-up, maintenance and troubleshooting is
completed.
E2PROM
The Electrical Erasable Programmable Read Only Memory (E2PROM) can store the
following tables and functions.
This feature preserves vital tables and functions if you have power failure. Changing any of
these tables or functions the GCC enters the change into RAM. To preserve the tables and
functions, you must save them to nonvolatile memory (E2PROM).
NOTE
This command saves tables and functions to nonvolatile memory to ensure an analyzer
failure will not erase them.
4-40 2000-OSM, C1
CAUTION
2. On the Commands screen, cursor down to STORAGE & CONFIG. and then press the
F2 (Save or Restore Tables) soft key.
3. On the Table Storage screen (see Figure 4-37), cursor to SAVE TABLES TO E2PROM
and press the F2 (Save Tables) soft key. The tables save to E2PROM.
[ ]
RESTORE TABLES FROM E2PROM
SAVE TABLES TO E2PROM
Escape
F1 F2 F3 F4
4. When “Are You Sure? Y or N” appears on the screen, press the “Y” key on the GCC
front panel to confirm you want to save the tables.
This command restores tables and functions from nonvolatile memory to RAM. It is used
when you have lost RAM for any reason.
2000-OSM, C1 4-41
CAUTION
Restoring tables and functions from E2PROM will erase any tables or
functions already residing in RAM. Since these tables and functions in
E2PROM will replace the tables already in RAM, be certain they are
correct before you perform this sequence.
NOTE
If tables and functions in E2PROM are corrupted, you will not be able to
restore them. To replace the E2PROM contents, re-enter the data from
the Data Sheets or your records and then save it to E2PROM as
described in "Save Tables to E2PROM."
2. On the Commands screen, cursor down to STORAGE & CONFIG. and then press the
F2 (Save or Restore Tables) soft key.
3. On the Table Storage screen (see Figure 4-37), cursor down to RESTORE TABLES
FROM E2PROM and then press the F2 (Restore Tables) soft key.
4. When “Are Your Sure? Y or N” appears on the screen, press the “Y” key on the GCC
front panel to confirm restoring the tables. When the GCC restores the tables to RAM,
they supersede any tables and functions already in RAM.
Physical Description
The Digital Temperature Controller's temperature zones represent areas in the analyzer
having heated components: the Isothermal Oven, the Temperature Programmable Oven, the
LSV, the Methanizer, and the TCD and/or FID cells.
NOTE
Operator Settings
You can set the controller type and the zone functions for the Digital Temperature Controller,
as well as program specific functions in the Method Table. Use the following screens to
make these changes:
4-42 2000-OSM, C1
Manual Temperature Control Mode Valve On/Off
Set Point, by zone
Ramp Rate, by zone
This screen allows operator control of the Digital Temperature Controller. The Manual
Temperature Control Mode screen allows you to change these fields: Valve #, Zone #, Set
Point, and Ramp Rate. Always check the original application-specific temperature limits
listed in the analyzer's Data Package to validate any changes. To access this screen
perform the following steps:
2. On the Manual Control Mode screen, press the F4 (Press. & Temp. Control) soft key.
3. On the Pres and Temp Control screen, cursor to TEMP CONTROL and press the F2
(Manual Temp Control) soft key.
2000-OSM, C1 4-43
4. On the Manual Temperature Control Mode screen (see Figure 4-38), select the desired
field using the Up and Down cursor keys. Enter two digits for valve numbers (e.g. 04),
as some installations have more than nine valves.
F1 F2 F3 F4
5. After you enter changes in the Set Point or Ramp Rate fields, press the F2 (Accept
Control Point) soft key to save the new data.
Data changes made on the screen go to the DTC Backplane PCB, which compares the new
settings with the application-specific temperature limits. If the new settings fall within the
limits, it accepts them and applies them to the analysis.
If entries in the Set Point or Ramp Rate fields fall outside the set limits, the * TEMP BD
ALARM * flashes on the screen’s message line. Temperature Zone specific alarms also
cause the zone name to flash. To identify the type of alarm, press Escape to return to the
Pres & Temp Control Screen, then press the F4 (Alarms) soft key to display the Alarm
Screen. After you note the type of alarm triggered and consult the Data Package for the set
limits, clear the alarm, return to the Manual Temperature Control Screen, and change the
entries to values within the set limits. If the DTC Backplane PCB accepts the new settings,
there will be no * TEMP BD ALARM * display on the screen after you press the F2 (Accept
Control Point) soft key.
Zero All Zones and Span All Zones settings are made in the factory and are not intended to
be changed.
This screen allows you to enter low and high alarm limits and change the temperature zone
names. Always check the original application-specific temperature limits listed in the
analyzer's Data Package to validate any changes. To access the 5 Zone Names and Limits
Table perform the following steps:
4-44 2000-OSM, C1
1. On the Background screen, press the F2 (Manual Control) soft key.
2. On Manual Control Mode screen, press the F4 (Press. & Temp. Control) soft key.
3. On the Pres and Temp Control screen (see Figure 4-39), cursor to TEMP
CONFIGURATION and press the F3 (Names and Limits) soft key.
TEMP CONTROL
PRES CONTROL
TEMP CONFIGURATION
Names
Escape Zone and Controller
Config Limits Type
F1 F2 F3 F4
2000-OSM, C1 4-45
4. On the 5 Zone Names and Limits Table screen (see Figure 4-40), select the desired field
using the cursor keys.
Exit
F1 F2 F3 F4
5. In the Names field you can change the zone name by typing a new name, up to a
maximum of ten characters long. When you have completed the name, cursor to
another field.
6. In the low and high alarm limits field, type the desired alarm value and then cursor to
another field.
7. After you have completed and verified the changes, press the F1 (Exit) soft key.
8. On the next screen, press the F2 (Exit And Update) soft key to save the changes, or
press the F1 (Escape) soft key to retain the original values. Pressing F2 saves the
values in the Name, Low Limit, and High Limit fields.
Configuring SWITCH
SWITCH displayed in the Config column indicates an Isothermal Zone with a temperature
Set Point configured at the factory and not intended to be changed. If it becomes necessary
to change the Set Point, perform the following sequence of steps.
CAUTION
Before opening any analyzer doors, ensure the area is safe and hazard-
free, and will remain so the entire time the analyzer is open. If the
analyzer has X Purge, operate the override function as described in "X
Purge Override Option."
4-46 2000-OSM, C1
1. Open the GCC control panel.
3. On Manual Control Mode screen, press the F4 (Pres & Temp Control) soft key.
4. On the Pres & Temp Control screen, cursor to TEMP CONTROL and then press the F2
(Manual Temp Control) soft key.
5. On the Manual Temperature Control Mode screen, cursor to the Zone # field and enter
the desired zone number (1 - 5).
6. Cursor to the Set Point field and enter the setpoint temperature (the required operating
temperature for this zone).
7. Press the F2 (Accept Control Point) soft key. The GCC displays “Hold Switch on Temp
Board to Accept New Set Point.”
8. Hold down the switch on the DTC Backplane PCB. The GCC displays the message
“Are You Sure?”
9. Continue holding the switch down and press Y on the keyboard to confirm the change.
The GCC sends the new setting to the DTC Backplane PCB where it is checked against
the established limits (this only takes a few seconds).
10. If it accepts the new temperature, the temperature appears on the screen in the Set
Point field. Release the switch and close the front panel.
11. If the GCC does not accept the Set Point, Temp Zone name flashes and * TEMP BD
ALARM * flashes on the message line. If this happens, release the switch and check
the temperature with the T-Rating on the Manual Temperature Control Mode screen.
12. Enter a set point temperature within T-Rating limits by repeating steps 5 through 10.
13. If you do not hold the switch long enough, * TEMP BD ALARM * will also display and the
new setting will not be accepted. Check the temperature with the T-Rating on the
Manual Temperature Control Mode screen and the temperature setting specified in the
Data Package and repeat steps 5 through 10.
14. To cancel the alarm press the F1 (Escape) soft key to return to the Pres & Temp Control
screen.
15. Verify that TEMP CONTROL is selected and press the F4 (Alarms) soft key to display
the alarm explanation on the Alarm Screen.
16. After noting the alarm explanation, press the F2 (Clear Alarms & Exit) soft key. If the
GCC cannot clear the alarm due to other activity, press the F1 (Exit) soft key and clear
the alarm as soon as possible.
17. Return to the Manual Temperature Control Mode screen and repeat steps 5 through 10
to set a temperature for a SWITCH Configured Isothermal Zone.
2000-OSM, C1 4-47
Temperature Control Table
This screen allows you to select zone names and change set points and ramp rates, all
related to the time they occur in the analysis method. To access this screen perform the
following steps:
2. On the Commands screen, cursor to TABLE EDIT and press the F2 (Methods) soft key.
3. On the Methods Table #?? screen, enter the number of the Method Table to be changed
and press the F2 (Edit the Table) soft key.
4. On the Cal Define & Cycle Time screen, press the F1 (Continue) soft key.
5. On the Method Table screen (see Figure 4-41), cursor to the appropriate line in the Time
field, or press the Insert Line soft key to insert a new line (just below the cursor) and
enter the time into the cycle when the function is to be performed.
6. Cursor to the Function field and scroll to Temp Contrl. In Figure 4-41, with Temp Contrl
in the Function field the Value column lists Two as the function to be performed from the
Temperature Control Table.
F1 F2 F3 F4
7. Move the cursor to the Value column and the Temperature Control Table appears, with
the cursor on Entry line 02 (see Figure 4-42). Note the Entry line number when you
enter the table so you can exit the table from the same line, if desired.
4-48 2000-OSM, C1
***** Temperature Control *****
Set Point Ramp Rate
Entry Zone C C/MIN
01 Temp Zone1 150.0 25.00
[02] Temp Zone1 250.0 50.00
03 Temp Zone1 100.0 01.00
04 Temp Zone1 0.000 0.000
05 Temp Zone1 0.000 0.000
06 Temp Zone1 0.000 0.000
07 Temp Zone1 0.000 0.000
08 Temp Zone1 0.000 0.000
More Below
Exit
F1 F2 F3 F4
8. On the Temperature Control screen, move the cursor as necessary to select the Zone
Name from among the names in the list, and to change Set Point and Ramp Rate
values of the desired entries.
CAUTION
When you exit the Temperature Control screen, the value in the Entry
line highlighted when you exit becomes the Value entry in the Method
Table. Unless you want to change the Value entry, exit on the same
Entry line number that you entered the Temperature Control screen.
9. Verify the changed values and place the cursor on the desired Entry number. Then
press the F1 (Exit) soft key.
This screen allows you to select zone names and change alarm temperature values and
alarm methods, all related to the time they occur in the analysis method. To access this
screen perform the following steps:
2. On the Commands screen, cursor to TABLE EDIT and press the F2 (Methods) soft key.
3. On the Methods Table #?? screen, enter the number of the Method Table to be changed
and press the F2 (Edit the Table) soft key.
4. On the Cal Define & Cycle Time screen, press the F1 (Continue) soft key.
2000-OSM, C1 4-49
5. On the Method Table screen (see Figure 4-41), cursor to the appropriate line in the Time
field, or press the Insert Line soft key to insert a new line (just below the cursor) and
enter the time into the cycle when the function is to be performed.
6. Cursor to the Function field and scroll to Temp Check. In Figure 4-41, with Temp Check
in the Function field the Value column lists One as the function to be performed from the
Temperature Check Table.
7. Move the cursor to the Value column and the Temperature Check Table appears, with
the cursor on Entry line 01 (see Figure 4-43). Note the Entry line number when you
enter the table so you can exit the table from the same, if desired.
8. On the Temperature Check screen, move the cursor as necessary to select the Zone
Name and to change less than (<), more than (>), alarm value, and the alarm mode of
the desired entries.
CAUTION
When you exit the Temperature Check screen, the value in the Entry
line highlighted when you exit becomes the Value entry in the Method
Table. Unless you want to change the Value entry, exit on the same
Entry line number that you entered the Temperature Check screen.
Exit
F1 F2 F3 F4
9. Verify the changed values and place the cursor on the desired Entry number. Then
press the F1 (Exit) soft key.
4-50 2000-OSM, C1
Controller Type
There are several types of temperature controllers, such as Sulfur, Sparger, PINA, PNA, and
Regular. This screen is set at the factory and should not have to be changed. If you want to
verify the setting, perform the following steps.
2. On the Manual Control Mode screen, press the F4 (Press. & Temp. Control) soft key.
3. On the Pres and Temp Control screen (see Figure 4-39), cursor to TEMP
CONFIGURATION and press the F4 (Controller Type) soft key.
4. On the Controller Type screen (see Figure 4-44), verify that the controller type is the
same as specified in the Data Package.
Exit
Escape and
Update
F1 F2 F3 F4
5. If you want to change the controller type, use the cursor arrow keys to select the desired
type and then press the F2 (Exit and Update) soft key to save the changes, or press the
F1 (Escape) soft key to retain the original controller type.
6. If you made changes, "Hold Switch on Temp Board" will appear on the screen.
7. Open the GCC Front Panel and hold down the switch on the DTC Backplane PCB.
8. The CRT will display the message, "Are You Sure? Y or N." Continue holding the
switch down and press "Y" on the GCC keyboard to accept the change.
2000-OSM, C1 4-51
9. If the change is accepted, an acknowledging message appears on the screen. Release
the switch and close the front panel.
10. Press the F1 soft key as necessary to return to the Background screen.
This screen allows you to select temperature zone names and sensor types. It also allows
you to select the heat/air relationship in zones 3 and 4. To access the Temperature
Configuration Table perform the following steps:
2. On the Manual Control Mode screen, press the F4 (Press. & Temp. Control) soft key.
3. On the Pres and Temp Control screen (see Figure 4-39), cursor to TEMP
CONFIGURATION and press the F2 (Zone Config) soft key.
4. On the Temp Config Table screen (see Figure 4-45), select the desired field using the
cursor keys.
Exit
F1 F2 F3 F4
5. In the Config field, you can change the temperature configuration by scrolling through
the list of titles and selecting the appropriate one for this zone, then cursor to another
field. The five Temperature Zone configuration choices are:
INACT Inactive
SWITCH Isothermal Controlled by toggle switch on Temp. Control PCB
ISO Isothermal Regular
PROG Programmable
PROG/C Programmable with Vortex Cooler
4-52 2000-OSM, C1
NOTE
6. In the Sensor field, you can toggle between Probe and TC. Refer to the Data Package
to ensure you select the appropriate sensor type.
7. In the Remove Heat On Air Loss field you can toggle between Yes and No. Refer to the
Data Package to ensure you make the appropriate selections.
8. After you have completed and verified the changes, press the F1 (Exit) soft key.
9. On the next screen, press the F2 (Exit And Update) soft key to save the changes, or
press the F1 (Escape) soft key to retain the original values.
CAUTION
Before opening any analyzer doors, ensure the area is safe and hazard-
free, and will remain so the entire time the analyzer is open. If the
analyzer has X Purge, operate the override function as described in "X
Purge Override Option."
11. Open GCC Front Panel and hold down the switch on the DTC Backplane PCB.
12. The screen will display the message, “Are You Sure? Y or N.” Continue holding the
switch down and press “Y” on the GCC keyboard to accept the change.
13. If the GCC accepts the change, an acknowledging message appears. Release the
switch and close the front panel.
14. On the Pres and Temp Control screen, cursor to TEMP CONFIGURATION and press
the F2 (Zone Config) soft key.
15. Verify that changes have been accepted and then press the F1 soft key as necessary to
return to the Background screen.
If the GCC accepts the new configuration settings, they appear on the screen in the
appropriate fields. If it does not accept them, the field settings do not change and a *TEMP
BD ALARM* signal appears. If you do not hold the switch long enough, a *TEMP BD
ALARM* signal appear and the new settings will not be accepted. Check the established
limits for the settings in the Data Package and try again.
Programming Notes
There are two types of programmable zones, standard programmable zone (PROG) and
programmable zone with the vortex cooler (PROG/C). You can program both types of
programmable zones from the Manual Temperature Control Mode screen.
2000-OSM, C1 4-53
The maximum value of Ramp Rate for any PROG or PROG/C zone is 50° C/minute, in
increments of one-tenth of a degree. Setting a Ramp Rate of 0.0° C/minute causes the
temperature controller to maintain the present temperature. A Ramp Rate of 50° C/minute
sends the temperature zone as rapidly as possible to the intended setpoint. This happens
without consideration of true rate or out of control conditions.
Programming for the PROG and PROG/C zones differs only in the cool down ramp rate. In
zones programmed as PROG/C, a coolant solenoid rapidly cools down the zones. This
solenoid activates when it receives a Ramp Rate of 0.1° C/minute. Once the solenoid
recognizes the 0.1° C setting, it forces vortex cooled air into the programmed zone to cool it
down. The rate of cool down depends solely on the zone temperature and the volume of the
cool air. Once the zone reaches the lower set point, power is applied to the heater for this
zone to maintain the new set point while the cool air is still flowing. The coolant solenoid
stops the air flow when a ramp rate other than 0.1° C/minute is received.
Both Set Points and Ramp Rates may originate from a Method Table being run automatically
by the GCC, or the Workstation, or may be entered manually on the Manual Temperature
Control Mode screen.
The last programming information entered runs the analysis, whether entered on the Manual
Temperature Control Mode screen or in the Method Table.
NOTE
On power loss, Set Points and Ramp Rates for all programmable zones
(PROG and PROG/C) are lost. You must re-enter the Values manually
or execute the method stored in the Method Table.
Alarms
The optional Electronic Pressure Control (EPC) replaces the mechanical regulators and
gauges in the Pressure Control Panel. The EPC provides up to five individually controlled
pressure zones.
Physical Description
The EPC is comprised of an Electronic Pressure Control Multibus PCB and an EPC Module
which contains up to five pressure zones.
NOTE
The EPC is set up at the factory and should not require adjustment on
site.
4-54 2000-OSM, C1
Operator Settings
You can set the zone functions for the EPC and also program specific functions in the
method tables. The functions you can set or program appear on the following screens:
Screen Function
This screen allows operator control of the Electronic Pressure Controller. The Manual
Pressure Control Mode screen allows you to change these fields: Enter Valve, Zone #, Set
Point, and Ramp Rate. Always check the original application-specific pressure limits listed in
the Data Package provided with the analyzer to ensure any changes are valid. To access
this screen perform the following steps:
2. On the Manual Control Mode screen press F4 (Press. & Temp. Control).
2000-OSM, C1 4-55
3. On the Pres and Temp Control screen (see Figure 4-46), cursor to PRES CONTROL
and press F2 (Manual Pressure Control).
TEMP CONTROL
PRES CONTROL
TEMP CONFIGURATION
F1 F2 F3 F4
4. On the Manual Pressure Control Mode screen (see Figure 4-47), select the desired field
to change using the cursor arrow keys. Enter two digits for valve numbers (e.g. 04), as
some installations have more than nine valves.
Accept Calibrate
Escape Control Zone
Point
F1 F2 F3 F4
4-56 2000-OSM, C1
5. After you enter and verify your changes, press F2 (Accept Control Point) to save the
new data.
The Electronic Pressure Control Multibus PCB compares the data changes made on the
screen with the application-specific pressure limits. If the new settings are within the limits,
they will be accepted and applied to the analysis.
If the Set Point (SP) or Ramp Rate (Rate) values are not within the set limits, the *
PRES BD ALARM * flashes on the screen’s message line. Pressure Zone specific alarms
also cause the zone name to flash. To identify the type of alarm, press Escape to return to
the Pres & Temp Control Screen, then press F4 (Alarms) to display the Alarm Screen. After
noting the type of alarm triggered and consulting the Applications Package for the set limits,
clear the alarm, return to the Manual Pressure Control Screen, and change the entries to
values within the set limits. If the new settings are accepted, there will be no * PRES BD
ALARM * display on the screen after F2 (Accept Control Point) is pressed.
Calibrate Zone settings are made in the factory and are not intended to be changed.
This screen allows you to enter a pressure range, change the configuration choices, and
change the pressure zone names. Always check the original application-specific pressure
limits listed in the analyzer's Data Package to ensure any changes are valid. To access the
Pressure Configuration Table perform the following steps:
2. On the Manual Control Mode screen press F4 (Press. & Temp. Control).
3. On the Pres and Temp Control screen, cursor to PRES CONTROL and press F3
(Pressure Config).
2000-OSM, C1 4-57
4. On the Pressure Config Table screen (see Figure 4-48), select the desired field using
the cursor keys.
Exit
F1 F2 F3 F4
5. In the Name field you can change the zone name by typing a new name, up to a
maximum of ten characters long. When you have completed the name, cursor to
another field.
6. In the Config field, you can change the pressure configuration by scrollling through the
list of titles and selecting the appropriate one for this zone, then cursor to another field.
7. In the Range field, type the range value and then cursor to another field.
9. On the next screen press F2 (Accept Control Point) to save the changes, or press F1
(Escape) to retain the original values.
CAUTION
Before opening any analyzer doors, ensure the area is safe and hazard-
free, and will remain so the entire time the analyzer is open. If the
analyzer has X Purge, operate the override function as described in "X
Purge Override Option."
11. Open the GCC Front Panel and hold down the switch on the Electronic Pressure Control
PCB.
4-58 2000-OSM, C1
12. The screen will display the message, “Are You Sure? Y or N.” Continue holding the
switch down and press “Y” on the GCC keyboard to accept the change.
13. If the GCC accepts the change, an acknowledging message appears. Release the
switch and close the front panel.
14. On the Pres and Temp Control screen, cursor to PRES CONTROL and press F3
(Pressure Config).
15. Verify that changes have been accepted and then press F1 as necessary to return to
the Background screen.
If the GCC accepts the new configuration settings, it displays them on the screen in the
appropriate fields. If it does not accept them, the field settings do not change and a *PRES
BD ALARM* signal is displayed. If you do not hold down the switch long enough, a *PRES
BD ALARM* signal will display and the new settings will not be accepted. Check the
established limits for the settings in the Data Package and try again.
Configuring SWITCH
SWITCH displayed in the Config column on the Manual Pressure Control Mode screen or
the Pressure Config Table screen indicates a zone with a pressure Set Point that is not
intended to be changed. If it becomes necessary to change the Set Point, perform the
following steps.
CAUTION
Before opening any analyzer doors, ensure the area is safe and hazard-
free, and will remain so the entire time the analyzer is open. If the
analyzer has X Purge, operate the override function as described in "X
Purge Override Option."
3. On the Manual Control Mode screen press F4 (Pres & Temp Control).
4. On the Pres & Temp Control screen, cursor to PRES CONTROL and then press F2
(Manual Pressure Control).
5. On the Manual Pressure Control Mode screen, cursor to the Zone # field and enter the
desired zone number (1 - 5).
6. Cursor to the Set Point field and enter the setpoint pressure (the required operating
pressure for the component in this zone).
7. Press F2 (Accept Control Point). The GCC displays “Hold Switch on Pres Bd to Accept
SP.”
8. Hold down the switch on the Electronic Pressure Control PCB. The GCC displays the
message “Are You Sure?”
2000-OSM, C1 4-59
9. Continue holding the switch down and press Y on the keyboard to execute the change.
The GCC sends the new setting to the Electronic Pressure Control Multibus PCB where
it is checked against the established limits (this only takes a few seconds).
10. If the new pressure is accepted, it is displayed on the screen in the Set Point field.
Release the switch and close the front panel.
11. If the Set Point is not accepted, the Pres Zone name flashes and * PRES BD ALARM *
flashes on the message line. If this happens, release the switch and check the pressure
with the pressure limits prescribed for this zone.
12. Enter a set point pressure within these limits by repeating steps 5 through 10.
13. If the switch is not held long enough * PRES BD ALARM * will also be displayed and the
new setting will not be accepted. Check the pressure with the pressure setting specified
in the Data Package and repeat steps 5 through 10.
14. To cancel the alarm press F1 (Escape) to return to Pres & Temp Control screen.
15. Verify that PRES CONTROL is selected and press F4 (View Alarms) to display the alarm
explanation on the Alarm Screen.
16. After noting the alarm explanation, press F2 (Clear Alarms & Exit). If the GCC cannot
clear the alarm due to other activity, press F1 (Exit) and clear the alarm as soon as
possible.
17. Return to the Manual Pressure Control Mode screen and repeat steps 5 through 10 to
set a pressure for a SWITCH Configured Zone.
This screen allows you to select zone names and change set points and ramp rates, all
related to the time they occur in the analysis method. To access this screen:
3. On the Methods Table #?? screen, enter the number of the Method Table you want to
change and press F2 (Edit the Table).
5. On the Method Table screen (see Figure 4-49), cursor to the appropriate line in the Time
field, or press the Insert Line soft key to insert a new line (just below the cursor) and
enter the time into the cycle when the function is to be performed.
6. Cursor to the Function field and scroll to Pres Contrl. In Figure 4-49, with Pres Contrl
displayed, the Value column lists Two as the function to be performed.
4-60 2000-OSM, C1
***** Method Table #01 *****
F1 F2 F3 F4
7. Move the cursor to the Value column and the Pressure Control Table appears, with the
cursor on Entry line 02 (see Figure 4-50). Note the Entry line number when you enter
the table so you can exit the table from the same line, if desired.
Exit
F1 F2 F3 F4
2000-OSM, C1 4-61
8. On the Pressure Control screen, move the cursor as necessary to select the Zone
Name from among the names in the list, and to change Set Point and Ramp Rate
values of the desired entries.
CAUTION
When you exit the Pressure Control screen, the Entry line highlighted
when you exit becomes the Value entry in the Method Table. Unless
you want to change the Value entry, be sure to exit on the same Entry
line number on which you entered the Pressure Control screen.
9. Verify the changed values and place the cursor on the desired Entry number. Then
press F1 (Exit).
This screen allows you to select zone names and change alarm pressure values and alarm
methods, all related to the time they occur in the method. The Pressure Check Table is
reached from the Method Table as follows:
3. On the Methods Table #?? screen, enter the number of the Method Table you want to
change and press F2 (Edit the Table).
5. On the Method Table #01 screen (see Figure 4-49), cursor to the appropriate line in the
Time field, or press the Insert Line soft key to insert a new line (just below the cursor)
and enter the time into the cycle when the function is to be performed.
6. Cursor to the Function field and scroll to Pres Check. In Figure 4-49, with Pres Check in
the Function field the Value column lists One as the function to be performed from the
Pressure Check Table.
7. Move the cursor to the Value column and the Pressure Check Table appears, with the
cursor on Entry line 01 (see Figure 4-51). Note the Entry line number when you enter
the table so you can exit the table from the same, if desired.
4-62 2000-OSM, C1
***** Pressure Check *****
Pressure
Entry Zone psi Action
[01] Pres Zone1 < 0.0000 Abort
02 Pres Zone1 < 0.0000 Display
03 Pres Zone1 < 0.0000 Abort
04 Pres Zone1 < 0.0000 Display
05 Pres Zone1 < 0.0000 Display
06 Pres Zone1 < 0.0000 Display
07 Pres Zone1 < 0.0000 Display
08 Pres Zone1 < 0.0000 Display
More Below
Exit
F1 F2 F3 F4
8. On the Pressure Check screen, cursor to select the Zone Name and to change less
than (<), more than (>), alarm value, and alarm mode of the desired entries.
CAUTION
When you exit the Pressure Check screen, the Entry line highlighted at
exit becomes the Value entry in the Method Table. Unless you want to
change the Value entry, be sure to exit on the same Entry line number
on which you entered the screen.
9. Verify the changed values and place the cursor on the desired Entry number. Then
press F1 (Exit).
Alarms
Electronic Pressure Control alarms are described in "Pressure Board" alarms in Section 6.
When a pressure alarm occurs, it displays as *** ALARM *** flashing on the Background
screen and * PRES BD ALARM * flashing on the Manual Pressure Control Mode screen. To
identify the specific alarm, press the F4 (Alarms) soft key on the Background screen.
General
This is a standard feature on GCCs which have the VistaNET option, but it is optional on all
other units. Raw chromatogram storage gives GCCs the ability to remember an analysis
under a user specified condition (i.e., an alarm), after which the analysis can be checked for
problems. Checking involves looking at the chromatogram, feeding data back through the
controller (as if it were coming from the detector), and generating reports.
2000-OSM, C1 4-63
The raw chromatogram storage and reprocessing option allows only one chromatogram of
each type to be saved (last, calibration, benchmark, typical or alarm), regardless of the
length of the cycle. When the chromatogram is saved, the Raw Data Report is saved also
(but method tables are not saved). Raw chromatograms are saved in GCC memory but they
are not saved on E2PROM. You can save and release raw chromatograms manually or
automatically.
You can view the saved chromatogram on the screen and send the report to the printer. The
GCC does this by feeding the chromatogram back through the controller, allowing the
controller to reprocess it off-line, then displaying it on the screen and sending the report to
the printer.
Select the Raw Chromatogram Storage and Reprocessing option from the Commands
screen, as shown in Figure 4-52.
ANALYSIS CONTROL
REPORTS
TABLE EDIT
PRINTER
STORAGE & CONFIG.
NAMES
MISC.
TESTING/SETUP
[CHROMATOGRAM STORAGE]
F1 F2 F3 F4
To use this feature, ensure the GCC has sufficient memory to save chromatograms, save the
desired chromatograms, then display, save and reprocess chromatograms.
Before you select any chromatograms to save, first verify the status of available memory for
this purpose as follows:
1. On the Commands screen, cursor to CHROMATOGRAM STORAGE and then press the
F2 (Display Saved Data) soft key.
2. On the Display Saved Data screen, cursor to MEMORY USED/LEFT and press the F2
(Execute the Command) soft key. The Raw Chromatogram Memory Used/Left screen
will appear (see Figure 4-53).
4-64 2000-OSM, C1
**** Raw Chromatogram Memory Used/Left ****
Escape
F1 F2 F3 F4
This screen shows the total memory used and left, and the amount used by each saved
chromatogram. The available GCC memory resides in two separate “pools” that cannot be
shared: memory available for saving raw chromatograms (304KB), and memory available
for building operational tables and saving the Raw Data Reports with the chromatograms
(192KB).
The GCC saves the current analysis. At cycle end, the GCC determines if its program
specifies the analysis just saved as a type to be automatically saved. If it does not specify it
for automatic saving, the GCC erases the current analysis data from memory.
Chromatogram storage uses from 2 to 4 KB of memory for each minute of analysis cycle.
When estimating the memory needed, calculate 4 KB/cycle minute (e.g., 20 KB for a 5
minute cycle, 80 KB for a 20 minute cycle). Alarms and warning signals indicate when either
memory pool runs low. The GCC displays the message NOT ENOUGH MEMORY, NOT
SAVED if the 304KB pool empties or runs low.
If the GCC does not have enough memory, you must erase (release) some saved data. This
screen identifies analyses saved and memory used under “Type/Lock.” You can erase all
saved analyses or one saved analysis at a time (see next subsection).
When the GCC does not have sufficient memory to save new chromatogram data, you must
erase (release from memory) existing chromatograms. First you must identify which
chromatograms to erase. Then perform the following steps to erase these chromatograms:
2000-OSM, C1 4-65
2. Cursor to CHROMATOGRAM STORAGE and press the F2 (Define Save And Release)
soft key.
3. On the Define Save/Release screen, cursor to MANUAL RELEASE and then press the
F2 (Execute The Command) soft key.
4. On the Manually Release Analysis screen, select the type of data to release and press
the F2 (Manually Release Analysis) soft key. If you want to release more than one
analysis, you must select the type of data separately for each analysis released.
Alternatively, you can release all analyses at once by pressing the F3 (Release All
Analyses) soft key.
5. After you have released (erased) all desired data, press the F1 (Escape) soft key to
return to the Display Saved Data menu screen.
Saving Chromatograms
You must save chromatograms before you can display or reprocess them. You can save
chromatograms either manually or automatically.
2. On the Define Save/Release screen, cursor to MANUAL SAVE and then press the F2
(Execute The Command) soft key.
3. On the Manual Save Analysis screen, select which type of chromatogram you want to
save.
4. Next select how you want this chromatogram saved (as a calibration analysis,
benchmark, etc.)
5. Verify your selections and press the F2 (Manually Save Analysis) soft key.
6. When you have completed saving analyses, press the F1 soft key as necessary to
return to the Commands screen.
2. On the Define Save/Release screen, cursor to AUTO SAVE/RELEASE and then press
the F2 (Execute The Command) soft key.
3. On the Automatically Save Analyses screen (see Figure 4-54), select which types of
chromatograms you want to save. If you do not want any data saved automatically,
select No for each entry.
4. Note the number under Alarm Mask. This represents the alarm configuration set on the
Define Alarm Mask screen. If you want to verify or change the alarm mask, press the F4
(Expand Alarm Mask) soft key.
4-66 2000-OSM, C1
****** Automatically Save Analyses ******
Expand
Exit Alarm
Mask
F1 F2 F3 F4
5. On the Define Alarm Mask screen, select No or Yes, as applicable, for each alarm
category. The No/Yes designations (the choices are underlined) specify which alarms
the GCC should watch for when gathering data to be saved as the alarm analysis. Each
arrangement of alarm choices on this screen is represented by a different set of
numbers in the Alarm Mask field on the Automatically Save Analyses Screen.
6. Verify your selections and press the F1 (Continue) soft key. This returns you to the
Automatically Save Analyses screen.
7. On the Automatically Save Analyses screen, verify your selections and then press the
F1 (Exit) soft key.
8. On the second Automatically Save Analyses screen, press the F2 (Exit And Update) soft
key to save your changes, or press the F1 (Escape) soft key to retain the original
values.
9. When you have completed saving analyses, press the F1 soft key as necessary to
return to the Commands screen.
Once you have saved a chromatogram, you can display the chromatogram and print its raw
data report.
Displaying a Chromatogram
1. On the Display Saved Data screen, cursor to GRAPHICS and press the F2 (Execute
The Command) soft key.
2000-OSM, C1 4-67
2. On the Graphics Setup screen, select the type of chromatogram to save: Calibration
(Cal), Benchmark (Bench), most recent (Last), Alarm, or typical (Typ).
3. Next select the amount of screen offset, which determines where on the screen the
chromatogram will display. Start with “0” and adjust if necessary.
4. Then select the amount of screen attenuation, to ensure the entire chromatogram will
appear on the screen.
6. Set the chromatogram’s start time ("0" to start at the beginning of the analysis).
7. Set the end time according to how much of the analysis you want to see.
8. Verify the selections and then press the F2 (Execute The Command) soft key. The
chromatogram will start to scroll on the display screen.
9. Press the F1 (Escape) soft key to return to the Display Saved Data screen.
2. On the Send Report To Printer screen, select the type of data to be printed.
3. Next select whether you want calibration and benchmark data printed as raw data.
4. Verify the selections and press the F2 (Send Report To Printer) soft key. “The
Command is being updated” will appear on the message line and the raw data report
will be printed. The report will not appear on the display screen.
5. Press the F1 (Escape) soft key to return to the Display Saved Data screen.
The Reprocess Saved Data Screen (soft key F3 on the Command Screen) allows you to
select type of raw data to reprocess, how to process it, whether to send the report to the
VWS (No/Yes) and whether to update Alarms, Trends and Digitals (No/Yes).
Reprocessing takes saved data and sends it back through peak detection in an off-line
mode, then produces a report available to the VWS or VistaNET (but not displayed on the
screen). Because reprocessing uses some of the same program functions as the analysis,
the GCC cannot run a real analysis and reprocess a saved analysis at the same time. To
reprocess a chromatogram, perform the following steps:
2. On the Commands screen cursor to CHROMATOGRAM STORAGE and then press the
F3 (Reprocess Saved Data) soft key.
3. On the Reprocess Saved Raw Chromatogram screen (see Figure 4-55), select the type
of chromatogram to be reprocessed.
4-68 2000-OSM, C1
*** Reprocess Saved Raw Chromatogram ***
Process
As: Cal Bench Last
Method Table: 1
Report To VWS: No Yes
Update Alarms, Trends and Digitals: No Yes
Execute
Escape The
Command
F1 F2 F3 F4
6. Select whether you want the resulting raw data report sent to the VWS or VistaNET and
whether you want alarms, trends, and digitals to be updated.
7. After you complete the entries, verify the selections and press the F2 (Execute The
Command) soft key. The reprocessed chromatogram appears on the display and, if you
so selected, the data report will be sent to the VWS or VistaNET.
8. When the chromatogram is complete, if you have no further data to reprocess press the
F1 soft key as necessary to return to the Background screen. If you want to reprocess
another chromatogram, repeat steps 2 through 7.
The analyzer can operate with other ABB GCC front panels. To implement this option
requires the following changes to the analyzer: an optional PCB and several changes in
wiring connections and switch settings. This section of the manual explains how to prepare
the analyzer for remote operation and how to operate it in this configuration.
The optional Local Communications Module (LO COMM) PCB provides the remote access
for the analyzer. The analyzer has this board, mounted on the Front Panel PCB located
2000-OSM, C1 4-69
inside the GCC (see Figure 4-56), only when remote operation is specified. The LO COMM
PCB connections terminate at TB4 in the GCC cabinet.
LO COMM
FRONT PCB
PANEL PCB
LO COMM DISPLAY
CABLE PANEL
Each LO COMM PCB has a unique address to ensure positive communication. Switch SW1,
an eight-position dip switch on the LO COMM PCB (see Figure 4-57), sets this address.
LO COMM 0 1
CABLE
1
2
3
4
5
6
7
SW1
8
OFF ON
SW2
The first five switch positions on SW1 (labeled 0 through 4 on the PCB), determine the
analyzer's address. Switch positions 6, 7 and 8 are always ON ("1"). Figure 4-58 shows
how to identify the address from the switch positions.
4-70 2000-OSM, C1
Switch No. Switch No.
5 4 3 2 1 5 4 3 2 1
1 1 1 1 1 #1 0 1 1 1 1 #17
1 1 1 1 0 #2 0 1 1 1 0 #18
1 1 1 0 1 #3 0 1 1 0 1 #19
1 1 1 0 0 #4 0 1 1 0 0 #20
1 1 0 1 1 #5 0 1 0 1 1 #21
1 1 0 1 0 #6 0 1 0 1 0 #22
1 1 0 0 1 #7 0 1 0 0 1 #23
1 1 0 0 0 #8 0 1 0 0 0 #24
1 0 1 1 1 #9 0 0 1 1 1 #25
1 0 1 1 0 #10 0 0 1 1 0 #26
1 0 1 0 1 #11 0 0 1 0 1 #27
1 0 1 0 0 #12 0 0 1 0 0 #28
1 0 0 1 1 #13 0 0 0 1 1 #29
1 0 0 1 0 #14 0 0 0 1 0 #30
1 0 0 0 1 #15 0 0 0 0 1 #31
1 0 0 0 0 #16 0 0 0 0 0 #32
Address
NOTE
Switch SW2 on the LO COMM PCB provides two other user-selected switch settings. The
PCB labels these “No Analyzer” and “Lock Out Remote.” The OFF position is to the left of
SW2 as it is shown in Figure 4-57.
NOTE
When you set the No Analyzer switch ON, the front panel will communicate only with other
GC’s; the front panel will not communicate with an attached analyzer.
2000-OSM, C1 4-71
When the Lock Out Remote switch is ON, another front panel on the network cannot access
this front panel, but this front panel can access other network front panels.
Remote Operation
To understand remote mode operation, visualize the LO COMM PCB as directing analyzer
data traffic along three different routes.
• When the operator at this display/keyboard communicates only with this analyzer, data
runs back and forth between the display/keyboard and the analyzer. This represents
the standard, or stand-alone, mode of operating the analyzer.
• When the operator at this display/keyboard communicates with a remote GCC, data
runs back and forth between this display/keyboard and the remote GCC.
• When the operator at a remote display/keyboard communicates with this analyzer, data
runs back and forth between the remote GCC and this analyzer.
Since the remote mode functions simply by establishing communication routes, operating an
analyzer from a remote location is virtually identical to local operation once you establish the
communication link. The only differences are a remote front panel status message and the
method by which recorder outputs are handled.
1. From any screen menu, press and release the following keys in sequence: “Upper,”
“Enter,” “R”.
2. The Remote Front Panel Mode menu appears on the screen (see Figure 4-59). This
mode starts automatically if you turn power ON with No Analyzer switch ON.
CLEAR
EXIT ENTRY EXECUTE
F1 F2 F3 F4
4-72 2000-OSM, C1
3. Enter the number of the remote analyzer you want to access. Verify you have entered
the number correctly and then press the F3 (EXECUTE) soft key.
4. If you entered the remote number incorrectly, press the F2 (CLEAR ENTRY) soft key,
re-enter the number, and then press the F3 (EXECUTE) soft key.
NOTE
5. After a short time the Background screen will appear, with the remote number shown at
the top left of the screen in reverse video.
6. At the remote analyzer, a message appears on the screen indicating that analyzer is
being remotely controlled (see Figure 4-60).
OVERRIDE
REMOTE
OPERATOR
F1 F2 F3 F4
7. The only active keys on the remote GCC’s front panel are the soft keys. All other keys
are locked out until the accessing operator logs off the GCC or the operator at the
remote analyzer presses the OVERRIDE REMOTE OPERATOR soft key.
8. Use the screen and front panel keys as necessary to obtain the information desired. All
commands and displayed data will reflect what is happening at the remote analyzer.
9. When you complete the remote activity, press “Upper,” “ENTER,” “R”, to return to the
Remote Front Panel Mode screen.
10. On the Remote Front Panel Mode screen, press the F1 (EXIT) soft key to exit remote
mode and return to normal operation of the analyzer. Wait for the screen to
resynchronize before attempting any operations.
2000-OSM, C1 4-73
ANALOG OUTPUT OPTION
This option provides analog outputs to a printer, computer, or other external device. Up to
two optional PCBs, installed in the GCC Card Cage, provide different combinations of current
and voltage outputs. These combinations are:
• one voltage board (with up to 16 output channels) and one current board (with up to 16
output channels
With the current board, the output signal ramps from 4 to 20 ma in proportion to the signal
level. If the output is below the specified low range, the output signal will indicate the lowest
possible signal. If the output is above the specified high range, the output signal will indicate
the highest possible signal.
With the voltage board, the output signal ramps from 0 to 5 vdc in proportion to the signal
level. If the output is below the specified low range, the output signal will indicate the lowest
possible signal. If the output is above the specified high range, the output signal will indicate
the highest possible signal.
The Trend Table screen controls the Analog Output option. This screen lists each available
channel, the associated stream, the component being measured, and the low and high range
values for that component (see Figure 4-61). If you select stream “00” for a particular
channel, then the specified component will apply on that channel for all streams. At the end
of each analysis, each analog output sends the latest current or voltage value to the external
device connected to the Analog Output. When this value is between the low and high range
limits, the analog output represents a proportion of the difference between low and high. If
the analog output is outside the limits, the board will supply its lowest or highest possible
value.
3. On the Commands screen, cursor down to TABLE EDIT and then press the F3 (Other
Tables) soft key.
4. On the Edit Other Tables screen, cursor to TREND TABLE, if necessary, and then press
the F2 (Edit The Table) soft key.
5. When the first Trend Table screen appears, cursor across and down the table to
highlight a value you want to change. Then insert the new value.
6. When you have completed the changes to this Trend Table screen, review them to
ensure all items are correct and then press the F1 (Exit) soft key.
4-74 2000-OSM, C1
****** Trend Table ******
Range Range
Chan Stream Comp Low High
01 01 01 1.0000 100.00
03 01 03 0.5000 100.00
04 02 01 1.0000 100.00
05 02 02 0.5000 100.00
06 02 03 0.5000 100.00
07 08 01 1.0000 100.00
08 08 02 0.5000 100.00
More Below
Insert Delete
Exit Line Line
F1 F2 F3 F4
7. On the second Trend Table screen, press the F2 (Exit and Update) soft key to save the
changes or press the F1 (Escape) soft key to retain the original values.
The digital output channels provide component high and low alarm warnings, independent of
any other alarms in the analyzer. No alarms or other indications occur when component
concentrations are within their specified ranges, but if a component goes outside the
specified range it changes the state of the appropriate digital contact. The Digital outputs are
contact closures (rated at 30 vdc and 50 ma maximum), available to connect to audio or
visual alarms to alert the operator or technician.
The digital input channels can be read in Vista BASIC, permitting external digital information,
such as alarms, to be used in the analyzer.
The Digital Table screen controls the concentration alarm digital outputs. This screen lists
each available channel, the associated stream, the component being measured, and the low
2000-OSM, C1 4-75
and high range values for that component (see Figure 4-62). If you select stream “00” for a
particular channel, the specified component will apply on that channel for all streams.
Insert Delete
Exit Line Line
F1 F2 F3 F4
3. On the Commands screen, cursor down to TABLE EDIT and then press the F3 (Other
Tables) soft key.
4. On the Edit Other Tables screen, cursor to DIGITAL TABLE and then press the F2 (Edit
The Table) soft key.
5. When the first Digital Table screen appears, cursor across and down the table to
highlight a value you want to change. Then insert the new value.
6. When you have completed the changes to this Digital Table screen, review them to
ensure all items are correct and then press the F1 (Exit) soft key.
7. On the second Digital Table screen, press the F2 (Exit and Update) soft key to save the
changes or press the F1 (Escape) soft key to retain the original values.
4-76 2000-OSM, C1
VISTANET OPTION
If the analyzer is connected to VistaNET, you must set up the analyzer to work on this
network. Once the network connection is set up and running, it runs automatically.
NOTE
Before making changes to VistaNET screens, verify all data with your
Network Administrator to ensure proper connection and operation with
VistaNET.
2. On the Commands screen, cursor to TESTING/SETUP and then press the F4 (Status
Display) soft key.
3. On the Controller Status screen, press the F2 (Clear Highway Stats) soft key. This will
reset all data to zero so you will know when VistaNET data is sent and received.
4. On the Commands screen, cursor to VISTANET and then press the F2 (VistaNET
Tables and Commands) soft key.
5. On the VN Menu screen (see Figure 4-63), cursor to STARTUP and then press the F2
(Essential Addresses) soft key.
TABLES
STARTUP
TESTING
F1 F2 F3 F4
2000-OSM, C1 4-77
6. On the VistaNET Essential Addresses screen (see Figure 4-64), enter the GCC's
identification number on the Name line.
Name: [GCC10 ]
Tag: GCC10
Exit
Escape and
Update
F1 F2 F3 F4
7. Cursor down to the Tag line and enter the GCC's tag number.
8. Cursor to the Board Address line and enter the Communication Board's address.
9. Cursor to the Domain 1 line and enter your GCC's Domain 1 identification.
10. Cursor to the Domain 2 line and enter your GCC's Domain 2 identification.
11. Cursor to the VNSA Address line and enter the complete address of the VNSA serving
your GCC.
12. Cursor to the Router Address line and enter the complete address of the Router serving
your GCC.
13. When you have completed and verified your entries, press the F2 (Exit and Update) soft
key to save your entries.
14. On the VN Menu screen, press the F4 (Refresh VNSA Tables) soft key and then press
the Escape soft key to return to the Commands screen.
15. On the Commands screen, cursor to TESTING/SETUP and then press the F4 (Status
Display) soft key.
16. On the Controller Status screen, note that "Blocks Sent" and "Blocks Received" both
have numbers, indicating that your command to Refresh VNSA Tables was sent and
acknowledged. You are now connected to VistaNET.
17. Press the F1 soft key as necessary to return to the Background screen.
4-78 2000-OSM, C1
SECTION 5. MAINTENANCE
PREVENTIVE MAINTENANCE
The analyzer design eliminates the need for extensive and complex maintenance. Where
preventive maintenance procedures require specific time frames or intervals, you should
maintain an inspection log and inspection data. Figure 5-1 lists inspection routines, with
recommended time intervals for each routine. In addition, you should verify analyzer
calibration periodically to ensure operating efficiency.
To aid in preventive maintenance, keep system chromatograms for reference and compare
them to current data to ensure early detection of a problem, whether in the analyzer or in the
analysis itself.
INTERVAL ROUTINE
When you use two cylinders to supply a gas, connect the cylinders in an automatic
switchover configuration to ensure continuous flow to the analyzer when you replace an
exhausted cylinder. In this configuration, the second cylinder switches in automatically when
the first cylinder is exhausted (100 psig or less). When your check indicates an exhausted
cylinder, replace the cylinder with another containing the specified gas.
2000-OSM, C1 5-1
When you use a single cylinder to supply a gas, you should check this cylinder regularly and
replace it when the pressure falls below 100 psig, using another cylinder containing the
specified gas.
Cleaning
CAUTION
Prior to cleaning the analyzer, turn off the power to the unit. Avoid
using chemical agents which might damage the component parts of the
analyzer.
Remove loose dirt accumulated on the outside of the analyzer with a soft cloth or a small
paint brush. Remove any remaining dirt with a soft cloth dampened in a mild solution of
water and detergent. Do not use abrasive cleaners on the analyzer.
Remove dust in the inside of the analyzer, to eliminate electrical conductivity, and possible
short circuits under high humidity conditions. The best way to clean the interior is to dislodge
the accumulated dust with dry, low-velocity air and then remove any remaining dirt with a soft
paint brush and vacuum cleaner.
DIAGNOSTIC TESTS
The analyzer contains a number of built-in diagnostic tests and tools, identified as follows:
• ROM Checksum
• Chroma Board
• Digital Output
• Trend Output
• Hardware Setup
ROM Checksum
The ROM Checksum test checks all four ROMs for problems and posts the results on the
screen. To run this test, perform the following steps:
2. On the Commands screen (see Figure 5-2), cursor down to TESTING/SETUP and then
press the F2 (Diagnostic Tests) soft key.
5-2 2000-OSM, C1
***** COMMANDS *****
ANALYSIS CONTROL
REPORTS
TABLE EDIT
PRINTER
STORAGE & CONFIG.
NAMES
MISC.
[TESTING/SETUP]
CHROMATOGRAM STORAGE
VISTANET
Diagnostic Diagnostic
Exit Tests Tools
F1 F2 F3 F4
3. On the Diagnostic Tests screen (see Figure 5-3), cursor to DIAGNOSTIC TESTS and
press the F2 (ROM Checksum Test) soft key.
[DIAGNOSTIC TESTS]
DIAGNOSTIC TOOLS
ROM Chroma
Exit Checksum Board
Test Test
F1 F2 F3 F4
2000-OSM, C1 5-3
4. When the test is complete, this message will appear on the screen: “ROM Check
PASSED. Any key to continue.” Press any soft key to return to the Diagnostic Tests
screen. If the ROM check fails, contact your service representative.
Chroma Board
The Chroma Board test requests the Chroma I/O Board to test itself and display the results.
NOTE
The following test can only be run when the analyzer is stopped.
2. On the Commands screen, cursor down to TESTING/SETUP and then press the F2
(Diagnostic Tests) soft key.
3. On the Diagnostic Tests screen, verify that DIAGNOSTIC TESTS is highlighted and
press the F3 (Chroma Board Test) soft key.
4. When the test is complete, this message will appear on the screen: “Chroma Board
Check PASSED. Any key to continue.” Press any soft key to return to the Diagnostic
Tests screen. If the Chroma Board check fails, contact your service representative.
Digital Output
The Digital Output test allows changing states of individual or all digitals by board and
displays the status of inputs in real time. To run this test, perform the following steps:
CAUTION
You must stop the analysis before accessing the Digital Output test, to
ensure the digital output settings are not accidentally changed.
1. Determine which digital outputs you want to test and prepare to verify the test results.
3. On the Commands screen, cursor down to TESTING/SETUP and then press the F2
(Diagnostic Tests) soft key.
4. On the Diagnostic Tests screen (see Figure 5-4), cursor to DIAGNOSTIC TOOLS and
press the F2 (Digital Output Test) soft key.
5-4 2000-OSM, C1
***** Diagnostic Tests *****
DIAGNOSTIC TESTS
[DIAGNOSTIC TOOLS]
Digital Trend
Exit Output Output
Test Test
F1 F2 F3 F4
5. On the Manual Control of Digital Outputs screen (see Figure 5-5), select which board
you want to test.
Deactivate
Exit All
On Board
F1 F2 F3 F4
2000-OSM, C1 5-5
6. Cursor down to the line marked “Pin Number” and enter the desired Chroma I/O Board
pin number. On the corresponding line below the pin number, the digital value will
change from 0 to 1 or from 1 to 0.
7. When the digital value changes, check the output circuit to verify that it changed as
directed.
8. Repeat steps 4 and 5 for each digital pin you want to check. If any circuit does not work
properly, contact your service representative.
9. When you have completed checking digital channels, press the F1 (Exit) soft key to
return to the Diagnostic Tests screen. The Chroma I/O and Digital Board settings will
automatically reset to the values that were in effect when you accessed the Manual
Control of Digital Outputs screen.
10. After you complete diagnostic testing, press F1 as necessary to return to the
Background screen. If you are performing another diagnostic test, start that procedure
from the Diagnostic Tests screen.
Trend Output
The Trend Output test allows changing values of individual trend (analog) outputs. To run
this test, perform the following steps:
2. On the Commands screen cursor to ANALYSIS CONTROL, if necessary, and then press
the F4 (Start/Stop Analysis) soft key.
3. On the Start/Stop Analysis screen, verify that the highlighted area is on "End of
Analysis?" and press the F2 (Stop Analyzer) soft key. The analyzer will stop at the end
of the analysis.
5. Select a trend (analog) output channel to test and connect a meter or recorder to that
output.
7. On the Commands screen, cursor down to TESTING/SETUP and then press the F2
(Diagnostic Tests) soft key.
8. On the Diagnostic Tests screen, cursor to DIAGNOSTIC TOOLS and press the F3
(Trend Output Test) soft key.
9. On the Manual Control of Trend Outputs screen (see Figure 5-6), select the trend
channel you want to check.
10. Cursor down and enter the desired trend value. This value is a percentage of the total
trend range. Check your output to verify the trend value changed. If it did not change,
try a different value. If no valid entries will cause a change at the trend output, contact
your service representative.
5-6 2000-OSM, C1
11. When you have completed checking trend channels, press the F1 (Exit) soft key to
return to the Diagnostic Tests screen. The Trend Board settings will automatically reset
to the values that were in effect when you accessed the Manual Control of Trend
Outputs screen.
12. Press the F1 soft key as necessary to return to the Background screen.
Trend Channel: [ 1 ]
Value: 0.000000
Exit
F1 F2 F3 F4
Hardware Setup
2000-OSM, C1 5-7
3. On the Serial Configuration screen (see Figure 5-7), verify that the setup data is the
same as that specified in the Data Package.
Printer Setup
Baud Rate: 300 1200 2400 4800 9600
Parity: None Even Odd
Data Bits: 7 8
Stop Bits: 1 2
Exit Test
Escape and Printer
Update
F1 F2 F3 F4
4. If you want to make changes, use the cursor arrow keys to select the desired data line
and enter your changes.
5. When you have completed your changes, verify the data on the screen. To test these
changes press the F3 (Test Printer) soft key. If the results are not satisfactory, make
additional changes and test again.
6. When the results are complete and verified, press the F2 (Exit and Update) soft key to
save the changes, or press the F1 (Escape) soft key to retain the original values.
SOFTWARE VERIFICATION
This section describes software checks that are not part of normal operation, but which may
be used to troubleshoot the analyzer. The primary task is to verify the digital configuration by
performing the following steps.
Preliminary Steps
1. If you have not already done so, verify all reports as described in "Verify Reports" in
Section 2.
2. After all reports have been verified, press the F1 soft key as necessary until the
Background screen appears.
5-8 2000-OSM, C1
4. On the Commands screen, cursor to STORAGE & CONFIG and then press the F4
(Update Digital Config) soft key.
5. On the first Digital Configuration screen, enter RESETDIGIO as the password and then
press the F2 (Accept Entered Password) soft key.
6. On the second Digital Configuration screen, cursor to the board whose configuration
you want to verify and then follow the steps in the paragraph pertaining to that board.
Board Paragraph
The final steps for saving configuration changes are described in "Final Steps."
1. After you cursor to Chroma Board 1 on the second Digital Configuration screen, press
the F2 (Edit The Input Table) soft key.
2. On the first Chroma Board 1 Digital Input screen, cursor to VistaII and press the F1
(Continue) soft key.
3. On the second Chroma Board 1 Digital Input screen (see Figure 5-8), verify each pin
and function.
Exit
F1 F2 F3 F4
2000-OSM, C1 5-9
4. If all entries are correct, press the F1 (Escape) soft key to return to the second Digital
Configuration screen. If there are any errors on this screen, correct the errors and then
press the F2 (Exit and Update) soft key to save the corrected data and return to the
second Digital Configuration screen.
1. After you cursor to Chroma Board 1 on the second Digital Configuration screen, press
the F3 (Edit The Output Table) soft key.
2. On the first Chroma Board 1 Digital Output screen, cursor to VistaII and press the F1
(Continue) soft key.
3. On the second Chroma Board 1 Digital Output screen (see Figure 5-9), verify each pin
and function.
Exit
F1 F2 F3 F4
4. If all entries are correct, press the F1 (Escape) soft key to return to the second Digital
Configuration screen. If there are any errors on this screen, correct the errors and then
press the F2 (Exit and Update) soft key to save the corrected data and return to the
second Digital Configuration screen.
1. After you cursor to Digital Board 1 on the second Digital Configuration screen,
press the F2 (Edit The Input Table) soft key.
2. On the Digital Board 1 Digital Input screen (see Figure 5-10), verify each pin and
function.
5-10 2000-OSM, C1
***** Digital Board 1 Digital Input *****
Pin Function Number State
TB6-1 VistaBasic #5 NO
TB6-2 VistaBasic #6 NO
TB6-3 VistaBasic #7 NO
TB6-4 VistaBasic #8 NO
TB6-5 VistaBasic #9 NO
TB6-6 VistaBasic #10 NO
TB6-7 VistaBasic #11 NO
TB6-8 VistaBasic #12 NO
More Below
Exit
F1 F2 F3 F4
3. If all entries are correct, press the F1 (Escape) soft key to return to the second Digital
Configuration screen. If there are any errors on this screen, correct the errors and then
press the F2 (Exit and Update) soft key to save the corrected data and return to the
second Digital Configuration screen.
1. After you cursor to Digital Board 1 on the second Digital Configuration screen, press the
F2 (Edit The Output Table) soft key.
2000-OSM, C1 5-11
2. On the Digital Board 1 Digital Output screen (see Figure 5-11), verify each pin
and function.
Exit
F1 F2 F3 F4
3. If all entries are correct, press the F1 (Escape) soft key to return to the second Digital
Configuration screen. If there are any errors on this screen, correct the errors and then
press the F2 (Exit and Update) soft key to save the corrected data and return to the
second Digital Configuration screen.
Digital Board 2
2. To edit the input table, press the F2 (Edit The Input Table) soft key and follow the steps
in "Digital Board 1 Input Table."
3. To edit the output table, press the F3 (Edit The Output Table) soft key and follow the
steps "Digital Board 1 Output Table."
Chroma Board 2
2. To edit the input table, press the F2 (Edit The Input Table) soft key and follow the steps
in "Chroma Board 1 Input Table."
3. To edit the output table, press the F3 (Edit The Output Table) soft key and follow the
steps in "Chroma Board 1 Output Table."
5-12 2000-OSM, C1
Trend and Detector
1. Cursor to Other on the second Digital Configuration screen and press the F2
(Trend & Detector) soft key.
2. On the Trend And Detector Config screen (see Figure 5-12), verify each trend
setting and detector configuration.
Trend 1 00 11 21 12 22
Trend 2 00 11 21 12 22
DETECTOR CONFIGURATION
Chroma Board 1
Det #
1 None FID FPD T/C M1 M2 M3
2 None FID FPD T/C M1 M2 M3
More Below
Exit &
Escape Update
F1 F2 F3 F4
3. If all entries are correct, press the F1 (Escape) soft key to return to the second
Digital Configuration screen. If there are any errors on this screen, correct the
errors and then press the F2 (Exit and Update) soft key to save the corrected
data and return to the second Digital Configuration screen.
1. Cursor to Other on the second Digital Configuration screen and press the F3 (BASIC
COMMON! Size) soft key.
3. If it is correct, press the F1 (Escape) soft key to return to the second Digital
Configuration screen. If it is not correct, enter the correct size and then press the F2
(Exit and Update) soft key to save the corrected data and return to the second Digital
Configuration screen.
2000-OSM, C1 5-13
Final Steps
After all configuration changes are complete, you must save the tables to E2PROM and
reset the unit.
1. On the second Digital Configuration screen, press the F1 (Exit) soft key.
2. On the screen with instructions on saving the tables, press any soft key.
3. On the Commands screen, cursor to STORAGE & CONFIG. and press the F2 (Save or
Restore Tables) soft key.
4. On the Table Storage screen cursor to SAVE TABLES TO E2PROM and press the F2
(Save Tables) soft key.
5. When “Are Your Sure? Y/N” appears on the screen, press the “Y” key.
7. On the Single Board Computer PCB, press and release the Reset switch. This resets
the analyzer to use the data you just saved.
5-14 2000-OSM, C1
SECTION 6. TROUBLESHOOTING
TROUBLESHOOTING GUIDELINES
BASELINE PROBLEMS
Symptom: Baseline (detector signal) is continually offset to the positive or the negative with
no short term drift up or down scale (see Figure 6-1). This is indicated on the graphic
display, output recorder, and the detector signal.
AMOUNT OF
OFFSET
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
Causes:
2. No carrier gases applied to analyzer. Perform Test Procedure 1 (Carrier, Makeup, and
Utility Gas Supplies).
3. Large difference in reference and column carrier flow rate (example: reference 1 cc/
min, column 20 cc/min). Perform Test Procedure 2 (Carrier and Makeup Gas Flow
Adjustments).
2000-OSM, C1 6-1
5. Defective carrier regulator. Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas
Supplies), Test Procedure 2 (Carrier and Makeup Gas Flow Adjustments), and Test
Procedure 4 (Carrier or Makeup Gas Regulator), as applicable.
6. Column flooded with liquid sample. Perform Test Procedure 3 (Sample Valve Leaking/
Column Flooding).
8. A continuous presence of sample at the detector due to sample valve leakage. Perform
Test Procedure 3 (Sample Valve Leaking/Column Flooding).
10. Electronics failure in the TC circuits. Perform Test Procedure 7 (TCD Electronics).
Symptom: Baseline (detector signal) is experiencing a cyclic short term drift (see Figure 6-2)
indicated by detector signal, graphics display, or strip chart recorder (if used). If cyclic
behavior is only present on strip chart recorder, verify recorder is functioning properly and
that the recorder connecting wires are properly shielded. Ensure shield is connected to
ground at only one end.
BASELINE BASELINE
TIME TIME
NORMAL CYCLIC DRIFT
At the extreme, the signal may indicate a cyclic behavior with the period of each cycle
ranging from a few seconds to several minutes.
Causes:
1. Short term drift, especially cyclic operation, could be due to temperature out of control at
the TC detector or isothermal oven, “dirty” carrier, or defective flow controller. Perform
Test Procedure 31 (Checking Temperature Table Values), steps 1 to 3, 8 and 9; Test
Procedure 9 (Baseline Cyclic Temperature Controller); Test Procedure 10 (Baseline
Cyclic Carrier Regulator); or Test Procedure 11 (Baseline Cyclic Flow Controller), as
applicable.
2. Another possible cause is cell vent back pressure changing. Disconnect vents to check.
Perform Test Procedure 35 (Vent Back Pressure).
Symptom: Baseline (detector signal) is slowly drifting upward or downward (see Figure 6-3)
as indicated by the detector signal, graphics display, or strip chart recorder (if used).
6-2 2000-OSM, C1
BASELINE BASELINE
TIME TIME
Cause: This drift characteristic is generally related to detector response. Most common
causes are temperature zone temperature drift, column flooding or contamination by a
sample containing heavy hydrocarbons, leaking sample valve. Temperature zone drift
normally occurs during temperature zone warm up. Column bleed is less pronounced in
capillary columns than packed columns.
Perform Test Procedure 7 (TCD Electronics); Test Procedure 3 (Sample Valve Leaking/
Column Flooding); or Test Procedure 31 (Checking Temperature Table Values), steps 1 to
3, 8, and 9.
Symptom: Baseline (detector signal) with no sample injection appears as noise similar in
appearance to “grass” on a two dimensional drawing on the graphics display or strip chart
recorder (if used), as shown in Figure 6-4. If it is present only on the strip chart recorder,
verify the recorder is functioning properly and that the recorder connecting wires are properly
shielded. Ensure recorder wire shield is connected to ground at only one end.
NORMAL NOISE
Cause: Baseline or detector noise can result from contaminated carrier, makeup gas, tubing
or regulators. This type of contamination is much less pronounced with a TCD than for an
FID. Other causes include defective filaments (TCD), detector wiring, or electrical noise in
the detector electronics or power supplies.
Perform Test Procedure 12 (Common Usage of Gases); Test Procedure13 (Utility Gas
Contamination Procedure); Test Procedure 14 (Burner Air Catalytic Cleanup Unit), Test
Procedure 7 (TCD Electronics), and Test Procedure 15 (Coaxial Cable), as applicable.
2000-OSM, C1 6-3
Baseline or Signal Offset (FID)
Symptom: Baseline (detector signal) is continually offset to the positive or the negative with
no short term drift up or down scale (see Figure 6-5). This is indicated on the output
recorder.
AMOUNT OF
OFFSET
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
2. Column flooded with liquid sample. Perform Test Procedure 3 (Sample Valve Leaking/
Column Flooding).
3. Contamination can enter through the burner air, burner fuel, or carrier. Secondary
sources are contaminated air, fuel, carrier lines, or regulators.
a. Hydrocarbon contaminates in carrier gas, hydrogen fuel or air can cause the FID
to produce an output signal as they are burned.
4. A continuous presence of sample at the detector due to sample valve leakage. Perform
Test Procedure 3 (Sample Valve Leaking/Column Flooding).
Symptom: Baseline characterized by random noise and/or spikes (see Figure 6-6).
NORMAL NOISE
6-4 2000-OSM, C1
Cause: FID noise is generally the result of electrical noise or contamination.
1. Electrical noise is usually isolated to a defective FID amplifier, defective coaxial cable or
faulty electrical connections.
a. Electrical noise from the FID amplifier could result from a noisy power supply or
defective component of the PCB.
c. Since the FID amplifier input impedances are extremely high, low noise coaxial
cable connects the detector and the FID amplifier. Defective coaxial cables or
poor electrical connections are often sources of noise.
2. Contamination can enter through the burner air, burner fuel, or carrier. Secondary
sources are contaminated air, fuel, carrier lines, or regulators.
a. Hydrocarbon contaminates in carrier gas, hydrogen fuel or air can cause the FID
to produce an output signal as they are burned.
d. If water accumulates in the FID vent, the detector effluent flow can bubble
through the accumulated water. This in effect back-pressures the FID, causing
the flame intensity to fluctuate. This can appear as a noisy baseline as well.
Perform Test Procedure 12 (Common Usage of Gases), Test Procedure 14 (Burner Air
Catalytic Cleanup Unit), or Test Procedure 15 (Coaxial Cable), as applicable. Replace or
clean the FID (see "FID REPAIR" in Section 8).
NOTE
Because of the sulfur addition in the FPD detector, the FPD will always
have a background level. The auto zero circuitry compensates for this.
The background will usually use 15% to 50% of the available auto zero
range. If the background uses less than 10% of the auto zero range, the
flame detection electronics will assume the flame is out and the Flame
Out LED will illuminate. Baseline or signal offset is in addition to this
background.
2000-OSM, C1 6-5
Symptom: Baseline (detector signal) is continually offset to the positive or the negative with
no short term drift up or down scale (see Figure 6-7). This is indicated on the output
recorder.
AMOUNT OF
OFFSET
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
2. Column flooded with liquid sample. Perform Test Procedure 3 (Sample Valve Leaking/
Column Flooding).
4. A continuous presence of sample at the detector due to sample valve leakage. Perform
Test Procedure 3 (Sample Valve Leaking/Column Flooding).
NOTE
Because of the sulfur addition in the FPD detector, the FPD will always
have a background level. The auto zero circuitry compensates for this.
The background will usually use 15% to 50% of the available auto zero
range. If the background uses less than 10% of the auto zero range, the
flame detection electronics will assume the flame is out and the Flame
Out LED will illuminate. Baseline or signal offset is in addition to this
background.
Symptom: Baseline characterized by random noise and/or spikes (see Figure 6-8).
NORMAL NOISE
1. Electrical noise is usually isolated to a defective FPD amplifier, defective coaxial cable
or faulty electrical connections.
6-6 2000-OSM, C1
a. Electrical noise from the FPD amplifier could result from a noisy power supply or
defective component of the PCB.
c. Since the FPD amplifier input impedances are extremely high, low noise coaxial
cable connects the detector and the FID amplifier. Defective coaxial cables or
poor electrical connections are often sources of noise.
2. Contamination can enter through the burner air, burner fuel, or carrier. Secondary
sources are contaminated air, fuel, carrier lines, or regulators.
a. Hydrocarbon contaminates in carrier gas, hydrogen fuel or air can cause the
FPD to produce an output signal as they are burned.
c. If water accumulates in the FPD vent, the detector effluent flow can bubble
through the accumulated water. This in effect back-pressures the FPD, causing
the flame intensity to fluctuate. This can appear as a noisy baseline as well.
ANALYSIS PROBLEMS
No Peaks
Symptom: No peaks are indicated on strip chart recorder, graphic display, or detector signal
(see Figure 6-9).
Missing Peaks
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
Cause: This generally indicates that either no sample was injected, or the injected sample is
not being detected or processed.
1. Chroma not selected on manual control screen (affects recorder output only).
2000-OSM, C1 6-7
2. No sample flowing to the sample valve. Verify sample is flowing to the sample valve.
3. No carrier gas supplied to the analyzer. Perform Test Procedure 1 (Carrier, Makeup,
and Utility Gas Supplies) and Test Procedure 2 (Carrier and Makeup Gas Flow
Adjustments).
4. No air to the sample valve actuator. Perform Test Procedure 19 (Sample Valve
Actuation Air).
5. Baseline offset extreme. See "Baseline or Signal Offset (TCD)" or "Baseline or Signal
Offset (FID)."
7. TCD Failure. Perform Test Procedure 5 (TC Detector Balance) and Test Procedure 6
(Filament Test), as applicable.
8. FID Failure. Perform Test Procedure 18 (Verification FID Flame Is Ignited) and Test
Procedure 16 (FID Reduced Sensitivity), as applicable.
11. Active stream is stream 9 (no inject occurs on stream 9). Change to correct active
stream.
12. Check Method Table for correct entries. Perform Test Procedure 34 (Checking Method
Table Configuration).
13. Sample Valve Failure. Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas
Supplies) and Test Procedure 2 (Carrier and Makeup Gas Glow Adjustments), as
applicable. Also see "Baseline or Signal Offset (TCD)" and "Baseline or Signal Offset
(FID)." Repair sample valve (see "SAMPLE VALVE REPAIR" in Section 8). Check for
correct stem volume and length.
14. Actuation solenoid valve vent is plugged or obstructed. Check and remove any
obstruction.
15. Solenoid not moving. Replace solenoid valve, driver card, or Chroma I/O board.
Double Sampling
Symptom: The chromatogram peaks appear to have double apexes (see Figure 6-10). The
trailing peak apex is generally smaller than the leading due to the first having the greater
sample size.
6-8 2000-OSM, C1
TIME TIME
Cause: Double sampling problems are isolated to the sample valve. Generally the first
injection occurs when the valve is turned on (valve stem inserted into the injection chamber).
The second injection is made when the valve is turned off (the valve stem is withdrawn from
the injection chamber). Perform Test Procedure 20 (Double Sampling).
Unknown
TIME TIME
Cause: If only present on calibration sample and not on process, verify that the correct
calibration and proto fuel samples are being analyzed. Possibly a new calibration blend has
been installed that contains a blending error. Perhaps the wrong calibration sample has
been selected or incorrect analysis is attached to it.
If mystery peaks are present on all process or calibration samples, the analyzer is
experiencing a sampling problem. The sample valve seals may be leaking. The sample
valve may be double sampling (see "Double Sampling"). The sample stem may be
scratched or deformed. Peaks may also be originating from a previous analysis cycle.
Perform Test Procedure 20 (Double Sampling), and Test Procedure 37 (Residual Sample),
as applicable.
2000-OSM, C1 6-9
Variable Sample Size
Variable sample size can cause a nonrepeatibility of peak concentrations if the peak area is
varying (see Figure 6-12).
TIME TIME
ANALYSIS #1 ANALYSIS #2
Figure 6-12. VARIABLE SAMPLE SIZE
Symptom: Chromatogram area or height appears to change with each consecutive injection.
Failure: The liquid sample volume is not consistent between consecutive injections. This
can be related to sample flow, defective sample valve hardware, leaks in column train, or
sample bubbling.
Cause: Leaking sample valve seal can result in random bubbling of carrier into the sample
chamber causing the sample size to vary. If the sample chamber pressure is such that the
temperature is above the bubble point of the sample, the sample will bubble in the sample
chamber, causing an inconsistent liquid fill of the sample loop. This results in a continuously
variable sample size. A defective sample valve stem or leaking seal(s) can also cause
nonrepeatability.
Perform Test Procedure 21 (Variable Sample Size). If necessary, replace the sample valve
seals and stem (see "SAMPLE VALVE REPAIR" in Section 8).
t0 t 30 t0 t 27 t0 t 34
Symptom: Retention times of calibration and individually gated process components change
with each consecutive cycle.
1. Varying Carrier flow rate. Perform Test Procedure 2 (Carrier and Makeup Gas Flow
Adjustments).
6-10 2000-OSM, C1
2. Varying Isothermal Oven Temperature. Perform Test Procedure 31 (Checking
Temperature Table Values).
3. Defective flow controller. Perform Test Procedure 11 (Baseline Cyclic Flow Controller)
and Test Procedure 2 (Carrier and Makeup Gas Flow Adjustments), as applicable.
5. Variable back pressure on FID vent or TCD measurement vent. Perform Test
Procedure 35 (Vent Back Pressure).
Symptom: Chromatogram indicates all peaks are present; however, the data report shows
the peak to be nonexistent or unknown.
Cause: The gating in the method needs to be modified to ensure gating of the missing peak
in the report. This can be done by modifying the gate ON/OFF time in the method table.
See "PEAK DETECTION" in Section 4 for detailed instructions.
Peak Inversion
Symptom: The peaks on the strip chart recorder are reversed or negative (see Figure
6-14).
Baseline offset
adjusted up scale
NORMAL OFFSET
Cause: Negative peaks on the strip chart recorder could be due to reversed recorder wiring
at the analyzer or at the recorder. Some recorders are equipped with polarity reversal.
Ensure correct polarity setting on recorder. Other possible causes include reversal of sense
and reference tubing connections or filament wiring if a TCD is used, or a grounded jet or
missing jet voltage if a FID is used.
2. Check for reversed sense and reference tubing connections to the detector.
2000-OSM, C1 6-11
4. Perform Test Procedure 29 (FID Polarizing Voltage Test).
Symptom: The chromatogram or peak areas are excessively large. The condition may be
severe enough that all peaks are off scale on the highest attenuation (see Figure 6-15).
Chromatogram may go off scale at approximately the time of distillation on and not return to
scale until time of distillation off.
Cause: The attenuation could be set too low, making the chromatogram or peaks appear
large (loss of polarizing voltage on FID). Another possible cause is the wrong carrier gas is
being used (e.g. nitrogen used instead of helium).
The peaks may in fact be too large and saturating the detector or column. The splitter may
be out of adjustment, or the liquid sample size may be too large. Possibly the detector gain
jumper at the detector electronics is not setup correctly. The sample valve may be injecting
an excessively large sample volume due to deformation or a scratch in sample stem or worn
seals.
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
4. Repair sample valve (see "SAMPLE VALVE REPAIR" in Section 8). Check sample loop
size.
Symptom: The chromatogram or peaks have reduced in size from that of a previous
analysis. This is also characterized as a reduction in detector sensitivity.
Cause: The attenuation could be set too high, making the chromatogram or peaks appear
small. Another possible cause is the wrong carrier gas is being used (e.g. helium used
instead of nitrogen).
The peaks may be too small as a result of excessive sample splitting due to the splitter being
out of adjustment, or a small liquid sample volume injection. The sample groove in the
6-12 2000-OSM, C1
sample valve stem may be plugged or restricted. A programming error in sample valve on/off
timing may not allow adequate time for a proper sample injection. Sample valve actuation
malfunction can cause inadequate sample injection. Possibly the detector gain jumper
configuration at the detector amplifier is not set up correctly. The sample valve may have a
defective or wrong stem installed. Low polarizing voltage, defective Detector Amplifier, or
“dirty” FID can also reduce sensitivity.
2. Perform Test Procedure 2 (Carrier and Makeup Gas Flow Adjustments) to check
carrier and splitter flow rates.
4. Perform Test Procedure 29 (“FID Polarizing Voltage Test") to check polarizing voltage.
8. Inspect sample valve stem to check for scratches, deformation and plugging. Check
loop size and stem length.
Peak Discrimination
Symptom: Discrimination is the non linear unequal dilution of hydrocarbons in the column
train. Typically the heavier components will tend to dilute more than the lighter components.
Cause: Discrimination is usually the result of a leak or incorrectly adjusted sample splitter.
The leak or split might cause more of the heavier components to be exhausted out the
splitter vent or leak exit than the lighter components; thus, disproportionate dilution. Perform
Test Procedure 33 (Peak Discrimination) to test for discrimination.
Analyzers that are utilizing only one Vista Workstation (VWS) highway must have the second
highway jumpered on the backplane. If the input to highway 2 is left unconnected, the
communications controller may perceive electrical noise-induced line changes as
information. This extraneous “information” may cause the analysis to stop occasionally at
the end of an analysis method or exhibit other unpredictable behavior.
To prevent this problem from occurring it is recommended that the positive input of the
unused highway be connected to the +5 volt supply. The recommended connection
locations are as follows:
2000-OSM, C1 6-13
2. Connect one end of the jumper wire to J102 pin 5 (see Figure 6-16). If there is not a
connector already installed, ABB P/N 3617698-6 may be used at J102.
TB1
J110
1
J11
123456 01
J1A
123456
J1B
12
2 3 4 5
HIGHWAY #2
1 2 3 4 5
HIGHWAY
#2
6
J102
1
J102
Figure 6-16. BACKPLANE BOARD SHOWING VWS CONNECTIONS
3. Connect the other end of the jumper wire to J110 pin 1. If there is not a connector
already installed, ABB P/N 3617698-12 may be used at J110.
The following alarm indicators help to isolate hardware failures in the temperature controller.
6-14 2000-OSM, C1
Failure: The failure is most likely isolated to the zone indicating a temperature greater than
500 deg C. The temperature sensor(s) is a 400 ohm platinum thermocouple probe. As the
temperature of the probe increases, its resistance value increases. As the temperature of
the probe decreases, the resistance decreases. The maximum temperature range
measurable by the temperature controller is 500 degrees. An indication greater than 500
degrees corresponds to a high resistance value at the sensor input. The greatest resistance
possible is an open circuit to the sensor input or open probe or connection. The least
resistance would be a shorted probe or connection to the sensor input.
Cause: The sensor to the zone input has possibly opened, or is no longer connected to the
sensor input. Perform Test Procedure 22 (Open Temperature Sensor).
Failure: The failure is most likely isolated to the zone indicating a temperature less than -200
deg C. The temperature sensor(s) is a 400 ohm platinum thermocouple probe. As the
temperature of the probe increases, its resistance value increases. As the temperature of
the probe decreases, the resistance value decreases. The maximum scaled temperature
range measurable by the temperature controller is -200 degrees. This corresponds to an
extremely low resistance at the sensor input. The least resistance possible is a short circuit
to the sensor input or shorted probe or connection.
Cause: The sensor to the zone input has possibly shorted. Perform Test Procedure 23
(Shorted Temperature Sensor).
Symptom: At the temperature board in electronics enclosure, all LED’s are off as the
temperature control board shuts down.
2000-OSM, C1 6-15
On Manual Temperature *Temp Bd Alarm* (flashing)
Control Mode Screen
Failure: The isothermal oven heater temperature is greater than 500 degrees C.
Cause: The sensor input from the isothermal oven heater temperature monitor has opened,
or is no longer connected.
Symptom: Micro chip #2 monitors for over temperature conditions at the various
temperature zones. No heat being applied to a specific temperature zone. Actual
temperature as indicated in Manual Temperature Control Mode indicates greater than 500
deg C for a specific zone. At the temperature board in electronics enclosure, all LED’s are
off as the temperature control board shuts down.
Failure: The failure is most likely isolated to the zone indicating a temperature greater than
500 degrees.
Cause: The sensor to the zone input for temperature monitoring has possibly opened, or is
no longer connected. Perform Test Procedure 26 (Zone Input Sensor Open).
Loss of Air
Symptom: The isothermal oven (zone # 1) and programmed temperature oven (zone #2) are
not being heated. The actual temperature reduces and eventually approaches ambient.
These are the only temperature controllers that use air baths.
6-16 2000-OSM, C1
On Alarm Screen Temperature Board:
*Loss of Air
Failure: Malfunction is related to application of oven air to air bath ovens. The air bath
heater(s) will overheat and burn out if air is not applied to the heaters while power is applied.
The air provides the heat to ovens by displacing heat from the heaters. The presence or lack
of oven air is sensed by a pressure switch. If air is removed, the switch opens and power is
removed from the air bath heaters. When air is applied the switch closes allowing the
temperature controller to apply heat to the air bath heaters.
Cause: The oven air has been shut off or reduced below air pressure switch setting. The
oven loss of air pressure switch has failed or connection problem exists. Perform Test
Procedure 24 (Loss of Oven Air).
Triac Failure
Symptom: The Actual temperature is indicating below set point for zone and alarm is
indicating triac failure.
Cause: The output of the triac is connected to the zone heater(s). An optical isolator
connected parallel to the output senses the firing of the triac(s) as heat is applied to the
heater(s). This output is monitored by the Temperature Control board. If the triac does not
conduct when the gate signal is applied, the triac is diagnosed as failed. Problem could be
associated with triac monitoring optical isolators on output board, or an open heater element.
CAUTION
Perform Test Procedure 27 (Open or Shorted Heater) to check for shorted heater.
2000-OSM, C1 6-17
T-Rating Disagreement
Symptom: The temperature board has shut down and all the LED’s are off. The zone
temperatures are reducing and will approach ambient. The T-Rating display is alternating
between the two jumper settings.
If the T-Rating is in question, refer to final documentation provided with the chromatograph or
contact the ABB Service Department.
Remedy: The T-rating jumpers for Micro #1 and Micro #2 must be set up identically.
Determine the correct setting and configure the jumpers for both identically.
Symptom: The temperature board has shut down and all the LED’s are off. The zone
temperatures are reducing and will approach ambient.
Failure: Zones not used for temperature control are excluded to prevent operation. They
are also set INACTive in the software.
Remedy: Select correct exclusion jumper configuration. If in doubt contact ABB Service
Department.
6-18 2000-OSM, C1
Oven Temperature is Greater Than T-Rating
Symptom: The temperature board has been shut down. If the trouble is in Micro #1 then all
LED’s are Off on the Temperature Control board and the zone temperature is greater than
the T-Rating. If trouble is in Micro #2, then the top LED is ON and the actual temperature is
greater than the T-Rating.
Cause: The T-rating defines the maximum surface temperature allowed to prevent the
ignition of the flammable liquids and gases. The over-temperature limit prevents the
temperatures from reaching the T-rating limit. The over-temp must be less than the T-rating
limit to prevent the temperature from reaching the T-rating ignition temperature.
Remedy: Reconfigure T-Rating or upper limit to correct setting. To modify the temperature
configuration table, refer to "DIGITAL TEMPERATURE CONTROLLER" in Section 4.
Perform Test Procedure 31 (Checking Temperature Table Values).
Reasonableness
Cause: Micros #1 and #2 disagree by more than 30 deg C. Micro #1 monitors and controls
the temperature control board. Micro #2 monitors for over-temperature conditions. The
measurement of the two sensors must agree in order to ensure proper over-temp protection.
2000-OSM, C1 6-19
AC Zero Crossing Loss
The heater output board monitors the AC input with a comparator circuit. This determines
the zero crossover point, which occurs when the magnitude of the AC signal is zero. This
point occurs in both the positive and negative directions. The crossover point is used to
coordinate application of power from the triac to the heating element. Power is applied as
the zero crossover point occurs preventing unnecessary loading and surging on the
temperature output circuitry.
CAUTION
Cause: Temperature control did not detect the over-temperature condition when tested.
6-20 2000-OSM, C1
CAUTION
Remedy: The over-temp micro has possibly failed, may require replacement of temperature
control board or output board.
Symptom: The temperature board has shut down and all LED’s on temperature controller
board are off. Actual temperatures are reducing, approaching ambient. Alarm condition
present.
Cause: The controller housing temperature is monitored to ensure that the temperature
does not exceed 80° C. This is done to protect the associated heater electronics from high
temperature operation. Excessive temperatures could cause electronics failure and runaway
zone temperature control.
CAUTION
Install a temperature monitor and verify ambient temperature. Ensure air flow into the
Controller housing.
2000-OSM, C1 6-21
Set Point Unacceptable
Reconfiguration Failure
Out of Control
CAUTION
6-22 2000-OSM, C1
The temperature controllers must be stable with respect to tracking the set point.
Symptom: The actual temperature is not stabilizing at the set point temperature. This alarm
occurs when the zone temperature has remained outside the operational band of the set
point for more than 90 seconds.
2. Perform Test Procedure 22 (Open Temperature Sensor), steps 1-3, to check probe for
stability. If not stable replace probe.
Symptom: No heat to a specific temperature zone. Actual temperature is ambient, while set
point is at normal setting. The analyzer may indicate out of control or low temperature alarm.
Failure: The temperature controller and sensor input and heater output control board are
functioning normally. An open heater will not supply heat to the temperature zone.
Cause: The heater to the temperature zone is possibly open. Perform Test Procedure 27
(Open or Shorted Heater).
Cause: Open fuse causes power to be removed from zone heaters. The analyzer may
indicate an out of control or low temperature alarm. Perform Test Procedure 28 (Open
Fuse to AC Conditioning Board).
2000-OSM, C1 6-23
Low Oven Temperature
CAUTION
1. Low air pressure to analyzer ovens. Perform Test Procedure 1 (Carrier, Makeup, and
Utility Gas Supplies) and make necessary adjustment at analyzer air regulator(s).
2. Loss of air pressure switch; wiring or connection is defective. Perform Test Procedure
24 (Loss of Oven Air).
4. Heater orifice restricted by foreign matter. Check the heater orifice to ensure it is not
restricted or plugged.
Symptom: Programmed temperature oven ramps to final set point, but will not cool to initial
set point or is slow to cool to initial set point.
Cause: Cool down is initiated by the selection of temperature control table entry #2 in the
method tables. If this instruction is missing or incorrect values are placed in the temperature
parameters, cool down will be effected and may not occur. Cool down causes a cool down
solenoid to increase the cool air flow from the vortex cooler into the programmed
6-24 2000-OSM, C1
temperature oven. If the cool down solenoid or vortex cooler fails, cool down will not perform
as expected. If the air flow to the vortex cooler is inadequate, cool down will also be
affected. A rate of 0.1 is needed to activate the cool down solenoid in the temperature
control table entry #2.
The following can cause problems with programmed temperature oven cool down.
1. An error has been made in programming the method table. Perform Test Procedure 31
(Checking Temperature Table Values) to verify all control parameters.
2. Air supply pressure is low. Verify correct air pressures. If necessary make adjustment.
4. Listen for cool down solenoid to operate and introduce increased vortex cooler air flow.
If this does not happen, Perform Test Procedure 43 (Programmed Temperature Oven
Cool Down).
OUTPUT PROBLEMS
Cause: The printer may be turned off or malfunctioning. The printer may have a blown fuse
or be unplugged from power. The printer may be in alarm condition such as being out of
paper. Wiring to printer may be disconnected or in error. Printer and analyzer output driver
may be not be compatible or mismatched (RS-232).
If no reports are generated the report option may be set to NONE. The post analysis
calculations may still be in progress. If no report is generated before next analysis cycle
begins, there is a problem. Perform Test Procedure 36 (Printer Test) to verify correct printer
setup.
Symptom: There is no trend output at recorder or input device, or the trend output value is
not correct.
Cause: No trend output to an external device such as a recorder or DCS can be due to
wiring, loss of loop power or, Trend Board failure. Incorrect trend output at the peripheral
device could be due to loop power, input shunt resistance, Trend Board not scaled correctly,
Trend Board malfunction, or incorrect trend table. Perform Test Procedure 38 (Trend
Output) to test trend function.
Symptom: Valves do not switch and alarm digital output not functioning.
Cause: Wrong assignment of valve or alarm digital assignment in method or Vista BASIC
Program. Digital PCB malfunction or defect.
2000-OSM, C1 6-25
No Recorder Output
Cause: The strip chart recorder may not be powered, or may be malfunctioning. A fuse may
be blown at the recorder. Other causes include defective recorder cable, wiring error or
loose connection. Possibly the wrong attenuation is selected at the recorder or the shunt
resistor is not correct. The Manual Control Screen may not have the Chroma selection or
the Chroma I/O board could be malfunctioning.
The problem may be due to defective or damaged analyzer terminal connection, defective
wiring or connection to the front jacks or backplane connector, or to defective electronics.
Perform Test Procedure 39 (Digital I/O PCB) to test for recorder malfunction.
Cause: Possible communication failure due to electronics failure, control parameters, cable
or cabling connection.
Symptom: Pressing keypad on analyzer front panel produces no response on CRT or other
analyzer output.
Symptom: The CRT display indicates the message “CANNOT CONTACT CONTROLLER”
when attempting to communicate with a remote analyzer.
Cause: The remote analyzer switch address is incorrect. A remote analyzer cannot be
contacted if it is not powered or connected to the network. It is also imperative that the
network wiring be installed and wired correctly. Improper wiring may affect several analyzers
simultaneously.
Cause: The remote analyzer front panel address switch is not set correctly or
the “LOCK OUT REMOTE” switch is set to On.
6-26 2000-OSM, C1
2. Check analyzer address switch setting.
Symptom: Only local chromatograms are accessible at the local panel recorder
output jacks. Remote chromatograms cannot be accessed.
Cause: This feature can only be accessed when using the network. The
jumper at JP5 located on the CRT controller may not be configured correctly.
7. Search for analyzer that is accessing another remote, or that is itself being
accessed, then terminate the access.
Cause: The FID or FPD flame can be extinguished by insufficient burner fuel, air or column
pressure surges, or plugged vent line (possibly moisture).
The flame may in fact be burning and the thermocouple or the associated flame detection
electronics may have failed to detect the flame on condition.
Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas Supplies), Test Procedure 2
(Carrier and Makeup Gas Flow Adjustments), Test Procedure 30 (“Flame Out” LED
2000-OSM, C1 6-27
Remains On After FID Flame Ignition), and Test Procedure 35 (Vent Back Pressure), as
applicable.
If the flame will not light after repeated attempts to ignite it, go to the next paragraph.
Symptom: Flame Out LED on and continued attempts to light the flame have failed.
Cause: Flame-out thermocouple and its electronics detect that flame is extinguished. The
cause could be lack of or insufficient burner fuel, air, or in some cases carrier when hydrogen
carrier is used. The jet may be plugged or restricted, preventing burner fuel from passing
into the detector cell. The ignitor or ignitor electronics may be defective. The vent line may
be plugged.
Perform Test Procedure 18 (Verification FID Flame Is Ignited), Test Procedure 17 (FID Will
Not Light), Test Procedure 32 (Plugged Jet or Breather), and Test Procedure 35 (Vent
Back Pressure), as applicable.
Symptom: Low carrier gas alarm. If carrier is in short supply and not corrected, carrier flow
rates will reduce as the gas is depleted. Analyzer data will become erroneous as carrier
pressure drops below the analyzer requirement.
Causes: The following can be causes for low carrier pressure alarm.
1. Low carrier gas supply. Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas
Supplies).
CAUTION
Symptom: Rotometer and pressure gauge indications are below normal. Bubbles may be
seen in analyzer effluent rotometer. Individual components, RVP and V/L calculation values
are not repeating.
6-28 2000-OSM, C1
Causes: The following can be causes for low sample flow alarm.
1. The sample booster pump is not operating or has failed. Check pump inlet and
discharge pressure and power.
2. Defective or incorrectly adjusted sample flow switch. Perform Test Procedure 42 (Low
Sample Flow Hardware Alarm).
CAUTION
Symptom: If X purge system is installed, analyzer power will be removed and cannot be
restored until purge air is restored.
1. Air supply to analyzer has been shut off. Perform Test Procedure 1 (Carrier, Makeup,
and Utility Gas Supplies).
2. The purged sections in the analyzer have developed leak(s). Leak check with leak
detector.
4. Insect infestation or plugging of purge, atmospheric reference vent(s). Inspect and clear
vent.
5. Tubing to and from pressure switches has disconnected or developed a leak. Inspect
and replace if necessary.
2000-OSM, C1 6-29
3. Stream is not included in the Random Stream Stepping Table.
4. Stream step instruction missing from method table. Perform Test Procedure 34
(Checking Method Table Configuration).
CAUTION
2. Power is disconnected. Check power distribution circuit breakers and local disconnect
switch. (Watch for lock-out tag-out).
3. No air or insufficient air supply at analyzer. An alarm should be present indicating the
purge failure.
6. Air leak in purged analyzer housing preventing X-purge time from completing. See
"Loss of Purge Air."
7. X-purge is locked out. Cycle power (10 seconds) to reset X-purge, and allow X-purge
sequence to initiate.
6-30 2000-OSM, C1
ELECTRONIC PRESSURE CONTROL TROUBLESHOOTING
The Pressure Control Assembly (see Figure 6-17) requires special tools and equipment for
repair. If you suspect a problem with this assembly please contact your ABB service
representative.
"CAUTION"
TO PREVENT IGNITION OF HAZARDOUS ATMOSPHERES, DISCONNECT FROM THE
SUPPLY CIRCUIT BEFORE OPENING ENCLOSURE. KEEP TIGHTLY CLOSED WHEN
CIRCUITS ARE ALIVE. EACH TIME THE ENCLOSURE IS OPENED, THE FLAT
JOINTS (SURFACES) OF THIS ENCLOSURE AND COVER MUST BE THOROUGHLY
CLEANED BEFORE REPLACING COVER. METRIC SCREWS ARE USED TO SECURE
THE COVER.
"AVERTISSEMENT"
OUVRIR LE CIRCUIT AVANT D'ENLEVER LE COUVERCLE. GARDER LE
COUVERCLE BIEN FERME TANT QUE LES CIRCUITS SONT SOUS TENSION.
NETTOYER LES SURFACES DE CONTACT DU COUVERCLE AVANT DE LE REMETTRE
EN PLACE.
ELECTRICAL RATINGS: 115 VAC, 50/60 HZ, 1.2 AMPS
+5 VDC/+15 VDC/-15 VDC; 0.6 AMPS
TORQUE COVER BOLTS TO 16 IN-LBS (2 Nm)
MAXIMUM OPERATING AMBIENT TEMPERATURE = 50°C
CONTROLLER PROBLEMS
Input Power
Input power is connected to one or more of the following locations on the Backplane PCB in
the Controller Housing (see Figure 6-18):
TB1
TB1
J1A
1234 5 6
J1A
J1B 1234 5 6
J1B
2000-OSM, C1 6-31
TB1, which is called VAC #1
J1A, which is called VAC #2
J1B, which is called VAC #3
Input power is 115VAC. This may be supplied directly as 115VAC or stepped down from a
higher voltage. The input voltage may be conditioned or supplied from an uninterruptible
power supply (UPS). Each of these choices, made at the time of sale, affects how the power
is brought into the analyzer.
Power Distribution
The analyzer uses three power distribution circuits to route the power (see Figure 6-19):
TB1
Hot
1
115 to 230 VAC
(Not Filtered Neut RFI VAC #1
2
or Conditioned) Filter (to heaters)
Gnd
3
3
Hot
4
115 to 230 VAC Neut
(Conditioned VAC #2
5
or UPS) (to electronics)
Gnd
6
4
Gnd
3
115VAC Neut VAC #3
(Autoformer) 2 (to solenoids
Hot and detectors)
1
If all power supplied to the analyzer comes from a single source it will be connected to
TB1. Instead of input cables there will be jumper plugs installed at J1A and J1B to
connect their distribution circuits to the input power source.
6-32 2000-OSM, C1
If unconditioned power is routed to TB1 and conditioned power to J1A, then J1B will
have a jumper plug to connect its distribution circuits to J1A.
When checking input power make sure to note the connections for source power to
determine how power is routed.
If the analyzer is ON but it is difficult to read the LCD display, you may need to adjust
the display.
3. On the Front Panel PCB mounted on the door, locate the contrast adjustment. It is on
the front side of the board, at the bottom center (see Figure 6-20).
Front Panel
PCB
Contrast Display
Adjustment Panel
4. Adjust the contrast potentiometer clockwise a quarter turn to increase the contrast.
ALARMS
The analyzer has different types and levels of alarms to help you resolve analyzer problems.
You can review these alarms on the GCC display and on the customer's alarm indicators
(when they are connected to the digital outputs of the GCC—see "Alarm Common Output
Connections").
2000-OSM, C1 6-33
When an alarm signal appears on the Background Screen, press the F4 (Alarms) soft key to
display the ALARMS screen with the alarm message (see Figure 6-21).
Clear
Exit Alarms
and Exit
F1 F2 F3 F4
When you finish with the alarm messages, press the F1 (Exit) soft key to return to the
Background screen without deleting the alarms, or press the F2 (Clear Alarms and Exit) soft
key to clear the alarms and return to the Background screen.
Alarm messages are of two primary types: main alarms and subordinate alarms. Main
alarms identify a major alarm category. These alarms appear on the alarm screen at the left
margin (e.g., “Post Analysis Error:” in Figure 6-21). The main alarms are:
Subordinate alarms appear below the main alarms, indented and preceded by an asterisk (*)
to show their subordinate status (e.g., “*Valve Manually Switched” in Figure 6-21).
6-34 2000-OSM, C1
If a main alarm has subordinate alarms, the main alarm title will include a colon (:). The
following subsections list the main alarms that have subordinate alarms, together with their
associated subordinate alarms.
Sensors Active
When “Sensors Active:” appears as the main alarm, one or more sensor alarms appears
below the main alarm. “Sensors Active” appears when an alarm is active at the time you
look at the Alarms screen. Typical Sensors Active alarms and their descriptions are:
NOTE
* Purge Air—activates when purge air is lost. After purge air is restored the alarm
resets.
* Carrier Gas—activates when carrier gas is lost. After carrier is restored the alarm
resets.
* Low Oven Temp—activates when oven temperature goes below the lower setpoint.
When temperature comes back within the setpoints, the alarm resets.
* High Oven Temp—activates when oven temperature exceeds the upper setpoint.
When temperature comes back within the setpoints, the alarm resets.
* Sample Flow—activates when sample flow is lost. When the sample flow is
restored, the alarm resets.
Sensors Held
When “Sensors Held” appears as the main alarm, one or more sensor alarms appears below
the main alarm. “Sensors Held” appears when an alarm was active at some time during the
analysis, but before you looked at the Alarms screen. Typical Sensors Held alarms are the
same as those for Sensors Active.
You can manually reset Sensors Held alarms by entering the Alarms screen (after the
problem is corrected) and pressing the F2 (Clear Alarms and Exit) soft key. If you set
Sensors Held to clear at the end of the analysis, they will do so if the Sensors Active have
cleared.
2000-OSM, C1 6-35
Component High
When “Component High:” appears as the main alarm, one or more component alarms
appears below the main alarm. Typical Component High alarms and their descriptions are:
* Retention Time High—activates when retention time exceeds the upper setpoint.
Component Low
When “Component Low:” appears as the main alarm, one or more component alarms
appears below the main alarm. Typical Component Low alarms and their descriptions are:
* Component Low Low—activates when a component is below the "low low" setpoint.
* Retention Time Low—activates when retention time is below the lower setpoint.
* Response Factor Low—activates when response factor is below the lower setpoint.
Clock Error
When “Clock Error:” appears as the main alarm, one or more clock alarms appears below
the main alarm. Typical clock alarms are:
* No Active Streams—activates when the status of all streams in the stream table has
been set to inactive. To clear this alarm set at least one stream's status to
active.
* Memory Shortage < 20%—activates when the GCC is short of memory. This is
usually caused by chromatogram storage. To clear this alarm return all memory
that is being used for chromatogram storage back to the operating system and
reduce the number of points being saved by Chromatogram Storage function.
* Bad Base Projection Forward—activates when the beginning of a peak was not
defined in the analysis.
6-36 2000-OSM, C1
* Bad Base Projection Backward—activates when the end of a peak was not defined
in the analysis.
TCF Error
When “TCF Error:” appears as the main alarm, one or more time-coded function alarms
appears below the main alarm. These alarms are cleared by correcting the associated
method entry designated by the alarm. Typical TCF alarms and their descriptions are:
* Auto Zero During Noise—activates when auto zero is performed during noise
calculation.
* Auto Zero During Gate—activates when auto zero is performed during forced gate.
* Auto Zero During Slope Detect—activates when auto zero is performed during
slope detection.
* Gated During Noise—activates when slope detection is turned on at the same time
that a noise calculation is being performed.
* Gate Switched Off w/o Gate On—activates when a force gate is turned off without
the force gate being turned on.
* Noise Off w/o Noise On—activates when noise calculation is turned off but never
turned on.
* Not Enough Noise Points—activates when Noise On and Noise Off are too close
together in time to collect sufficient noise points to perform a calculation.
* Invalid Peak Width—activates when the peak setting in the TCF table is greater
than 64.
* Too Many Peaks in Analysis—activates when there are more than 254 peaks in the
analysis.
When “Post Analysis Error:” appears as the main alarm, one or more post analysis alarms
appears below the main alarm. Typical post analysis alarms and their descriptions are:
2000-OSM, C1 6-37
* Invalid Peak End—activates when the program is unable to define an end to a peak
in the analysis (the peak did not end on a baseline or a valley point).
* Cal Fail: RF Out of Range—activates when calibration fails because the new
response factor for a peak was out of the limits specfied for the component.
* Unknown Component—activates when a peak was detected in the analysis and not
defined in the method.
* Vista Basic Run-Time Error—activates when an error occurs in the Vista Basic
program when it runs.
Communications Error
When “Communications Error:” appears as the main alarm, one or more communications
alarms appears below the main alarm. Which set of subordinate alarms appears depends
on the communications link used in your system, Vista Workstation (VWS) or VistaNET.
Typical communication alarms and their description are:
VistaNET Link
* Block dropped—activates when VistaNET messages are being received from the
Communication PCB faster than they can be processed.
6-38 2000-OSM, C1
* Socket purged—activates when a VistaNET message is received in which there is
no waiting task.
VWS Link
* Undefined Message Channel 1—activates when the GCC receives a message from
the VWS that the GCC cannot interpret (often caused by a VWS failure).
* Undefined Message Channel 2—activates when the GCC receives a message from
the VWS that the GCC cannot interpret (often caused by a VWS failure).
* Checksum Error Channel 1—activates when the GCC receives a message that is
corrupted (often cause by an on-line or VWS failure).
* Checksum Error Channel 2—activates when the GCC receives a message that is
corrupted (often cause by an on-line or VWS failure).
* Transmit Failure Channel 1—activates when the GCC sends a message to the
VWS but does not receive acknowledgement.
* Transmit Failure Channel 2—activates when the GCC sends a message to the
VWS but does not receive acknowledgement.
Pressure Board
When “Pressure Board:” appears as the main alarm, one or more pressure alarms appears
below the main alarm. Pressure alarms are of two types, overall alarms and zone-specific
alarms, with the zone-specific alarms subordinate to the overall alarms. Typical overall
pressure alarms and their descriptions are:
2000-OSM, C1 6-39
If the “*Zone Specific” subordinate alarm appears, at least two additional lines appear below
that. The first line identifies which zone produced the alarm and the second line identifies the
specific alarm condition. Typical zone specific alarms and their descriptions are:
* Out of Control—activates when the ramp rate settings exceed an acceptable range
or the analyzer is unable to maintain set point.
* Zero Failed—activates when the Zero pressure is not present, or the switch has not
been depressed.
* Set Point Failed—activates when Zone is inactive; zone is SWITCH zone and
switch not depressed or set point is greater than the configured pressure range.
* Ramp Rate Failed—activates when the ramp rate settings exceed an acceptable
range.
* High Alarm—activates when the maximum pressure limit set in configuration is too
low.
* Low Alarm—activates when the minimum pressure limit set in configuration is too
high.
NOTE
Temperature Board
When “Temperature Board:” appears as the main alarm, one or more temperature alarms
appears below the main alarm. Temperature alarms are of two types, overall alarms and
zone-specific alarms, with the zone-specific alarms subordinate to the overall alarms.
Typical overall temperature alarms and their descriptions are:
* Loss of Air—activates when there is temporary loss of air to Zones 1 and 2 heaters.
The analysis cycle aborts. When this alarm occurs, power will be removed from
the heaters of air-operated zones for as long as the loss or air condition exists.
When air pressure is restored, power is restored to the heaters.
6-40 2000-OSM, C1
NOTE
If one of the following alarms occurs, the analyzer will stop and power
will be removed from all heaters. To resume operation, you must turn
power OFF and back ON, and then restart the analysis.
* Overtemp Test—activates when the overtemp micro fails. It may signify a zone triac
failure.
* Analysis Shutdown—activates when the Temperature Board alarm has signaled the
SBC with information that will be used to determine whether to abort the
analysis.
If the “*Zone Specific” subordinate alarm appears, at least two additional lines appear below
that. The first line identifies which zone produced the alarm and the second line identifies the
specific alarm condition. Typical zone specific alarms and their descriptions are:
* Out of Control—activates when the ramp rate settings exceed an acceptable range
or the analyzer is unable to maintain set point.
* Zero Failed—activates when Zero resistance is not 400 ohms, or the switch is not
depressed (Zero is not required in the field).
* Span Failed—activates when Span resistance is not 1000 ohms, or the switch is not
depressed (Span is not required in the field).
* Set Point Failed—activates when Zone is inactive; zone is SWITCH zone and
switch not depressed or set point is greater than T-Rating.
* Ramp Rate Failed—activates when the ramp rate settings exceed an acceptable
range (50° C per minute).
2000-OSM, C1 6-41
* High Alarm—activates when the maximum temperature limit set in configuration is
too low.
NOTE
NOTE
If one of the following alarms occurs, the analyzer will stop and power
will be removed from all heaters. To resume system operation, turn the
power OFF and back ON, and then restart the analysis.
When “Raw Chromatogram Storage:” appears as the main alarm, one or more
chromatogram alarms appears below the main alarm. Typical chromatogram alarms and
their descriptions are:
* Memory Below 20%—activates when the memory pool used for chromatogram
storage is below 20%.
* Current Analysis Save Aborted—activates when the GCC is unable to save the last
chromatogram.
* Could Not Save Analysis—activates when the GCC is unable to save the last
chromatogram.
You can view analyzer alarms at the customer's alarm indicator when this indicator is
connected to Hardware Alarm connector J111A and Software Alarm connector J111B on the
GCC Backplane PCB (see Figure 6-22).
6-42 2000-OSM, C1
TB1
J111A
HARDWARE
1 2 3 4 5 6 J111A
J1A ALARM
1
J111B
1 2 3 4 5 6
J111B
J1B
1 SOFTWARE
ALARM
When the Common Digital Output Mask screen has "Common DO" selected for a given
alarm, an alarm condition will illuminate the appropriate alarm LED on the GCC Front Panel
(Hardware Fault LED or Software Fault LED) and will send an alarm signal to the customer's
alarm indicator (when that indicator is connected to J111A or J111B on the Backplane PCB).
When the Common Digital Output Mask screen has "Masked" selected for a given alarm, no
alarm signals will be generated.
2. On the Commands screen, cursor to MISC. and press the F2 (Control Parameters) soft
key.
2000-OSM, C1 6-43
3. On the Control Parameters screen (see Figure 6-23), press the F4 (Common Digital
Out. Mask) soft key.
Analyzer Name:
[ABB Analytical GCC ]
Unknown Peak Alarm: No Yes
Missing Comp Alarm: No Yes
Update Trends on Alarm: No Yes
Auto Update of RF: No Yes
Max RF Variation: 0.000000
Unknown Peak RF: 0.000000
Unknown Peak Units: % ppm
More Below
F1 F2 F3 F4
4. On the Common DO Mask, Main screen (see Figure 6-24), cursor down to the desired
alarm name and verify the selection in the right-hand column.
Expand
Exit Mask
F1 F2 F3 F4
6-44 2000-OSM, C1
5. To change the alarm common output, toggle the left or right cursor to obtain the desired
selection (Common DO or Masked).
6. If the selected alarm has "(Expanded)" after the alarm name, the alarm has subordinate
indicators. To view these subordinates, cursor to the desired alarm line and press the
F2 (Expand Mask) soft key.
7. On the expanded alarm screen, repeat steps 4 and 5 to change a specific alarm's
output.
8. Press the F2 (Exit and Update) soft key to save the new alarm data, or press the F1
(Escape) soft key to retain the original data.
2000-OSM, C1 6-45
For further information or assistance contact:
ABB Inc.
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
6-46 2000-OSM, C1
SECTION 7. TEST PROCEDURES
If you suspect a gas supply (flame, fuel, air) problem, perform the following test.
1. Stop Analysis at end of current analysis, and make no sample injection until procedure
is completed.
2. Check gas supply pressures at the analyzer pressure gauges or EPC screens.
Pressure indications should indicate normal operational values as indicated on the
application data sheets or last valid record.
3. If values are low, check gas supply at source gauges. Verify gas cylinder valve(s) are
open and that gas cylinder regulator(s) are adjusted for the correct outlet pressure.
Verify isolation valves which supply carrier or makeup gases to the analyzer are open.
Verify the cylinder gas supply is not depleted. Make necessary adjustments and replace
empty gas cylinders with full ones.
NOTE
Gas pressures include all carrier, hydrogen fuel, burner air and utility
air supplies.
CAUTION
1. Stop Analysis at the end of the current analysis and make no injection until procedure is
completed.
3. Refer to the application data sheets supplied with your analyzer and verify correct
reference and column carrier flow rates, correct hydrogen fuel and burner air flow rates
(if FID or FPD), correct splitter adjustment, and correct air pressure adjustments.
4. (TCD) Make necessary adjustments and balance detector using Test Procedure 5 (TC
Detector Balance).
2000-OSM, C1 7-1
TP 3: SAMPLE VALVE LEAKING/COLUMN FLOODING
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
CAUTION
1. Stop Analysis at the end of the current analysis, and make no sample injections until
procedure is completed.
2. Isolate sample valve from the sample system using sample system isolation valves.
4. Using stainless steel tubing connect a source of 25 psig nitrogen directly to the sample
valve inlet fitting (bottom). Purge all sample from the sample valve into the waste
container via the short piece of tubing previously connected. When nitrogen purging is
complete, (30 seconds), shut off nitrogen purge gas.
5. Raise the oven temperature to final set-point +20% and hold. Perform Test Procedure
31 (Checking Temperature Table Values), steps 1 to 3, 8 and 9, and observe the oven
temperature (column).
NOTE
Steps 6 and 7 are optional. The existing column can be removed and
another installed prior to performing step 5.
6. Observe baseline for two times the normal cycle time. If baseline offset is reduced, the
sample valve is most likely leaking.
7-2 2000-OSM, C1
TP 4: CARRIER OR MAKEUP GAS REGULATOR
CAUTION
1. Stop Analysis at the end of current analysis, and make no sample injection until the
procedure is completed.
2. Ensure carrier or makeup gas is applied to the analyzer by performing Test Procedure
1 (Carrier, Makeup, and Utility Gas Supplies).
4. Leak check every connection outside the analyzer on the entire carrier flow path.
Perform step 5 only after step 4 has been completed and all leaks are repaired.
5. Loosen inlet fitting nut and check for presence of carrier or makeup gas using a leak
detector solution.
6. If carrier or makeup gas is present, repair or replace the analyzer carrier or makeup gas
regulator. If carrier or makeup gas is not present, continue checking for the presence of
carrier or makeup gas working back toward the gas supply. Loosen each fitting one-at-
a-time. Check each fitting for the presence of gas using a leak detector. Once carrier or
makeup gas is detected, the trouble is isolated between the present and last connection
checked. Make necessary repairs. Tighten all fittings and check for leaks.
7. Adjust carrier or makeup gas pressure for pressure indicated on the analyzer carrier
pressure gauge. If pressure adjusts to the correct value, stop this test and perform Test
Procedure 2 (Carrier and Makeup Gas Flow Adjustments) and, if the system has a
TCD, perform Test Procedure 5 (TC Detector Balance).
TP 5: TC DETECTOR BALANCE
1. Stop Analysis at the end of the current analysis and make no injection until procedure is
completed.
3. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
4. On the Chroma Board screen press the F3 (Manually Zero Baseline) soft key. The
Detector Reading should change to a value of 2.00 mV ±0.05 mV.
2000-OSM, C1 7-3
5. On the Chroma Board screen note the Hardware Zero, Software Zero, and Detector
Reading values.
6. Open the Controller front door and locate the Detector Amplifier on the left side wall of
the Controller.
7. Adjust the TCD Adjust potentiometer (located on the Detector Amplifier) until the
Detector Reading is equal to the sum of the Hardware Zero and Software Zero values
noted in step 5.
8. Press the F3 (Manually Zero Baseline) soft key and recheck the readings. The detector
is adequately zeroed when the Hardware Zero percentage is less than 10%.
CAUTION
1. Stop Analysis at the end of the current analysis cycle, and make no sample injection
until procedure is completed.
4. Open the Controller front door and locate the Detector Amplifier on the left side wall.
5. Remove the six thumb nuts, cover, and plastic shield from the Detector Amplifier. Then
locate TB16 .
7. Connect ohmmeter leads between TB16 terminal 7 and the white wire removed from
terminal 8, and measure the resistance of the measure filament.
8. Connect ohmmeter leads between TB16 terminal 1 and the red wire removed from
terminal 2, and measure the resistance of the reference filament. The measured values
of the two filaments should be within one ohm of each other.
9. If the filaments are not within one ohm of each other, replace the filaments. See
“FILAMENT TCD REPAIR” in Section 8.
7-4 2000-OSM, C1
10. Check filament to ground resistance with an ohmmeter. It should indicate an open
circuit.
12. Check all connections, then replace the Detector Amplifier plastic shield, cover, and
thumb nuts.
16. When analyzer temperature stabilizes, perform Test Procedure 5 (TC Detector
Balance).
TP 7: TCD ELECTRONICS
2. Note the wire colors on Detector Amplifier TB16 terminals 1 (orange), 2 (red), 7 (black),
and 8 (white). Remove filament wires from TB16 terminals 1, 2, 7 and 8, and substitute
a pair of filaments that are mounted in a “dummy” detector cell body.
5. If detector balances and noise is eliminated, the electronics is functioning normally. The
trouble is associated with filaments, filament wiring, filament wiring connections, carrier
flow or contaminated sample train associated with sample valve. Perform Test
Procedure 6 (Filament Test), Test Procedure 2 (Carrier and Makeup Gas Flow
Adjustments), Test Procedure 3 (Sample Valve Leaking/Column Flooded), and Test
Procedure 8 (Column Train Problems), as applicable. Then proceed to step 15.
6. If the detector does not balance or has excessive noise, locate the respective detector
signal connector, J13A or J13B, on the mother board.
7. Remove power from analyzer. Disconnect the cable assembly from J13A or J13B.
8. Short between connector pins 1 and 2. Apply power and perform Test Procedure 5
(TC Detector Balance).
11. If the Chroma I/O Test fails, remove power and replace the Chroma I/O PCB.
12. If the detector does not balance or noise remains, remove power and replace the
Detector Amplifier. Take care to copy the jumper configuration of the original Detector
Amplifier.
2000-OSM, C1 7-5
13. Apply power and perform Test Procedure 5 (TC Detector Balance).
15. Remove the substitue filaments and replace the filament wires.
17. Replace the Detector Amplifier plastic shield, cover, and thumb nuts.
21. When analyzer temperature stabilizes, perform Test Procedure 5 (Detector Balance).
CAUTION
1. Stop Analysis at the end of the analysis and make no sample injection until procedure is
completed.
4. Inspect for disconnected or loose tubing connections or broken column in the column
train from the carrier regulator outlet to the column vent. Reconnect or tighten all tubing
fittings. Check for leaks and make necessary repairs. If corrections or repairs were
made, proceed to step 8.
5. Loosen the fitting connecting the column to the LSV and verify carrier presence with a
leak indicator solution.
7-6 2000-OSM, C1
7. If carrier flow is present and not restricted, reconnect the fitting to the LSV. Beginning at
the column vent, work back toward the previously disconnected fitting, loosing each
fitting in the column train one-at-a-time, checking each loosened fitting for the presence
of carrier. When full or nonrestricted carrier flow is detected, the trouble has been
isolated between the present and last connection checked. Make necessary repairs.
Reconnect or tighten all fittings and check for leaks.
8. Check for correct carrier flow adjustment. Perform Test Procedure 2 (Carrier and
Makeup Gas Flow Adjustments), Test Procedure 5 (TC Detector Balance), and Test
Procedure 45 (FPD Setup), as applicable.
1. Refer to temperature control troubleshooting section and monitor temperature zones for
stability and control from the manual temperature control screen. Alarms relating to
unstable temperature may be present (Out of Control).
1. Observe the carrier and column pressure gauges in isothermal conditions. Often
contaminated, dirty or cyclic regulator performance can be observed as the carrier
pressure oscillates between two pressure gauge indications. The gauge pointer
movement can be as little as ±0.25 psig or as great as several pounds.
1. If the cyclic baseline is not a function of the isothermal oven temperature or the carrier
regulator, and a flow controller is installed, the flow controller should be replaced.
2. Perform Test Procedure 31 (Checking Temperature Table Values) and Test Procedure
10 (Baseline Cyclic Carrier Regulator), as applicable.
1. Are other analyzers serviced from the same burner air, carrier, or burner fuel source,
experiencing noise? If Yes, then the noise problem is most likely related to a common
utility gas, tubing, fitting, or regulator.
1. Verify Burner Fuel is UHP Hydrogen (FID or FPD). If not, replace hydrogen cylinder
with UHP Hydrogen. If noise is eliminated, this test is completed. If noise is still
present, continue to step 2.
2000-OSM, C1 7-7
2. Verify carrier purity. If purity questionable, replace carrier gas cylinder. If noise is
eliminated, this test is completed. If noise is still present, continue to step 3.
3. Replace burner fuel cylinder (FID or FPD). If noise is eliminated, this test is completed.
If noise is still present, continue to step 4.
4. Replace carrier or burner fuel cylinder regulators. If noise is eliminated, this test is
completed. If noise is still present, continue to step 5.
6. Disassemble and clean Detector (see “FID REPAIR/Cleaning the Collector” in Section
8).
1. Determine if air cleanup unit is operational and at operating temperature. Perform Test
Procedure 31 (Checking Temperature Table Values), steps 1 to 3, 8 and 9.
2. If available, connect high purity bottled air to burner air connection. If noise disappears,
see “METHANIZER/AIR CLEANUP REPAIR” in Section 8.
CAUTION
2. Gently move or touch coaxial cable, while monitoring detector output on recorder. Some
movement of signal is normal, but spikes of noise should not occur.
3. If noise spikes are systematically generated, check the coaxial cable connections.
7-8 2000-OSM, C1
TP 16: FID REDUCED SENSITIVITY
CAUTION
1. Stop analysis at the end of the current cycle and make no sample injection until the
procedure is complete.
6. Verify correct sample valve ON and OFF times in method table. Perform Test
Procedure 34 (Checking Method Table Configuration).
7. Refer to the application data sheet supplied with your chromatograph and check carrier,
makeup gases particularly splitter flow, and make any necessary adjustments.
8. If significant corrections were made in steps 2 through 7, run a single cycle analysis to
determine if sensitivity has improved. If sensitivity is now satisfactory, Test Procedure
16 is complete. If sensitivity is still reduced, continue to step 9.
10. Perform Test Procedure 29 (FID Polarizing Voltage Test). If sensitivity is normal, Test
Procedure 16 is complete. If sensitivity continues to be reduced, continue to step 11.
12. Apply power and gases to analyzer. After temperature stabilizes, check sensitivity. If
satisfactory, Test Procedure 16 is complete. If not, perform steps 13 through 15.
2000-OSM, C1 7-9
TP 17: FID WILL NOT LIGHT
CAUTION
Do not ignite the FID flame if the temperature is below operational level.
Low oven temperature will result in condensation damage to the flame
cell.
1. Ensure burner air and burner fuel are adjusted to the values shown on application data
sheets.
2. If flows and pressures cannot be adjusted, perform Test Procedure 32 (Plugged Jet or
Flame Arrester) to test for jet or air restriction.
3. Remove power and open the Controller front door. Locate the Detector Amplifier on the
left side wall of the Controller and remove the six thumb nuts, cover, and plastic shield.
5. On the Chroma Board screen, press the F4 (Manual Ignitor On) soft key to ignite the cell
flame. The meter should indicate 1.2 to 1.5 volts AC. If voltage is not present, the
ignitor could be shorted to ground, the auto ignite board could be defective, or wiring
could be disconnected. If the voltage is present, the defect could be an open ignitor coil.
6. Turn off the burner fuel to extinguish the FID flame and then remove power from the
analyzer.
7. Disconnect the wires from TB16 terminals 3 and 4. Connect an ohmmeter between
these two wires to measure the resistance of the ignitor coil.
8. The resistance of the ignitor coil should measure 0.1 to 1 ohm. If an extremely high
resistance is measured, and the ignitor coil is open, replace the ignitor. See “FID
REPAIR/Replacing the Ignitor Assembly” in Section 8.
9. Connect the ohmmeter leads to one of the wires and chassis ground.
10. Measure the resistance of the ignitor coil to ground. If maximum ohms is not measured,
the ignitor is shorted to ground. Replace the ignitor (see “FID REPAIR/Replacing the
Ignitor Assembly” in Section 8).
12. If the ignitor coil was replaced, apply power to the analyzer. On the Chroma Board
screen, press the F4 (Manual Ignitor On) soft key. If the FID ignites, proceed to step 14.
13. If the ignitor is operating properly and no voltage is present between TB16 terminals 3
and 4 when step 11 is performed, replace the Detector Amplifier.
14. Remove power and replace the Detector Amplifier plastic shield, cover, and thumb nuts.
Close and tighten the Controller front door.
7-10 2000-OSM, C1
TP 18: VERIFICATION FLAME IS IGNITED
One of the primary products of combustion is water. Water vapor produced by the flame is
discharged from the FID/FPD vent. One way to verify the flame is ignited is to observe the
condensation of the water vapor.
1. Disconnect the FID/FPD vent and hold a reflective surface such as a mirror, wrench or
other suitable object at such an angle that you can see the reflective surface.
2. If the flame is ignited, you will be able to see the condensed water vapor form on the
reflective surface.
CAUTION
2. Verify actuation air is being applied to the sample valve. Gently loosen the two 1/8 inch
fittings at the actuator. Apply “Leak Tech”, “Snoop” or other similar liquid leak detector to
the back of the fittings.
3. From the background screen turn on valve 1. The outside actuation tube fitting should
produce bubbles. Turn off valve 1. The bubbles should now be produced on the inside
fitting.
4. If no air is present, check to ensure air is being applied to solenoid valve by loosening
the solenoid air supply inlet connection and test for the presence of air with a leak
detection solution. If air is applied to the solenoid valve, test to ensure that the solenoid
actuation voltage is being applied.
7. Connect voltmeter leads across DC Solenoid Driver PCB S1 terminals 1 and 2. From
the Background screen operate valve 1. The voltage to the 4-way solenoid valve should
measure 110 Vdc when the valve is on and zero Vdc when the valve is off.
8. If the voltage is being applied, yet the valve is not switching, replace the solenoid valve.
9. If no voltage is present, remove power and disconnect both solenoid valve leads from
S1 terminals 1-2.
2000-OSM, C1 7-11
10. Apply power and repeat step 7.
11. If no voltage is present, check the AC voltage to the DC Solenoid Driver PCB. Adjust
the voltmeter to read 120 Vac.
12. Connect the voltmeter leads between J9 terminals 1 and 2. If voltage is present,
proceed to step 15.
13. If 120 Vac is not present, check the voltage at Solenoid #1 VAC J9A terminals 1 and 2.
If voltage is present at J9A terminals 1 and 2, check the connections at both ends of the
cable connecting J9A and J9.
14. Remove power and disconnect the cable between J9A and J9. Check continuity
between J9A terminals 1, 2, and 3 and J9 terminals 1, 2, and 3, respectively. If any
wires are open replace the cable, apply power and repeat step 11.
15. Apply power to analyzer and switch DC solenoid driver using procedure in step 7.
16. If voltage does not switch, replace DC solenoid valve driver PCB.
3. When the analysis begins, stop the analysis at the end of the cycle.
5. Run a second analysis. When the second analysis begins, stop analysis at the end of
the cycle. If valve is double sampling, the peak shape will now be normal in most cases.
7. Manually switch the Sample Valve Off and observe the chromatogram. A second set of
peaks may now appear. (This is another indication of double sampling.)
9. Replace sample valve seals and stem (see “SAMPLE VALVE REPAIR” in Section 8).
7-12 2000-OSM, C1
11. Request calibration analysis to verify problem is solved.
1. For a liquid sample valve, observe the analyzer effluent sample flow rotometer for the
presence of bubbles. The sample pressure and temperature must be such that the
sample pressure at the sample valve is 25 psig above the bubble point of the sample.
2. Ensure that the sample pressure at the sample valve is above the bubble point of the
sample.
3. A booster pump may be necessary for process sample if the supply pressure is below
the bubble point of the sample or the sample flow rate is not adequate at the supply
pressure.
4. Compare the temperature zone temperatures with those of your application data sheets
sent with your chromatograph. Perform Test Procedure 31 (Checking Temperature
Table Values) and make any necessary table corrections. Bubbles at the sample valve
effluent generally indicate the sample temperature is above the bubble point of the
sample. Carrier gas displacement of sample stem groove volume may be occurring due
to leaking valve seals, causing varying sample size.
5. Increase sample flow and backpressure by adjusting metering valves at sample system.
Perform an analysis and check repeatability. If the analyzer repeats, proceed to step 11.
6. For a vapor sample valve, ensure the sample valve effluent is referenced at atmospheric
pressure. A sample shutoff valve may be required or is not operating or is not
functioning properly.
9. Open isothermal oven door and the programmed temperature cover (if applicable).
Remove the cover to access the column.
10. Leak test column train. When complete, close ovens with reverse procedure of step 9.
11. If leaks were found, restore air and power. After temperatures stabilize, perform an
analysis to test repeatability. If analyzer repeats, Test Procedure 21 is complete.
12. Repair sample valve, replacing stem and seals (see “SAMPLE VALVE REPAIR” in
Section 8).
13. Apply air, carrier, sample, and power to the analyzer. Let temperatures stabilize and
perform an analysis and check the repeatability.
2000-OSM, C1 7-13
TP 22: OPEN TEMPERATURE SENSOR
CAUTION
4. Disconnect the sensor and measure its resistance value. The resistance of the
temperature probe should be approximately 440 ohms at 75°F (24°C). If open
(extremely high), replace probe. The respective probes may be tested at the locations
given below:
Temperature J48A
Zone Board Terminals Assignment
CAUTION
7-14 2000-OSM, C1
1. Remove power from analyzer.
4. Disconnect the sensor and measure its resistance value. The resistance of the
temperature probe should be approximately 440 ohms at 75°F (24°C). If shorted or
considerable lower, replace probe. The respective probes may be tested at the locations
given below:
Temperature J48A
Zone Board Terminals Assignment
CAUTION
2000-OSM, C1 7-15
3. Disconnect the oven air pressure switch by removing the connector from J42B on the
DTC Backplane PCB (see Figure 7-1).
J42B
J42B
4. Connect an ohmmeter between the terminals of the connector removed from J42B.
6. Unscrew the pressure switch slightly and check for leakage to ensure air is present at
the switch.
8. The switch should close. Remove air and the switch should open. If switch does not
function as described, replace the oven air pressure switch.
CAUTION
7-16 2000-OSM, C1
CAUTION
5. Disconnect the thermocouple sensor from J49A terminals 1 and 2 of the Zone 1
Temperature Zone PCB.
6. Connect ohmmeter leads between the two disconnected wires and measure the
resistance value. If the resistance is extremely high, the thermocouple is open.
Replace thermocouple.
CAUTION
5. Disconnect the RTD sensor from J49A terminals 4 and 5 of the appropriate Temperature
Zone PCB.
6. Connect ohmmeter leads between the two disconnected wires and measure the
resistance value. Typical resistance will be approximately 430 to 450 ohms at ambient
temperature. If resistance is extremely high, the RTD is open. Replace the RTD. The
respective probes may be tested at the locations given below:
2000-OSM, C1 7-17
Temperature J49A
Zone Board Terminals Assignment
CAUTION
Temperature
Service Zone Board J49B
5. Remove one of the two wires to the defective temperature zone heater. Connect an
ohmmeter across these heater wires and measure the resistance of the heater.
6. If open, the measurement will be extremely high. Typical resistance value is 10 to 120
ohms. Also check for shorted heater to ground. A shorted heater may have opened the
heater fuse.
7-18 2000-OSM, C1
8. If resistance indicates the heater is opened or shorted, replace the defective heater (see
“REPLACING HEATERS” in Section 8).
CAUTION
4. Remove the fuse(s) in question and test with an ohmmeter. The measurement should
be approximately zero ohms. If the fuse is open, the measurement will be extremely
high.
5. Replace blown fuse. Since a blown fuse may indicate other possible malfunctions or
failures, continue with this procedure to verify the analyzer’s operational status.
6. Test for shorted heater by performing Test Procedure 27 (Open or Shorted Heater).
CAUTION
2000-OSM, C1 7-19
1. Stop the analysis.
3. Locate the Detector Amplifier on the left side wall of the Controller. Remove the six
thumb nuts, cover, and plastic shield from the Detector Amplifier.
4. Connect a DC voltmeter from Detector Amplifier TB16 terminal 5 to chassis ground. The
meter should indicate -110 volts DC. If voltage is -110 VDC, Test Procedure 29 is
complete. If the voltage is less than -110 VDC continue with step 5.
5. Disconnect the wire to the polarizer at TB16 terminal 5 and measure the voltage as in
step 4.
6. If the voltage indication is below -110 VDC at the 110 volt power supply, replace the 110
volt power supply.
7. If the voltage is -110 VDC, remove power from the analyzer and shut down carrier and
makeup gases.
8. Remove polarizer wire from TB16 terminal 3 and connect an ohmmeter between the
disconnected wire and chassis ground. The meter should indicate an extremely high
resistance (infinity), meter maximum. A lower resistance value may indicate a short, or
presence of corrosion or water. The high value gives no assurance that the polarizer is
contacting the jet.
9. If any repairs were made, the sensitivity should be checked by applying power to the
analyzer and allowing temperatures to equilibrate. Balance detector per Test
Procedure 5 (TC Detector Balance) and perform an analysis. If analysis demonstrates
correct sensitivity, Test Procedure 29 is complete.
10. Remove power from the analyzer and shut down carrier and makeup gases.
12. Reconnect the wire to TB16 terminal 3 and apply power to the analyzer.
13. Measure with a DC voltmeter between the jet and chassis ground for -110 VDC. Once
confirmed remove power for reassembling.
15. Close and tighten the Controller front door and the isothermal oven door.
17. Allow temperatures to equilibrate and perform an analysis to confirm correct sensitivity
and detector operation.
7-20 2000-OSM, C1
TP 30: “FLAME OUT” LED REMAINS ON AFTER FID FLAME IGNITION
CAUTION
Do not ignite the FID flame if the isothermal oven temperature is below
operational level. Low oven temperature will result in condensation
damage to the flame cell.
1. Stop Analysis at the end of analysis cycle and make no sample injections until
procedure is completed.
2. Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas Supplies) and Test
Procedure 2 (Carrier and Makeup Gas Flow Adjustments), if not previously checked.
3. Remove power from the analyzer and open the Controller front door.
4. Locate the Detector Amplifier on the left side wall of the Controller and remove the six
thumb nuts, cover, and plastic shield from the Detector Amplifier.
6. Connect an ohmmeter between the two thermocouple leads. The ohmmeter reading
should indicate continuity. If it does not, the thermocouple is open. Replace the
thermocouple (see “FID REPAIR/Replacing the Thermocouple Asembly” in Section 8).
7. Connect the ohmmeter between one of the thermocouple leads and chassis ground.
The resistance should be high. If it is not high, the thermocouple may be shorted to
chassis ground. Replace the thermocouple (see “FID REPAIR/Replacing the
Thermocouple Assembly” in Section 8).
2000-OSM, C1 7-21
10. Connect a digital voltmeter across capacitor C6 (see Figure 7-2).
C6
C6
11. Extinguish the FID flame. The “Flame Out” LED should illuminate. The DVM should
indicate 2.5 mV or less.
12. Ignite flame and the LED should go out. The DVM should indicate 3.0 mV or greater.
13. If the electronics does not perform as described in steps 9 through 11, remove power
and replace the Detector Amplifier.
14. Perform FID cell maintenance for cleaning jet and flame out thermocouple (see “FID
REPAIR/Cleaning the FID Jet” in Section 8).
15. Replace the plastic shield, cover, and thumb nuts on the Detector Amplifier.
Verify that the software and hardware temperature parameter values are correct and have
not been inadvertently changed. To perform this operation, it is necessary to access the
temperature configuration table and the manual temperature control mode.
1. Press the F1 soft key until the Background screen is displayed (see Figure 7-3).
7-22 2000-OSM, C1
********** B A C K G R O U N D **********
ABB Analytical GCC Remote 0.1
803V029-1R (Std GCC) (C) 2001
**ALARM**
**ALARM** 18-JUN-2002 TUE 08:16:01
**ALARM**
Analysis Time :00114 Peaks Found:00
Cycle Time :00000 State:Idle
F1 F2 F3 F4
3. On the Manual Control Mode screen (see Figure 7-4), press the F4 (Press. & Temp.
Control) soft key.
F1 F2 F3 F4
2000-OSM, C1 7-23
4. On the Pres & Temp Control screen (see Figure 7-5), cursor up or down to highlight
TEMP CONFIGURATION.
TEMP CONTROL
PRES CONTROL
TEMP CONFIGURATION
Names
Zone and Controller
Escape Config Limits Type
F1 F2 F3 F4
5. Press the F3 (Names and Limits) soft key to view the 5 Zone Names and Limits Table
screen (see Figure 7-6). This table is factory set and is NOT intended to be field
modified. In the unlikely event that one of the parameters was changed, the values
should be compared to those in the table listing provided with the analyzer.
Exit
F1 F2 F3 F4
7-24 2000-OSM, C1
6. If the values shown in the table agree with those of the listing, there is no need for table
modification. Exit this screen by pressing the F1 (Exit) soft key and go to step 8.
7. If the values do not agree, the values have been changed since the analyzer was
shipped from the factory. The correct value(s) should be entered. To modify the
temperature configuration table, refer to the “DIGITAL TEMPERATURE CONTROLLER”
in Section 4.
9. On the Pressure and Temperature Control screen (Figure 7-5), cursor up or down until
TEMP CONTROL is highlighted. Press the F2 (Manual Temp Control) soft key to
access the Manual Temperature Control Mode screen (see Figure 7-7).
F1 F2 F3 F4
10. Compare the set point values of temperature zones 1 through 5 with those of the factory
table listing that was provided with the chromatograph. If the values agree, there is no
need to modify the table. Exit this screen by pressing the F1 (Escape) soft key and
proceed to step 12.
11. If the values do not agree, the values have been changed since the analyzer was
shipped from the factory. The correct values should be entered.
12. Return to the background screen by repeatedly pressing the F1 soft key until the
Background screen is displayed.
13. From the Background screen press the F1 (Exit to Commands) soft key.
2000-OSM, C1 7-25
14. On the Commands screen(see Figure 7-8), cursor up or down to highlight TABLE EDIT.
Then press the F2 (Methods) soft key to access the methods tables.
ANALYSIS CONTROL
REPORTS
TABLE EDIT
PRINTER
STORAGE & CONFIG.
NAMES
MISC.
TESTING/SETUP
SIM DISTILLATION
Go to Other
Background Methods Tables
F1 F2 F3 F4
15. When the Method Table #?? screen appears, enter “1” for the method and then press
the F2 (Edit the Table) soft key.
16. The Cal Define & Cycle Time screen appears. Press the F1 (Continue) soft key to
display the first eight lines of Method Table # 01 (see Figure 7-9).
F1 F2 F3 F4
7-26 2000-OSM, C1
17. Move the cursor up or down to highlight the time associated with Temperature Control
Function Two. Then move the cursor to the right to highlight the value “Two”. The
Temperature Control screen appears (see Figure 7-10).
Exit
F1 F2 F3 F4
18. Compare the set point and ramp rate values with those in the factory table listings
provided with your chromatograph. If they agree, press the F1 (Exit) soft key. If they do
not agree, modify the Temperature Control screen as explained in “DIGITAL
TEMPERATURE CONTROLLER” in Section 4.
19. Return to background screen by repeatedly pressing the F1 soft key until the
Background screen is displayed.
CAUTION
2. If the jet is totally plugged, flame will be extinguished. If restricted, the flame could
possibly still be burning at low intensity.
2000-OSM, C1 7-27
3. Extinguish flame by reducing burner air, fuel and carrier to zero by rotating regulator
adjustment counterclockwise until burner air fuel and carrier gauges indicate zero.
When flame is out, the “Flame Out” LED will illuminate.
5. Increase carrier pressure to value indicated on the application data sheets provided with
the chromatograph. Both carrier pressure and carrier vent flow measurement at the FID
vent should be the same as indicated on data sheets. If values are the same, jet and
flame arrester are not plugged, Test Procedure 32 is complete. If values are low or
nonexistent, the jet or flame arrester may be plugged.
6. Reduce the temperature programmed (if applicable) and isothermal oven air pressures
to zero psig as indicated by their respective gauges.
9. Disconnect the column fitting at the bottom of the FID. Connect the loose column end to
a flow meter.
10. Measure the carrier flow. If flow is restored to the expected measurement, the jet or
breather is plugged. Proceed to step 12. If flow is deficient, reconnect the column to
the FID and perform step 11.
11. Perform Test Procedure 1 (Carrier, Makeup and Utility Gas Supplies), Test Procedure
2 (Carrier and Makeup Gas Flow Adjustments), and Test Procedure 8 (Column Train
Problems), as applicable. If flow is restored, Test Procedure 32 is complete.
12. Remove the breather and replace with a female connector. Attach the flow meter to the
open end of connector. Measure the carrier flow. If flow is restored to normal, the flame
arrester is plugged. Replace the flame arrester.
13. Repeat steps 4 and 5 above. If flow remains restricted, the jet is plugged.
14. Inspect jet by removing FID cap (see “FID REPAIR” in Section 8). If jet plugging can not
be corrected by removing accumulated matter on jet tip, the FID must be replaced. The
FID must be returned to the factor for jet replacement. See “FID REPAIR” in Section 8
for instruction on removing and reinstalling the FID.
15. Disconnect flow meter, reconnect and tighten all fittings, check for leaks, reattach
programmed temperature oven cover and close isothermal oven door using reverse
procedure of steps 7 and 8.
2. Observe the peak areas and new response factors. If a greater percentage change has
occurred in the peak height, peak area, and response factors in the heavier components
than in the lighter, the presence of peak discrimination is apparent.
7-28 2000-OSM, C1
4. Perform Test Procedure 8 (Column Train Problems).
1. Press the F1 soft key until the Background screen is displayed (see Figure 7-11).
********** B A C K G R O U N D **********
ABB Analytical GCC Remote 0.1
803V029-1R (Std GCC) (C) 2001
**ALARM**
**ALARM** 18-JUN-2002 TUE 08:16:01
**ALARM**
Analysis Time :00114 Peaks Found:00
Cycle Time :00000 State:Idle
F1 F2 F3 F4
2000-OSM, C1 7-29
3. On the Commands screen (see Figure 7-12) cursor to highlight TABLE EDIT. Then
press the F2 (Methods) soft key.
ANALYSIS CONTROL
REPORTS
TABLE EDIT
PRINTER
STORAGE & CONFIG.
NAMES
MISC.
TESTING/SETUP
SIM DISTILLATION
Go to Other
Background Methods Tables
F1 F2 F3 F4
4. When the Method Table #?? screen appears, enter “1” for the method number and then
press the F2 (Edit the Table) soft key.
5. The Cal Define & Cycle Time screen appears. Press the F1 (Continue) soft key to
display the first eight lines of Method Table # 01 (see Figure 7-13).
F1 F2 F3 F4
7-30 2000-OSM, C1
6. Refer to the table listings provided with your chromatograph. The function scheduling
should be similar to the following:
2000-OSM, C1 7-31
CALIBRATION STREAM METHOD TABLE
The various time coded functions are defined as follows. Section 4 contains more complete
descriptions of these functions.
7-32 2000-OSM, C1
0120 Noise Calc On
0125 Noise Calc Off
This function samples the baseline to determine the random noise level of the baseline and
is applicable only to slope detection.
NOTE
2000-OSM, C1 7-33
3. Replace flame arrester. Check for water in the detector. If necessary clean FID (see
“FID REPAIR/Cleaning the Collector” in Section 8).
2. Cursor to PRINTER and then press the F2 (Test Printer) soft key. A string of characters
should print.
3. If characters do not print, cursor to TESTING/SETUP and then press the F3 (Hardware
Setup) soft key.
4. Match baud rate, parity, parity check and data bits to printer setup.
5. Check the power. The Disconnect switch or circuit breaker to printer must be ON.
8. Ensure printer has serial interface installed and set up correctly, using the printer or
interface operations manual.
2. Observe the chromatogram. At the end of the cycle, stop the analysis NOW.
5. If peaks elute, analyzer is experiencing a residual sample analysis. After all peaks have
eluted, proceed to step 6. If peaks do not elute, Test Procedure 37 is complete.
6. Turn off power and sample to analyzer. Replace sample valve seals and O-rings (see
“SAMPLE VALVE REPAIR” in Section 8).
7. Restore power and allow temperature zones to come to temperature and stabilize.
7-34 2000-OSM, C1
TP 38: TREND OUTPUT
CAUTION
4. If current output, disconnect one wire from the output to be tested, and place the
milliammeter in series with the load. See output terminal assignment below.
1 1 2 5
2 3 4 5
3 6 7 10
4 8 9 10
5 11 12 15
6 13 14 15
7 16 17 20
8 18 19 20
9 21 22 25
10 23 24 25
11 26 27 30
12 28 29 30
13 31 32 35
14 33 34 35
15 36 37 40
16 38 39 40
7. On the Commands screen, cursor down to TESTING/SETUP and then press the F2
(Diagnostic Tests) soft key.
8. On the Diagnostic Tests screen, cursor down to DIAGNOSTIC TOOLS and then press
the F3 (Trend Output Test) soft key.
2000-OSM, C1 7-35
9. Enter the a trend test value. The output signal at the meter should respond to
equivalent percentage of output. Test for low, middle, and high.
10. If output does not respond or does not reach the expected output value, check the
following:
a. Connect meter to the output terminal strip TB7 (see connection list below) of the
analyzer and repeat step 9. If functioning normally, problem is in loop wiring,
connection, or input device and proceed to step 11.
c. Access Trend Table and determine if it is setup correctly. Make any necessary
corrections.
11. If board functions normal locally, but receiving device is not correctly reporting signal,
check the following:
a. With authorized permission, remove one wire from input device of loop to be
tested and connect the ammeter in series (voltage parallel). Perform step 9 to
determine if loop wiring to input device is functional.
CAUTION
2. On the Commands screen, cursor down to TESTING/SETUP and then press the F2
(Diagnostic Tests) soft key.
3. On the Diagnostic Tests screen, cursor down to DIAGNOSTIC TOOLS and then press
the F2 (Digital Output Test) soft key and follow screen instructions.
7-36 2000-OSM, C1
4. Connect ohmmeter between output terminal of Digital PCB and output common using
proper polarity (these are transistor outputs).
6. If Digital I/O PCB does not function, it is defective. Replace the Digital I/O PCB.
CAUTION
3. If top LED is not active (flickering), there is no transmit activity. The analyzer is off line
with VWS. This must be corrected by accessing the Command Mode parameters.
5. If the bottom LED is not active (flickering), there is no data receive activity. The VWS is
not functioning or there is a possible wiring or connection problem.
CAUTION
1. Check to ensure that the carrier has not been shut off. If so, restore carrier supply.
2000-OSM, C1 7-37
3. Disconnect oven carrier pressure switch at J23A terminals 1 and 2.
4. Connect ohmmeter leads between the two wires previously disconnected from J23A
terminals 1 and 2.
6. The switch contacts should close. Remove carrier pressure; switch contacts should
open.
7. If switch does not function as described, remove carrier pressure and replace pressure
switch.
8. If switch functions as described in step 7, but the alarm remains after the switch wiring
has been reconnected and carrier applied, replace Chroma I/O PCB.
CAUTION
1. Check to ensure that the sample flow has not been shut off. If so, restore sample flow.
5. With sample flowing, the switch should open. Stop sample flow and the switch should
close.
7. If switch functions as described in step 5, but the alarm remains after the switch wiring
has been reconnected and sample flow established, replace Chroma I/O PCB.
7-38 2000-OSM, C1
TP 43: PROGRAMMED TEMPERATURE OVEN COOL DOWN
CAUTION
2. Check air pressure for correct adjustment. Perform Test Procedure 1 (Carrier,
Makeup, and Utility Gas Supplies).
5. Monitor the actual zone 2 temperature. When it reaches 100 degrees, change the set
point to the normal initial set point value and rate to 0.1.
6. You should hear the coolant solenoid valve operate and hear a sudden discharge of air
into the programmed temperature oven.
7. If you do not hear the solenoid valve operate, override the X purge using the procedure
given in Section 4. If you hear the solenoid valve switch, proceed to step 23.
8. Open electronics housing door. LED DS8 should be illuminated. If not, replace
temperature control board.
10. Connect voltmeter leads across J42D terminals 1 and 2 and check for the presence of
zero VAC.
11. Monitor the actual zone 2 temperature. When it reaches 100 degrees, change the set
point to the initial set point value and rate to 0.1.
12. Connect voltmeter leads across J42D terminals 1 and 2 and check for the presence of
115 VAC. If voltage is present, replace the solenoid valve.
13. If no voltage is measured between J42D terminals 1 and 2, check for presence of 115
VAC between J42C terminals 1 and 2.
2000-OSM, C1 7-39
14. If voltage is not present at J42C terminals 1 and 2, check for 115 VAC at J46A terminals
1 and 2.
15. If voltage is present at J46A terminals 1 and 2, shut off power and replace motherboard.
16. If voltage is present at J46D terminals 1 and 2, remove power from the analyzer.
17. Disconnect the solenoid valve coil wires from J42D terminals 1 and 2 and connect an
ohmmeter between the solenoid valve wire leads. The solenoid coil will have a small
resistance. Check each lead to chassis ground. If shorted to ground or questionable,
replace solenoid valve or coil. Inspect leads for bare insulation that could contact
chassis or other grounded part and make necessary repairs.
18. Disconnect the solenoid valve coil wires from J42D terminals 1 and 2 and connect an
ohmmeter between the solenoid valve wire leads. If the coil resistance is extremely high
or infinity, replace the solenoid valve or coil and fuse. Repeat procedure in step 17.
20. Check vortex cooler efficiency in the following manner. Access the Manual Temperature
Control Mode by performing steps 1 to 3, 8 and 9 of Test Procedure 31 (Checking
Temperature Table Values). Change zone 2 set point to 0 deg and rate to 0.1.
21. Monitor the actual zone 2 temperature until temperature measurement is stable.
WARNING
Discharge air from the vortex cooler is extremely hot and can cause
severe burns.
22. Protecting your hands with insulated gloves, adjust the vortex cooler at the discharge
end for maximum cooling (minimum temperature) as indicated on actual zone
temperature.
CAUTION
7-40 2000-OSM, C1
1. Check valve assignment in method tables.
4. If air operated valves are used for stream switching, verify actuation air is being applied
to the stream select valve actuator. Gently loosen the two fittings at the actuator. Apply
“Leak Tech”, “Snoop” or other similar liquid leak detector to the back of the fittings.
5. Request an analysis for the steam in question. At stream step, the stream will begin to
purge as indicated on the background screen. Actuation air will be applied to the
respective actuator, producing bubbles at the loose fitting. When the next different
stream is selected, bubbles should cease at the present actuation line. If the actuation
is double acting, air will be present at the other actuation line and bubbles will be
produced by the leak detector. All streams can be tested in this manner. Reconnect or
tighten each fitting that was loosened.
6. If no air is present, check to ensure air is being applied to solenoid valve by loosening
the solenoid valve air supply inlet connection. Loosen the inlet air fitting and test for the
presence of air with a leak detection solution.
7. If air is applied to the solenoid valve, test to ensure that the solenoid actuation voltage is
being applied.
9. Loosen the four screws that retain the front cover of the heater box.
10. Request an analysis for the stream in question. At stream step the stream will begin to
purge as indicated on the background screen. Connect voltmeter leads across the
stream switch soleniod valve (process) or the calibration solenoid valve (calibration).
The voltage to the solenoid valve should measure 110 VDC when the valve is on and
zero volts when the valve is off. If the voltage is being applied, yet the valve is not
switching, replace the solenoid valve.
11. If no voltage is present, remove power and disconnect both solenoid valve leads.
12. Connect an ohmmeter between the two solenoid valve coil leads. If open, (extremely
high resistance), replace the solenoid valve or coil.
14. Apply power to analyzer and switch D.C. solenoid driver using procedure in step 8.
15. If voltage does not switch, replace D.C solenoid valve driver PCB.
17. Reconnect and tighten all loose or disconnected fittings, and check for and repair any
leaks.
2000-OSM, C1 7-41
20. Allow temperature to equilibrate.
1. Stop Analysis at the end of the current analysis and make no injection until procedure is
completed.
3. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft key.
4. On the Chroma Board screen press the F3 (Manually Zero Baseline) soft key. The
Detector Reading should change to a value of 2.00 mV ±0.05 mV.
5. On the Chroma Board screen note the Hardware Zero, Software Zero, and Detector
Reading values. The hardware zero should be 15 to 100 mV maximum. On a clean
system it whould be 15 to 50 mV.
6. If the hardware zero reading is less than 15 mV, adjust potentiometer R71 on the FPD
Electrometer PCB clockwise slightly.
7. Repeat steps 4, 5 and 6 until the hardware zero reading in step 5 is 20 mV.
7-42 2000-OSM, C1
SECTION 8. REPAIR
REPLACING HEATERS
Temperature
Sensor
Detector
Thermocouple
Oven
Heater
Column
CAUTION
1. Open the Controller front and side doors and the isothermal oven door.
2. On the Zone 1 PCB in the Digital Temperature Controller, disconnect J49B and remove
the isothermal oven heater wires from pins 1 and 2.
3. On the Zone 1 PCB, disconnect J49A and remove the thermocouple wires from pins 1
and 2.
4. On the DTC Backplane PCB disconnect J42A and remove the thermocouple wires from
pins 1 and 2.
5. Connect a small feeder wire (at least 36 inches long) to one of the heater wires.
2000-OSM, C1 8-1
6. In the isothermal oven disconnect the 1/4-inch fitting from the heater.
8. Withdraw the heater and wires from the feedthrough grommet and into the oven.
9. Connect the wires from the new heater assembly to the feeder wire pulled through the
tubing.
10. Install the new heater assembly using the reverse procedure, pulling the wires through
the tubing.
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
CAUTION
1. Remove power, sample flow, and air from analyzer and allow to cool.
2. Open the Controller front and side doors, and the isothermal oven door.
3. Locate the Zone Sense Board and disconnect the LSV heater and sensor wires.
4. Withdraw the free end of the vaporizer cable from beneath the Card Cage into the
Controller housing.
5. Inside the isothermal oven, loosen any cable clamps securing the vaporizer cable
assembly and free the cable.
8-2 2000-OSM, C1
7. Disconnect the air lines from the LSV actuator.
9. Support the valve with your hand and remove the four Allen screws securing the valve
to the analyzer.
11. Remove the vaporizer assembly collar from the valve, separate the vaporizer halves,
and remove the vaporizer.
12. Reassemble and connect the vaporizer using the reverse procedure.
You must take extreme care to avoid having the sample lines exert force on the sample
connections of the Liquid Sample Valve. For example, if stiff 1/4-inch tubing or heat-traced
lines are bent into position and attached to the valve, the force will cause premature failure of
the valve and possibly bend the stem. A loop of 1/8-inch tubing or a flex hose is
recommended between the valve and the sample line (this may be insulated if necessary).
Figure 8-2 illustrates the incorrect and correct connection methods.
INCORRECT CORRECT
It is also important to use two wrenches when tightening the sample line connections to the
sample chamber. One wrench must be used to back up the force applied to tighten the fitting
(direct wrench force will bend the stem).
2000-OSM, C1 8-3
Refer to Figure 8-3 for typical sample valve component location.
3 4 6 7
1 5 8
2
22 9
21
20 17
16
19 18 15 14 13 12 11 10
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
CAUTION
Disassembly
3. Remove the two cone point set screws (1 in Figure 8-3) from the cylinder (22).
8-4 2000-OSM, C1
4. Slide the cylinder (22) off of piston (21) and body (2).
5. Using an Allen wrench, rotate the sleeve (20) counterclockwise until it is loose.
6. Unscrew the body (2) from the flange (13) and vaporizer chamber (10).
8. Slide the seal (3) from the stem (12) using sample chamber (4).
9. Withdraw the piston (21) and the rod assembly (18) from the sleeve (20).
10. This will free the seal (3) from the stem (12).
11. Inspect the seals for visible imperfections. If imperfections are found, replace the seals.
12. Inspect the stem for visible imperfections. If imperfections are found, replace the stem.
13. Remove the rear valve seat (14) from the body (2).
14. Remove the 15 Belleville springs (15) from the body (2).
15. Remove the O-rings (19) from the body (2) and piston (21).
16. Unscrew the piston rod (18) from the piston (21). and extract the stem assembly (12)
from the piston rod (18).
17. Remove the O-ring (16) from the piston rod (18).
Reassembly
NOTE
1. Clean the seals (3) with acetone and air dry them.
2. Clean the sample chamber (10) with acetone and air dry it.
3. Lightly lubricate O-Ring (17), sleeve threads (2), and internal threads and bore of the
body (2) with High Vacuum Grease.
5. Screw the sleeve (20) into the body (2) until the back of the sleeve (20) is flush with the
ears on the back of the body (2), then back the sleeve (20) out 1-1/2 turns.
6. Lightly lubricate the O-ring (16) and the threads of the piston rod (18). Install the O-ring
(16) onto the piston rod (18). Do not allow grease to enter the small hole through the
center of the piston.
2000-OSM, C1 8-5
7. Insert the stem assembly (12) into the rear of the piston rod (18). Screw the piston rod
(18) into the piston (21) and tighten to 27-30 in-lb. Do not overtighten or bend the rod or
stem! Do not allow grease to contact the stem.
8. Lightly lubricate the two O-rings (19). Install the O-rings (19) onto the body (2) and the
piston (21).
9. Insert the piston (21) and the rod assembly (18) into the sleeve (20). Be careful not to
cut the O-ring. Fully insert the piston (21) until it contacts the stops.
10. Stack the 15 Belleville springs (15) (see Figure 8-4) onto the 1/4-inch thin wall plastic
tubing. Using the tubing as a guide, slide the springs (15) over the stem (12) into the
bore of the body (2).
11. Install the rear valve seat (14) over the stem (12) and let it rest against the springs (15).
Do not allow the seat to scratch the stem.
12. Clean all the exposed area of the stem (12) with acetone. Ensure the stem and groove
are free of grease and contamination. Inspect the stem for visible imperfections. If
imperfections are found, replace the stem.
13. Slide the first cleaned seal (3) over the stem (12) using the “A” end of Seal Insertion Tool
TL-791A006B. The 30° angle (pointed end) of the seal (3) must face the springs (15).
14. Slide the cleaned sample chamber (4) over the stem onto the seal (3).
15. Slide the second cleaned seal (3) over the stem (12) using the “B” end of Seal Insertion
Tool TL-791A006B. The 30° angled (pointed end) of the seal (3) faces out, away from
the sample chamber (4).
16. Install the vaporizer chamber (10) into the flange (13) as shown. Lightly lubricate the
threads on the body (2). Screw the body (2) into the flange (13) against the vaporizer
chamber (10) until tight. The sample chamber (4) should be loose in the assembly at
this point. If not, back out the sleeve (20) until the sample chamber (4) is loose. Use
the end of a 0.156 Allen wrench in the slot of the sleeve (20) to adjust to the point of
eliminating the longitudinal play of the sample chamber (4).
17. Tighten the sleeve (20) in 24 1/4-turn increments (6 turns total) to preload the seals.
18. Lightly lubricate the inside bore of the cylinder (22). Align the fittings on the cylinder (22)
with the sample chamber (4) tubes, or with air lines if servicing. Slide the cylinder (22)
onto the piston (21) and the body (2). Install two cone point set screws (1) into the
cylinder #(22) and tighten into the groove on the body (2).
8-6 2000-OSM, C1
COLUMN INSTALLATION OR REPLACEMENT
CAUTION
Column Removal
3. Reduce Isothermal Oven temperature by reducing oven air pressure to zero psig.
4. Shut off carrier and other FID makeup gases (if applicable).
6. To remove the column, loosen the fittings on both ends of the column and gently extract
the column from the respective fitting connections.
7. Loosen any screw securing the column to the column mounting brackets and remove
the column.
1. Install the column, orienting it in such a way that one end can be connected to the fitting
at the LSV and the other into the bottom of the detector.
2. Fasten and secure column in place at the column mounting bracket with the retaining
screws.
3. Insert the column end into the appropriate fitting connection and finger-tighten the nut.
Then tighten it an additional 1/4 turn and test column for a secure connection.
4. Apply carrier gas and leak check. Further tighten the two fittings as required to ensure
no leaks are present.
2000-OSM, C1 8-7
Capillary Column Installation
1. Inspect the ends of the column. The ends should be round and burr free. If either
column end is not round or burr free, the column end must be trimmed as described in
"Cutting Capillary Columns."
2. Insert the end of the column through the back of the tubing nut.
4. Slide the ferrule down the length of the column approximately three inches.
5. Insert the extended column length and the end of the ferrule into the appropriate tubing
connection at the sample valve.
6. Connect the tubing nut and finger-tighten; then tighten it an additional 1/4-turn with an
open-end wrench.
7. Test the column for a secure connection by gently pulling the column at the 1/8-inch
tubing nut. Any withdraw should be corrected. Continue to tighten the nut until the
column is securely connected at the fitting.
9. For columns connected to an FID, insert the column end into the FID analysis inlet
connection until it stops against the jet. Then withdraw the column approximately 1/16-
inch and tighten the nut finger tight. Tighten the nut an additional 1/4-turn with an open-
end wrench, then check it for a secure fit.
NOTE
10. Apply carrier gas and check for leaks. Further tighten the two fittings as required to stop
any leaks.
The procedure for cutting glass or metal capillary columns is the same, except that a small
sharp file may be used to score metal columns.
NOTE
8-8 2000-OSM, C1
1. Use a diamond or ceramic scoring tool to score the surface of the outside tubing wall
approximately one inch from the end of the column. Take care not to cut through the
tubing wall.
2. Wipe the scored area clean to prevent material from entering the column.
3. Secure the column with your fingers 1/2-inch on each side of the score and gently bend
the tubing at the score, in the direction opposite the score. When the score point opens,
bend the tubing back towards the score. The tubing should make a clean break.
4. Inspect the end of the column for roundness and ensure it is burr free. If the end is not
round and burr free, repeat the procedure until it is.
FID REPAIR
CAUTION
Breather Microdot
Adapter Connector
Thermocouple
Ignitor Polarizer
Jet
2000-OSM, C1 8-9
FID Cell Access
CAUTION
CAUTION
Caution should be used when working with the soldering iron. The
soldering iron, melted solder and heated wiring can cause severe
burns. Safety glasses and protective gloves should be used to protect
against hot molten solder and hot surfaces. Personal protective
equipment such as goggles, face shield, lab coat and rubber gloves
should be used while cleaning with solvents such as acetone. Cleaning
with solvents should be done in a well ventilated area.
2. Turn off oven air to the Isothermal Oven and allow all temperature zones to cool.
5. For temperature programmed units, you must remove the insulated covers surrounding
the FID cell body to access any of the FID cell internal components.
1. Disconnect the red coaxial cable located on the top of the detector.
2. Loosen the breather set screw using a 0.050-inch Allen wrench, then extract the adapter
fitting from the detector.
3. Using a 9/16-inch open-end wrench and a 1/2-inch backup wrench, disconnect the 1/4-
inch vent connection from the breather.
4. Remove the breather with adapter fitting from the analyzer oven.
8-10 2000-OSM, C1
5. Remove the adapter fitting from the breather using 3/4-inch and 1/2-inch open-end
wrenches.
6. Using a 3/4-inch open-end wrench and a 1/2-inch backup wrench, remove the 1/4-inch
male connector from the existing breather.
7. Remove the existing Teflon tape from the nipple of the adapter fitting and apply new
tape.
8. Remove the existing Teflon tape from the male connector and apply new tape.
9. Install the detector outlet adapter into the breather and finger tighten. Finish tightening
using 3/4-inch and 1/2-inch open-end wrenches.
10. Install the 1/4-inch male connector into the breather using 3/4-inch and 1/2-inch open-
end wrenches.
11. Connect the 1/4-inch detector vent tubing to the breather. Finger tighten, then tighten
with a 9/16-inch open-end wrench and a 1/2-inch backup wrench.
12. Ensure the detector vent O-ring is in place in the adapter fitting.
13. Finish installing the breather by inserting the cylindrical end of the adapter fitting
completely into the detector outlet and tightening the set screw with a 0.050-inch Allen
wrench. Note the set screw will fit into the groove of the adapter fitting when installed
correctly.
14. Reconnect the red coaxial cable to the top of the detector.
1. Disconnect the red coaxial cable located on the top the detector.
2. Locate the thermocouple assembly as identified by the two red and black wires.
3. If applicable, remove any cable ties and free the wiring to expose the wire splices.
4. Cut and remove the heat shrink and glass tape from the red and black wires to expose
the soldered connections.
6. Using a 3/8-inch open-end wrench, carefully remove the thermocouple. Note its
location for reassembly.
7. Carefully insert the replacement thermocouple into the detector body and finger tighten,
taking care not to damage it. Finish tightening using a 3/8-inch open-end wrench.
8. Roll each end of the red and black wires of the new thermocouple assembly between
your forefinger and thumb, causing the wire ends to be tightly spiral wrapped.
9. Using the 40 watt soldering iron and approved high temperature solder, “tin” the wire
ends.
2000-OSM, C1 8-11
10. Spread or expand the end of approved heat shrink to allow easy installation over the
solder connection.
11. Install the heat shrink over each of the wires and slide it as far as possible from the
connection. This will prevent premature shrinking of it when the connection is soldered.
12. Overlap the “tinned” ends of the red wire from the analyzer electronics and red element
assembly wire, then solder the wires together using approved high temperature solder
and the 40 watt soldering iron.
15. Slide the heat shrink over the soldered connection and shrink it with a heat gun.
16. Reconnect the red coaxial cable to the top of the detector.
1. Disconnect the red coaxial cable located on the top of the detector.
2. Cut cable ties securing the detector element assembly wiring and straighten the wires
to increase accessibility.
4. Visually trace the capillary tubing connections from the detector to the nearest unions.
Place temporary tape labels on each side of the union tubing connections.
NOTE
6. Rotate the detector cover latch counterclockwise until it is freed from the detector body.
7. Slide the detector cover from the detector heater housing and set aside.
8. Remove enough of the insulation from the detector heater housing to expose the
polarizer and ignitor; retain it for later use.
9. Position the wiring and capillary tubing such that the housing can be lifted from the
detector base up over the detector, then lift off the housing, fully exposing the detector
body and elements.
1. After accessing the detector elements as described in "Accessing the Polarizer and
Ignitor Elements," locate the polarizer as identified by the element with the single green
wire.
8-12 2000-OSM, C1
2. If applicable, remove any cable ties and free the wiring to expose the wire splices.
3. Cut and remove the heat shrink and glass tape from the green wire to expose the
soldered connection.
5. Using a 3/8-inch open-end wrench, carefully remove the polarizer assembly. Note its
location for reassembly.
6. Carefully insert the replacement polarizer into the detector body and finger tighten,
taking care not to damage it. Finish tightening using a 3/8-inch open-end wrench.
7. Roll each end of the green wire of the new polarizer between your forefinger and thumb,
causing the wire ends to be tightly spiral wrapped.
8. Using the 40 watt soldering iron and approved high temperature solder, “tin” the wire
ends.
9. Spread or expand the end of approved heat shrink to allow easy installation over the
solder connection.
10. Install heat shrink over each wire and slide it as far as possible from the connection.
This will prevent premature shrinking when the connection is soldered.
11. Overlap and solder the “tinned” ends of the green wire from the wiring harness and the
green polarizer assembly wire using approved high temperature solder and 40 watt
soldering iron.
13. Slide the heat shrink over the taped connection and shrink it with a heat gun.
1. After accessing the detector elements as described in "Accessing the Polarizer and
Ignitor Elements," locate the ignitor as identified by the element with the two white wires.
2. If applicable, remove any cable ties and free the wiring to expose the wire splices.
3. Cut and remove the heat shrink and glass tape from the two white wires to expose the
soldered connections.
5. Using a 3/8-inch open-end wrench, continue loosening and carefully remove the Ignitor
assembly. Note its location for reassembly.
6. Carefully insert the replacement ignitor into the detector body and finger tighten, taking
care not to damage it. Finish tightening using a 3/8-inch open-end wrench.
7. Roll each end of the two white wires of the new ignitor between your forefinger and
thumb, causing the wire ends to be tightly spiral wrapped.
2000-OSM, C1 8-13
8. Using the 40 watt soldering iron and approved high temperature solder, “tin” the wire
ends.
9. Spread or expand the end of approved heat shrink to allow easy installation over the
solder connection.
10. Overlap and solder the “tinned” ends of one white wire from the wiring harness and one
white ignitor assembly wire and solder the wires together using approved high
temperature solder and 40 watt soldering iron.
13. Slide the heat shrink over the taped connection and shrink it with a heat gun.
NOTE
3. Slide the housing down over the insulation and detector body onto the base. The
housing must slide over the circular base and rest on the mounting bracket.
4. Bend the capillary tubing back into place, then route the wiring to the back of the
detector housing and install insulation into the housing.
5. Install the detector cover by channeling the cover slot through the machined groove in
the detector body, while sliding the cover into place. Note that the wiring exits through
the slot in the cover, and that the capillary tubing exits the can through the sheared edge
of the top cover.
6. Rotate the detector cover latch clockwise until is secured by the detector. Note the
small slot in the latch also fits into the same machined groove the cover fits.
8. Using the previously installed temporary labels, connect the capillary tubes to their
respective unions.
11. Install the red coaxial cable to the connector on top of the detector.
8-14 2000-OSM, C1
Cleaning the FID Jet
NOTE
1. Remove the three screws securing the detector can assembly, using a 9/64-inch Allen
wrench or ball driver.
3. CENELEC and CSA flame ionization detectors are identified by the presence of three
packing adapter nuts (5/8-inch, 1/2-inch and 7/16-inch). Other models contain only two
packing adapter nuts (5/8-inch and 1/2-inch).
4. On CENELEC AND CSA models, loosen the 7/16-inch packing adapter nut using a 7/
16-inch open-end wrench, backed up with a 1/2-inch open-end wrench on the 1/2-inch
packing adapter nut. Continue to loosen by hand until disconnected.
5. For all models, loosen the 1/2-inch packing adapter nut using a 1/2-inch open-end
wrench with a 5/8-inch open-end back-up wrench. Continue to loosen by hand until
disconnected.
6. Withdraw the column and associated ferrules and adapters from the detector.
7. Loosen the 5/8-inch adapter fitting from the bottom of the detector.
8. Extract the jet with the adapter fitting from the jet cavity in the detector.
9. Inspect the end of the jet for damage. It should not be pitted or plugged. If pitted,
replace with a new jet.
10. Insert a 0.016-inch diameter piano wire into the jet and rod it out. If the piano wire will
not pass through, replace the jet.
11. Using a syringe and protective equipment and clothing, flush the jet with a mild solvent
such as acetone; then blow dry with 15 psig clean air, nitrogen or helium.
12. Use a 5/8-inch adapter fitting to insert the jet into the jet cavity. Finger tighten and finish
tightening using a 5/8-inch open-end wrench.
13. Insert the column end, ferrule and adapter nut into the detector inlet and finger tighten;
then loosen 1/8 turn.
14. If the ferrule was loose and slid any length on the column, continue to push the column
into the detector analysis inlet until it stops.
15. Withdraw the column approximately one mm and tighten the 1/2-inch adapter nut finger
tight. Tighten the nut 1/4 turn more with a 1/2-inch open-end wrench, then check it for a
secure fit by gently attempting to pull the column slightly away from the detector.
Carefully tighten the adapter until the column is secure.
2000-OSM, C1 8-15
16. For CENELEC and CSA models, slide the 7/16-inch packing adapter nut and ferrule
toward the detector and install finger tight. Tighten the nut an additional 1/4 turn with a
7/16-inch open-end wrench.
17. For temperature programmed units, install the detector can assembly and secure it with
the hex head screws using a 9/64-inch Allen wrench or ball driver. Be sure to align the
three holes such that the edge of the can is parallel with edge of the temperature
programmed oven.
1. For temperature programmed units, remove the temperature programmed oven covers
as described in "Cleaning the FID Jet."
2. Disconnect the column and remove the jet as described in Cleaning the FID Jet."
5. Access the detector elements as described in "Accessing the Polarizer and Ignitor
Elements."
6. Remove the polarizer and ignitors described in "Replacing the Polarizer" and "Replacing
the Ignitor Assembly."
7. Use a small stainless steel brush precleaned with acetone to remove chloride
accumulations from the collector, by inserting the brush through the detector inlet
connection and briskly scrubbing with an in-and-out motion.
8. Install the detector elements as described in "Accessing the Polarizer and Ignitor
Elements."
10. For temperature programmed units, install and secure the temperature programmed
oven covers.
NOTE
1. Disconnect the Microdot connector located on top of the detector (see Figure 8-5).
2. Cut the cable just below where it passes through the Oven into the Control Housing and
remove the cable from the Oven.
8-16 2000-OSM, C1
3. Disconnect the other end of the cable from the FID Amplifier Assembly and remove the
cable from the Control Housing.
4. Remove the grommets from the grommet holes (located in the bottom of the Control
Housing and the top of the Oven) that will accommodate the routing of the new cable.
5. The new FID Cable Assembly has a Microdot connector on one and and a BNC
connector on the other end (see Figure 8-6). Screw the Microdot connector end of the
new cable assembly into the Insertion Tool.
Microdot BNC
Connector Connector
6. Pass the Insertion Tool through the grommet holes from the Control Housing to the
Oven.
8. Make a slit in each grommet from the outer diameter to the inner hole. (This is
necessary because the cable connector will not pass through the grommet.)
9. Position the cable in the grommets in the Control Housing and the Oven.
11. Connect the cable connectors to their respective locations (BNC connector to the FID
Amplifier Assembly and Microdot connector to the top of the detector).
Refer to Figure 8-7 for Filament Thermal Conductivity Detector (TCD) component location.
Reference Measure
Filament Filament
Reference Vent
Sample In
Sample Vent
TC Assembly
Reference In
2000-OSM, C1 8-17
CAUTION
CAUTION
The filaments are fragile and can be easily damaged if not handled with
extreme care. Do not touch the end of the elements.
2. Turn off oven air to the Isothermal Oven and allow all temperature zones to cool.
1. Use a Phillips screwdriver to loosen the two Phillips head screws located on the front
underside of the mounting bracket.
2. Remove the mounting bracket cover by sliding it out and away from the detector
assembly.
4. If they are not already labeled, label the wire pair connected to the measurement
filament “M” and the wire pair connected to the reference filament “R”.
5. If the detector filament wiring connections are spliced, perform steps 6 through 8. If they
are not spliced, go to step 9.
6. Position the detector wiring such that the wired splices can be accessed.
8-18 2000-OSM, C1
7. Cut and remove the heat shrink from each of the spliced filament wire connections to
expose the soldered connections.
8. Using a 40 watt soldering iron, de-solder and disconnect the wire splices.
9. If the detector filament wiring connections are not spliced, cut the existing detector
harness wires approximately three inches from the detector end.
10. Remove the harness retaining clamp and free the harness.
11. Clean the area around the two detector filaments to reduce the chance of foreign
particles entering the detector cavity when the filaments are removed.
12. Loosen the two detector filament retaining gland nuts with a 3/8-inch open-end wrench.
Continue to loosen by hand.
13. Carefully extract the filaments from the detector cell cavity.
Replacement filament installation kits are supplied with two cable glands, a wire spreader,
736 RTV, high temperature solder, and heat shrink.
1. Cut the four filament wires approximately the same length as the wires on the filaments
that were removed.
2. Insert one pair of filament wires through the threaded end of the gland nut, then carefully
insert the filament into the detector cell cavity marked “M” (measurement).
3. Slide the nut down the length of the wires to insert and align it with the measurement
cavity.
4. Tighten the cable gland finger tight, then finish tightening with a 3/8-inch open-end
wrench.
5. Insert the second pair of filament wires through the threaded end of the gland nut, then
carefully insert the filament into the detector cell cavity marked “R” (reference).
6. Slide the nut down the length of the wires to insert and align it with the reference cavity.
7. Tighten the cable gland finger tight, then finish tightening with a 3/8-inch open-end
wrench.
8. Using wire strippers, remove approximately 1/4 inch of insulation from the end of each
detector filament wire.
Filament Checkout
1. Obtain a multimeter and select the ohms function and a range capable of measuring 40
ohms.
2. Connect one multimeter lead to each wire of the measurement filament (installed in the
detector cavity labeled “M”). The resistance measurement should be approximately 40
ohms.
2000-OSM, C1 8-19
3. Connect one multimeter lead to each wire of the reference filament (installed in the
detector cavity labeled “R”). The resistance measurement should be within one ohm of
the measurement filament resistance.
4. If the resistance measurements are not within one ohm of each other, ensure the
multimeter is connected and functioning correctly, and that the correct meter function is
selected.
5. If the detector filaments are not in tolerance, the detector filaments are defective. The
filaments must be replaced and the checkout repeated.
6. Neither filament should contact the detector cell body. Connect the multimeter leads to
one of the filament wires and the detector cell body. The meter reading should range
from several hundred megohms to infinity.
7. Repeat this measurement for each of the other three filament wires. If all resistance
measurements are correct, go to "Connecting the Filaments." If any resistance is too
low, go to step 8.
9. Inspect the filament for damage or bending. If it is damaged, the filament pair will have
to be replaced.
10. If the filament is slightly bent, use small needle nose pliers to gently and carefully bend it
straight.
11. If the filament orientation now appears to be correct, reinstall the detector filament and
repeat the complete checkout. If it fails again, replace the detector filament pair and
repeat the harness checkout.
12. If the filament is damaged during this attempted correction process, the filament pair
will have to be replaced.
1. Roll the ends of each stripped harness wire between your thumb and index finger to
tightly spiral wrap the wire ends.
2. Using a 40 watt soldering iron and approved high temperature solder, “tin” each of the
harness wire ends.
3. Roll the ends of each stripped filament wire between your thumb and index finger to
tightly spiral wrap the wire ends.
4. Using a 40 watt soldering iron and approved high temperature solder, “tin” each of the
filament wire ends.
5. Slide the insulating sheath of each filament back to reveal the stranded wire, install
approved heat shrink over each of the four filament wires, and slide it as far from the
free wire end as possible.
8-20 2000-OSM, C1
6. Select a harness assembly wire with the “R” label designation and overlap the “tinned”
ends of this harness wire with one of the reference filament wires.
7. Solder the wires using a 40 watt soldering iron and approved high temperature solder.
Apply solder sparingly, allowing it to flow evenly. Do not overheat the solder or a high
resistance connection could result.
8. Repeat steps 6 and 7 for the remaining harness wire labeled “R” and reference filament
wire.
9. Repeat steps 6 through 8 for the harness wires labeled “M” and the measurement wires.
10. Slide heat shrink over each connection and shrink with a heat source.
Leak Test
1. Restore carrier to the analyzer and establish carrier flow to both the measurement and
reference ports of the detector.
2. Verify carrier and reference flow using a flow meter. Typically the flows should be 30 to
40cc per minute if packed columns are used; 10 to 15 cc per minute if 0.53 mm ID
capillary columns are used, and 3 to 5 cc per minute if 0.32 mm ID capillary columns are
used.
3. Test for leaks around the detector filament gland nut with a nonconductive liquid leak
detection solution. Correct all leaks before proceeding.
5. Gently remove any excess leak detection solution with a soft cloth or tissue and blow
dry with 15 psig clean dry air, helium or nitrogen.
Perform this procedure if you know that your analyzer is constructed to CENELEC or CSA
specifications or the if existing detector filament is potted.
1. Gently slide the insulation sheath out of and away from the gland nut.
2. Using a syringe filled with Silastic compound “Dow 736 RTV,” completely fill the gland
cavity with the Silastic compound.
3. With the insulation still pulled away from the gland nut, use needle nosed pliers to install
the wire spreader.
4. Separate and insert filament wires into the slots on either side of the spreader. The
spreader should be positioned between the end of the sheath insulation and the back of
the gland nut.
5. Press the spreader into the recess in the gland nut. The retainer must be installed such
that it is not in anyway tilted. It is normal for the retainer to protrude slightly from the
gland recess.
6. Slide the sheath insulation toward the wire spreader until it contacts the face of the
spreader.
2000-OSM, C1 8-21
7. Replace the mounting bracket insulation.
8. Install the mounting bracket cover and secure it with two Phillips head screws.
Refer to Figure 8-8 for Thermistor Thermal Conductivity Detector (TCD) component location.
Measure Reference
Thermistor Thermistor
CAUTION
CAUTION
The filaments are fragile and can be easily damaged if not handled with
extreme care. Do not touch the end of the elements.
8-22 2000-OSM, C1
CAUTION
2. Turn off oven air to the Isothermal Oven and allow all temperature zones to cool.
1. Use a Phillips screwdriver to loosen the two Phillips head screws located on the top
cover.
2. Remove the top cover by sliding it out and away from the detector assembly.
3. Remove the top sleeve from the detector assembly.
4. If they are not already labeled, label the wire pair connected to the measurement
thermistor “M” and the wire pair connected to the reference thermistor “R”.
5. Position the detector wiring such that the wired splices can be accessed.
6. Cut and remove the heat shrink from each of the spliced thermistor wire connections to
expose the soldered connections.
7. Using a 40 watt soldering iron, de-solder and disconnect the wire splices.
8. Clean the area around the two detector thermistors to reduce the chance of foreign
particles entering the detector cavity when the thermistors are removed.
9. If necessary, remove the two standoffs that hold the top cover in place and retain them
for re-installation.
10. Loosen the two detector thermistor retaining gland nuts with a 5/16-inch open-end
wrench. Continue to loosen by hand.
11. Carefully extract the thermistors from the detector cell cavity.
Replacement thermistor installation kits are supplied with a matched pair of thermistor
assemblies, high temperature solder, and heat shrink tubing.
1. Cut the four thermistor wires approximately the same length as the wires on the
thermistors that were removed.
2. Insert one thermistor assembly into the detector cell cavity marked "M" (measurement)
and screw the cable gland finger tight.
2000-OSM, C1 8-23
3. Finish tightening the cable gland with a 5/16-inch open-end wrench.
4. Insert the second thermistor assembly into the detector cell cavity marked “R”
(reference) and screw the cable gland finger tight.
6. Using wire strippers, remove approximately 1/4 inch of insulation from the end of each
detector thermistor wire.
Thermistor Checkout
1. Obtain a multimeter and select the ohms function and a range capable of measuring 40
ohms.
2. Connect one multimeter lead to each wire of the measurement thermistor (installed in
the detector cavity labeled “M”). The resistance measurement should be approximately
40 ohms.
3. Connect one multimeter lead to each wire of the reference thermistor (installed in the
detector cavity labeled “R”). The resistance measurement should be within one ohm of
the measurement thermistor resistance.
4. If the resistance measurements are not within one ohm of each other, ensure the
multimeter is connected and functioning correctly, and that the correct meter function is
selected.
5. If the detector thermistors are not in tolerance, the detector thermistors are defective.
The matched set of thermistor assemblies must be replaced and the checkout repeated.
6. Neither thermistor should contact the detector cell body. Connect the multimeter leads
to one of the thermistor wires and the detector cell body. The meter reading should
range from several hundred megohms to infinity.
7. Repeat this measurement for each of the other three thermistor wires. If all resistance
measurements are correct, go to "Connecting the Thermistors." If any resistance is too
low, go to step 8.
9. Inspect the thermistor for damage or bending. If it is damaged, the matched set of
thermistor assemblies will have to be replaced.
10. If the thermistor is slightly bent, use small needle nose pliers to gently and carefully
bend it straight.
11. If the thermistor orientation now appears to be correct, reinstall the detector thermistor
and repeat the complete checkout. If it fails again, replace the matched set of thermistor
assemblies and repeat the harness checkout.
8-24 2000-OSM, C1
12. If the thermistor is damaged during this attempted correction process, the matched set
of thermistor assemblies will have to be replaced.
1. Roll the ends of each stripped harness wire between your thumb and index finger to
tightly spiral wrap the wire ends.
2. Using a 40 watt soldering iron and approved high temperature solder, “tin” each of the
harness wire ends.
3. Roll the ends of each stripped thermistor wire between your thumb and index finger to
tightly spiral wrap the wire ends.
4. Using a 40 watt soldering iron and approved high temperature solder, “tin” each of the
thermistor wire ends.
5. Install approved heat shrink over each of the four thermistor wires and slide it as far
from the free wire end as possible.
6. Select a harness assembly wire with the “R” label designation and overlap the “tinned”
ends of this harness wire with one of the reference thermistor wires.
7. Solder the wires using a 40 watt soldering iron and approved high temperature solder.
Apply solder sparingly, allowing it to flow evenly. Do not overheat the solder or a high
resistance connection could result.
8. Repeat steps 6 and 7 for the remaining harness wire labeled “R” and reference
thermistor wire.
9. Repeat steps 6 through 8 for the harness wires labeled “M” and the measurement wires.
10. Slide heat shrink over each connection and shrink with a heat source.
Leak Test
1. Restore carrier to the analyzer and establish carrier flow to both the measurement and
reference ports of the detector.
2. Verify carrier and reference flow using a flow meter. Typically the flows should be 30 to
40cc per minute if packed columns are used; 10 to 15 cc per minute if 0.53 mm ID
capillary columns are used, and 3 to 5 cc per minute if 0.32 mm ID capillary columns are
used.
3. Test for leaks around the detector thermistor gland nut with a nonconductive liquid leak
detection solution. Correct all leaks before proceeding.
5. Gently remove any excess leak detection solution with a soft cloth or tissue and blow
dry with 15 psig clean dry air, helium or nitrogen.
2000-OSM, C1 8-25
FPD REPAIR
CAUTION
FPD Electrometer
(in Controller Housing)
FPD
Electrometer
Cables
Cables
Nuts Nuts
Photomultiplier Photomultiplier
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
8-26 2000-OSM, C1
3. Turn off air supply to air cleanup unit.
5. Disconnect the cables to the Photomultiplier Assembly and set them aside.
6. Remove the four nuts securing the Photomultiplier Assembly to the analyzer, being
careful to retain the nuts to reinstall the Photomultiplier Assembly.
2000-OSM, C1 8-27
Replacing the Burner Block
Heater
Vent Line
Mounting
Thermocouple Screws
Sample
H2 and/or
Carrier Thermocouple
Heater
Sulfur Addition
Wafer
Figure 8-11. BURNER BLOCK
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
9. Disconnect the hydrogen (H2) and carrier lines from the Burner Block.
10. Remove the bracket screws that fasten the Burner Block to the oven.
11. Slide the Burner Block off the end of the Photomultiplier Assembly and remove the
Burner Block from the oven.
12. Install the new Burner Block in reverse order of removing it.
2. To remove a particular O-Ring, carefully remove the associated connector and then
remove the O-Ring.
8-28 2000-OSM, C1
O-Ring
O-Ring 45051-4-106
45051-5-18
O-Ring O-Ring
45051-4-13 45051-4-106
CAUTION
2000-OSM, C1 8-29
The analyzer uses two different types of Methanizer/Air Cleaner Assembly, Type 781 and
Type 805. These are essentially the same except for appearance.
The Methanizer/Air Cleanup Assembly comes from the factory supplied with both air cleanup
and methanizer tubes. The larger tube is used for air cleanup and the smaller tube for the
methanizer. If a tube is not being used, its inlet and outlet connections will be plugged. It is
necessary to replace only the tube that is in use.
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
5. Label the tubing on both sides of the associated unions with temporary numbered tape
labels. The labels are later used to ensure correct tubing connections when the air
cleanup/methanizer is reinstalled.
Harness Assy
3 1 2 4
4 2 1 3
Air
Cleanup
Tube
Methanizer
Tube
6. Using 7/16-inch and 5/16-inch open-end wrenches, disconnect the tubing connections
from the reducing unions.
8-30 2000-OSM, C1
8. Remove the four Phillips head screws attaching the support brackets to the isothermal
oven wall. Secure the unit with your hand while removing the final top screws.
9. Lay the Methanizer/Air Cleanup Assembly on a suitable work surface within the
constrained length of the heater harness. If only the catalytic tubes are to be replaced,
the harness will not require further disconnection.
10. Type 781 only: Remove the four Phillips head screws attaching the support bracket to
the top unit end caps and lay them aside.
CAUTION
11. Mark the top and bottom caps and housing with a grease pencil or permanent marker.
When the caps are replaced with the marks aligned, the support bracket holes will be
correctly aligned.
12. Using a 9/64-inch Allen wrench, remove the four Allen head screws attaching the air
cleanup/methanizer top cap to the outer housing.
13. Grasp the housing and top cap. Withdraw the internal body assembly from the housing.
14. Using tweezers or a small screw driver, remove the insulation from around the body
assembly. Retain it for later use.
1. Using a 1/4-inch open-end wrench, disconnect the catalytic connections from the bottom
side of the cap.
2. To remove a catalytic tube, remove the Phillips head screw and flat washer located in
the center of the body at the opposite end from the harness.
3. Grasp the long coiled or “pig tail” end of the tubing and pull the short nutted end through
the body assembly.
5. Carefully rotate the body assembly and remove the Phillips head retaining screw and
flat washer.
6. Note the location of the cartridge heater, temperature probes and thermocouple.
Carefully extract the cartridge heater, probes and thermocouple from the air cleanup
body.
7. Inspect the probe end of the wiring harness for damage. If any harness wiring or
devices are damaged, replace the harness as described in "Packing the Housing" and
"Installing the Methanizer/Air Cleanup Assembly."
2000-OSM, C1 8-31
Installing the Catalytic Tubes
1. To install the air cleanup tube, insert the short end of the catalytic air tube through the
larger tube passage of the body and align it with the inside air inlet port connection of
the top cap.
2. To install the methanizer tube, insert the short end of the catalytic methanizer tube
through the smaller tube passage of the body and align it with the inside methanizer
inlet port connection.
3. Insert the tube fitting into the cap and tighten the inlet fitting nut finger tight.
6. Insert the flat washer retaining screw assembly into the center hole located in the end of
the body assembly opposite the harness and tighten it with the Phillips screwdriver.
7. If a new tube is being installed, a small loop or “pig tail” should be coiled in the tubing to
compensate for the excess tubing length. If installing an existing tube, the pig tail will
already be present.
8. Bend and position the coiled tubing such that the end fitting can be inserted into the
corresponding air or methanizer outlet connection port located on the bottom of the top
cap.
9. Tighten all inside catalytic tube inlet and outlet fittings, using a 1/4-inch open-end
wrench.
1. Pack a small amount of insulation around the probes, thermocouple, heater, and
associated wiring of the body assembly and set the assembly aside.
2. Using a 9/64-inch Allen wrench, loosen and remove the four Allen head screws
attaching the air cleaner/methanizer bottom cap to the outer housing. Separate and set
the bottom cap aside.
3. Carefully insert and press the body assembly into the outer housing.
4. Align the top cap with the marks on the outer housing. This will align the mounting
bracket holes in the top cap.
5. Install the four Allen head screws that secure the top cap to the outer housing and
tighten with a 9/64-inch Allen wrench.
6. Place a small quantity of insulation into the housing cavity and gently pack it down using
an object such as a screwdriver. Continue adding and packing in insulation until the
cavity is filled, taking care not the damage any wiring.
7. Install the bottom cap, aligning the mark on the cap with the mark on the housing. This
will align the bottom mounting bracket holes.
8-32 2000-OSM, C1
8. Install the four Allen head screws to secure the bottom cap to the housing, and tighten
with a 9/64-inch Allen wrench.
9. Type 781 only: Install the two mounting brackets with four Phillips head screws. The
mounting brackets should be aligned parallel to one another.
1. Attach the Methanizer/Air Cleanup Assembly to the interior of the isothermal oven wall.
Secure the air cleanup/methanizer with your hand while installing the four Phillips head
screws through the support bracket holes and into the mounting holes located in the
isothermal oven back interior wall.
2. Connect the tube connections to their respective reducing unions while matching the
numbers on the temporary labels.
5. Using a liquid leak detection solution, test for leaks and make necessary repairs before
proceeding.
6. Route the heater harness in the oven interior, following the same path as the original
harness installation.
7. Connect heater one wires to J48E terminals 1 and 2, and connect heater two wires to
J48E terminals 5 and 6.
9. Close and secure the isothermal oven door, and the Controller front and side doors.
1. Restore burner air to the cleanup unit by adjusting the burner air regulator for the correct
burner air pressure as indicated at the burner air pressure indicator.
2. If a methanizer is used, restore carrier gas by adjusting the carrier regulator for the
correct carrier pressure indication at the carrier pressure indicator.
3. Using a suitable liquid leak detection solution, test and repair any leaks that may be
present in the connections loosened or disconnected during the maintenance
procedure.
2000-OSM, C1 8-33
5. Restore carrier gas, oven air and fuel gas, if necessary, by adjusting the regulators for
the correct indications at the pressure indicators.
6. After ensuring the area is safe, and the proper permits are in effect, apply AC power.
8. Access the Manual Control Mode screen by pressing the F2 (Manual Control) soft key.
9. Access the Pressure and Temperature Control Mode by pressing the F4 (Press. and
Temp. Control) soft key.
10. From the Pres and Temp Control screen, position the cursor up or down to highlight
TEMP CONTROL and press the F2 (Manual Temperature Control) soft key to access
the Manual Temperature Control Screen.
11. On the Manual Temperature Control screen observe the setpoint value. If necessary,
change the setpoint of the air cleanup/methanizer temperature controller to 450° C.
12. The temperature of the Methanizer/Air Cleanup Assembly can also be monitored from
this screen. The time required to achieve stability is two hours.
13. Press the F1 soft key as necessary to return to the Background screen.
1. Restore all utility gases and verify that the pressures and flow rates are correct. These
include oven air, purge air, carrier, burner fuel, and burner air. If the faces of the
pressure gauges were previously marked and the marked location is known to be
correct, simply adjust the pressure regulators until the gauge pointers are aligned with
the pressure indicating marks. Refer to the engineering data package supplied with
your analyzer for the correct values.
2. After sufficient air purge time and when authorized by your safety administrator, apply
power to the analyzer.
3. Verify that all Digital Temperature Control setpoint values are correct. Refer to the
engineering data package supplied with your analyzer for the correct values.
5. Verify that sample is being introduced to and is sufficiently flowing through the analyzer
sample valve.
7. Once analyzer operation and performance have been verified, place the analyzer back
in service.
8-34 2000-OSM, C1
REPAIRING THE CARRIER GAS PANEL (ANALOG)
2. Remove the screw from the Carrier Gas Panel (see Figure 8-14).
(5) Unscrew
feedthroughs
2000-OSM, C1 8-35
5. In the isothermal oven, unscrew the feedthroughs (see Figure 8-15) and pull them down
approximately 0.5 inches; it is not necessary to completely remove them.
6. Open the Controller front door to gain access the mother board.
7. In the Control Housing access area, unplug the alarm switches from the mother board
and unscrew them from the manifold (see Figure 8-16).
8. In the Control Housing access area, remove the plugs from the manifold (see Figure
8-16).
9. In the Control Housing access area, remove the five socket head screws from the
manifold (see Figure 8-16).
Replacing a Regulator
8-36 2000-OSM, C1
9. Install the adjusting knob on the regulator.
Replacing a Gauge
3. Loosen the screws on the plate that secures the gauge to the panel and then remove
the plate.
7. Tighten the screws holding the gauge and plate to the panel.
1. Insert the Carrier Gas Panel into the Control Housing access area of the analyzer
controller.
2. In the Control Housing access area, install the five socket head screws into the manifold
(see Figure 8-16), making sure the sealing gasket is in place.
3. In the Control Housing access area, install the plugs into the unused ports of the
manifold (see Figure 8-16).
4. In the Control Housing access area, screw the alarm switches into the manifold (see
Figure 8-16) and plug the ware harness into their original locations on the mother board.
8. Install the screw in the Carrier Gas Panel (see Figure 8-14).
2000-OSM, C1 8-37
REPAIRING THE EPC CONTROL ASSEMBLY
2. Remove the two screws holding the EPC cover and remove the cover panel.
5. In the isothermal oven, unscrew the feedthroughs and pull them downward
approximately 0.5 inches; it is not necessary to remove them completely.
6. Open the Controller front door to gain access to the mother board.
7. At the left side of the mother board, disconnect the EPC Control Assembly cable from
J44.
8. On the EPC Multibus PCB in the card cage, disconnect the EPC Control Assembly
cable from J43 (near the bottom of the PCB).
9. In the Control Housing access area, unplug the alarm switches from the mother board
and unscrew them from the manifold.
10. In the Control Housing access area, remove the plugs from the manifold.
11. In the Control Housing access area, remove the five socket head screws from the
manifold.
12. Remove the four screws holding the Purge Air Panel in place and carefully pull the panel
forward and down.
13. On the side wall behind the Purge Air Panel remove the lock nut on the pipe nipple
which retains the EPC Panel cables (see Figure 8-17).
Lock Nut
8-38 2000-OSM, C1
14. Remove the screw on the side of the EPC Control Assembly.
Install the new EPC Control Assembly in the reverse order of removal, following the steps of
"Removing the EPC Control Assembly.".
CAUTION
The Zones are arranged in the EPC Control Assembly enclosure with Zone one on the left
and Zone 5 on the right (see Figure 8-18).
Screw and Proportional Valve, Sensor PCB,
Washer Zone 5 Zone 5
Proportional Valve,
Zone 1
Heater
Sensor PCB,
Zone 1
Control PCB
1. Remove the two screws holding the EPC cover and remove the cover panel.
2. Remove the ten screws holding the EPC Control Assembly cover and remove the cover.
Be careful not to damage the flame-proof or explosion-proof surfaces of the cover or the
body of the Control Assembly.
2000-OSM, C1 8-39
3. Unplug the large ribbon cable from the Control PCB (see Figure 8-19).
Heater Cable
AC Power Cable from
Backplane PCB J44
Valve Cable, Zone 1
Sensor PCB Cable, Valve Cable, Zone 2
Zone 1
Valve Cable, Zone 3
Sensor PCB Cable, Valve Cable, Zone 4
Zone 2
Valve Cable, Zone 5
Sensor PCB Cable,
Zone 3
4. Locate the Sensor to be replaced. Using a 1.5 mm hex socket wrench, remove the
screws and washers that retain the Sensor PCB.
6. Grasp the Sensor PCB at opposite corners and gently remove it from the EPC
Controller Assembly.
7. Check to ensure that o-ring is still on the Sensor PCB and not in the installation cavity.
If the o-ring is in the cavity, carefully remove it.
8. Remove the protective cap from the bottom of the new Sensor PCB and verify the
presence of an o-ring.
9. Place the Sensor PCB into position, with the cable iat the bottom right edge.
10. Place screws with nylon washers through holes in the Sensor PCB, then through the
spacers. (The spacers go into the recessed holes in the block.)
11. Alternate tightening the screws using a 1.5 mm torque limiting screwdriver set at 7 in.-
oz.
12. Plug the Sensor PCB cable into the corresponding connector on the Control PCB.
14. Reinstall the EPC Control Assembly cover and then insert the ten screws and tighten
them to 16 in.-lb. Ensure that the flame-proof or explosion-proof surfaces of the cover
or the body of the Control Assembly are not damaged.
15. Reinstall the EPC cover panel and insert the two holding screws.
1. Remove the two screws holding the EPC cover and remove the cover panel.
8-40 2000-OSM, C1
2. Remove the ten screws holding the EPC Control Assembly cover and remove the cover.
Be careful not to damage the flame-proof or explosion-proof surfaces of the cover or the
body of the Control Assembly.
3. Unplug the large ribbon cable from the Control PCB (see Figure 8-19).
4. Locate the valve to be replaced (See Figure 8-18) and disconnect the valve cable at the
connector on the Control PCB.
NOTE
You may need to remove the Sensor PCB cable from the Control PCB
to allow access to the connector of some zones.
5. Using a 3 mm hex socket wrench, remove the screws and washers that secure the
valve in place.
7. Before inserting the new valve, check the position of the o-ring on the valve. If the o-
ring is positioned at top of groove, use a solder aid or non-metal pick to roll the o-ring
down to the bottom of the groove. The o-ring must not be twisted.
8. Insert the new valve into its position in the enclosure. The wires coming out of the coil
should face the Control PCB (See Figure 8-18).
9. Assemble the spring or Belville washer and hex socket head screw, ensuring that the
concave side of the washer is facing away from the head of the screw.
10. Start the screw with the spring washer in the hole next to the valve.
11. Press down on the center of the valve and finish tightening the screw.
12. Inspect the area around the valve to ensure the o-ring has not been damaged.
13. Insert and tighten the second screw and washer, if applicable.
14. Plug all cables back into their corresponding connectors on the Control PCB.
15. Reinstall the EPC Control Assembly cover and then insert the ten screws and tighten
them to 16 in.-lb. Ensure that the flame-proof or explosion-proof surfaces of the cover
or the body of the Control Assembly are not damaged.
16. Reinstall the EPC cover panel and insert the two holding screws.
CAUTION
1. Remove the two screws holding the EPC cover and remove the cover panel.
2000-OSM, C1 8-41
2. Remove the ten screws holding the EPC Control Assembly cover and remove the cover.
Be careful not to damage the flame-proof or explosion-proof surfaces of the cover or the
body of the Control Assembly.
3. Unplug the large ribbon cable from the Control PCB (see Figure 8-19).
5. Using a 2.5 mm hex socket wrench, remove four screws and washers (two from the
triacs and two from the PCB mounting brackets).
6. Pull the Control PCB straight out of the enclosure toward you.
8. On the new Control PCB, place a thin layer of thermal joint compound on all sides and
the bottom of each RTD, and on the back of each triac.
9. Insert the Control PCB into enclosure with components and connectors facing up.
10. Align RTDs with the holes in the enclosure and ensure the RTDs are inserted in the
holes flush with the enclosure.
11. Using a 2.5 mm hex socket wrench, attach the Control PCB to the enclosure with four
screws and washers.
12. Insert the fish paper insulator between the enclosure and the back side (solder side) of
the Control PCB.
13. Plug all cables back into their corresponding connectors on the Control PCB.
14. Reinstall the EPC Control Assembly cover and then insert the ten screws and tighten
them to 16 in.-lb. Ensure that the flame-proof or explosion-proof surfaces of the cover
or the body of the Control Assembly are not damaged.
15. Reinstall the EPC cover panel and insert the two holding screws.
1. Remove the two screws holding the EPC cover and remove the cover panel.
2. Remove the ten screws holding the EPC Control Assembly cover and remove the cover.
Be careful not to damage the flame-proof or explosion-proof surfaces of the cover or the
body of the Control Assembly.
3. Unplug the large ribbon cable from Control PCB (see Figure 8-19).
4. Locate the Sensor PCBs for Zones 1 and 2 (see Figure 8-18).
5. Using a 1.5 mm hex socket wrench, remove screws and washers that mount the
Sensors and set these screws and washers aside for later use.
6. Remove the Sensor PCBs and set them aside for later reinstallation.
8-42 2000-OSM, C1
8. Carefully extract the heater from its cavity in the enclosure.
10. Insert the new heater in its cavity in the enclosure, making sure it goes all the way down
in the cavity.
13. Replace the Sensor PCBs, following steps 9 through 13 of "Replacing a Sensor PCB."
14. Reinstall the EPC Control Assembly cover and then insert the ten screws and tighten
them to 16 in.-lb. Ensure that the flame-proof or explosion-proof surfaces of the cover
or the body of the Control Assembly are not damaged.
15. Reinstall the EPC cover panel and insert the two holding screws.
The EPC should only require calibration if a component has been replaced. You should only
need to calibrate the particular zone affected by the servicing. To calibrate a zone:
3. Eliminate any back pressure to the zone by loosening the feedthrough fitting associated
with the zone to be calibrated (see Figure 8-20).
1 2 3 4 5
ZONE FITTINGS
4. On the Controller, verify the Background screen is displayed and then press the F2
(Manual Control) soft key.
5. On the Manual Control Mode screen press the F4 (Press. & Temp. Control) soft key.
2000-OSM, C1 8-43
6. On the Pres and Temp Control screen (see Figure 8-21), cursor to PRES CONTROL
and press the F2 (Manual Pressure Control ) soft key.
TEMP CONTROL
PRES CONTROL
TEMP CONFIGURATION
F1 F2 F3 F4
7. On the Manual Pressure control Mode screen (see Figure 8-22), enter the zone number
of the zone you want to calibrate.
Accept Calibrate
Escape Control Zone
Point
F1 F2 F3 F4
8-44 2000-OSM, C1
8. Press the F3 (Calibrate Zone) soft key. The GCC displays “Calibrate zone, hold switch
on board.”
9. Hold down the switch on the EPC Multibus PCB. The GCC displays “Are You Sure?”
10. Continue holding down the switch and press “Y” on the keyboard to save the new
calibration.
11. When the GCC displays “This zone has been calibrated,” release the switch.
12. If the Set Point shows an unexpected value, enter the desired set point value. (The
unexpected value is an offset corrected by the calibration; this is a software reporting
function only, which is not used by the system.)
1. Remove the four screws holding the panel in place (see Figure 8-23).
Mounting
Screws
Replacing a Regulator
2. Disconnect the lines from the back of the regulator, using 1/2-inch and 9/16-inch open-
end wrenches.
4. Remove the nut and sealing gasket securing the regulator to the panel.
2000-OSM, C1 8-45
7. Insert the new regulator through the hole in the panel.
8. Install the sealing gasket and fasten the nut securing the regulator to the panel.
Replacing a Gauge
2. Disconnect the line from the back of the gauge, using a 9/16-inch open-end wrench.
3. Loosen the screws on the plate that secures the gauge to the panel and then remove
the plate.
5. Insert the new gauge and sealing gasket through the hole in the panel.
7. Tighten the screws holding the gauge and plate to the panel.
1. Carefully put the panel back in place, aligning the mounting holes.
SETTING JUMPERS
The following paragraphs describe how to set the various PCB jumpers.
Backplane PCB
The Controller Backplane PCB has six jumpers to set up (see Figure 8-24).
Jumpers JP1 and JP5 are used to bypass pressure switch connection points for certain
analyzer configurations. Since the purge switches are daisy chained in series, it is
necessary to jumper across switches that are not connected. Jumper JP1 has its shunt
installed between pins 1 and 2 for standard or Sparger oven usage; the shunt is installed
between pins 2 and 3 for temperature programmed applications. Jumper JP5 has its shunt
installed between pins 1 and 2 for single purge area; the shunt is installed between pins 2
and 3 for dual purge location applications.
8-46 2000-OSM, C1
Jumpers JP2, JP3 and JP6 are associated with the purge alarm switch closures applied to
the Chroma I/O PCB. Jumper JP2 has its shunt installed between pins 1 and 2 for X Purge
applications only; the shunt is installed between pins 2 and 3 for Y or Z purge applications.
Jumper JP3 has its shunt installed between pins 1 and 2 for standard analyzers; the shunt is
installed between pins 2 and 3 for temperature programmed and Sparger applications.
Jumper JP6 has its shunt installed between pins 1 and 2 for single purge configurations; the
shunt is installed between pins 2 and 3 for dual purge applications.
Jumper JP4 is used to connect two detectors to a single Chroma I/O PCB. The location of
the jumper shunt depends on the revision of the Backplane PCB. Backplane PCBs that do
not have JP5 and JP6 are artwork revision D or earlier, while those having JP5 and JP6 are
artwork revision E or later.
• For revision D or earlier, the shunt is installed between pins 1 and 2 when the outputs of
two detector amplifiers are applied to a single Chroma I/O PCB; the shunt is installed
between pins 2 and 3 for normal operation (a Chroma I/O PCB dedicated to a single
detector amplifier).
• Revision E or later: the shunt goes between pins 1 and 2 for normal operation (a
Chroma I/O PCB dedicated to a single detector amplifier); the shunt is installed between
pins 2 and 3 when the outputs of two detector amplifiers are applied to a single Chroma
I/O PCB.
JP5 JP1
JP3
JP2
JP6
JP4
2000-OSM, C1 8-47
DTC Backplane PCB
The Digital Temperature Controller (DTC) PCB has eight jumpers and one switch to set up
(see Figure 8-25 for location).
Switch SW1 is used to save configuration information to protected memory. Its use is
described in “DIGITAL TEMPERATURE CONTROLLER” in Section 4, by the statement “Hold
down the switch on the DTC Backplane PCB.”
JP4
JP4
JP1
JP1
JP5
JP6
JP5
JP6
J2
J2
JP3
JP3
JP2
JP2
SW1
SW1
J3
J3
Jumpers J2 and J3 are T-Rating jumpers. The jumper shunts must be installed exactly as
shown below to ensure the temperature control operates properly. If they are set incorrectly,
T-Rating disagreement alarms will result (0 = no jumper; 1 = jumper installed).
8-48 2000-OSM, C1
JP1 is the service diagnostics jumper. For normal operation the shunt is installed between
pins 1 and 2. For service diagnostic screen use (only) the shunt is installed between pins 2
and 3. After servicing, the shunt must be reinstalled between pins 1 and 2.
JP4 is the VAC Conditioning Board jumper. If the analyzer has one VAC Conditioning PCB
installed, the shunt should be between pins 2 and 3. If the analyzer has two VAC
Conditioning PCBs installed, the shunt should be between pins 1 and 2.
JP2, JP3, JP5, and JP6 are the jumpers for the temperature zone boards. These jumpers
are required for the software to recognize unused zones. Jumpers are installed from the
even pins of unused zones to the even pins of used zones, for both Micro #1 (JP2 and JP3)
and Micro #2 (JP5 and JP6). If all zones are in use, no jumpers are installed. Zone jumpers
are identified as follows:
Example: if Zone 5 is not used, one jumper must be run between JP2-4 and JP2-2 or one of
the other pins listed under Micro #1 Pins, and a second jumper must be run between JP6-4
and JP6-2 or one of the other pins listed under Micro #2 Pins.
There can be up to five zone boards, one for each designated temperature zone. The
only jumper on a zone board is JP1 (see Figure 8-26). How this jumper is set
depends on the type of temperature sensor used for the zone. The jumper shunt
should be between pins 1 and 2 for a 400 ohm platinum probe sensor; it should be
between pins 2 and 3 for a thermocouple sensor.
3 2 1
JP1
2000-OSM, C1 8-49
VAC Conditioning PCB
There can be either one or two VAC Conditioning PCBs, depending on the application. Each
board has two jumpers to be set, JP4 and JP5 (see Figure 8-27). These jumpers are set
according to the voltage supplied to the board, as follows (JP4 is the hot side and JP5 is the
neutral side):
VAC CONDITIONING
ASSY 802A009B-
JP4
1
2
JP5
1
JP5
There is one adjustment and three jumpers on this board (see Figure 8-28). The adjustment
is potentiometer R56, which is used to set the display contrast for optimum viewing.
R56
The jumpers relate to the LOCOM option. JP5 has its shunt is between pins 1 and 2 for
normal operation, between pins 2 and 3 for LOCOM installations. JP6 and JP7
8-50 2000-OSM, C1
have the shunts in place for normal operation and the shunts removed for LOCOM
installations.
The jumper on this PCB relates to intercolumn detector usage. For normal operation shunts
should be installed in the first two positions at the right side of J18. These
shunts are removed for an application using intercolumn detectors (see Figure 8-29).
J18
J18
The jumpers on this PCB relate to amplifier gain, single or dual carrier, temperature ranges,
intercolumn detectors, and special testing (see Figure 8-30 for location).
WT13
GAIN HI
WT12
GAIN LO
WT11
WT9 WT10
CARRIER SINGLE
CARRIER DUAL
WT7 WT8
TEMP HI
WT3 WT6
WT2 WT1 WT4 WT5
TEMP LO TEMP LO CONSTANT TEMPERATURE
SERIAL NO.
FILIMENT BRIDGE
ASSY 802A003B-
TEMPERATURE JUMPERS
WT1 - WT6
2000-OSM, C1 8-51
The gain jumper is normally connected between WT11 and WT12. For high gain applications
this jumper is connected between WT12 and WT13.
The carrier jumper is normally connected between WT9 and WT10 (single carrier). For dual
carrier applications this jumper is connected between WT7 and WT8.
The temperature jumpers are normally connected between WT1 and WT2 and between
WT4 and WT5 (low temperature). For high temperature applications these jumpers are
connected between WT1 and WT3 and between WT4 and WT6.
For normal operation shunts should be installed in the first two positions at the right side of
J18. These shunts are removed for an application using intercolumn detectors.
The jumper between WT14 and WT15 must be in place for normal operation. It is only
removed when when hi-pot testing is to be performed.
The Thermistor Amplifier Interface PCB currently supports one or two Thermistor
Amplifier PCBs (see Figure 8-31).
JP2 JP2A
JP1 JP1A
1 2 3 1 2 3 1 2 3 1 2 3
JP2 JP1 JP1A JP2A
For single detector applications, one Thermistor Amplifier PCB is used, mounted in the
Amplifier #1 position. Jumpers JP-1, JP-2, JP-1A and JP-2A all have their shunts between
terminals 1 and 2. The output signal is routed through J13A.
For dual detector applications, two Thermistor Amplifier PCBs are used, mounted in the
Amplifier #1 and Amplifier #2 positions. Jumpers JP-1, JP-2 and JP-2A all have
8-52 2000-OSM, C1
their shunts between terminals 1 and 2. Jumper JP-1A has its shunt between terminals 2
and 3. The output signal of Amplifier #1 is routed through J13A and the output signal of
Amplifier #2 is routed through J13B.
This board has one jumper and one switch to set up (see Figure 8-32).
JP1 is the service diagnostics jumper. For normal operation the shunt is installed between
pins 1 and 2. For installation and service the shunt is installed between pins 2 and 3. After
installation or service, the shunt must be reinstalled between pins 1 and 2.
Switch SW1 is used to save configuration information to protected memory. Its use is
described in “ELECTRONIC PRESSURE CONTROL OPTION” in Section 4, by the
statement “Hold down the switch on the Electronic Pressure Control PCB.”
SW1
JP1
2000-OSM, C1 8-53
EPC Control PCB
This board has a single jumper, JP2 (see Figure 8-33). For normal operation JP2 has a
shunt between pins 2 and 3. For servicing of the block, the shunt is placed between pins 1
and 2 to turn off the heater.
JP2
U1 U18
CAUTION
This board can only be used when the analyzer also has the old type
Single Board Computer PCB (identified by having a toggle Reset
switch).
This board, part number 3528515-2, has two jumpers which are mutually exclusive. When
there is only one Chroma I/O PCB in the analyzer, or the board is used as Chroma I/O PCB
#1 in a simultaneous dual detector analyzer, the jumper will be located between the terminals
of JP1 (see Figure 8-34). This jumper is part of the printed circuit trace on this version of the
Chroma I/O PCB.
8-54 2000-OSM, C1
When a second Chroma I/O PCB is used, Chroma I/O PCB #2 must have the JP1 jumper
trace cut and a jumper installed between the JP2 terminals.
This board, part number 802A028D-_, has six jumpers, JP1 through JP6 (see Figure 8-35).
JP1: When there is only one Chroma I/O PCB in the analyzer, or the board is used as
Chroma I/O PCB #1 in a simultaneous dual detector analyzer, the shunt is installed
between pins 1 and 2.
When the board is used as Chroma I/O PCB #2, the shunt is installed between pins 2
and 3.
JP2 through JP6: These jumpers are installed between pins 2 and 3 on the Chroma I/O
PCB (later revisions of this board will have the jumpers hard-wired).
JP1
JP3
JP2 JP4
JP6 JP5
JP3
JP2
JP6 JP5 JP4
2000-OSM, C1 8-55
Power Supply PCB
This board has two jumpers (see Figure 8-36), neither of which should have a shunt installed
during normal operation. During troubleshooting a shunt can be installed between pins 1
and 2 of JP4 to enable the power supply LEDs. This shunt must be removed before
returning the analyzer to normal operation.
1 2 3
JP2
1 2 3
JP4
JP2 JP4
The Valco DV22-2110 ten-port diaphragm valve is used in some analyzers (see Figure 8-37).
This procedure and the accompanying illustrations were reprinted with permission of VICI,
Houston, TX, USA.
2. Using a 1/4-inch wrench, remove the connections from the valve cap.
8-56 2000-OSM, C1
3. Using a 7/64-inch hex key wrench, loosen the clamp ring screw.
4. Remove the valve from the clamp ring and take it out of the analyzer.
2. Note the location of port 1 on the valve, opposite the air inlet (see Figure 8-38).
3. Using a 9/64-inch hex key wrench, remove the screw from the valve cap (see Figure
8-39).
Hex Head
Screw
Plungers
Alignment
Pins
Body
4. Carefully remove the valve cap from the two alignment pins.
5. Set the cap aside, with the polished side up so that it does not get scratched.
2000-OSM, C1 8-57
7. Remove the plungers.
8. Install new plungers, ensuring that the counterbored end is up toward the valve cap (see
Figure 8-39).
9. Install new diaphragm, ensuring that the marking “TOP” is toward the valve cap. If there
is no marking, ensure the indentation in the diaphragm is toward the valve body (see
Figure 8-39).
10. Reinstall the valve cap, verifying that port 1 is correctly located.
11. Install the valve cap screw and tighten with a 9/64-inch hex key wrench.
1. Place the valve in the clamp ring and rotate it to the orientation of the valve that was
removed.
2. Using a 7/64-inch hex key wrench, tighten the clamp ring screw.
3. Install the connections to the valve cap, matching the numbering on the valve to the tags
on the connections.
Purpose
The VistaNET Communications Board in the Card Cage has an on-board debug monitor that
allows examination of the token bus communications. Several parameters accessible from
the debug connector allow the technician to easily troubleshoot common problems.
CAUTION
You must work carefully with the Debug Monitor. Inserting erroneous
information can cause networking problems. If such problems occur
you must reset the network to reinstate proper operation.
The VistaNET Communications Board has a connector that allows a serial cable to be
connected to the board. ABB Aftermarket Spares can provide this cable (P/N 3617695-1).
The RS-232 communications protocol allows the use of a laptop PC for access. Included in
Windows 95 is the Hillgraeve HyperTerminal Application, which emulates several popular
devices. This cable should be connected to the Communications Board (see Figure 8-40)
and to the appropriate COM port (Domain 1 or 2) on the laptop PC.
On the laptop PC, set the terminal emulation to VT100, and the associated serial parameters
to 9600 baud, 8 data bits, no parity, 1 stop bit, no handshaking.
8-58 2000-OSM, C1
J4
COMMUNICATIONS
PCB
COMMUNICATIONS
PCB
DEBUG J3
DOMAIN 1 J2
DOMAIN 2 J1
Startup
When you have set up the terminal application and connected to the communications board,
press <CTRL> A to invoke the Main Menu (see Figure 8-41).
When you exit the application, press <CTRL> Z to end the session.
CAUTION
Always end the session before exiting the monitor. While the monitor
is intended to be non-invasive, it can affect operation over time. Some
performance parameters are degraded by the monitor program.
2000-OSM, C1 8-59
The Main Menu is divided into three sections: the Information Display at the top of the
screen, Menu Items just below this information, and Statistical Data between the two
horizontal lines.
Information Display
Firmware Revision: Indicates the part number and revision of the communications board
firmware. The last digit of the revision indicates the position of the high-speed jumper
on the board (L indicates low speed operation, H indicates high-speed operation).
IRQ: Indicates “0” when the laptop PC is connected to the GC Communications Board.
Menu Items
Fill Memory: Entered as FM XXXX YYYY ZZ where XXXX is the starting address, YYYY
ending, ZZ pattern to be used to fill the memory block (all in hex).
Dump Packet: Entered as DP X where X = 0 to 16, indicating the buffer address of the
packet to be examined (0 is the DP RAM buffer last uploaded to the host).
8-60 2000-OSM, C1
Read/Write Memory: Entered as RWM XXXX YY where XXXX is the hexadecimal
addressed to be written with pattern YY, then read (all in hex).
Show Registers: Entered as SR (see Figure 8-43). The internal register contents of the
80C152 microcontroller are shown. Refer to the manufacturer’s data sheet for an
explanation of the contents. Type MM to return to the Main Menu.
Ignore Token: Entered as IT, used for software loading tests. In this mode, the
communications board remains part of the token bus, however tokens are merely
passed, and no UDP packets are transmitted or received at this node. THIS
COMMAND IS NOT TO BE USED IN THE FIELD.
Main Menu From the SFR display, this command returns to the main menu.
WARNING
Reset Statistics: Entered as RS, this command resets the cumulative statistics collected at
this node.
Reset stats Globally: Entered as RG, this command resets all cumulative statistics
collected at all nodes by sending a reset statistics command to all nodes by transmitting
a special token.
2000-OSM, C1 8-61
CAUTION
The Dump History command is rather invasive, and may cause this
station to drop tokens.
Dump History: Entered as DH, the history buffer maintained at this node is displayed (see
Figure 8-44).
Displayed are the source addresses of the last 255 stations to send a token on the wire.
Note that the address of the station displaying this buffer is not seen. The location of the
asterisks (***) shows the starting point of the display. The escape key will return to the
main menu. Pressing Enter will display the content of the next buffer captured.
Statistical Display
On the screen, several items of interest to the technician are displayed. The Statistical
Display is divided, roughly, into three columns: Transmit, Receive and General Statistics.
Following is an explanation of each screen element.
Transmit Statistics
Transmit Requests: Number of requests for UDP transmission from the host.
Buffers Recycled: Number of requests for UDP transmissions processed by this board.
8-62 2000-OSM, C1
Retries: Number of UDP transmissions retried. Under normal conditions, such as a
station off-line, this will be exactly twice the number of Transmit Errors.
Collisions: Number of times this station has detected a loss of transmission on the wire
due to collision with another station or overcome by noise.
Tokens Issued: Number of times this station has detected a dead line and the slot
assignment time has expired, resulting in an issuance of a token.
Tokens Dropped: Number of times the token destination did not accept the token, or
the token was lost. This indicates the number of times this station has seen a
station go off-line, or line noise caused the packet to be corrupted.
Receive Statistics
Errors: Number of unintelligible packets received by this station. Since there is an error
condition, it is indeterminate whether this was a UDP packet or a token.
Last Error: Encoded error condition indicating the failure detected by a receiver error,
as follows:
1. Overrun - indicates a new character received before the last was processed.
4. Alignment - indicates a new start of frame was detected before an end of frame.
16. Unknown - indicates more than one error condition existed during reception.
32. DMA Overrun - indicates the sending station attempted to send a packet larger
than UDP size, 524 bytes.
Uploads: Number of packets moved from the receive buffer pool into dual port memory
for transfer to the host.
Dequeued: Number of interrupts issued to this board from the host indicating
acknowledgement of a queued packet.
Backups: Number of times this station has run out of receive buffers due to host
interrupt latency.
Invalid: Number of times the host issued unknown commands to this board.
Tokens Received: Number of tokens received by this station. Tokens are broadcast
objects, all tokens are seen by every station.
2000-OSM, C1 8-63
Tokens Dumped: Number of tokens disposed of due to load at this station, or another
station issued a token (indicating a receiver problem at that station). A token was
seen on the wire while this station had a token.
General Statistics
Mode: Indicates the Software State of this station. These conditions are additive, bits
encoded as follows:
1. Receive Request Pending - A UDP packet has been received and needs
processing.
2. Receive Buffer Needed - The receiver buffer pool is full. When one is available,
re-enable the receiver.
8. Transmit Completed - The last UDP transmission was successful, notify host.
16. Transmit in Error - The last UDP transmission was in error, notify host.
32. Upload Completed - The last DMA transfer to the host is completed, notify host
a UDP packet has been received.
64. Initialization Requested - The host has requested the board reinitialize itself.
128. Line Timer Expired - The current transmission is taking too long, go into
override mode. The communications board will attempt to clear line condition.
(Caused by incorrect line biasing.)
256. Send Token - A token is ready to be sent to the next station in the token
algorithm.
512. Terminal Input Pending - Carriage return pressed by debug operator, Process
command.
1024. Debug Mode - Update screen each pass through processing loop.
Max Slack: Maximum difference between input and output, or host efficiency (lag).
8-64 2000-OSM, C1
Next Alive: Address of next station detected on the line.
Next Recvd: Address of the source address of the token seen on the wire subsequent
to this station sending a token.
Rate: Number of total detected errors per billion opportunities to generate errors.
The Dual Air Cleanup Assembly appears in analyzers having two detectors. Refer to Figure
8-45 for Dual Air Cleanup Assembly component location.
Harness
Assembly
3 1 2 4
CAUTION
Let the Dual Air Cleanup Assembly cool a minimum of 30 minutes prior
to disassembly. Internal surface temperatures can cause severe burns
if they are touched before they have cooled.
2000-OSM, C1 8-65
CAUTION
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
5. Label the tubing on both sides of the associated unions with temporary numbered tape
labels. The labels are later used to ensure correct tubing connections when the air
cleanup is reinstalled.
6. Using 7/16-inch and 5/16-inch open-end wrenches, disconnect the tubing connections
from the reducing unions.
8. Remove the four Phillips head screws attaching the support brackets to the isothermal
oven wall. Secure the unit with your hand while removing the final top screws.
9. Lay the air cleanup assembly on a suitable work surface within the constrained length of
the heater harness. If only the air cleanup tubes are to be replaced, the harness will not
require further disconnection.
CAUTION
10. Mark the top and bottom caps and housing with a grease pencil or permanent marker.
When the caps are replaced with the marks aligned, the support bracket holes will be
correctly aligned.
11. Using a 9/64-inch Allen wrench, remove the four Allen head screws attaching the air
cleanup top cap to the outer housing.
12. Grasp the housing and top cap. Withdraw the internal body assembly from the housing.
13. Using tweezers or a small screw driver, remove the insulation from around the body
assembly. Retain it for later use.
8-66 2000-OSM, C1
Removing the Air Cleanup Tubes
1. Using a 1/4-inch open-end wrench, disconnect the air cleanup tube connections from
the bottom side of the cap.
2. To remove an air cleanup tube, remove the Phillips head screw and flat washer located
in the center of the body at the opposite end from the harness.
3. Grasp the long coiled or “pig tail” end of the tubing and pull the short nutted end through
the body assembly.
4. Repeat steps 2 and 3 for the second air cleanup tube, if applicable.
5. Carefully rotate the body assembly and remove the Phillips head retaining screw and
flat washer.
6. Note the location of the cartridge heater, temperature probes and thermocouple.
Carefully extract the cartridge heater, probes and thermocouple from the air cleanup
body.
7. Inspect the probe end of the wiring harness for damage. If any harness wiring or
devices are damaged, replace the harness as described in "Packing the Housing" and
"Installing the Dual Air Cleanup Assembly."
1. To install an air cleanup tube, insert the short end of the catalytic air tube through the
larger tube passage of the body and align it with the inside air inlet port connection of
the top cap.
2. Insert the tube fitting into the cap and tighten the inlet fitting nut finger tight.
3. Repeat steps 1 and 2 for the second air cleanup tube, if applicable.
5. Insert the flat washer retaining screw assembly into the center hole located in the end of
the body assembly opposite the harness and tighten it with the Phillips screwdriver.
6. If a new tube is being installed, a small loop or “pig tail” should be coiled in the tubing to
compensate for the excess tubing length. If installing an existing tube, the pig tail will
already be present.
7. Bend and position the coiled tubing such that the end fitting can be inserted into the
corresponding air or methanizer outlet connection port located on the bottom of the top
cap.
8. Tighten all inside catalytic tube inlet and outlet fittings, using a 1/4-inch open-end
wrench.
1. Pack a small amount of insulation around the probes, thermocouple, heater, and
associated wiring of the body assembly and set the assembly aside.
2000-OSM, C1 8-67
2. Using a 9/64-inch Allen wrench, loosen and remove the four Allen head screws
attaching the air cleaner/methanizer bottom cap to the outer housing. Separate and set
the bottom cap aside.
3. Carefully insert and press the body assembly into the outer housing.
4. Align the top cap with the marks on the outer housing. This will align the mounting
bracket holes in the top cap.
5. Install the four Allen head screws that secure the top cap to the outer housing and
tighten with a 9/64-inch Allen wrench.
6. Place a small quantity of insulation into the housing cavity and gently pack it down using
an object such as a screwdriver. Continue adding and packing in insulation until the
cavity is filled, taking care not the damage any wiring.
7. Install the bottom cap, aligning the mark on the cap with the mark on the housing. This
will align the bottom mounting bracket holes.
8. Install the four Allen head screws to secure the bottom cap to the housing, and tighten
with a 9/64-inch Allen wrench.
1. Attach the Dual Air Cleanup Assembly to the interior of the isothermal oven wall. Secure
the air cleanup/methanizer with your hand while installing the four Phillips head screws
through the support bracket holes and into the mounting holes located in the isothermal
oven back interior wall.
2. Connect the tube connections to their respective reducing unions while matching the
numbers on the temporary labels.
5. Using a liquid leak detection solution, test for leaks and make necessary repairs before
proceeding.
6. Route the heater harness in the oven interior, following the same path as the original
harness installation.
7. Connect heater one wires to J48E terminals 1 and 2, and connect heater two wires to
J48E terminals 5 and 6.
9. Close and secure the isothermal oven door, and the Controller front and side doors.
8-68 2000-OSM, C1
Air Cleanup Testing
1. Restore burner air to the cleanup unit by adjusting the burner air regulator for the correct
burner air pressure as indicated at the burner air pressure indicator.
2. Using a suitable liquid leak detection solution, test and repair any leaks that may be
present in the connections loosened or disconnected during the maintenance
procedure.
4. Restore carrier gas, oven air and fuel gas, if necessary, by adjusting the regulators for
the correct indications at the pressure indicators.
5. After ensuring the area is safe, and the proper permits are in effect, apply AC power.
6. To check the temperature of the air cleanup assembly, exit to the Background screen by
pressing the F1 soft key.
7. Access the Manual Control Mode screen by pressing the F2 (Manual Control) soft key.
8. Access the Pressure and Temperature Control Mode by pressing the F4 (Press. and
Temp. Control) soft key.
9. From the Pres and Temp Control screen, position the cursor up or down to highlight
TEMP CONTROL and press the F2 (Manual Temperature Control) soft key to access
the Manual Temperature Control Screen.
10. On the Manual Temperature Control screen observe the setpoint value. If necessary,
change the setpoint of the air cleanup/methanizer temperature controller to 450° C.
11. The temperature of the air cleanup assembly can also be monitored from this screen.
The time required to achieve stability is two hours.
12. Press the F1 soft key as necessary to return to the Background screen.
1. Restore all utility gases and verify that the pressures and flow rates are correct. These
include oven air, purge air, carrier, burner fuel, and burner air. If the faces of the
pressure gauges were previously marked and the marked location is known to be
correct, simply adjust the pressure regulators until the gauge pointers are aligned with
the pressure indicating marks. Refer to the engineering data package supplied with
your analyzer for the correct values.
2. After sufficient air purge time and when authorized by your safety administrator, apply
power to the analyzer.
3. Verify that all Digital Temperature Control setpoint values are correct. Refer to the
engineering data package supplied with your analyzer for the correct values.
2000-OSM, C1 8-69
5. Verify that sample is being introduced to and is sufficiently flowing through the analyzer
sample valve.
7. Once analyzer operation and performance have been verified, place the analyzer back
in service.
This section describes how to replace the CP Valve slider, wedges, and o-rings. The bulletin
applies to both the 40 psig and 60 psig valves (see Figure 8-46).
VALVE BODY
VALVE PLATE
CARRIER
ASSEMBLY
CAUTION
NOTE
8-70 2000-OSM, C1
3. Turn off power and carrier gas.
The Slider is part of the Carrier Assembly. To ensure you have the correct slider for your
application, verify the slider part number from the Data Sheets supplied with your analyzer.
2. Open both Carrier Assembly latches by pulling down on the end of the latches.
3. Remove the Carrier Assembly from the Valve Plate and Valve Body, being careful to
keep the latches in their open position.
4. Compare the old slider with the new slider to ensure they are the same.
7. Insert the new slider, ensuring that the ports are aligned in the same way as the old
slider.
8. Wipe the bottom of the Valve Plate with methanol and a lint-free wipe to remove any
slider residue or contamination.
10. Close the back Carrier Assembly latch. This ensures the Carrier Assembly is locked into
the hole in the piston stem.
The four wedges (part number 3527279-1), located on the Carrier Assembly, center the
Valve Plate on the Carrier Assembly.
2. Open both Carrier Assembly latches by pulling down on the end of the latches.
3. Remove the Carrier Assembly from the Valve Plate and Valve Body.
2000-OSM, C1 8-71
5. Note the orientation of the wedges and push out each wedge from the outside of the
Carrier Assembly.
6. Insert a wedge from the inside of the Carrier Assembly, being careful not to scratch the
Carrier Assembly. Using a cold chisel, push the wedge into position, ensuring the back
of the wedge is against the carrier body.
10. Close the back Carrier Assembly latch. This ensures the Carrier Assembly is locked into
the hole in the piston stem.
Since the o-rings are inside the valve, you will have to remove the Valve Body from the
analyzer. The o-rings come in a kit, with different kits for 40-psig and 60-psig CP valves (see
Figure 8-47). The rework procedure is the same for both valves.
PART NUMBER
NOTE
2. Tag each port connection to the valve, using the port numbers stamped on the Valve
Plate.
8-72 2000-OSM, C1
3. Remove the port connections.
4. Remove the air connection on the Valve Body. (You do not have to remove the
connection on the Mounting Plate that attaches to the analyzer.)
5. Using a 7/64- inch hex key wrench, loosen the four screws that attach the Valve Body to
the Mounting Plate.
6. Rotate the Valve Body counterclockwise and remove it from the Mounting Plate.
7. Open both Carrier Assembly latches by pulling down on the end of the latches.
8. Remove the Carrier Assembly from the Valve Plate and Valve Body.
9. Push the piston rod into the Valve Body to release the piston, being careful not to
scratch any valve surfaces.
10. Remove the piston and piston rod from the Valve Body.
11. Remove the piston rod o-ring and the piston o-ring.
12. Wipe all surfaces of the piston and piston rod to remove contamination.
13. Verify that the screw holding the piston rod to the piston is tight.
14. Lubricate one o-ring part number 45051-4-11 with Molykote 33.
15. Position O-Ring Tool part number 3122-1 over the piston rod (see Figure 8-48).
LOCKWASHER
PISTON
PISTON O-RING
PISTON ROD
INSTALLATION TOOL
Figure 8-48. INSTALLING THE O-RINGS ON THE PISTON ROD AND PISTON
16. Install the o-ring over the O-Ring Tool and into the o-ring groove on the piston rod.
17. Lubricate o-ring part number 45051-4-61 (40-psig valve) or 45051-4-29 (60-psig valve)
with Molykote 33 and install it in the o-ring groove of the piston.
2000-OSM, C1 8-73
18. Remove the old o-ring from the Valve Body (see Figure 8-49).
O-RING
VALVE BODY
19. Wipe the inside of the Valve Body to remove contamination and old lubricant.
20. Inspect the piston rod bore to ensure the bore is clean.
21. Lubricate O-Ring part number 45051-4-35 (40-psig valve) or 45051-4-31 (60-psig valve)
with Molykote 33 and install it in the o-ring groove in the Valve Body.
22. Lubricate the piston rod and the inside of the Valve Body (the piston housing area) with
Molykote 33.
23. Insert the piston rod and piston rod assembly into the Valve Body. Before seating the
piston, ensure the flat surface on the piston rod is facing up.
25. Close the back Carrier Assembly latch. This ensures the Carrier Assembly is locked into
the hole in the piston stem.
27. Install the Valve Body over the screws on the Mounting Plate and rotate the Valve Body
clockwise to seat it. The port connections must face the same direction as when it was
originally installed.
28. Tighten the four screws securing the Valve Body to the Mounting Plate.
30. Reinstall the port connections, being careful to get each connection to the correct port.
31. Perform a leak check on the valve (see "Leak Check" in Section 2).
33. Check the operation of the valve (see "Manual Operation of Valves" in Section 2).
8-74 2000-OSM, C1
SECTION 9. REPLACEMENT PARTS
ORDERING INFORMATION
NOTE
Since the component parts specific to any given system are defined by
the particular application, you should refer to the “Recommended
Spare Parts Lists” in the Data Package supplied with the analyzer, to
obtain the full and correct part number for the desired part or assembly.
Equipment Identification
The following information, found in the Data Package and on the analyzer nameplate, should
be included in any communication concerning replacement parts or components:
• For serial numbered subassemblies such as PC boards, include the serial number and
the part number (including dash number and revision letter) for the subassembly in the
request. If a PC board requires conformal coating, prefix the PCB part number with the
letters "CC."
• Applicable references from the “Recommended Spare Parts List” of the Data Package,
included with each analyzer.
• Description of part.
The nameplate (see Figure 9-1), which is located on the right side of the Oven Compartment,
lists the hardware configuration information.
ABB
ABB AUTOMATION INC.
LEWISBURG WEST VIRGINIA 24901
TEMPERATURE CODE:
PRESSURIZATION TYPE: TYPE
The hardware configuration consists of the model number, customer order number, and T-
Rating.
2000-OSM, C1 9-1
Software Configuration Identification
The software configuration appears at the top of the Background screen just below "ABB
Analytical GCC." In Figure 9-2 the software configuration is 803V029-1G.
Software
Configuration
** B A C K G R O U N D **
ABB Analytical GCC Remote 0.1
803V029-1R (Std GCC) (C) 2001
**ALARM**
**ALARM** 18-JUN-12002 TUE 08:16:01
**ALARM**
Analysis Time :00114 Peaks Found : 00
Cycle Time :00000 State : Idle
F1 F2 F3 F4
Who to Contact
Contact Aftermarket Spares for specific ordering instructions. Include a complete description
of the component, analyzer, symptoms and problems with your request.
ABB Inc.
Attention: Aftermarket Spares
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
The remainder of this section lists the replaceable parts and components by their location in
the equipment. Part numbers and drawing numbers listed here are for identification
purposes only. When you order parts for replacement, use the list of parts included in the
Engineering Data Package provided with your equipment to ensure you have the correct
version of each part.
9-2 2000-OSM, C1
GC CONTROLLER
LO COMM
FRONT PCB
PANEL PCB
LO COMM DISPLAY
CABLE PANEL
Electronic Pressure
Control PCB
2000-OSM, C1 9-3
GCC Chassis (see Figure 9-5)
FID Amplifier
and/or
TCD
Amplifier
or
FPD
Amplifier Carrier
Solenoid Driver Alarm
PCB Switch
AC Conditioning PCB
(has both fuses) Panel
Assembly
DTC Zone
PCB
9-4 2000-OSM, C1
PURGE AIR PANEL (SEE FIGURE 9-7)
Pressure
Gauge Heater Air
Pressure Switch
1/4-inch
0 0 Tubing
Proportional
Valve
Sensor PCB
Heater
Control PCB
2000-OSM, C1 9-5
CARRIER GAS PANEL (SEE FIGURE 9-9)
Gauges
0 0 0 0 Filter/Restrictor
Regulators
NOTE
9-6 2000-OSM, C1
Temperature
Sensor
Detector
Thermocouple
Oven
Heater
Seals Stem
2000-OSM, C1 9-7
Flame Ionization Detector (see Figure 9-12)
Thermocouple
Polarizer
Ignitor
Jet
Reference Measure
Filament Filament
Reference Vent
Sample In
Sample Vent
TC Assembly
Reference In
9-8 2000-OSM, C1
Thermistor Type Thermal Conductivity Detector (see Figure 9-14)
Cable
Measure Reference
Thermistor Thermistor
Measurement Reference
Vent Vent
Measurement Reference
In In
Slider
Carrier
2000-OSM, C1 9-9
Type 781 Methanizer/Air Clean Up System (see Figure 9-16)
Harness Assy
4 2 1 3
Methanizer Tube
9-10 2000-OSM, C1
Valco Diaphragm Valve (see Figure 9-18)
Hex Head
Screw
Plungers
Alignment
Pins
Body
3 1 2 4
2000-OSM, C1 9-11
FLAME PHOTOMETRIC DETECTOR (FPD)
Transformer 3617648-1
Capillary Tubing, Burner Fuel (not shown) 5514584-39
Coaxial Cable Assy 3528546-1
Photomultiplier Assy 804A003-1
Solenoid, 3 Way (for X Purge) 3616261-3
Pressure Sensor 3615565-6
FPD Electrometer* 804A010-1
*see "GCC Chassis" for alternate location
Burner Block (see "Burner Block Components")
Pressure Sensor
Solenoid
Transformer
0 0
FPD Electrometer
Coaxial Cable
Photomultiplier
Burner Block
9-12 2000-OSM, C1
O-Ring 3/8-in OD, Fluorocarbon 45051-4-13
Breather Vent 3528205-1
Breather Line 753A038-5
Fitting 804M009-1
Sulfur Addition Wafer 3617453-_
Sulfur
Addition
Wafer
Detector
(FID shown)
Heater
2000-OSM, C1 9-13
Flame Ionization Detector with Heater Block (see Figure 9-23)
Detector
Heater
Block
Insulation
Detector
Heater
Block
Insulation
9-14 2000-OSM, C1
SECTION 10. VISTA BASIC
INTRODUCTION
Vista BASIC is for the user familiar with the fundamentals of BASIC programming languages
and general programming techniques. This information is provided for reference only, not as
a tool for teaching BASIC programming. "ALPHABETIC LISTING" lists the Vista BASIC
commands, functions and statements in alphabetical order, with descriptive information
included in each listing. "SUBJECT LISTING" lists the Vista BASIC commands, functions
and statements in subject order, as a quick reference guide.
Metacharacters are used to indicate language rules for syntax, but are not actually put into
the source program. Metacharacters and their meanings are as follows:
where 0000 is a Line Number from 0 - 9999; the Text Field has 33 spaces for program
text. The Line Number is not contained in the source program text file and is not
interpreted by Vista BASIC. It functions as a line location indicator only. The editor
automatically sorts the lines in ascending order by the Line Numbers.
Adding Lines: To add lines, press the soft key labeled “Insert.” A new line will be added
with the cursor positioned in the line number field. Entering a line number is optional but
is recommended to facilitate moving lines of text. When you move to the text field by
pressing the right arrow key, you can enter characters into the text field of the line.
Positioning the Cursor to a Line: You position the cursor on a particular line by moving it
with the up or down arrow key. The cursor will move up and down only when the cursor
is in the line number field.
Deleting Lines: To delete a line, move the cursor to the line to be deleted with the up and
down arrow keys and press the soft key labeled “Delete.”
Inserting Lines: To insert a line between two existing lines, position the cursor on the line
above where the new line is to be inserted, then press the soft key labeled “Insert.”
Lines are inserted after the line with the cursor.
Moving Lines: To move a line, cursor to the line number field of the line to be moved. Then
change the line number to a number greater than or equal to the line number of the line
above the new location and less than the line number below the new location.
Modifying Text: To make changes to a text line, position the cursor at the line to be
changed. Then move the cursor to the text field by pressing the right arrow key. Next
position the cursor at the character position to be changed. Corrections are made in an
overstrike mode rather than with character insertion and deletion.
2000-OSM, C1 10-1
Restrictions: Programming in Vista BASIC is limited according to the following
specifications.
In each program,
Vista BASIC program lines are contained in the Text Fields of edit lines and have the
following format:
Where "nnnnn" is the optional statement number in the range 1 through 65535. The
statement number is only required when it is the destination of a GOTO or GOSUB.
Where the statement is a valid Vista BASIC statement, a line may contain more than one
statement separated by colons (:). A statement can span more than one line by using a
continuation character (:) in the first column of the continuation line.
Character Set
Character Usage
_ underscore Identifiers
= equal sign Assignment and Relational Operator
+ plus sign Addition Operator
- minus sign Subtraction Operator and Unary Negation
* asterisk Multiplication Operator
/ slash Division Operator
( left parenthesis Delimiter
) right parenthesis Delimiter
> greater than Relational Operator
< less than Relational Operator
, comma Argument Separator
: colon Statement Separator/Continuation Character
. period Decimal Point
“ quotation mark String Delimiter
% percent sign Integer Type Declaration
$ dollar sign String Type Declaration
! exclamation point Single Precision Type Declaration
10-2 2000-OSM, C1
Constants
Integer Constants: Integer constants are whole numbers between -32768 and 32767,
inclusive. A decimal point indicates a floating point constant and is not allowed in
integer constants. Negative values are produced with the unary negation operator (-).
Floating Point Constants: A floating point constant is a number that contains a decimal
point and must have a digit or unary negation operator for the first character. Floating
point constants are of two forms: fixed point form and exponential form. Fixed point
constants must have a leading digit and decimal point somewhere within the number.
For exponential form floating point numbers, a fixed point constant is followed by the
letter E and an optionally signed integer with no blanks separating them.
Numbers between 0 and 1.0E ±38 approximately can be represented. Negative values
are indicated with the unary negation operator (-).
0.
0.123
-10.123
0.123E3
0.123E-3
Variables
Variable names and data types can be up to 40 characters (no spaces) and must start with a
letter. Subsequent characters may be letters, digits, or underscore (_) characters. The last
character may be an exclamation mark (!), dollar sign ($), or per cent sign (%) to indicate the
data type.
Integer Variables: Integer variables have names that end with the per cent sign (%) or
without any sign. These variables are used to store whole numbers between -32768
and 32767.
Floating Point Variables: These variables have names that end with an exclamation point
(!); these variables can store real numbers between -1.0E ±38 and +1.0E ±38.
String Variables: String variables have names that end with the dollar sign ($) and are
used to store strings of up to 255 characters. Examples of variable declaration:
2000-OSM, C1 10-3
ABC! declares a floating point variable
XYZ% declares an integer variable
A$ declares a string variable
I defaults to an integer variable.
Arrays
An array is a collection of scalar variables, all of which have the same data type and variable
name. An individual scalar variable or element of an array is referenced with the use of a
subscript.
The DIM statement defines the number of elements or extent of the array. For example, an
array with a dimension of ten has ten elements. A subscript must be in the range from 1 to
the number of array elements. For an array with a dimension of ten, subscripts go from 1 to
10. A subscript of one refers to the first array element. Usage of an array element before the
DIM statement is not allowed.
The COMMON! array is an array of floating point variables shared between all of the BASIC
programs. A reference to a particular element of COMMON! by any of the BASIC programs
accesses the same memory locations in memory. Values can be stored in COMMON! by a
BASIC program and those values can then be accessed by another BASIC program. Thus,
the COMMON! array is a mechanism whereby information and data values can be passed
between BASIC programs.
Another characteristic of the COMMON! array is that the memory allocation is static. That is,
the COMMON! array stays around forever and the values are retained between program
modifications and compilations. As a result, the contents of the COMMON! array normally
only change when a value is assigned to an array element by using the assignment
statement. If the analyzer is reset using the Reset switch on the Single Board Computer
PCB, the COMMON! array contents are reset to zero. All other variables are local and their
memory allocation is dynamic. Local variables maintain their values between program
executions, but not between compilations. When a program is successfully compiled, all
local variables are initialized to zero and the previous contents are destroyed.
+ addition
- subtraction
* multiplication
/ division
unary - operates on a single operand to yield the negation of the
operand.
10-4 2000-OSM, C1
Relational Operators: Relational operators are used to compare operands of the same
data type yielding a logical (Boolean) result. Since there are no Boolean type variables
in this implementation, the result of a relational operator cannot be stored in a variable,
unless a conversion routine is used. Relational operators are:
Logical Operators: The logical operators NOT, AND and OR operate on logical operands
to yield a logical result: TRUE or FALSE.
String Operators: The only string operator is concatenation, which is accomplished using
“+.”
() Parentheses
unary - Arithmetic
*/ Arithmetic
+- Arithmetic
< <= <> = >= > Relational
NOT Logical
AND Logical
OR Logical
ALPHABETIC LISTING
This section lists the Vista BASIC commands, functions and statements alphabetically, with
descriptive information in each listing to guide you in using the listing. VistaNET commands
are listed separately at the end of this section.
ACTIVATED BY Function
Description: Returns the code that defines how the Vista BASIC program was activated.
Syntax: ACTIVATED_BY
Comments: 0 = status cleared
1 = Manually
2 = Time Module
2000-OSM, C1 10-5
3 = End of Analysis
4 = End of Benchmark
5 = End of Calibration
Example: 0010 CODE = ACTIVATED_BY
0020 IF CODE = 1 THEN
0030 :LPRINT “ACTIVATED MANUALLY”
Description: Adds a Time Coded Function (TCF) to a method table (Sim Dis analyzers
only).
Syntax: ADD_TCF(method%,time%,function$,value$)
Comments: method% is the method table (1-8).
time% is the time at which the TCF is to occur.
function$ is the TCF the method table is perform at the specified time.
value$ is the TCF’s value.
Example: 0010 N = ADD_TCF(1,100,“FORCED GATE
0020 :”,“ON @ BASE”)
A Forced Gate TCF is added to method table 1 at 100 seconds.
Note: In the example, N represents one of the following numbers which is used to
indicate if the function was successful, or why it was unsuccessful, where:
0 means the TCF was successfully added to the method table.
-1 means there is no room to add TCFs.
-2 means time% has exceeded the cycle time of the method table.
-3 means function$ did not have a valid TCF.
-4 means value$ was not valid.
-13 means method% is not in the range 1-8.
ALARM Function
ASC Function
10-6 2000-OSM, C1
ASSIGN STREAM Command
BPRINT Statement
Description: Functions identically to LPRINT except BPRINT converts numeric values into
a string and places it in a string variable. See LPRINT statement for all
options.
Syntax: BPRINT TO string_var$ [USING format$;][expression[,expression]...]
Comments: string_var$ is a string variable.
format$ is a string constant or string variable whose value specifies the
format for conversions as defined for LPRINT.
Example 1: 0010 BPRINT TO A$ USING %3D;0,-1,
0020 :10,100
will put the following into A$: 000 0-1 010 100
Example 2: 0010 BPRINT TO A$ USING %9.2R;-0.12,
0020 :100.23
will put the following into A$: - 0.12 100.23
CHAIN Statement
CHR$ Function
CLEAR Command
2000-OSM, C1 10-7
Syntax: CLOCK_ERROR_ALARM
Example: 0010 IF CLOCK_ERROR_ALARM GOTO 12
Description: Is a predeclared array of floating point variables shared among all BASIC
programs. A reference to a particular element of COMMON! by any of the
BASIC programs accesses the same locations in memory. Values can be
stored in COMMON! by a BASIC program and then be accessed by another
BASIC program. COMMON! passes information and data values between
BASIC programs. The operator sets the maximum value for this array on the
Digital Configuration screen.
Syntax: COMMON!(index%)
Comments: index% are integers representing start point and end point of array.
Example: 0010 FOR I = 1 TO 3048
0020 COMMON!(I) = FLT(I)
0030 NEXT I
0040 END
Description: Returns a string containing the type of the component (% , PPM , or CALC).
Since each must have four characters to be correctly read, % must be
followed by three spaces and PPM followed by one space.
Syntax: COMP_TYPE$(method%,component%)
Comments: method% is the method table (1-8).
10-8 2000-OSM, C1
component% is the component number for which the type is sought.
Example: 0005 N = N_COMP(1)
0010 FOR I = 1 TO N
0015 IF COMP_TYPE$(1,I)<>"CALC"
0017 :GOTO 100
0020 LPRINT GET_CC(1,I)
For every component in method one (statements 5 and 10), check for the
units (statement 15). If the component is calculated, print the component’s
value; otherwise skip to statement 100.
Description: Returns the method for the stream currently being analyzed.
Syntax: CUR_METHOD
Comments: The value returned ranges from 1 to 8.
Example: 0010 N = CUR_METHOD
Note: use PREV_METHOD for stream that has just been analyzed.
Description: Returns the Cycle Time for the specified method table.
Syntax: CYCLE_TIME(method%)
Comments: method% is the method table (1-8).
Example: 0010 A% = CYCLE_TIME(1)
Gets the cycle time from analysis method one and assigns it to integer
variable A%.
2000-OSM, C1 10-9
DEACTIVATE STREAM Command
Description: Deletes all Forced Gate Time Coded Functions (TCFs) from a method table
(Sim Dis analyzers only).
Syntax: DELETE_ALL_GATE_TCFS (method%)
Comments: method% is the method table (1-8).
Example: 0010 N = DELETE_ALL_GATE_TCFS(1)
0020 FOR I = 1 TO N
0030 IF I/2*2 = I THEN
0040 :X = ADD_TCF(1,100+I*10,
0050 :“FORCED GATE”,“ON @ BASE”)
0060 :ELSE X = ADD_TCF(1,100+I*10,
0070 :“FORCED GATE”,“OFF @ BASE”)
0080 NEXT I
All Gate TCFs are deleted from method table 1; then a Gate TCF is added for
each one deleted.
Note: In the example, N represents one of the following numbers that
indicates if the function was successful, or why it was unsuccessful:
-1 means method% is not in the range 1-8.
-2 means the method table does not exist.
>0 is the number of TCFs deleted from the method table.
Description: Deletes all Time Coded Functions (TCFs) of the type specified from a method
table (Sim Dis analyzers only).
Syntax: DELETE_ALL_TCFS(method%, function$)
Comments: method% is the method table (1-8).
function$ is the TCF to be deleted from the method table.
Example: 0010 N = DELETE_ALL_TCFS(1,
0020 :“FORCED GATE”)
0030 LPRINT N
All Forced Gate TCFs are deleted from method table 1; then the number of
deleted TCFs is printed.
Note: In the example, N represents one of the following numbers that
indicates if the function was successful, or why it was unsuccessful, where:
-1 means method% is not in the 1-8 range.
-2 means the method table does not exist.
-3 means function$ did not have a valid TCF.
>0 is the number of TCFs deleted from the method table.
DIM Statement
10-10 2000-OSM, C1
Syntax: DIM variable(extent)[,variable(extent)]....
Comments: variable is the variable name of the array.
extent is the number of elements in the array.
Notes: a) Only one dimension is allowed.
b) Array subscripts must be from 1 to the array dimension (extent).
c) To use a variable as an array, it must be declared before use in the
DIM statement.
Example: 0020 DIM A!(N_COMP(1)),B$(10),C%(50)
Declares an array A! of floating point variables with as many elements as
there are components in analysis method 1, array B$ of 10 strings, and array
C% of 50 integer variables.
END Statement
EXPONENT Function
Description: Returns e (i.e., 2.71828) raised to the power of the floating point expression.
Syntax: EXP(fp!)
Comments: fp! is a floating point expression.
Example: 0010 A! = EXP(T!)
Raises e to the power of floating point variable T! and assigns it to floating
point variable A!.
FOR...NEXT Statements
2000-OSM, C1 10-11
Example: 0010 FOR I = 100 TO -100 STEP -2
.
.
0020 NEXT I
Executes loop 101 times with loop counter values of 100, 98, 96, ..., 0, ..., -96,
-98, and -100.
Description: Returns the setting for the Sim Dis ASTM parameter in the Sim Dis Setup
Screen (Sim Dis analyzers only).
Syntax: GET_ASTM
Comments: 0 is returned when the ASTM parameter is set to ASTM-2887.
1 is returned when the ASTM parameter is set to ASTM-3710.
Example: 0010 IF GET_ASTM = 0 THEN END
0020 FOR I = 1 TO 10
0030 D86!(I) = 0.0
0040 NEXT I
Checks Sim Dis Setup screen parameter ASTM. When ASTM 3710 is not
selected the program ends. Otherwise, program variables are set to zero.
Description: Returns the setting for the Sim Dis Blend Number parameter in the Stream
Table (Sim Dis analyzers only).
Syntax: GET_BLEND(stream)
Example: 0010 LPRINT GET_BLEND(1)
The Blend Number for stream one is printed.
10-12 2000-OSM, C1
Syntax: GET_CAL_CONC(method%,component%)
Comments: method% is the method table (1-8).
component% is the component number for which the calibration
concentration is to be retrieved.
Example: 0010 A! = GET_CAL_CONC(1,2)
Gets the calibration concentration of component two from analysis method
one and assigns it to floating point variable A!.
Description: Reads one of the 25 Sim Dis Correlation Factor Tables into a BASIC array
(Sim Dis analyzers only).
Syntax: GET_FACT_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the destination of the data
read from the table.
table% is the table (1-25).
Example: 0010 N = LEN_FACT_TBL(1)
0020 DIM FACT!(N)
0030 GET_FACT_TBL(FACT!,1)
Variable N gets the number of entries in the Correlation Factor table; array
FACT! is dimensioned to have as many elements as entries in the table; the
table is read into the array.
Description: Returns the Sim Dis Maximum Peak parameter from the Sim Dis Setup
Screen (Sim Dis analyzers only).
Syntax: GET_MAX_PEAK_PARM
Example: 0010 LPRINT GET_MAX_PEAK_PARM
Prints Max Peak from the Sim Dis Setup Screen.
2000-OSM, C1 10-13
GET MULTIPLIER EXPONENT Function
Description: Returns the Sim Dis Peak Type from the Sim Dis Setup Screen (Sim Dis
analyzers only).
Syntax: GET_PEAK_TYPE
Comments: 0 means peaks are selected by area
1 means peaks are selected by height
Example: 0010 LPRINT GET_PEAK_TYPE
The Sim Dis Setup screen parameter, Peak Type, is printed on the teleprinter.
Description: Returns the percent off for a given temperature using a specified Time vs.
Boiling Point Table (Sim Dis analyzers only).
Syntax: GET_POFF(temperature!,time_vs_bp_table%)
Comments: temperature! is the temperature to convert to a percent off.
time_vs_bp_table% is the Time vs. Boiling Point Table (1-8) to use for the
conversion.
Example: 0010 PERCENT! = GET_POFF(212.0,1)
Returns the percent off for 212.0 degrees.
Description: Returns a percent off for a given time using a specified Time vs. Boiling Point
Table (Sim Dis analyzers only).
Syntax: TIME_TO_OFF(time!,time_vs_bp_ table%)
Comments: time! is the time to convert to a percent off.
time_vs_bp_table% is the Time vs. Boiling Point Table (1-8) to use for the
conversion.
Example: 0010 PERCENT! = TIME_TO_OFF(100.0,1)
Returns the percent off that occurred at 100.0 seconds.
10-14 2000-OSM, C1
GET PERCENT OFF TABLE Command
Description: Returns the percent off column of one of the eight Time vs. Boiling Point
tables (Sim Dis analyzers only).
Syntax: GET_POFF_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the destination of the Percent
Off Table.
table% is the table number (1-8).
Example: 0010 N = LEN_POFF_TBL(1)
0020 DIM A!(N)
0030 GET_POFF_TBL(A!,1)
Gets the Percent Off Table size, dimensions an array to hold it, copies the
table into array A!.
Description: Returns the temperature for a given percent off using a specified Time vs.
Boiling Point Table (Sim Dis analyzers only).
Syntax: GET_TEMP(percent_off!,time_vs_bp_table%)
Comments: percent_off! is the percent off to convert to a temperature.
time_vs_bp_table% is the Time vs. Boiling Point Table (1-8) to use for the
conversion.
Example: 0010 TEMP! = GET_TEMP(50.0,1)
Returns the temperature for 50.0 percent off.
2000-OSM, C1 10-15
GET TEMPERATURE FOR A TIME Command
Description: Returns a temperature for a given time using a specified Time vs. Boiling
Point Table (Sim Dis analyzers only).
Syntax: TIME_TO_TEMP(time!,time_vs_ bp_table%)
Comments: time! is the time to convert to a temperature.
time_vs_bp_table% is the Time vs. Boiling Point Table (1-8) to use for the
conversion.
Example: 0010 TEMP! = TIME_TO_TEMP(100.0,1)
Returns the temperature that occurred at 100.0 seconds.
Description: Returns the temperature column from one of the eight Time vs. Boiling Point
Tables (Sim Dis analyzers only).
Syntax: GET_TEMP_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the destination of the
Temperature Table.
table% is the table number (1-8).
Example: 0010 N = LEN_TEMP_TBL(1)
0020 DIM A!(N)
0030 GET_TEMP_TBL(A!,1)
Gets the size of the Temperature Table, dimensions an array to hold it, copies
the table into array A!.
Description: Returns a time for a given percent off using a specified Time vs. Boiling Point
Table (Sim Dis analyzers only).
Syntax: POFF_TO_TIME(percent_off!,time_vs_bp_table%)
Comments: percent_off! is the percent off to convert to a time.
time_vs_bp_table% is the Time vs. Boiling Point Table (1-8) to use for the
conversion.
Example: 0010 TIME! = POFF_TO_TIME(50.0,1)
Returns the time that 50.0 percent off occurred.
Description: Returns a time for a given temperature using a specified Time vs. Boiling
Point Table (Sim Dis analyzers only).
Syntax: TEMP_TO_TIME(temperature!,time_vs_bp_table%)
Comments: temperature! is the temperature to convert to a time.
time_vs_bp_table% is the Time vs. Boiling Point Table (1-8) to use for the
conversion.
Example: 0010 TIME! = TEMP_TO_TIME(212.0,1)
Returns the time that 212.0 degrees occurred.
10-16 2000-OSM, C1
GET TIME VS. BOILING POINT TABLE Command
Description: Returns one of the eight Time vs. Boiling Point Tables (Sim Dis analyzers
only).
Syntax: GET_TVSBP_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the destination of the Time vs.
Boiling Point Table.
table% is the table number (1-8).
Example: 0010 N = LEN_TVSBP_TBL(1)
0020 DIM A!(N)
0030 GET_TVSBP_TBL(A!,1)
Gets the size of the Time vs. Boiling Point Table, dimensions an array to hold
it, copies the table into array A!.
GOTO Statement
GO TO SUBROUTINE Statement
2000-OSM, C1 10-17
Example: 0010 IF IDLE_ALARM THEN LPRINT “ALARM”
IF Statement
Description: Returns a string with the sample inject date and time for the current stream,
uses the same format as TIME$ and PREV_INJT.
Syntax: INJT
Example: 0010 A$ = INJT
String variable A$ gets inject time and date for the current sample.
Description: Returns a two-element array with the sample inject date and time for the
current stream. The first element in the array gives the UCT date since 1
January 1970. The second element gives the time in seconds since midnight.
Syntax: INJT_UCT(T!)
Example: 0010 DIM T!(2)
0020 INJT_UCT(T!)
INSTR Function
0010 P = INSTR(“ABCDEFGHIJKLMNOP”,“RS”)
The variable P is set to zero.
0010 P = INSTR(“ABCDEFGHIJKLMNOP”,“HO”)
The variable P is set to zero.
10-18 2000-OSM, C1
Example: 0010 I = INT(A!)
Converts the value of floating point variable A! to an integer and assigns it to
integer variable I.
Description: Returns the number of entries in the specified Sim Dis Correlation Factor
Table (Sim Dis analyzers only).
Syntax: LEN_FACT_TBL(table%)
Comments: table% is the specified Sim Dis Correlation Factor Table (1-25).
Example: 0010 N = LEN_FACT_TBL(1)
0020 DIM FACT!(N)
0030 GET_FACT_TBL(FACT!,1)
Variable N gets the number of entries in the Sim Dis Correlation Factor Table;
array FACT! is dimensioned with as many elements as entries in the table; the
table is read into the array.
Description: Returns the length of the percent off column of one of the eight Time vs.
Boiling Point Tables (Sim Dis analyzers only).
Syntax: LEN_POFF_TBL(table%)
Comments: table% is the table number (1-8).
Example: 0010 N = LEN_POFF_TBL(1)
Gets the length of the Percent Off Table.
Description: Returns the length of the temperature column of one of the eight Time vs.
Boiling Point Tables (Sim Dis analyzers only).
Syntax: LEN_TEMP_TBL(table%)
Comments: table% is the table number (1-8).
Example: 0010 N = LEN_TEMP_TBL(1)
Gets the length of the Temperature Table.
Description: Returns the length of one of the eight Time vs. Boiling Point Tables (Sim Dis
analyzers only).
Syntax: LEN_TVSBP_TBL(table%)
Comments: table% is the table number (1-8).
Example: 0010 N = LEN_TVSBP_TBL(1)
Gets the length of the Time vs. Boiling Point Table.
2000-OSM, C1 10-19
LET Statement
LPRINT Statement
Note: With USING, all data items contained in the LPRINT statement
must be of the same data type and agree in type with the format
specification.
10-20 2000-OSM, C1
“p” is an optional number that specifies the precision, or number of
digits to the right of the decimal point. If “p” is not specified,
it is assumed to be 2.
2000-OSM, C1 10-21
Example: 0010 LPRINT USING %3I;0,-1,10,100
will print “0 -1 10 100”
Description: Returns the maximum Sim Dis peak height (Sim Dis analyzers only).
Syntax: SD_PEAK_HEIGHT
Example: 0010 HEIGHT! = SD_PEAK_HEIGHT
Returns the maximum height found during the Sim Dis analysis.
Description: Returns natural Logarithm (to the base e) of floating point expression.
Syntax: LN(fp!)
Comments: fp! is a floating point expression.
Example: 0010 A! = LN(2.71828)
The natural logarithm (logarithm to the base e) of 2.71828 is assigned to
floating point variable A!.
10-22 2000-OSM, C1
OPERATOR MESSAGE ALARM Function
Description: Returns the component number whose retention time matches the crest time
for the peak.
Syntax: PK_COMP_NUM(peak%)
Comments: peak% is the peak number (1 to N_PEAKS).
Example: 0010 LPRINT COMP_NAME$(1,
0020 :PK_COMP_NUM(2))
Prints the name of the component in method one for the second peak
detected in the analysis.
2000-OSM, C1 10-23
Example: 0010 FOR I = 1 TO N_PEAKS
0020 LPRINT PK_END_AMP(I)
0030 NEXT I
Prints the amplitude of each peak’s end.
10-24 2000-OSM, C1
POST ANALYSIS ERROR ALARM Function
Description: Returns a string containing date and time for the sample injection performed
in the most recently completed analysis cycle. The string has the following
format:
hh:mm:ss Day DD Mon YYYY
(e.g., 17:46:31 Mon 6 Nov 1989)
Syntax: PREV_INJT
Example: 0010 A$ = PREV_INJT
The string variable A$ gets the time and date for the sample injection.
Description: Returns a two-element array containing date and time for the sample injection
performed in the most recently completed analysis cycle. The first element in
the array gives the UCT date since 1 January 1970. the second element
gives the time in seconds since midnight.
Syntax: PREV_INJT_UCT(T!)
Example: 0010 DIM T!(2)
0020 PREV_INJT_UCT(T!)
Description: Returns the method for the stream that has just been analyzed.
Syntax: PREV_METHOD
Comments: The value returned ranges from 1 to 8.
Example: 0010 N = PREV_METHOD
2000-OSM, C1 10-25
Example: 0010 IF HIGH_CONC_ALARM THEN PURGE(3)
If a high concentration alarm occurs, purge stream 3.
Description: Sets the Sim Dis ASTM parameter in the Sim Dis Setup Screen (Sim Dis
analyzers only).
Syntax: PUT_ASTM(setting%)
Comments: setting% is the ASTM parameter in the Sim Dis Setup Screen, where:
0 sets the ASTM parameter to ASTM-2887
1 sets the ASTM parameter to ASTM-3710
Example: 0010 PUT_ASTM(0)
The ASTM parameter in Sim Dis Setup Screen is set to ASTM2887.
Description: Sets the Sim Dis Blend Number parameter in the Stream Table (Sim Dis
analyzers only).
Syntax: PUT_BLEND(stream%,setting%)
Comments: stream% is the stream to get the blend for.
setting% is the Sim Dis Blend Number (1-25), also known as the Correlation
Factor Table.
10-26 2000-OSM, C1
Example: 0010 PUT_BLEND(1,25)
Sim Dis Blend Number for stream 1 in the Stream Table is set to 25.
Description Writes an array into one of the Sim Dis Correlation Factor Tables (Sim Dis
analyzers only).
Syntax: PUT_FACT_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the data source.
table% is the Sim Dis Correlation Factor Table (1-25).
Example: 0010 N = LEN_FACT_TBL(1)
0020 DIM FACT!(N)
0030 GET_FACT_TBL(FACT!,1)
0040 PUT_FACT_TBL(FACT!,2)
Variable N gets the number of entries in the Correlation Factor Table; array
FACT! is dimensioned to have as many elements as entries in table 1. Then
the table is read into the array and the array is written back to table 2.
2000-OSM, C1 10-27
PUT EXPECTED RETENTION TIME Command
Description: Changes the expected retention time for a particular component and sorts all
method table components in ascending order of expected retention times.
Syntax: PUT_EXPECTED_RT(method%,component%,retention_time%)
Comments: method% is the method table (1-8).
component% is the component number for which the expected retention time
is to be updated.
retention_time% is the new expected retention time for the specified
component.
Example: 0010 PUT_EXPECTED_RT(1,2,123)
The peak for the second component is expected to crest at approximately 123
seconds into analysis method one.
Description: Writes an array into the %off column of a Time vs Boiling Point Table (Sim Dis
analyzers only).
Syntax: PUT_POFF_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the data source.
table% is the Sim Dis TvsBP Table (1-8).
Example: 0010 N = LEN_POFF_TBL(1)
0020 DIM POFF!(N)
0030 GET_POFF_TBL(POFF!,1)
0040 PUT_POFF_TBL(POFF!,2)
Variable N gets the number of entries in the TvsBP Table; array POFF! is
dimensioned to have as many elements as entries in table 1. Then the table
is read into the array and the array is written back to table 2.
Description: Updates the set point and ramp rate of the specified zone.
Syntax: PUT_PRESS(zone%,set point!,ramp rate!)
Comments: zone% is the zone number (1-5).
set point! is the desired set point value.
ramp rate! is the desired ramp rate value.
Example: 0010 Z1! = GET_PRESS(1)
0020 PUT_PRESS(2,Z1!,0)
Gets the actual pressure of zone 1 and gets 0 ramp rate and inserts them as
the set point and ramp rate values for zone 2.
Description: Updates settings for the teleprinter report parameters, the same parameters
set in the Printer Report Type screen.
10-28 2000-OSM, C1
Syntax: PUT_REPORT_TYPE(report_type%)
Comments: report_type
0 = RAW DATA and NEVER
1 = RAW DATA and ALWAYS
2 = RAW DATA and ON ALARM
4 = REGULAR and NEVER
5 = REGULAR and ALWAYS
6 = REGULAR and ON ALARM
8 = SHORT and NEVER
9 = SHORT and ALWAYS
10 = SHORT and ON ALARM
Example: 0010 PUT_REPORT_TYPE(2)
A raw data report will be printed on the teleprinter at the end of analysis if an
alarm has been set.
Description: Updates the set point and ramp rate of the specified zone.
Syntax: PUT_TEMP(zone%,set point!,ramp rate!)
Comments: zone% is the zone number (1-5).
set point! is the desired set point value.
ramp rate! is the desired ramp rate value.
Example: 0010 Z1! = GET_TEMP(1)
0020 PUT_TEMP(2,Z1!,0)
Gets the actual temperature of zone 1 and gets 0 ramp rate and inserts them
as the set point and ramp rate values for zone 2.
Description: Writes an array into the boiling point column of a Time vs Boiling Point Table
(Sim Dis analyzers only).
Syntax: PUT_TEMP_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the data source.
table% is the TvsBP Table (1-8).
Example: 0010 N = LEN_TEMP_TBL(1)
0020 DIM TEMP!(N)
0030 GET_TEMP_TBL(TEMP!,1)
0040 PUT_TEMP_TBL(TEMP!,2)
Variable N gets the number of entries in the TvsBP Table; array TEMP! is
dimensioned to have as many elements as entries in table 1. Then the table
is read into the array and the array is written back to table 2.
2000-OSM, C1 10-29
PUT TIME VS. BOILING POINT TABLE Command
Description: Writes to one of eight Time vs. Boiling Point Tables (Sim Dis analyzers only).
Syntax: PUT_TVSBP_TBL(array!,table%)
Comments: array! is a previously dimensioned array that is the destination of the Time
vs. Boiling Point Table.
table% is the table number (1-8).
Example: 0010 N = LEN_TVSBP_TBL(1)
0020 DIM A!(N)
0030 GET_TVSBP_TBL(A!,1)
0040 PUT_TVSBP_TBL(A!,2)
Variable N gets the number of entries in the TvsBP Table; array A! is
dimensioned to have as many elements as entries in table 1. Then the table is
read into the array and the array is written back to table 2.
NOTE
The Chroma I/O Board must have A/D Converter ICs UG1 and UH1
installed (see Figure 10-1) in order for this function to operate.
UH1 UG1
Example: For this example, let a temperature sensor register -4096 at -30°C and 4095
at 1000°C.
0010 SLOPE! = (1000.-(-30.))/(4095.-(-4096.))
0020 T_ZERO! = 1000. - SLOPE! * 4095.
0030 TEMPERATURE! = SLOPE! * FLT(
0040 :RAI(0)) + T_ZERO!
10-30 2000-OSM, C1
Use “T=mx+T0” to compute temperature from the reading of the A/D
converter, where “m” is the slope of the line, “x” is the A/D value, and “T0” is
the temperature at an A/D value of zero.
REMARKS Command
Description: Returns an integer indicating the report selected in the Printer Report Type
screen.
Syntax: REPORT_TYPE
Comments: 0 = RAW DATA and NEVER
1 = RAW DATA and ALWAYS
2 = RAW DATA and ON ALARM
4 = REGULAR and NEVER
5 = REGULAR and ALWAYS
6 = REGULAR and ON ALARM
8 = SHORT and NEVER
9 = SHORT and ALWAYS
10 = SHORT and ON ALARM
Example: 0010 IF REPORT_TYPE/4<>0 GOTO 9999
0020 LPRINT REPORT
0030 9999 END
If RAW DATA reports are selected on the Printer Report Type screen,
REPORT is printed; otherwise, nothing is printed.
2000-OSM, C1 10-31
Comments: stream% is the stream (from 1 to the maximum number of streams) to be
analyzed.
Example: 0010 RQANA(1)
Requests an analysis for stream one.
Description: Resets BASIC’s time limit allowing the program more time to execute (Sim Dis
analyzers only).
Syntax: RESET_TIME_LIMIT
Example: 0010 FOR I = 1 TO 10000
0020 NEXT I
0030 RESET_TIME_LIMIT
The time limit is reset to allow the program to continue executing past the
normal time limit.
10-32 2000-OSM, C1
a name from the Sensor screen on the analyzer.
Example: 0010 SET_BASIC_COMP_ALARM(2)
SPACE Function
2000-OSM, C1 10-33
SUBSTRING Function
Description Returns the state of GCC Time Coded Function Error Alarms.
Syntax: TCF_ERROR_ALARM
Example: 0010 IF TCF_ERROR_ALARM GOTO 100
Description: Returns units of temperature for the analyzer as specified in the Sim Dis
Setup Screen (Sim Dis analyzers only).
Syntax: T_UNITS
Comments: 0 = Temperature Units in Fahrenheit
1 = Temperature Units in Celsius
2 = Temperature Units in Kelvin
Example: 0010 IF T_UNITS = 1 THEN
0020 :T!=9.0/5.0*T!+32.0
Temperature in degrees Celsius is converted to Fahrenheit when the
Temperature Units Parameter in the Control Parameters Screen has been set
to Fahrenheit.
TIME Function
Description: Returns a string containing the date and time in the following format:
hh:mm:ss Day DD Mon YYYY
(e.g., 17:46:31 Mon 6 Nov 1989)
Syntax: TIME$
Example: 0010 A$ = TIME$
The string variable A$ gets the time and date.
Description: Returns a two-element array containing the date and time. the first element in
the array give the UCT date since 1 January 1970. the second element gives
the time in seconds since midnight.
Syntax: TIME_UCT(T!)
Example: 0010 DIM T!(2)
0020 TIME_UCT(T!)
10-34 2000-OSM, C1
TIME VS. BOILING POINT TABLE Function
Description: Returns the Time vs. BP Table number that is to be used for a particular
stream (Sim Dis analyzers only).
Syntax: TVSBP_TBL(stream%)
Comments: stream% is the stream number (from 1 to the maximum number of streams).
Example: 0010 T = TVSBP_TBL(1)
0020 LPRINT GET_TEMP(0.5,T)
The number for the proper Time vs. BP Table is obtained by the function
TVSBP_TBL and assigned to variable T. The temperature for the Initial Boiling
Point is obtained by the function GET_TEMP using the Time vs. BP Table
specified in the stream.
Description: Returns the total area value for all the peaks detected in an analysis.
Syntax: TOT_PK_RAW_AREA
Example: 0010 FOR I = 1 TO N_PEAKS
0020 LPRINT PK_RAW_AREA(I)
0030 NEXT I
0040 LPRINT TOT_PK_RAW _AREA
For each peak, print the uncorrected area of the peak.
Description: Returns the total Sim Dis area measured during the analysis (Sim Dis
analyzers only).
Syntax: SD_TOTAL_AREA
Example: 0010 AREA! = SD_TOTAL_AREA
Returns the total measured Sim Dis area.
Description: Converts time expressed as UCT array to time as time and date.
Syntax: UCT_TO_TIME$(T!)
Example: 0010 DIM T!(2)
0020 TIME_UCT(T!)
0030 TM$ = UCT_TO_TIME$(T!)
0040 LPRINT TM$
VALUE Function
Description: Returns a floating point number that is the result of a conversion of the string
passed.
Syntax: VAL(string$)
Comments: string$ is any string expression. If a valid conversion cannot be performed,
VAL returns zero. Leading non-numeric characters will cause an invalid
conversion. Trailing blanks without a decimal point are interpreted as decimal
places.
Examples: 0010 A! = VAL( -10)
The floating point variable A! becomes -10.
2000-OSM, C1 10-35
0010 A! = VAL(10 )
The floating point variable A! is assigned the value 100000.
0010 A! = VAL(10. )
The floating point variable A! is assigned the value 10.
VALVE Command
Description: Sets the specified Trend output to the percentage level desired, by writing an
integer between 0 and 4095.
Syntax: WTO(channel%,value%)
Comments: channel% is the output channel (1-96).
value% is the trend output value.
Example: 0010 FOR I = 1 TO 96
0020 WTO(I,0)
0030 NEXT I
All trend outputs that exist are set to their lowest value.
Y2X Function
Description: Removes all pending requests from the Analysis Request Queue.
Syntax: ZERO_OUTSTANDING_REQUESTS
Example: 0010 RQANA(1) : RQANA(2)
10-36 2000-OSM, C1
0020 ZERO_OUTSTANDING_REQUESTS
0030 RQCAL(8)
Requests an analysis for streams one and two, removes all requests including
the ones just made for streams one and two, then requests a calibration on
method 8.
VistaNET is a UDP-based communications protocol. The protocol is such that any message
can be sent from one device to another. In order to do this, a message header must be built
that instructs the UDP messaging layer how the message should be handled. To that
message header, a user-defined datagram is attached. Vista BASIC messages are ASCII
text blocks attached to these UDP headers.
The user can define ASCII messages to be sent to another device. These ASCII messages
can be parsed for the content at the receiving end.
2000-OSM, C1 10-37
Comments: header$ is the UDP message header received using the RECEIVE HEADER
Command.
data$ is the ASCII data block to be sent.
Example: shown below
The sending application is located at VistaNET address 0.1.0.5. The receiving application is
located at VistaNET address 0.1.0.4
A BASIC program (usually in real-time BASIC table number 8) is written to accept VistaNET
messages:
0010 HDR$ = RCV_HDR$
0020 IF LEN(HDR$) = 0 THEN END
0030 DATA$ = RCV_DATA$
To reply, at 0.1.0.4:
SUBJECT LISTING
This lists the Vista BASIC commands, functions and statements (shown on the left side of
the page) in subject order. If you need additional information on a particular listing, use the
key term on the right side of the page to refer to the appropriate detailed alphabetical listing.
10-38 2000-OSM, C1
General Statements
BPRINT BPRINT
CHAIN CHAIN
COMMON! COMMON floating point array
COMMON$ COMMON string array
DIM DIM
END END
FOR...NEXT FOR...NEXT
GOSUB...RETURN GO TO SUBROUTINE
GOTO GOTO
IF IF
LET LET
LPRINT LPRINT
REM REMARKS
Math Routines
ASC(string$) ASC
CHR$(integer%) CHR$
FLT(integer%) FLOATING POINT
INSTR(string1$,string2$) INSTR
INT(fp!) INTEGER TYPE
LEN(string$) LENGTH OF STRING
MID$(string$,position%,length%) SUBSTRING
SPACE(length%) SPACE
STR_NAME$ STREAM NAME
UCT_TO_TIME$ UCT TO TIME
VAL(string$) VALUE
2000-OSM, C1 10-39
CYCLE_TIME(method%) CYCLE TIME
DACS_EVT_MSG(message$) DACS EVENT MESSAGE
DEACT(stream%) DEACTIVATE STREAM
FLAME_OUT_ALARM FLAME OUT ALARM
GET_ACTUAL_RT(method%,component%) GET ACTUAL RETENTION TIME
GET_ASSIGN(stream%) GET STREAM ASSIGNMENT
GET_BENCH_CONC(method%,component%) GET BENCHMARK CONCENTRATION
GET_CAL_CONC(method%,component%) GET CALIBRATION CONCENTRATION
GET_CC(method%,component%) GET COMPONENT CONCENTRATION
GET_EXPECTED_RT(method%,component%) GET EXPECTED RETENTION TIME
GET_MULTIPLIER_EXP(method%) GET MULTIPLIER EXPONENT
GET_OUTSTANDING_REQUESTS GET OUTSTANDING REQUESTS
GET_PRESS(zone%) GET PRESSURE OF A ZONE
GET_RF(method%,component%) GET RESPONSE FACTOR
GET_TEMP(zone%) GET TEMPERATURE FOR A % OFF
HARDWARE_ALARM HARDWARE ALARM
HIGH_CONC_ALARM HIGH CONCENTRATION ALARM
IDLE_ALARM IDLE ALARM
INJT INJECT TIME
INJT_UCT(T!) INJECT UCT
LOW_CONC_ALARM LOW CONCENTRATION ALARM
N_COMP(method%) NUMBER OF COMPONENTS
N_PEAKS NUMBER OF PEAKS
OFFLINE_ALARM OFFLINE ALARM
OP_MSG_ALARM OPERATOR MESSAGE ALARM
PK_AREA(peak%) PEAK AREA
PK_COMP_NUM(peak%) PEAK COMPONENT NUMBER
PK_CREST_AMP(peak%) PEAK CREST AMPLITUDE
PK_CREST_TIME(peak%) PEAK CREST TIME
PK_END_AMP(peak%) PEAK END AMPLITUDE
PK_END_TIME(peak%) PEAK END TIME
PK_HEIGHT(peak%) PEAK HEIGHT
PK_RAW_AREA(peak%) PEAK RAW AREA
PK_START_AMP(peak%) PEAK START AMPLITUDE
PK_START_TIME(peak%) PEAK START TIME
POSTAN_ERROR_ALARM POST ANALYSIS ERROR ALARM
POWER_FAIL_ALARM POWER FAIL ALARM
PREV_INJT PREVIOUS INJECT TIME
PREV_INJT_UCT(T!) PREVIOUS INJECT UCT
PREV_METHOD PREVIOUS METHOD
PREV_STRM PREVIOUS STREAM
PRG_STRM PURGING STREAM function
PURGE(stream%) PURGING STREAM command
PUT_ACTUAL_RT(method%,component%,retention!)
PUT ACTUAL RETENTION TIME
PUT_BENCH_CONC(method%,component%,concentration!)
PUT BENCHMK CONCENTRATION
PUT_CAL_CONC(method%,component%,concentration!)
PUT CALIB CONCENTRATION
PUT_CC(method%,component%,concentration!)
PUT COMP CONCENTRATION
PUT_COMP_NAME(method%,component%,name$)
PUT COMPONENT NAME
PUT_EXPECTED_RT(method%,component%,retention%)
10-40 2000-OSM, C1
PUT EXPECTED RETENTION TIME
PUT_MULTIPLIER_EXP(method%,value%) PUT MULTIPLIER EXPONENT
PUT_PRESS(zone%,set point!,ramp rate!) PUT PRESSURE OF A ZONE
PUT_REPORT_TYPE(type%) PUT REPORT TYPE
PUT_RF(method%,component%,response!) PUT RESPONSE FACTOR
PUT_TEMP(zone%,set point!,ramp rate!) PUT TEMPERATURE OF A ZONE
RAI(channel%) READ ANALOG INPUT
RDI(channel%,type%) READ DIGITAL INPUT
REPORT_TYPE REPORT TYPE
RQANA(stream%) REQUEST ANALYSIS
RQBEN(method%) REQUEST BENCHMARK
RQCAL(method%) REQUEST CALIBRATION
SENSOR_ALARM SENSOR ALARM
SET_BASIC_ALARM(alarm%) SET BASIC ALARM
SET_BASIC_COMP_ALARM(method%,component%,alarm%)
SET BASIC COMPONENT ALARM
START START ANALYSIS
STATUS(stream%) STREAM STATUS
STOP(n%) STOP ANALYSIS
TCF_ERROR_ALARM TCF ERROR ALARM
TIME$ TIME
TOT_PK_RAW_AREA TOTAL PEAK RAW AREA
VALVE(number%,state%) VALVE
WDO(channel%,state%) WRITE DIGITQL OUTPUT
WTO(channel%,state%) WRITE TREND OUTPUT
ZERO_OUTSTANDING_REQUESTS ZERO OUTSTANDING REQUESTS
2000-OSM, C1 10-41
SD_PEAK_HEIGHT MAXIMUM SIM DIS PEAK HEIGHT
SD_TOTAL_AREA TOTAL SIM DIS AREA
TEMP_TO_TIME(temperature!,time_vs_bp_table%)
GET TIME FOR A TEMPERATURE
TIME_TO_OFF(time!,time_vs_bp_table%) GET % OFF FOR A TIME
TIME_TO_TEMP(time!,time_vs_bp_table%) GET TEMPERATURE FOR A TIME
T_UNITS TEMPERATURE UNITS
TVSBP_TBL(stream%) TIME VS BOILING POINT TABLE
Numerous Vista BASIC command functions have been modified to accommodate the extra
Chroma I/O Board used in GCCs with Simultaneous Dual Detectors. They are:
ALARM(Chroma%) ALARM
CLOCK_ERROR_ALARM(Chroma%) CLOCK ERROR ALARM
COMM_ERROR_ALARM(Chroma%) COMMUNICATION ERROR ALARM
CUR_METHOD(Chroma%) CURRENT METHOD
CUR_STRM(Chroma%) CURRENT STREAM
GET_OUTSTANDING_REQUESTS(Chroma%) GET OUTSTANDING REQUESTS
HARDWARE_ALARM(Chroma%) HARDWARE ALARM
HIGH_CONC_ALARM(Chroma%) HIGH CONCENTRATION ALARM
IDLE_ALARM(Chroma%) IDLE ALARM
INJT(Chroma%) INJECT TIME
INJT_UCT(Chroma%,T!) INJECT UCT
LOW_CONC_ALARM(Chroma%) LOW CONCENTRATION ALARM
POSTAN_ERROR_ALARM(Chroma%) POST ANALYSIS ERROR ALARM
PREV_INJT(Chroma%) PREVIOUS INJECT TIME
PREV_INJT_UCT(Chroma%,T!) PREVIOUS INJECT UCT
PREV_METHOD(Chroma%) PREVIOUS METHOD
PREV_STRM(Chroma%) PREVIOUS STREAM
RAI(Chroma%,channel%) READ ANALOG INPUT
RDI(Chroma%,channel%,type%) READ DIGITAL INPUT
RQANA(Chroma%,stream%) REQUEST ANALYSIS
RQBEN(Chroma%,method%) REQUEST BENCHMARK
RQCAL(Chroma%,method%) REQUEST CALIBRATION
SENSOR_ALARM(Chroma%) SENSOR ALARM
SET_BASIC_ALARM(Chroma%,alarm%) SET BASIC ALARM
SET_BASIC_COMP_ALARM(Chroma%,method%,component%,alarm%)
SET BASIC COMPONENT ALARM
START(Chroma%) START ANALYSIS
STOP(Chroma%,n%) STOP ANALYSIS
TCF_ERROR_ALARM(Chroma%) TCF ERROR ALARM
ZERO_OUTSTANDING_REQUESTS(Chroma%)
ZERO OUTSTANDING REQUESTS
VistaNET Commands
Since VistaNET commands are interlinked, these commands have little meaning shown as
independent commands. See "Vista Basic Support for VistaNET Communications" in Section
2 for an explanation of this command structure.
10-42 2000-OSM, C1
ERROR MESSAGES
Invalid Integer Constant: An integer constant is too large. Integer constants must be in the
range from -32768 to 32767.
Invalid Floating Point Constant: Floating Point constant does not conform to proper
syntax.
String Too Long: String constant contains more than 255 characters. Reduce the number
of characters within the string and make sure the string constant ends with the double
quotation mark (”).
Illegal Character: A character not recognized by the compiler has been encountered. This
error should not occur and should be reported to ABB Lewisburg.
Syntax Error: The compiler has encountered something which does not conform to the
rules for proper syntax of the language. A major cause for this diagnostic message is
the incorrect spelling of commands and keywords, as well as, other typographical
errors, such as missing commas or parentheses.
Data Type Mismatch: An expression contains operands which are not of the same data
type. If the expression contains floating point operands, then all of the operands must
be floating point or converted to floating point. Expressions with integer operands must
contain all integer operands or conversions to integer type. Another cause for this error
occurs when an argument passed to a command or function does not agree with the
data type expected for the parameter.
Array Not Defined: A variable contains a subscript when the variable has not previously
been declared as an array with the DIM statement. All arrays, with the exception of the
COMMON! array, must be declared in a DIM statement.
Duplicate Declaration: This error occurs when an attempt is made to name a variable to a
name already used for a command or function. The error can also occur in a DIM
statement when the variable name is already in use by another variable, or by a function
or command.
Unreachable Statement: An attempt has been made to branch to a statement that does
not exist. For instance, a GOTO or GOSUB statement contains a statement number that
does not otherwise exist in the source program. Confusing Line numbers with
Statement numbers might be a cause for this error. Line numbers are not interpreted by
Vista BASIC and are used strictly for editing purposes. A Statement number is a
number at the beginning of a statement in the statement field of the source program.
Insufficient Memory: Not enough free memory exists for the compiler to operate properly.
The corrective action is to retry the compilation when more free memory is available.
2000-OSM, C1 10-43
Restriction: Code Size: An implementation restriction that limits the number of object code
instructions has been exceeded. The corrective action is to reduce the number of
statements in the source program.
Restriction: Variable Allocation: A restriction that limits the number of variables allowed
has been exceeded. The corrective action is to reduce the number of variables in the
source program.
Array Index Missing: An array has been referenced without the use of an index. This error
frequently occurs when there is a duplicate declaration of an array and a scalar variable
having the same variable name for both. The corrective action is to use a different
name for the scalar variable or provide an index for the array element.
Illegal DIM Number: An array dimension (extent) of zero is not allowed in the DIM
statement.
Internal Error: No Such Error: This is an error that should never occur, but if it does,
indicates a design or modification error to the internal software that should be reported
to ABB Lewisburg.
Illegal Opcode: This is an error that should never occur, but if it does it indicates a design
or modification error to the internal software that should be reported to ABB Lewisburg.
Array Index Out of Bounds: An array subscript is negative or exceeds the array dimension
(extent).
FOR and NEXT Variables Not the Same: The variable name in the NEXT statement does
not agree with the variable name for the counter in the matching FOR statement.
Index Pointer Out of Bounds: An instruction pointer out of bounds error may indicate a
wild branch and is probably caused by an internal error that should be reported to ABB
Lewisburg.
Stack Pointer Out of Bounds: A stack pointer out of bounds error could be caused by an
expression that contains too many operands for the stack to hold. Corrective action
requires splitting excessively long expressions into more than one statement and to use
intermediate variables for temporary storage of results.
NEXT without FOR: A NEXT statement occurred that did not have a matching FOR
statement.
RETURN without GOSUB: A RETURN statement occurred that did not have a matching
GOSUB statement.
GOSUB without RETURN: A GOSUB was executed, but no RETURN statement was
executed before the physical/logical end of the program.
FOR without NEXT: A FOR statement was executed, but no NEXT statement was executed
before the physical/logical end of the program.
10-44 2000-OSM, C1
Stream Number Out of Range: A stream number passed as an argument to a command or
function is too large or too small.
Component Table Does Not Exist: A method number or component table number passed
as an argument to a command or function was too large or too small.
Ratio Table Number Out of Range: This error occurs when you chain to a nonexistent
Vista BASIC program.
Interpreter Called without Program: The Interpreter was called at end-of-analysis for a
program to be executed according to the program-to-stream assignment, but the
program was nonexistent. The corrective action for this case would be to compile the
program.
Time Limit Exceeded: The execution time limit for a given program has been exceeded.
The execution time limit is the actual time for execution as measured by the number of
Vista BASIC instructions executed. Corrective action would be to reduce time needed
for execution of a program by:
Insufficient Memory: This error occurs when not enough free memory exists for the
interpreter to dynamically allocate memory for arrays in the DIM statement or for buffers
in the LPRINT statement. The corrective action is to retry the execution when more free
memory is available.
Illegal DIM Number: An array dimension (extent) of zero is not allowed in the DIM
statement.
Introduction
Vista BASIC is a programming language that allows the operator to customize some
analyzer operations. Vista BASIC programs can be set up to run manually, at the end of the
analysis of a given stream, or at a specified time of day.
Vista BASIC can also run continuously in the background (this is called running in real time).
Running in real time allows the Vista BASIC program to watch the state of the analyzer and
make decisions based on that state. Six commands in the Vista BASIC language support
running in real time.
2000-OSM, C1 10-45
Real Time Operation
Only Vista BASIC table number eight can run in real time. If more space is needed, then this
table can chain to another Vista BASIC table. Once it is started manually, table number eight
runs continuously; as soon as it finishes, it starts again.
Table eight can still be used as a normal Vista BASIC table if it is not started manually as
Real-Time Vista BASIC.
How often the table runs depends on how long it takes to execute and what other functions
the analyzer is performing at that time. For example, with the analyzer idle and a very short
table, Real-Time Vista BASIC may run up to forty times per second. At the end of the
analysis, Real-Time Vista BASIC may not run at all for several seconds. At any given time it
is difficult to determine how often it will run.
For this reason, the Vista BASIC table should be written very carefully, taking into
consideration table length and the time required for execution.
Screens
Three screens support Real-Time Vista BASIC. These screens are accessed from the
Background Screen (see Figure 10-2).
********** B A C K G R O U N D **********
ABB Analytical GCC Remote 0.1
803V029-1R (Std GCC) (C) 2001
**ALARM**
**ALARM** 18-JUN-2002 TUE 08:16:01
**ALARM**
Analysis Time :00114 Peaks Found:00
Cycle Time :00000 State:Idle
F1 F2 F3 F4
Press the F3 (Cur Report, Basic I/O & Options) soft key on the Background Screen to
display the Report, Basic I/O and Options menu (see Figure 10-3).
10-46 2000-OSM, C1
****** Report, Basic I/O and Options ******
CURRENT REPORT
[BASIC INPUT AND OUTPUT ]
START/STOP AND EDIT BASIC
OPTIONS
View Edit/View
Escape Basic COMMON!
Output Area
F1 F2 F3 F4
This screen allows you to start and stop Real-Time Vista BASIC. Real-Time Vista BASIC
uses two other screens: one to display Real-Time Status, and one to Edit/View the
COMMON! Area. To review the state of the Real-Time Vista BASIC program (running or
idle), any text sent to it (using RT_TEXT), and the state of any input requested from it (using
RT_INPUT$), press the F2 (View Basic Output) soft key. The Real Time Basic Status screen
appears (see Figure 10-4).
ALARM EXISTS
Clear Answer
Escape All Input
Messages Request
F1 F2 F3 F4
2000-OSM, C1 10-47
To edit or view the COMMON! Area, press the F3 (Edit/View COMMON! Area) soft key on the
Report, Basic I/O and Options screen. The Basic COMMON! Area Edit screen appears (see Fig-
ure 10-5) and updates once each second.
COMMON! Number:[1 ]
COMMON! Value : 0.00000000
F1 F2 F3 F4
While all standard Vista BASIC commands are available for use with Real-Time Vista BASIC,
the following commands are specifically for running in real time.
WARNING
When using Real-Time Vista BASIC, do not use these commands: LPRINT
and DACS_EVT_MSG!
10-48 2000-OSM, C1
Real-Time Text
Description: Sends a line of text to the Real-Time Vista BASIC Status Screen
Syntax: RT_TEXT(string)
Comments: string is the line of text to be sent to the Real-Time Vista BASIC Status
Screen. A total of ten lines are supported, with the newest line printed on the
bottom of the screen and older lines scrolled up and off.
Example: 0100 IF ALARM THEN
0110 :RT_TEXT(“ALARM EXISTS”)
Description: Clears all the text on the Real-Time Vista BASIC Status Screen
Syntax: RT_CLEAR
Example: 0100 RT_CLEAR
Real-Time Input
Sleep
Temperature
Description: Returns the temperature of a zone of the Five Zone Temperature Controller.
Syntax: temp = TEMPS(zone)
Comment: zone is zone 1 through 5 of the controller
temp is the floating point temperature of the zone
Example: 0100 IF TEMPS(1) > 280.0 THEN
0200 : STOP(0)
Aborts the analysis if the temperature gets too high.
2000-OSM, C1 10-49
For further information or assistance contact:
ABB Inc.
843 North Jefferson Street
P.O. Box 831
Lewisburg, WV 24901
10-50 2000-OSM, C1
SECTION 11. DRAWINGS AND DIAGRAMS
USE OF DRAWINGS
The drawings and diagrams contained in this manual are of a general nature. Since
analyzer configuration depends on the particular application, you should refer to the
drawings provided in the engineering drawings supplied with your analyzer as the final
authority. In addition there is an Application Data Package which contains information on
application-dependent components or subassemblies, outline and mounting diagrams, and
flow diagrams.
The following drawings and diagrams, which make up this section of the manual, provide
general information about the analyzer that is not covered elsewhere.
2000-OSM, C1 11-1
SERIAL I/O JUMPER CONNECTIONS
JP10-2 JP10-3
JP10-4 JP10-5
INTERRUPT JP7-2 JP7-8 JP7-5
JUMPERS JP7-4 JP8-12
JP7-3 JP8-9
JP7-1 JP10-8
CHO JP11-1 JP13-1 HIGHWAY #1
DATA CH1 JP11-2 JP14-1 FRONT PANEL
INPUTS CH2 JP11-3 JP13-2 HIGHWAY #2
TO S.B.C. CH3 JP11-4 JP12-4 PRINTER
DATA CHO JP11-5 JP16-3 HIGHWAY #1
OUTPUTS CH1 JP11-6 JP13-6 FRONT PANEL
FROM CH2 JP11-7 JP16-6 HIGHWAY #2
S.B.C. CH3 JP11-8 JP12-8 PRINTER
SERIAL I/O
JUMPERS JP14-7 JP15-7 FRONT PANEL
RS-422
JP14-8 JP15-8 DRIVER
SWITCH SETTINGS
I/O POSITION (ON) STATE
TERMINAL I/O
HIGHWAY #1: [+] 7-34
[-] 7-35
[+] 7-45
[-] 7-44
[+] 7-49
[-] 7-48
11-2 2000-OSM, C1
Air In PURGE AIR
PANEL
Heater Air
Purge Air
Digital Out
Analog Out
Sample In Recorder
OVEN GCC
Printer
VistaNET
Burner Fuel
Burner Air
Carrier
Air In
H2 In CARRIER
GAS
PANEL
Carrier In
2000-OSM, C1 11-3
PURGE AIR PANEL
Regulator
& Gauge
Air In Regulator
& Gauge
Solenoid Solenoid
Valve Valve
Heater Air
Purge Air
Purge Air
OVEN
Heater
Burner Air
Carrier
Air In Adj
Valve
H2 In Adj
Valve
Carrier Adj
In Valve
CARRIER GAS PANEL (Analog)
11-4 2000-OSM, C1
To LOCOM
Circuit
Display LOCOM
PCB
Keypad
SBC Trend
PCB #1
Analog
EPC
Outputs
Sensors Power
Trend
Supply
#2
PCB
EPC
Control EPC
Digital
PCB Multibus
I/O #1
PCB Digital
Zone Inputs &
PCB Outputs
Digital
(5) DTC
I/O #2
Backplane
AC PCB
Cond VistaNET
PCB Multibus VistaNET
PCB Domains
GCC
2000-OSM, C1 11-5
ABB Analytical Products
www.abb.com/analytical
ABB Inc.
843 N. Jefferson Street
Lewisburg, WV 24901 USA