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HongYi ® 弘益® Solvent Recycling Machine User’s Manual Revised:2020/02/20 Page 1 of 40

►Intelligent & Safe◄


---Solvent Recycling Machine---

USER’S MANUAL
(Hy20/40/60/90/125Ex)

◄2020►

HONGYI (HK) ENVIRONMENTAL EQUIPMENT CO., LIMITED


© Copy righted. All rights reserved.
CONTENTS

Chapter 1 Statement ................................................................................... 3

Chapter 2 Product Introduction .................................................................. 4

Chapter 3 Installation Environmental Requirements ................................ 8

Chapter 4 Machinery Installation & Installation Requirements................. 9

Chapter 5 Machine Operation Instructions .............................................. 10

Mixed Solvent & Single Solvent .................................................................. 23

Chapter 6 Scope Of Application Of The Machine ................................... 32

Chapter 7 Machine Maintenance & Repair.............................................. 34

Chapter 8 Common Causes Of Failure & Fault Exclusion Method ........ 37

Chapter 9 Reference Appendix ................................................................ 40

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CHAPTER 1
Statement

◆◆◆The machine and equipment installation and use, must comply with national and state fire
safety requirements for explosive gas atmospheres specifications, and electrical
equipment installation and operation environmental requirements. The manufacturer has
no legal obligations where national safety standards, machine operation environmental
requirements are neglected by the user(s). Problems arising from neglect of safety and
operation standards have nothing to do with the manufacturers.

◆◆◆Machine strain, wear and tear parts, consumables replacement, handling of corrosive
solvents on the corrosion of the machine, improper operation and maintenance of
equipment damage caused by bad, man-made destruction and force majeure factors,
leading to machine failure, are not product quality problems.

◆◆◆Trademarks and product design patent:"HongYi®", "弘益®" trademark and product


design patent is a Hongyi Environmental Protection Equipment Co., Ltd. legal property.
No organization or individual should copy our products without Hongyi Environmental
Equipment Co., Limited written permission. Use of counterfeit products is prohibited.

◆◆◆The manufacturers retain the "manual" interpretation and explanation rights, the contents
of the manual with the product technology updates may be updated accordingly, without
notification.

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CHAPTER 2
Product Introduction

I. Attentions: This machine is used to recover organic solvents from a liquid solution / mixture, not
suitable for recycling gaseous solvent and solid-state materials.

Solutions / solvents as below are not applicable for recycling:


◆Mixture/Solutions are mixed by solutions from different processes or different
manufacturers, recovery is prohibited!

◆Solutions contain more nitrocellulose, oxidants or inflammable dangerous materials,


recovery is prohibited.

◆Solutions are corrosive to stainless steel or copper, such as: strong acid, strong
alkaline solvent, strong solvents, or contain more salts, recovery is prohibited.

II.Operation Principles:
HongYi ®弘益® Solvent Recycling Machine works by distillation principle.

1. Pour the solution to be recycled or recovered into distillation bucket / tank.

2. Heating rod heats up the heating transfer oil in the recovery tank;Heating oil
transfers heat to the distillation bucket / tank containing waste solution;The
solution heats up, organic solvents warm up and the liquid turns into gaseous state.

3. Gaseous solvents enter the cooling system and condense into liquids; Separated
clean solvents flow into recovery container.

4. After the recycling process, to clean up the residue in the distillation tank.

By distillation and cooling, clean organic solvents are recycled for reuse, users can
achieve the purpose of recycling and reuse.

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III. Signs & Symbols: The meanings of the signs & symbols on machine’s nameplate:

Don’t put out fire with water.

Smoking and fire are strictly prohibited


around work area.

When components are very hot,


don’t touch them.

When machine is in operation,


please use safety goggles.

When operating the machine,


please use safety mask.

When operating the machine,


please use protective gloves.

There’s high electric current on the power


control board. Don’t touch it.

IV. Performance: HongYi® Solvent Recycling Machine has the following performances:

1. Whole machine explosive proof structure:


The machine has explosion proof components, the products passed the explosion-proof
test of electrical products through the China National Quality Supervision and Inspection
Center for Testing and Certification:
① All electronic control systems and components are of explosion-proof structure, for
example: explosion proof power box, explosion proof heater, explosion-proof fans
and other condensation, explosion-proof electric control system is made of cast
aluminum material, all sealed explosion-proof design, prevent getting solvents in
contact with electric sparks;
②If temperature display has no electrical contacts, there won’t be sparks.

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③ All cable connectors are designed with explosion-proof seals, Stainless steel hose are
used as protective material, it can not corrode, safety is guaranteed.
④ Recovery tanks are made of stainless steel materials, two-tiers structure, indirect
heating, reinforced lid design, accurate temperature control, explosion proof, and leak
proof.

2. Intelligent control system & display screen:


Adopts the single-chip control system & the display screen visual display technology, it
is very convenient and very simple to modify or adjust preset parameter values; The
equipment is intelligent running and safe, and can be equipped with liquid level
control system and automatic feeding system to achieve automatic feeding, automatic
continuously feeding and continuous running.

3. Temperature shutdown function:


Preset a stop temperature/shutdown temperature, when recovery is completed,
solvent steam/vapor inside the steam pipe is gradually reduced, the temperature
drops gradually in the condenser, then shutdown system is activated, and the
machine shuts down automatically. Then, the display scroll “Stop…”.
◆ This feature makes the machine to completely stop running and end recovery process; its
function is to turn off the whole machine.

4. Shutdown Timer Function:


The machine recovery time is pre-set, when the machine starts, it can run a long
time to reach the preset time; By this function, it can reach the proper recovery time
and shut off automatically. To ensure that recovery is complete recycling tanks
reserved for a small solution to make liquid-like residue to enhance convenient
cleaning of the recovery tank, it will effectively prevent burning and explosion. The
timing protection systems play the role of turning on and turning off the machine.
◆ This function is to stop running and end recovery process. Attention, after the machine
stops heating, the cooling fan will automatically run for a while.

5. Over-temperature protection function.


The heating maximum temperature is pre-set, when the heat transfer oil
temperature reaches a pre-set maximum temperature, the red light for over
temperature protection shows, the heater stops heating. Then, the display scroll
“Over temp alarm”. This feature ensures that the machine is set at a temperature
range that enhances safe operation, and effectively prevent the heating temperature
is too high.

6. Over high-pressure protection.


In case of pipe clogging, steam will not be discharged through the steam piping, the
tank pressure increases more than outside pressure by 0.38Bar, the lid safety valve
will automatically open to ensure the safety of equipment and operation. Then, the
display scroll “Pressure alarm”.

7. Cooling fault protection:

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When the cooling system fails, the heating temperature is set too high, and the
solvent cannot be cooled completely and the temperature exceeds 50℃, the control
system will automatically stop heating and give an alarm. The screen will scroll to
display "Condenser over temp".
※This function is not available for the air-cooling model with type B electric control box.

V. Technical Specifications.

Type / Model Hy20Ex Hy40Ex Hy60Ex Hy90Ex Hy125Ex

Feed Capacity (L) 20 40 60 90 125

Heating Components (Kw) 2.0 4.0 4.0 5.0 6.0

Cooling Fan Power (Kw) 0.12 0.09 0.12 0.12 0.12

Max Current (A) 6.9 6.9 8.4 10

Voltage (ACV/50~60Hz) 220/1Ph 380/3Ph

Control voltage (ACV/Hz) 220/50-60

Heating mode Indirect heating by heating transfer oil

Length (mm) 800 950 1100 1100 1150

Width (mm) 750 750 750 850 850

Height (mm) 1160 1200 1200 1260 1435

Weight (kg) 100 140 160 260 300

Operation temp range (℃) 50~210

Ambient temperature
suitable for operation (℃) 5~35

Noise (dB) 65

Recovery ratio 95%

Recovery Time (hr.) 2.5-3.0 2.5-3.0 2.5-3.0 2.5-3.0 3.0-3.5

Note: Values listed of the recovery rate and recovery time above is referenced Values, the actual
recovery rate and recovery time is related to the solvent type, impurity content of the waste solution
and environmental temperature.
A lower environmental temperature (<30°C or <20°C) is required for recycling the solvent with low
boiling point (<50°C).

◆Important Notes: Please check whether heat transfer oil has been added to new machine.
Usually, new machine’s heat transfer oil is ready, no need to feed again!
If the buyer requests the manufacturer not to add heat transfer oil to the machine, users need to add
heat transfer oil to new machine before using the machine at the first operation.

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CHAPTER 3
Installation Environmental Requirements
I. Workplace safety requirements.
1. Handling method:

Wrong Handling Mode Correct Handling Mode


2. Workplace: It must be spacious, open and cool; it must be away from inflammable and explosive
dangerous goods and have separate work area. Flammable materials in the workplace
must be equipped with fire-fighting facilities.

3. Environmental temperature requirements:


The appropriate environmental temperature for operating the machine is 5°C~40°C.
◆A very low environmental temperature(<30°C or <20°C) is required for recycling the solvent
with low boiling point(<50°C).

4. Ventilation : ※Operation is prohibited without ventilation.


An explosion-proof exhaust fan is installed at the top of the machine or installed on the
wall in the work area; maintain a rapid flow of air, to reduce the solvent concentration
in the air. The concentration of solvents in the air should be within the scope of the fire
safety requirements, to prevent accidents.

5. Solution / agent storage security:


①Storage of untreated organic solution or recovered cleaning solvents is prohibited in
the equipment operation area.
②Solvents or organic solution to be processed should be placed in storage safety area.
Before the machine is running; fill in the waste solution according to the capacity of the
recovery tanks.
③ After the machine running, clean the recovery tank and the waste / residue
immediately removed from the work area.
④The recovered solvent must be stored into a vessel and kept in a safe area.

II.Power supply requirements and safety requirements:


1. Power:Power supply voltage required for equipment operation should be the current fit for the
machine. Switch or circuit breaker must be able to load 32A current.

2. Cable Explosion proof: Power supply system should be explosion-proof line, Explosion-proof
switch, Explosion-proof lighting etc., must comply with fire safety and explosion-proof
requirements, Power Supply System, Electrical wiring should be consistent with
(GB3836.15-2000) Electrical Apparatus for Explosive Gas Atmospheres, Article 15 some
Hazardous Location Electrical Installation (Except mine). Requirements and not less than the
device explosion-proof signs marking requirements of the standard approved.

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CHAPTER 4
Machinery Installation & Installation Requirements
I. Installation Requirements:
1. Isolated work area: Equipment must be installed in a separate work area.
2. Equipment bottom fixed: Placement of the equipment should be on a platform or ground solid
enough to withstand the weight of the machine, for example:Reinforced concrete floor.
Equipment should be firmly fixed on the solid ground.
3. Safe distance from the wall: If the machine is installed near the wall, the machine and the wall
should be 50cm apart from the wall.
4. Grounding: The ground cable must be connected to prevent incidents of power leakage.
※ Do not connect ground cable to zero line.

II.Installation Procedure:
Step 1:Fix the machine: Fix the machine to the concrete floor.
Step 2:Connect the power distribution cables.
Step 3:Power connection: ※Please choose copper wire for power cord. Don’t use aluminum wire!
Hy40/60/90/125Ex are equipped with 3* 2.5㎜2+2*1.5㎜2 (Hy20Ex: 3* 4.0㎜2) sheathed
cable supply of electricity, in the workplace, it must be the end of a main line that will need to
be manually operated using independent distribution device. When necessary, the machine
electrical system can disconnect from the power supply system, switch or circuit breaker
must be able to load 32A current. The machine ground cables must be grounded.
Step 4:Connect the solvent outlet with a Teflon plastic pipe: There is a Teflon plastic pipe in the
distillation tank; mount the plastic pipe to the recycling machine’s solvent outlet and fasten it
with locking ring. (If equip with Vacuum Device, need to connect the solvent Inlet to the machine’s
solvent outlet with the Teflon plastic pipe and lock the joint.)
Step 5: (If equip with Vacuum Device) Connect the recycling machine’s solvent outlet with the plastic
pipe to Vacuum’s solvent Inlet and lock the joint. Vacuum Device is connected to a
compressed air supply pipe (4~5Kg compressed air source).
Step 6: (If equip with Feeding Pump) Assemble feeding pipe to connect distillation tank’s feeding inlet
and feeding pump; The feeding pump is connected to the suction pipe and pressured air
supply pipe.

III. Installation & Adjustment.


1.Check for steam pipe blockage or leakage. Method of pipeline inspection:Turn off the main power
switch, Loose the lid knob and Open the lid, use compressed air of 0.2Bar to blow solvent
outlet pipe from the outside to the inside;Be sure that the air makes smooth exit from
solvent flow pipe to the outlet.
2.Check whether the sealing gasket is leaking: Use compressed air of 0.2bar to blow solvent outlet
pipe from the outside to the inside, use soapy water rub the lid edge. If there’s a continuous
uniform bubbling, and the bubble does not pop, it means that the sealing is effective. If
proved otherwise, there’s a leakage.
3.Operating Inspection:Check and confirm that the cooling electric fan is operating normally and the
heater is working normally.
4.Do pre-settings following the boiling point and the characteristics of the solvent to be recovered.

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CHAPTER 5
Machine Operation Instructions

STEP 1: Check before Starting the Machine.

1. Check for steam pipe blockage or leakage: Turn off the main power switch, Loose the lid
knob and Open the lid , use compressed air of 0.2Bar to blow solvent outlet pipe from the
outside to the inside;Make sure the air goes smoothly from the distillated solvent outlet
into distillation tank (If equipped with Vacuum Device, don’t need this step).

2. Check heat transfer oil and loosen exhaust valve (oil inlet).

◆ Please check whether heat transfer oil has been added to new machine.
Usually, new machine’s heat transfer oil is ready, no need to feed again!
If the buyer requests the manufacturer not to add heat transfer oil to the machine, users need to add
heat transfer oil to new machine before using the machine at the first operation.

3. Check solvent containers:Place a container under the outlet pipe to collect the recovered
clean solvent. The container must be non-corrosive, conductive, and it must be grounded in
order to prevent static electricity.
4. Prepare dirty solvent for recovery.
(if equipped with feeding pump, need to insert Feeding Pump’s suction pipe into dirty solvent tank and
open Feeding Inlet Valve of distillation tank before transfer dirty solvent into the tank).

5. Check the joint: the recycling machine’s clean solvent outlet is connected to the solvent
inlet of Vacuum Device, and Vacuum’s inlet valve is open (this step is not required if there is
no vacuum device).

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STEP 2: Feeding/Transfer Dirty Solvent into Distillation Tank.

1. Feeding manually (by hand or by feeding pump):


①Loosen the locking handle, and open the distillation tank cover;
②Transfer the dirty solvent into distillation tank, not above the maximum level line and
don’t let dirty solvent into vapor outlet pipe of distillation tank;
(Please open Feeding Inlet Valve of distillation tank, before manually feeding by pump.)

③Wipe distillation tank edge, keep the edge clean.


④Cover the tank, tighten the locking handle in pairs.

(Please close Feeding Inlet Valve of distillation tank, after manually feeding by pump.)

◆ Notes: If the solvent is foaming, or forms bubbles, users need to reduce the quantity.
Be sure no dirty solvent goes into vapor/steam outlet pipe in the distillation tank when feeding manually.

2. Automatic Feeding: (Equipped with automatic feeding system: level controller + feeding pump.)
①Wipe distillation tank edge, keep the edge clean.
②Cover the tank, tighten the locking handle in pairs.
③Prepare dirty solvent for recovery, and insert the suction pipe into the dirty solvent tank.
④Turn power switch to “ON” position to connect the power, then the display is initialized.
⑤Press the "Dn/Start" button for more than 1 second; The recycling machine will feed
automatically and start the heating system automatically, and the cooling fan will also start.
If equipped with vacuum Device, need to start Vacuum Device at the same time!

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Important Notes:
If equipped with Vacuum Device, Vacuum’s solvent inlet valve is open and Vacuum’s
discharge valve is closed and start Vacuum Device at the same time!

◆ Caution:
If the solution contains more nitrocellulose, oxidants and other inflammable dangerous
materials, recovery is prohibited. Follow procedure for handling dangerous waste solutions
and materials.

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STEP 3: To Set Recovery Running Parameters:

1. The Electric Control Box & Control Panel:

Electric Control Box & Control Panel:Type A

Electric Control Box & Control Panel:Type B

Indicator Light on the Electric Box Panel:

1) POWER Light (red):Power supply indicator light. It lights up when connect the power.

2) RUN Light (green/yellow): Running indicator light. It lights up after press “Start” button
until the recovery process ends and automatically turn off when the recovery process
ends.

3) ALARM Light (red): It’s a high heating temperature alarm / buzzer.


The buzzer will sound and the led starts blinking, when the actual temperature of
heat-transfer oil is greater than 210℃(maximum temperature limit), or when the actual
temperature is higher 15℃ than the preset heating temperature, and stop heating at the
same time.

Power Switch:

4) OFF/ON Power Switch: Turn it on the “ON” position,the recycler is on standby; Or turn it
on the “OFF” position to cut off power supply.

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5) Emergency Stop button: Emergency stop switch. Press it to stop running in emergency.

Display Windows on the Control Panel:

6) Left window on the control panel of the electrical control box:


Left display window is the display of the intelligent control system. It displays the control
home page/working interface, main menu, parameters setting interface, etc.

Home Page/Working Interface:Stop

Home Page/Working Interface:Running

Heating Temp: Preset Heating Temperature. Oil Temp: Real-time oil heating temperature.
Heating Time: Preset Heating Time/Duration. Running Time: Actual heating time/duration.
Steam Temp: Real-time solvent steam temperature. Stop◎: Stop/Running indicator.

※ Important Notes: Press any button to wake up the display screen. Don’t press the button for a long time (>2
seconds) when awakening the display screen, otherwise, input a wrong program's commands by mistake.

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Main Menu Parameter Setting Interface

7) Right window on the control panel of the electrical control box:


This is a heating display window to display heating temperature.
PV: Display the real-time temperature values of the Heat-Transfer Oil.
SV: Display values of Preset Heating Temperature.

Buttons of the display on the Control Panel:

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8) Up/Menu: Cursor shift position, cursor move up or left; Press this button to enter the
selection main menu.

9) Dn/Start: Cursor shift position button, to move down or right; Press this button for
more than 1 second to start solvent recovery process.
10) +/Stop: Press it to increase the data/value to do settings; During the recovery process,
press it to stop recovery process back to on standby mode.

11) -/Heating Pause: Press it to decrease the data/value to do settings; Press it to


temporarily stop heating during the unit is running.
12) Ent/Feeding Pause: Enter key, press it to enter or save data/value; During feeding,
press this button to temporarily stop feeding, or press it to resume feeding.

Important Notes:
Press any button to wake up the display screen. Don’t press the button for a long time (>2 seconds)
when awakening the display screen, otherwise, input a wrong program's commands by mistake.

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2. Procedures to Set Parameters of Recovery Process:
The power supply is connected. Then begin to set the preset values / parameters: Heating
Temperature, Heating Duration, Stop Temperature, Stop mode, Screen Saver time, etc.

※ Operational environment must have proper ventilation, be safe.


※ If the machine has been preset and the preset values/parameters are all ready, it doesn’t need to preset the
running parameters again at next time.
If users want to recycle another dirty solvent at the next time, users need to preset the running parameters
according to the boiling point of the solvent.

1) Connect power: Turn Power switch to “ON” position, the recycling machine is powered
on and the display screen displays the working interface.

Home Page/ Working Interface Page: On Standby Mode

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2) Enter Main Menu: Press the "Up"/" Menu "button on the control panel to enter
the main menu.

Main Menu
3) Enter “Input Password” Page:
Press “Up” or “Dn” button to move the cursor to select “1 Parameter Setting”.

Then press “Ent” button to display the "password" interface.

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Password:2018
press the “Up” button to move the cursor to the left;
press the “Dn” button to move the cursor to the right;
Press "+" to add a number;
Press "-" to delete the number.

Press “Ent” button to display parameter setting interface.

4) Enter Parameter Setting Interface: After input password: 2018, press


“Ent” button to display Parameter Setting Interface.

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Parameter Setting Interface

Notes: “Item” in the table above is Heating stages.


“Temp” in the table of Parameter Interface is Heating Temperature.
“Time” in the table of Parameter Interface is Heating Time (heating duration).
“Stop Temp” is stop temperature (Shut down).
“Feeding Delay” is Delay time from receiving the execution of the feeding instruction. Don’t
need to change it.
“Feeding Time” means automatic or continuous feeding within this specified period of time.

5) Input Preset Parameters for recovery process:


Press “Up, Dn, +, -” button to input “Temp” (Heating Temperature), “Time”
(Heating Time, heating duration), “Feeding Delay”, “Stop Temp” (Stop/Shut down
temperature), “Screen Saver” time.

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Press “Up” button to move the cursor up; Press “Dn” button to move the cursor down.
Press "+" button to increase the parameter value;
Press "+" button for more than 1 second, the value increases rapidly.
Press "-" button to reduce the parameter value.
Press "-" button for more than 1 second, the value decreases rapidly.

Parameter Setting: The parameters of recycling Acetone (56.53°C) (for reference)

※ Important Notes:
1. Heating Temp & Heating Time Values in the table of Parameter Interface:
Users input parameters values for the items in the table according to their solvent
distilling needs. After input Heating Temp & Heating Time values in required table, the
Heating Temperature values & Heating Time values in other tables must be "0”.

For example, they need one heating stage to distill their dirty solvent, if so, they only
need to set values for Item 1; the others must be "0”.

For another example, users need two heating stages to distill their dirty solvent, if so,
they need to set values for Item 1 and Item 2, the others must be "0”.

2. Max pressure value: The standard value is 30Kp. Users don’t change this value.

3. Feeding Delay: (Delay time from receiving the execution of the feeding instruction. Don’t need
to change it.) Its value range is 3~5 minutes. (Don’t need to preset this item, if without
automatic feeding system.)

4. Feeding Time: (means automatic or continuous feeding within this specified period of time.)
A: Single-cycle recovery process (Preset value of Heating Time is <240 minutes): Recovery
process only needs to feed dirty solvent once for each cycle: reference Value is 30~50
minutes.
B: Continuously Running(Preset value of Heating Time is >300 minutes): Its reference
value range is “Heating Duration time – 180~210 minutes(3~3.5hrs)” minutes. For
example, if users want to continuously running for 8 hours, the reference value ranges
of Feeding Time are “480 minutes (8hrs) – 180~210 minutes = 270~300 minutes
(4~5hrs)”.

5. Stop Temp (shutdown temperature): Shutdown temperature must be below the


solvent boiling temperature by 5~10℃. For example, a mixture, containing several

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organic solvents, the shutdown temperature is determined according to the solvent
with the highest boiling point in the mixture.

6. Temp Err: Users don’t need to change this value.

7. Stop Mode: Value “0”, means standard mode to stop running.

8. Screen saver: Users can set a value to meet their needs, for example, “5”, mean the
screen will not display after 5 minutes.

6) Save Parameter values:


After input the preset parameters, press “Ent” button to save the parameters,
and then press “Up” button for 2 seconds to return to Working Interface.

Parameter Setting Interface

Home Page/Working Interface

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Mixed Solvent & Single Solvent
Before doing preset parameter settings, users need to know the composition of mixture: single
solvent or mixed solvents, boiling points and their characteristics.
◆ Single Solvent:
If there is only one kind of organic solvent in a mixture, we call it single solvent, means a mixture
containing only one kind of organic solvent and we only need to recovery one kind of solvent from the
mixture. Only need to preset one Heating Temperature value & heating time for “item 1” in the
parameter input form is suitable for recycling single solvent.

Parameter Setting: The parameters of recycling Acetone (56.53°C) (for reference)

◆ Mixed Solvent:
If there are many solvents in a mixture, in other words, a mixed solvent / solution is composed of more
than two kinds of single solvent; we call it mixed solvent, means a mixture is composed of more than
two different solvents or containing a number of organic solvents, and we need to recovery more than
two kinds of solvents by one recycling process.

Here, mixed solvent refers to a variety of mixed solvents produced using a specified or certain
percentage of solvent during preparation
For example, Isoamyl (banana oil) solution doesn’t come from variety of processes and even different
manufacturers as a mixture of waste solution.
Need to preset Heating Temperature values & heating time for “Item 1” and “Item 2” in the parameter
input form / interface for recycling mixed solvent.

This kind of method is suitable for recycling mixed solvent / solution.

Parameter Setting Interface: Three Stages Parameters for mixture with boiling: 60℃, 110℃ & 140℃.
◆Caution: Solutions are mixed by solutions from different processes or different manufacturers, the recovery is
prohibited! In other words, solutions produced by different processes or by different manufacturers are prohibited.

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3. Set Preset Parameters for Recycling Single Solvent / Solution:

To set the preset values/preset parameters of the machine’s control program for
recycling single solvent solution:
※The following one heating stage (Item=1) recovery method is suitable to recovery of single
solvent. For example: The preset values/ parameters of Acetone (56.53°C) are below:

◆Important Notes:
※ During the running of the machine, if you want to stop the recovery process, or to stop the trial
recovery, please press “STOP” key. It means to stop recovery process.

※ The preset values/preset parameters (110, 150) in the picture above must be adopted from
the actual recovery test of the solvent that you want to recycle. So, we suggest users to do a trial
recovery in order to obtain the actual parameters from the test at first.

※ Set Heating Time (Heating Duration): First step is to do a trial recovery, and note the actual
time spent, set the exact recovery heating duration/time and in accordance with the recovery
of the amount of solution.

※ Set Heating Temperature: the heating temperature is set 40℃~50℃ higher than to the
boiling point of the solvent.

When there are many solvents in a mixture, use the highest boiling point of the solvent in the
mixture as the standard for setting the heating temperature.
For unknown solvent’s boiling point, first set the heating temperature to 60℃;Gradually, increase
the temperature until the solvent begins to flow out, when the flow becomes stable, observe the
gaseous solvent temperature to know the actual Heating Temperature.

※ Stop Temp (shutdown temperature): Shutdown temperature must be below the solvent boiling
temperature by 5~10℃. If a mixture, containing several organic solvents, the shutdown
temperature is determined according to the solvent with the highest boiling point in the
mixture.

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4. Set Preset Values/Parameters for Recycling Mixed Solvent:

To set the preset values/parameters for recycling mixed solvent/solution:

●If the dirty solvent/mixed solvent is composed of three kinds of single solvent, and their boiling points
are 60℃, 110℃ and 140℃, the following settings, Three-stage recovery method, are suitable for the
recovery of mixed solvent/solution:

◆Important Notes:
※ The preset values parameters in the picture above must be adopted from the actual recovery test of the
solvent that you want to recycle. So, we suggest users to do a trial recovery in order to obtain the actual
parameters from the test at first.

※ Heating Time (Heating Duration): First step is to do a trial recovery, and note the actual time spent, set
the exact recovery heating duration/time and in accordance with the recovery of the amount of solution.
Heating Time preset values (60, 80, 30 minutes) in the picture above are only for reference purpose, the
actual values depend on the recovery of the amount of solution and the ratio of different solvents.

※ Heating Temperature: the heating temperature is set 40℃~50℃ higher than the boiling point of the
solvent.
If there are many solvents in a mixture, use the highest boiling point of the solvent in the mixture as the
standard for setting the heating temperature.

※ For unknown solvent’s boiling point, first set the heating temperature to 60℃;Gradually, increase the
temperature until the solvent begins to flow out, when the flow becomes stable, observe steam
temperature in the display’s Home Page/Working Interface to know the boiling point of the solvent.

※ During the recovery process, if you want to stop the operation, or to stop the trial recovery process, please
press “STOP” key for 2 seconds. It means to stop recovery process.

※ Stop Temp (Shutdown temperature) must be below the solvent boiling point by 5 °C~10 °C.
The shutdown temperature must be chosen according to the highest boiling point of mixed solvent. For
example: If the boiling points of the solvent in the mixed solvent / solution are 56 °C, 110 °C and 126 °C;
therefore, we choose “126 °C” as the standard to set→120, or →115.

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5.To Do a Trial Recovery:

The preset values/preset parameters must be adopted from the actual recovery test of
the solvent that you want to recycle. So, we suggest users to do once or twice trial recovery
in order to obtain the actual parameters from the recycling trial test.
◆To set the preset values/preset parameters for a trial recovery as below:

※ Set Heating Temperature: the heating temperature is set 40℃~50℃ higher than the boiling
point of the solvent.

Mixture solvent: If there are many solvents in a mixture, use the highest boiling point of the
solvent in the mixture as the standard boiling point temperature value to set Heating
Temperature value.

Unknown solvent: For unknown solvent’s boiling point, first set the heating temperature to 60℃;
Gradually, increase the temperature until the solvent begins to flow out, when the flow becomes
stable, observe the thermometer to know the boiling point of the solvent.

※ Heating Time (Heating duration): Choose appropriate values according to unit’s type below:
Hy20Ex: 120 Hy40Ex: 150 Hy60Ex: 180 Hy90Ex: 180 Hy125Ex: 180
Note: These values above is only a reference, users need to do a trial test to obtain actual values.

※ Stop Temp. (Shutdown temperature): Must be below solvent’s boiling point temperature by
5~10℃.

※ Modify Preset Parameters/values: During the operation of recovery process, if users need to
modify the preset parameters, please press “Menu” button to enter the parameter setting
interface for modification, and then press “Ent” button to save the parameters. The modified
parameters take effect at once. Press “Up/Menu” button for 2 seconds back to working Interface.

Notes: Press any button to wake up the display screen. Don’t press the button for a long time (>2 seconds) when
awakening the display screen, otherwise, input a wrong program's commands by mistake.

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A. Recycling Single Solvent:
To set preset Heating Temperature value 40℃~50℃ higher than the boiling point
of the solvent and others parameter according to the table above.

If you have done the settings, it’s all ready now!

Let’s begin to do a trial recovery of single solvent.


●Transfer dirty solvent into distillation tank and tighten the cover of distillation tank.
●Turn the power switch to “ON” position, the machine into standby mode.
●Press “Start” for about 1 second to start recovery process.
●After about 30~40 minutes, the solvent begins to flow out from recycler’s solvent
outlet, then flow out stably, and gradually becomes significantly reduce to drip;
Meanwhile, observe the gaseous solvent temperature significantly falling.

Attention, from the beginning up to now, note the actual time spent, this is the exact
Heating Duration.

Attention:
◆During the running of the machine, if you want to stop the operation, or to stop the trial
recovery, please press “STOP” key for 2 seconds. It means to stop recovery process.

◆After about 30~40 minutes, if the solvent has not flowed out, press the “Menu” button, enter
parameter interface to increase Heating Temperature by 10℃ per 10 minutes (Press “Ent”
button each time to save modified value and the modified value take effect at once.), until the solvent
begins to flow out.

◆If the distillate solvent flowed out and it is very hot, because:

◎ Cooling Fan’s wind direction: To check the cooling fan’s wind direction, to ensure the fan
blow to condenser directly.

◎ Heating Temperature is too high, therefore, to press the “Menu” button, enter parameter
setting interface to decrease Heating Temperature (Press “Ent” button for each time to save
modified value and the modified value take effect at once . Press “Up/Menu” button for 2 seconds back
to working Interface.), until the solvent begins to flow out.
※ Notes: Press any button to wake up the display screen. Don’t press the button for a long time (>2 seconds)
when awakening the display screen, otherwise, input a wrong program's commands by mistake.

◆If the residue is too dry, can reduce Heating Time (Heating Duration) value; If it is too wet,
then increase Heating Duration figure.
However, preset values/parameter of Heating Duration must be adopted from the actual
recovery test of the solvent that you want to recycle.

Caution:
When you need to recycle the solvent (amount of nitrocellulose≯5%), it is very important to
leave a little amount of solvent in the distillation tank/bucket at the end of the solvent recovery
process, to avoid dryness and burning.
When the content amount of nitrocellulose is more than 5%, it is dangerous for processing.

If the solution contains more nitrocellulose, oxidants and other inflammable dangerous
materials, recovery is prohibited.

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B. Recycling Unknown Solvent:
If you want to recycle a solvent, but you don’t know its boiling point. Please use “One
Heating-stage” (Item=1) method to do settings.

The operation as below:

►To enter Parameter Interface and set Heating Temp. & Heating Time value for
“Item 1” in the parameter table.

►To set Heating Temperature is 60 °C.


※For unknown solvent’s boiling point, set the heating temperature to 60°C at first).

►To set Heating Time: 150, (Choose appropriate values according to recycler’s type).

►To begin the recovery process:


Turn power switch to “ON” position and press “Start” button for about 1 second to
start the recycler and begin the recovery process.

► To obtain the actual values:


After about 30~40 minutes, if the solvent has not flow out, press the “Menu”
button, enter Parameter Setting Interface to modify Heating Temp value, increase
the Heating Temperature by 10°C per 10 minutes, (Press the “Ent” button each time
to save the settings.) until the solvent begins to flow out.
※ Notes: Press any button to wake up the display screen. Don′t press the button for a long time (>2
seconds) when awakening the display screen, otherwise, input a wrong program's commands by
mistake.

When the flow becomes stable, observe the gaseous solvent temperature to know
the solvent’s boiling point temperature, and now the display’s real-time heating
temperature is actual Heating Temperature.

Here, the trial recovery of solvent ends.

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STEP 4: TURN ON / TURN OFF

1. TURN ON:
Turn the power switch to “ON” position, the machine into standby mode.
Press the “Start” button for about 1 second to start recovery process, then the
display on the left in the control panel displays the working interface. Start/Run
Indicator in the screen displays “run” and displays running items with white
background on the display screen.
(Attention: Forget to press “Start” button to start recovery process, the recycler will not start running.)

2. TURN OFF:
During the recovery process, if you want to stop running, press “ STOP” button for 2
seconds, the recycler will stop recovery process.
Turn the power switch to “OFF” position, power indicator goes off.
(The recycler can automatically shutdown according to the preset running time).
►Press “Stop” button for 2 seconds, display “Stop”. The recycler stops running and
on standby mode.

►Turn Power Switch to “OFF” position to cut off the power supply.
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STEP 5: Machine Operation & Management.

1. Fill in the Machine Operation Record Form:


Write detailed record of the solvent solution, machine operation time, heating,
recovery progress, recovery speed and the machine run-time parameters.
2. Always check the indicator light status and machine running conditions.
3. Replace recovery containers appropriately to avoid leaks.

STEP 6: Shut off & Residue Cleaning.

1. After recovery, there are residues in distillation tank.


◆Please clean the tanks to avoid solidification of the residue.
Accumulation of residue in the recovery tank is dangerous!
2. Turn the power switch to “OFF” position to cut off the power supply.
3. The temperature of Heat transfer oil must drop below 60°C, then to loosen the
locking handle of distillation tank lid/cover.
◆Be careful when cleaning the residue to avoid burns.
4. Loosen locking handle, open the distillation tank lid/cover.
5. Grab the handle, pull the safety lock pin, gradually tilt and pour out residue.
Insert the safety lock handle, stabilize the recovery tank;
Clean the residue in the tank. Here, special blade can be used when necessary, to
clean-up the residue.

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CAUTION:
※Accumulation of residue in the recovery tank is dangerous! It needs to be cleaned up
after each run. Residue accumulation not only reduces the recovery efficiency but also
leads to overheating and deformation of the recovery tank. It even gives rise to smoky
residue and fire.

※If the heating temperature is too high in the end of the recovery process, the residue in
the tank may become smoky. On the other hand, turn off the power supply first, and let
the machine cool down itself. Opening distillation tank lid is strictly prohibited on this
condition! Opening the tank will lead to oxygen flow into the tank causing fire outbreak.

●Safety Precaution: No matter the situation, do not take the following risky behaviors:
◆When the machine is running and heating up, and the recovery tank is of high temperature,
don’t touch the tank to avoid high temperature burns.
◆Do not tilt the tank when the machine is running.
◆Do not loosen the tank lid knob or open the lid when the machine is running.
◆Do not open the power box when the machine is running!

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CHAPTER 6
Scope of Application of the Machine
I. Applicable Industry:

1. Automobile manufacturing and repair industry: Vehicle spraying equipment pipe and
spray gun cleaning, such as banana oil (Isoamyl acetate), toluene, xylene, MEK, butyl
acetate etc.;solvents produced in the process of cleaning gasoline engines.

2. Electronic products manufacturing industry (such as: LCD, LED etc.): cleaning mold,
cleaner used in cleaning electronic products, such as: Ethanol, acetone,
trichloroethylene.

3. Precision instruments and hardware manufacturing industry: organic solvents used


in cleaning mold and processed products, such as Isoamyl acetate(banana oil),
hydrocarbons, kerosene, gasoline and other solvents.

4. Sports Equipment Manufacturing Industry: golf, melting wax casting rods and other
cleaning agents, spraying and cleaning clubs, solvent rods, rods and other solvents.

5. Shoe Material Industry: Cleaning spray equipment, and variety of organic solvents, such as:
shoe sole, heel spray, upper printing process, cleaning etc.

6. Plastic Materials: Organic solvents for cleaning mold and processed products, such as:
cleaning solvent used after printing process after.

7. Printing Industry: cleaning agent used in washing printing machines, such as plate
washing solvents, machine washing solvents etc.

8. Manufacture of chemical coatings: Cleaning equipment, solvent containers and filling


equipment, variety of organic solvents for mixing paints, such as banana oil, xylene,
MEK, butanone, etc.

9. FRP products industry: solvents used in anti-corrosion coating of surfaces and polishing
during production process, such as yacht production, wind turbine blade
production etc.

10. Jewelry industry: solvents used in Surface pretreatment cleaning and plating
pre-treatment.

11. Optical products: solvents used in cleaning of components during production process,
solvents used in coating pre-treatment etc.

12. Furniture Manufacturing Industry: organic solvents used in cleaning paint spraying and
mixing equipment such as amyl acetate (banana oil), xylene, MEK, acetone etc.

13. Other Industries that use organic solvents as cleaning agents.

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II. Solvents Can Be Recovered as below:

※ This machine is suitable to recover organic solvents from a liquid solution, not
suitable for recycling gaseous solvent and solid-state materials.

It’s suitable to recover organic solvents from waste solution, such as waste solution
resulting from spray gun cleaning industry, trichlorethylene solution for cleaning
electronic products, toluene solvent, optical lens cleaning IPA, ethanol, banana oil used
in printing industry etc, can be simply categorized as follows:

1. Aromas: toluene, xylene, trimethyl benzene,

2. Aliphatic hydrocarbons: pentane, hexane, octane

3. Alicyclic hydrocarbon: cyclohexane, cyclohexanone, toluene cyclohexanone.

4. Halogenated hydrocarbons: chlorobenzene, dichlorobenzene, dichloromethane,


trichlorethylene, etc.

5. Alcohol: Methanol, ethanol, Isopropyl alcohol etc.

6. Ether: ethyl ether, propylene oxide, etc.

7. Esters: Acetate, ethyl acetate, butyl acetate.

8. Ketones: Acetone, butanone, methyl isobutyl ketone.

9. As well as other organic solvents not listed.

III. Following Solvents Are Not Suitable for Recovery:

1. Solvents containing nitrogen, oxidizer solvents, other dangerous chemicals.

2. Strong acid or strong alkaline solvents.

3. Oxic solvents,

4. Strong solvents, they are corrosive to stainless steel or brass.

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CHAPTER 7
Machine Maintenance & Repair

I. Preparation for Machine Maintenance & Repair Operations:

1.Operator safety: Wear protective gloves, protective glasses, and protective mask.
2.Switch off the machine, disconnect the machine power supply.
3.Clean up the recovery tank; be sure it’s cleaned up.
4.Be sure that heat transfer oil temperature is restored at room temperature.

II. Machine Maintenance:

1. Machine Cleaning: After running, clean the recovery tank! Always maintain the
overall cleanliness of equipment.
2. Pipeline Maintenance: Maintain the machine once a week, keep the pipeline
flowing, be sure the meter display is normal.
3. Power Line Maintenance: check the supply line, keep the lines working, avoid
aging, damage, current leak and other security implications.
4. Replacement of heat medium oil / HTF (heat transfer fluid): Usually, when the
machine runs for a full year or 1000 hours, the heat transfer oil must be replaced.
Otherwise it may damage the heating rods or reduce the heating efficiency of the
machine. Replace the heat transfer oil following the steps below:
①Stop the machine running; be sure the machine has been disconnected from
main power supply.
②Heat transfer oil temperature must be restored to room temperature for the
next step to be taken.
③Loosen the oil outlet screw to discharge the old oil. Then tighten the oil outlet
screw.
④Loosen the air hole screw and remove the oil inlet screw, follow machine
specifications by adding a corresponding amount of new oil; then tighten the
air hole screw and screw the oil inlet screw.
5. Stop using (more than 60 days), please follow the request maintenance:
①Disconnect the power cord.
②Pour out the residue, and clean recycling tank.
③Remove clean solvent outlet pipe.
④Keep the machine in a cool and dry place.

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CAUTION:In order to ensure normal operation of the machine, use “ HongYi®” solvent
recovery machine’s exclusive heat transfer oil.

◆To replace the transfer oil, the old oil must be cleaned up, the underneath oil
outlet screw must be tightened up after oil replacement.

◆The manufacturer has no legal liability when the machine develops problems
resulting from use of another brand of heat transfer oil.

III. Replacement of Major Components of the Machine (Disassembly) Operation.

1. Process of heat transfer oil replacement.

● At the bottom of the machine, there’s an outlet for heat transfer oil. Place a container; discharge

the oil and let the oil flow into it.

● Loosen the air valve / oil inlet valve, and the air hole screw.

● Loosen the oil outlet screw and remove the screw out.

● Let the old oil flow out into the container.

● Tighten the oil outlet screw.

● Loosen and remove the oil inlet / air value, and air hole screw.

● Use a funnel and fill in new heat transfer oil through the air valve / oil inlet.

● Tighten the air hole screw, then screw the air valve/ oil inlet screw.

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Type Hy20Ex Hy40Ex Hy60Ex Hy80Ex Hy90Ex Hy125Ex Hy250Ex Hy450Ex

Heat-transfer
10L 18L 22L 30L 30L 32L 112L 200L
Oil Quantity

2. Heating Rod Replacement Process.

● Loosen the oil outlet screw, and discharge the heating transfer oil.

● Remove the heating rod plate, remove the top shell explosion-proof screw, and open the heater

explosion-proof shell cover.

● Loose the heater connector screws; loosen the explosion-proof shell connector.

● Loosen the explosion-proof sealing rubber ring and clamping screws, to protect hose and cable

pull outward slightly to loosen it.

● Pull out the heating cable from the explosion proof shell, remove the explosion proof shell.

● Remove the heating rod.

● Install a new heating rod.

● Fill in heating transfer oil.

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CHAPTER 8
Common Causes of Failure
& Fault Exclusion Method

I. After power is switched on, indicator light not showing, machine is not running:
Fault Characteristics: After power is switched on, power indicator fails to show,
machine fails to run:

Cause of the malfunction: No power supply system, the fuse burns out;
Solution:Check the power supply system line current, power fuse and main power
switch has been properly closed, ensure a regular supply of electricity,
check that the fuse over the transformer in the control box, if burnt,
replace with a new one.

II.If after recovery the solvent appears turbid or foaming:


Fault Characteristics: Solvent collected appears murky (not clear), easily
appears turbid or foamy.

Cause of the malfunction: Excess residue in the recovery tank, exceeding


maximum level line, solution containing foam material, the heating
temperature is set too high, leading to excessive boiling of the
solution in the tank, excess waste water solution.

Solution: ①If waste solution added is over the maximum level line, reduce the
solution to the proper level line. Clean up the tank and add 5 liters of
solution, start the recovery process, to clean up the flow channels.

②If the solution contains foamy material, reduce the quantity of


waste solution or add an appropriate defoamer; clean up the
recovery tank, then add 5 liters of clean solvent to clean up the flow
pipes.

III. Outflow of hot solvent through recovery pipe:


Fault Characteristics: outflow solvent is of high temperature.
Cause of failure: ①Abnormal condenser;
②Heating temperature is set too high;
③Poor ventilation.

Resolution: ①Check if condenser is covered with dirt, dust, or if the condenser


does not work properly, removes the dirt or fixes it properly.
②Check that the temperature controller settings are normal.
③Proper ventilation should be provided.

IV. If organic solvents in a waste solution can’t be fully recovered:


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Fault characteristics: After recovery, there remains large quantity of
unrecovered organic solvents in the tank showing that the recycling
rate is low.

Cause of failure: ①.The heating temperature is set too low.


②. Waste solution still contains solvent with boiling point above
170℃.
③. Heating temperature time setting is incorrectly set.

Resolution of fault: ①. Check the heating temperature controller, set the


correct heating temperature;
②. If it contains a high boiling point solvent, use Hongyi vacuum
device, to reduce the boiling point of high boiling point solvents;
③. If the heating time is set too short, then an appropriate extension
of the heating time is recommended.

V. When the machine is in operation and no solvent outflow:


Fault Characteristics: Normal heating without outflow.

Cause of failure: ①.Steam pipe blockage, Solvent vapor does not normally flow
through the cooling system pipes. ②. Recovery tank has residues,
leading to undesirable heat conduction, causes low heating. ③.
Heating temperature setting is low.

Resolution of failure: ①. Check that pipes are not blocked, open the tank lid,
blow compressed air of 0.2bar through the outlet pipe; Check
whether there is enough air blowing through the solvent outlet. ②. If
recovery tank has much residue, heating is abnormal, clean up the
tank residue. ③. Follow the solvent’s boiling point to set the heating
temperature correctly.

VI. Tank Burning.


Fault characteristics: The seal of the tank lid becomes smoky or discovering
burns on opening the tank.

Cause of failure: Heating temperature is set too high; Too much residue
accumulation, causing residue fire; Over heating will cause tank
deformation or cracks.

Resolution method: When smoke occurs, opening recovery tank at this time is
strictly prohibited. First switch off the power; let the machine cool off.
Then lower the heating temperature and appropriately shorten the
heating time. After recovery, leave a little amount of solvent in the
tank to avoid dryness and burns. Third, clean up the residue in the
tank.

VII. When the tank lid leaks air/ vapor.

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Common malfunction characteristic: when the machine is in operation,
vapor leaks through the lid seal.

Cause of the malfunction: ①. Most of the time, it’s because the vapor pipe is
blocked;
②. Lid is not tightened or the seal is tampered with;
③. If the heating temperature setting is too high, it may lead to
excessive boiling, excessive vapor and too much steam pressure.
Resolution method: ①.Check whether the steam condenser pipe is congested.
②. Check the lid rotary knob and tighten the handle.
③. Check the gasket sealing performance, replace if broken or
smoothen it if flattened.
④. Check the solvent outlet pipe using 0.2bar air pressure, check the
heating temperature setting, Check if pressure is too high or the
heating temperature is set too high and reset appropriately.

VIII. When the machine is running, recovery tank isn’t heating & the thermometer
fails to show temperature rise:
Malfunction characteristics: Power switch turned on, indicator light shows
but the recovery tank isn’t heating, and the thermometer fails to
show temperature rise.

Cause of malfunction: ①.Heating temperature is not set, heat transfer oil is


old and useless;
②. Heat transfer oil is not fit causing malfunction.
③. Heating temperature controller or relay switch is broken.
Resolution Method: ①. Check the heating temperature setting; ensure that the
heating temperature has been set.
②. Check to determine whether the heat transfer oil is aged to
replace with new oil.
③. Check whether heating controller and the relay switch are
damaged. Check the heating component using the ammeter to know
whether the current is normal.

IX. When it can not automatically shutdown:


Malfunction characteristics: Steam thermometer can not rise to the set
shutdown temperature, after solvent recovery the machine can’t shut
down.
Cause of the malfunction: Heating temperature is set incorrectly or shut down
temperature setting has error, or the main power switch is not reset.
Resolution Method: According to solvent boiling point and features, set the
correct heating temperature and shutdown temperature; ensure the
main power switch is restored to the original position.

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CHAPTER 9
Reference Appendix
Common Organic Solvents Boiling Point, Density Table
No. Solvent Boiling Point (℃) Density
1 Toluene 110.0 0.8669
2 Xylene 137.0 0.8540
3 Trimethylbenzene 164.7 0.8650
4 Tetramethylbenzene 205.0 0.9020
5 Acetone 56.1 0.7905
6 Methylethylketone 79.64 0.8049
7 Methyl isobutyl ketone 115.9 0.8000
8 Cyclohexanone 155.65 0.9478
9 Methanol 64.51 0.7913
10 Ethanol 78.32 0.7893
11 Butyl alcohol sec. 107.9 0.8020
12 Butyl alcohol 117.0 0.8100
13 Cyclohexanol 161.0 0.9493
14 Isopropyl alcohol 82.4 0.7860
15 Diethylene glycol; diglycol 240.0 1.1200
16 N-Butyl-Acetate 126.3 0.8820
17 Ethyl acetate 77.0 0.9000
18 Butyl acetate sec. 112.2 0.8700
19 Ethoxy ethyl acetate 156.3 0.9730
20 Monoglicol acetate 178.0 1.1090
21 Propyl bromide 70.97 1.3597
22 Cyclohexane 80.719 0.7790
23 Methylene chloride 39.750 1.3260
24 Dichloroethane 84.0 1.2550
25 Dichloropropane 96.4 1.1560
26 Methyl chloride 61.0 1.4890
27 Trichloroethane lll 74.0 1.3492
28 Trichlorethylene 87.19 1.4640
29 Tetrachlorethane 146.3 1.6000
30 Perchlorethylene 121.2 1.6230
31 N,N-Dimethyl formamide 153.0 0.9430
32 Ethyl ether 34.6 0.7140
33 Freon 113 47.6 1.5650
34 Isophorone 205.0 0.9200
35 Butyl cellosolve 170.2 0.9008
36 Ethyl cellosolve 135.6 0.9295
37 White Spirits/White gas 60-11 0.68-0.72

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