Professional Documents
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Radiation Protection
Radiation Protection
SAFETY MANUAL
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RADIATION PROTECTION PROCEDURE
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TABLE OF CONTENTS
1. INTRODUCTION ................................................................................................. 2
2. SCOPE ................................................................................................................ 2
3. DEFINITIONS...................................................................................................... 2
4. PROCEDURE ..................................................................................................... 4
5. RESPONSIBILTIES .......................................................................................... 25
6. REFERENCES .................................................................................................. 28
ATTACHMENT......................................................................................................... 28
APPENDIX ............................................................................................................... 29
Sara Khamis /
Carl
4 01-Jul-12 Refer to Appendix R Lloyd G Askham Amit Parikh
Poldrack
Carl Poldrack
Sara Khamis / Carl
3 04-Jul-11 Refer to Appendix R Lloyd G Askham
Amit Parikh Poldrack
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1. INTRODUCTION
Exposure to ionizing radiation; however small the amount, is presumed to involve some
risk. Radioactive sources are to be handled and used safely in order to minimise the risk
of radiation exposure to all personnel and the general public.
The instructions outlined in this procedure are not intended to detail working procedures
for radiation work. They detail the safety aspects within which the work shall be
conducted.
2. SCOPE
This procedure is applicable to all Q-Chem employees and its contractors and describes
the minimum requirements to be followed to minimize the risk of exposure to ionising
radiation while transporting, handling, storing and using equipment containing radioactive
material. Q-Chem in this document refers to Q-Chem, Q-Chem II and RLOC.
3. DEFINITIONS
ALARA (As Low As Reasonably Achievable) means making every reasonable effort to
maintain exposures to radiation as far below the dose limits as is practical, taking into
account the state of technology, the economics of improvements in relation to state of
technology, and the economics of improvements in relation to benefits to public health
and safety.
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Curie (Ci) is a unit used to measure radioactivity. One curie is that quantity of a
radioactive material that shall have 37 x 109 disintegrations in one second.
“Classified Radiation Worker” means any employee who is likely to receive a dose of
ionising radiation which exceeds three-tenths (3/10) of the annual dose limit (i.e. >6
mSv).
Dose means the quantity of ionizing radiation absorbed, per unit of mass, by the body or
by any portion of the body.
Dosimeter is a device used to determine the external radiation dose a person has
received.
Effective Dose is the dose that takes into account the type of the organ that is being
exposed to radiation. The unit of measurement is Sievert (Sv).
Equivalent Dose is the dose that takes into account the type of radiation being absorbed
by the body tissue. The unit of measurement is Sievert (Sv).
Radiation (Ionizing Radiation) includes alpha rays, beta rays, gamma rays, X-rays,
neutrons, high-speed electrons, high-speed protons, and other atomic particles; but such
term does not include sound or radio waves, or visible light, or infrared or ultraviolet light.
Sievert is a unit used to derive a quantity called equivalent dose. This relates the
absorbed dose in human tissue to the effective biological damage of the radiation.
Equivalent dose is often expressed in terms of millionths of a Sievert, or micro-Sievert.
One Sievert is equivalent to 100rem (Roentgen).
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mSv) in 1 hour at 30 centimeters from the radiation source or from any surface that the
radiation penetrates.
4. PROCEDURE
4.1.1. All work involving sealed radioactive sources shall be carried out in accordance
with a Permit-To-Work (PTW) and Radiation Clearance Certificate (RCC)
system.
NOTE
4.2.1. A list of all radioactive sources used at Q-Chem is maintained by the Q-Chem
RPO.
• Innov-X System Alpha 2000 XRF Analyzer, Serial Number 9567 – Ras
Laffan Complex
4.3.1. The Q-Chem Radiation Protection Officer (RPO) shall oversee radiation safety
matters on site.
Mesaieed Complex
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4.4.3. Exposures received from diagnostic, therapeutic, X-Ray machines for medical
treatment and background radiation, shall not be included in any of these
exposure limits:
• TLD or Film badges shall be required for each Classified Radiation Worker
where applicable.
• The TLD / Film badges shall be worn by Classified Workers at all times
when working with or handling radioactive materials.
The badge shall only be worn by the individual to whom it was issued.
Badges shall only be worn at work; i.e. they are for assessing
occupational exposure.
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• The badge shall not be left or stored in a highly humid environment, in high
temperatures or inside a vehicle.
• Where applicable, all personnel entering and / or performing work that may
expose them directly or indirectly with a radioactive source shall be supplied
with either a pen type chargeable pocket dosimeter or a battery operated
electronic dosimeter.
The dosimeters are not a substitute for TLD / Film badges that may be
issued to employees (Classified Radiation Workers).
They shall be worn in conjunction with TLD / Film badges (for Classified
Radiation Workers only).
• Each individual shall enter the dose received in the daily dose record after
completion of the job (see Attachment 2).
• If the pocket dosimeter goes out of scale or does not function properly, the
employee shall immediately stop all radiation work and contact the
applicable RPO to make a complete survey of the area for radiation
exposure levels.
The job shall not be resumed until the defective dosimeter is replaced.
These medicals shall include, but shall not be limited to the following
tests:
Chest X-Rays
Employee medical reports shall be maintained as per the Q-Chem Medical Records
Policy.
4.6.2. Radiation survey meters used for monitoring shall be in good working condition
and measure within the applicable ranges:
4.6.3. All survey meters used shall have a valid third party calibration.
4.6.4. In case of a survey meter becoming inoperable during radiation work; the area
shall be barricaded (if no barricades already available), and all work within that
area shall be suspended until a replacement meter is available.
4.7.1. Each Supervised Radiation Area shall be conspicuously posted with a sign or
signs bearing the radiation caution symbol (Appendix E) and the words:
CAUTION
CAUTION
4.7.3. Each area or room in which radioactive material is used or stored and which
contains any radioactive material (other than natural uranium or thorium) in any
amount exceeding 10 times the quantity of such material specified in Appendix
C to 10 CFR part 20 shall be conspicuously posted with a sign or signs bearing
the radiation caution symbol (Appendix E) and the words:
CAUTION
RADIOACTIVE MATERIALS
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CAUTION
RADIOACTIVE MATERIALS
NOTE
4.8.2. The following conditions shall apply during the storage of radioactive sources
not in use:
• The storage area shall be clearly marked with the radiation caution warning
sign (Trefoil) – see Appendix E.
• The storage area shall be designed such that the dose rate on the outer
surface does not exceed 1µSv/hr.
• If this limit is exceeded the area around the store shall be marked off at the
7.5µSv/hr boundary and indicated by means of trefoils and warning notices.
The source register shall be kept by the relevant Authorized Person and
be available on request.
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• The Contractor RPO shall have an up-to-date inventory of all sources under
his / her control while at the Q-Chem site.
4.9.1. A properly equipped and marked vehicle shall be used to transport shielded
equipment containing radioactive sources.
• The vehicle shall be equipped with a suitable storage container in which the
radioactive package shall be placed during transport by road.
4.9.2. The transport vehicle shall be clearly marked with the following signage:
Contact Number
4.9.3. The source container shall be marked with the radiation caution warning symbol
(Appendix E).
4.9.4. The relevant RPO is responsible for accompanying a radioactive source when it
is transported by road:
• At all times while on the Q-Chem site (unless locked away as stated in
Section 4.11.9).
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• Carry out a radiation survey to check that the radiation intensity does not
exceed the following limits:
4.10.1. The gamma gauges are located in the Polyethylene Reactor Structures, i.e.
Trains 1, 2 and 3 (see Attachment 3):
Polyethylene Train 3:
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4.10.2. These instruments are intended to remain in service for the lifetime of the plant.
4.10.3. Any maintenance work that involves potential exposure to the radiation source /
beam shall be conducted while the shutter is in the OFF position and AFTER
confirmation that the device shutter is properly CLOSED.
4.10.4. The following two methods shall be utilized to confirm that the device shutter is
closed properly:
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4.11.1. All work involving Industrial Radiography shall commence under the supervision
of a contractor-nominated Radiation Protection Officer who shall report to the
Q-Chem Designated Site Representative (DSR) / Designee.
4.11.2. A Permit To Work (PTW) shall only be initiated upon the completion of the
following:
• Job Safety Analysis (JSA) Meeting. The following items shall be discussed
and approved at the JSA meeting:
Site-specific procedures,
4.11.3. The following are the minimum required personnel for the JSA:
• Permit Issuer, or
4.11.4. The Contractor’s Emergency Response Plan (ERP) shall be presented at the
JSA meeting for all Industrial Radiography work.
• The JSA shall not be concluded and signed off without the Emergency
Response Plan.
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4.11.5. A toolbox talk shall be conducted by the Contractor RPO / Lead Worker to
explain the permit conditions to all Classified Radiation Workers under the
permit.
• The content of the JSA shall be discussed with all Classified Radiation
Workers in the tool box talk (if Radiographers were not part of the initial
JSA) by the contractor RPO / Lead Worker.
• A copy of the JSA shall be available with the PTW / RCC at the entry point
to the Controlled Radiation Area by the contractor RPO.
4.11.6. The contractor RPO shall be present at all times at the worksite when the work
is being carried out.
• The RPO shall manage the Controlled Radiation Area at all times while
radiography is in progress.
4.11.7. A “Controlled Radiation Area” shall be established for all Industrial Radiography
operations.
• It is the duty of the Contractor RPO to patrol / supervise the area and warn
Non-Classified persons from coming near this outer cordon.
• Barricade tape (of a bright colour e.g. yellow & black) and radiation signs in
Arabic and English, shall be used to cordon off Controlled Radiation Areas.
The safe working distance shall be calculated for the radioactive source
strength being used and the demarcation barriers shall be positioned
accordingly prior to exposing the radioactive source.
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4.11.8. Whenever possible during radiography, the radiographer shall use collimators
to reduce the area affected by radiation.
NOTE
All personnel entering Controlled Radiation Areas shall wear their TLD /
Film badges and Digital Radiation monitor / Dosimeter at all times and
shall be excluded if found not wearing them.
4.11.9. The exposure container shall not be left unattended at any time during
radiography.
• The Radiographer (Contractor RPO) shall keep the key of the locking
device until radiographic operations recommence.
4.11.11. Monitoring shall be carried out to ensure the safe return of the source to its
container.
NOTE
4.11.12. All radiographic work shall be suspended if any part of the equipment is noticed
to have become defective or damaged during radiographic operations.
4.11.13. Prior to the commencement of radiation work, the following steps shall be
taken:
• The DSR / Designee shall inform all relevant parties about the planned
radiation work including locations and timing
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• All permits within the Radiation Controlled Area or as specified by the Shift
Coordinator / Shift Supervisor (RLOC), shall be withdrawn prior to issuing
the permit for radiation work.
• Safe barrier distances shall take into account all working levels around
radiographic work.
The Radiation worker shall return the work permit / radiation clearance
certificate to the Shift Coordinator / Shift Supervisor (RLOC) and remove
only one barrier.
The Radiation worker shall then remain close to the removed barrier
point and keep a strict control of personnel movement into the restricted
area.
• Radiation work can be resumed after people have cleared the restricted
area and all barriers reinstated, and the Radiation worker has the work
permit / radiation clearance certificate in his possession.
CAUTION
Under no circumstances shall persons other than the classified
radiation workers cross the safety barrier during radiographic
operations!
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4.12.3. This survey shall also be performed to verify if equipment can be shipped to an
offsite facility for maintenance / repair.
4.12.5. Entry into vessels suspected of containing NORM, any welding on NORM-
contaminated equipment, or any abrasive work (e.g., scraping, grinding, buffing,
polishing, etc.) of NORM-contaminated equipment requires additional PPE
which at a minimum shall include, but is not limited to, the following:
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• Safety glasses.
• Neoprene rubber gloves [If leather gloves are used, e.g. due to
requirements of task, they must be disposed of after use).
4.12.6. Employees working on contaminated equipment shall not eat, smoke, and
drink, etc. while engaged in such activities.
4.12.7. Skin contact shall be avoided with interior surfaces where practicable.
4.12.8. All workers involved with such equipment shall be required to wash their hands
thoroughly with soap and warm water before smoking, drinking, eating, etc. and
at the end of work.
4.12.9. Gloves, respirator cartridges, disposable clothing and rags used on suspected
contaminated equipment shall be put into plastic bags, sealed and tested by the
Q-Chem RPO to determine disposition.
4.12.10. Every effort shall be made in the preparation of N.O.R.M. containing equipment
for maintenance that personnel exposure is kept AS LOW AS REASONABLY
ACHIEVABLE (ALARA). This can be accomplished by purging, steaming, and
time (allowing items to stand for a long period).
4.12.11. Any item removed from contaminated equipment, (i.e. pump packing, mil scale,
etc.), shall be put into plastic bags, sealed, and tested by the Q-Chem RPO /
Designate to determine disposition.
NOTE
The levels of N.O.R.M. found in process equipment can vary with feed
stocks; therefore it may not be present in a piece of equipment one time
and present the next. No assumptions shall be made.
Refer to Appendix J for guidelines on N.O.R.M.
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• Removing any outer components that normally conceal the source / source
holder,
Contact the Q-Chem RPO / Designate for tasks not listed in this document!
4.13.2. The Contractor’s Radiation Safety Manual (RSM) together with all the
necessary certifications of the affected radiation workers shall be presented and
reviewed by the Q-Chem RPO for all industrial radiography work before the
RCC can be issued.
4.13.3. No radiation clearance certificate shall be issued when working with exposed
radioactive sources / materials if there is no RPO to supervise the operation.
• The Contractor RPO shall be physically present at worksite for all Industrial
Radiography.
• Shutter closing / opening as part of normal Lock Tag & Try (LT&T)
procedures,
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• Planned Maintenance (PM) on the outer surface of the gauge, e.g. cleaning
or applying lubricants for the shutter closing mechanisms.
Contact the Q-Chem RPO / Designate for tasks not listed in this document!
4.13.5. The RCC shall be posted together with the PTW at the entry point of the
radiation work area (boundary of entry point) with the following attachments:
• Copy of JSA
• The RCC is only valid for the duration authorized on the certificate provided
there is no change in job scope or Radiation Protection Officer.
The RCC shall be re-validated or re-issued by the Q-Chem RPO for any
changes to the original scope.
NOTE
• When radiation work is completed or stopped for the day, the contractor
RPO shall notify the Lead Worker or Work Permit Issuer, i.e. Area Operator
or Area representative.
• The Permit Issuer shall carry out a joint inspection of the work area along
with the Contractor RPO and verify that all radioactive materials / sources
have been safely retrieved and the area is safe.
The Contractor RPO (Industrial Radiography) shall scan the work area
with the radiation survey meter to ensure no significant radiation dose
rates are detected.
The radiation clearance survey dose rates shall be recorded on the RCC
(as required on the RCC) before the PTW is closed out.
• The Contractor RPO (receiver of the RCC) shall deliver the completed RCC
to the Q-Chem RPO / Designate for final closure. The following
documentation / equipment shall be returned with the RCC when applicable:
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• The Q-Chem RPO shall retain the closed out RCC for a minimum period of
one (1) calendar year.
NOTE
4.14.1. All users of radioactive materials shall be familiar with the Emergency
Response Procedures before any emergency arises.
4.14.2. Refer to Appendix A for Q-Chem Emergency Contact Details for dealing with
radioactive materials.
4.14.3. If a gas detector alarms or the plant alarm sounds at any time during the job:
• The contractor RPO or Lead worker shall notify the Permit Issuer.
4.15.1. The Q-Chem “Incident Reporting and Investigation Procedure” shall be followed
in reporting and investigating an incident (or near miss) involving radioactive
materials.
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4.15.2. The Q-Chem RPO or designate shall be notified promptly of all accidents,
incidents, or near misses involving the following scenarios:
4.15.4. In addition, the Q-Chem RPO / Designate shall report IMMEDIATELY to the
Corporate RSO within the Corporate EHS organization by telephone of any
incident involving radiation which may have caused or threatens to cause:
• Exposure of the skin of the whole body of any individual to 150rems [1.5Sv /
1500mSv] or more of radiation;
4.15.5. The Q-Chem RPO / Designate shall report by telephone within Twenty-four
(24hrs) to the Corporate RSO of any incident involving radiation which may
have caused or threatens to cause:
• Exposure of the skin of the whole body of any individual to 30rems [0.3Sv /
300mSv] or more of radiation;
NOTE
The Q-Chem RPO shall also notify such individual of the nature and
extent of exposure. This notice shall be in writing and shall contain the
following statement:
"You should preserve this report for future reference."
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4.16.1. All records documenting compliance with this procedure shall be kept in the Q-
Chem office or as indicated in the applicable sections of this procedure.
4.16.2. Where applicable; a list of all Classified Radiation Workers shall be maintained
by the Q-Chem RPO.
4.16.3. Records of the results of surveys and personnel (where applicable) radiation
exposure monitoring shall be maintained for the life of the facility.
4.16.4. Radiation survey meter calibration and maintenance records shall be available
on request from the Q-Chem RPO.
4.17. Training
4.17.2. Training is necessary to ensure that safe work practices are followed, to
prevent overexposure of the operator and others, and to avoid contamination of
the surroundings.
4.17.3. Employees who during the normal course of their duties are required to perform
radiation-related tasks in “Controlled or Supervised Radiation Controlled Areas”
shall at a minimum receive annual training in the following areas:
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4.17.4. Specific issues in the operation of the various instruments, e.g. PMI and XRF
spectrometer, shall be provided within the applicable workgroup by
appropriately experienced personnel, the equipment / instrument vendors or
under their guidance.
4.18.1. Program reviews shall be conducted at least annually, with time between
reviews not to exceed twelve months.
4.18.3. The following items shall be addressed during the review process:
• New work practices or work locations (if any) involving potential exposure to
Ionizing Radiation sources.
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5. RESPONSIBILTIES
5.1.1. Prepare the Radiation Protection Procedure and facilitate its review.
5.1.3. Authorize radiation clearance certificates for all radiation work at Q-Chem.
5.1.4. Conduct radiation surveys, audits & sealed source wipe tests where required.
5.1.5. Manage and monitor the usage and interpretation of electronic radiation
dosimeters used by Q-Chem employees.
5.1.6. Inspect and clear all items arriving / received at the Q-Chem site that contain
radioactive materials.
5.1.8. Report on radiation safety incidents to the Ministry of Environment (MoE) and
the Corporate RSO within the Corporate EHS organization.
5.1.9. Develop and provide Radiation Safety Training to affected end users.
5.1.10. Ensure contractor radiography service providers used on site are made familiar
with the requirements of the Q-Chem Radiation Protection Procedure.
5.2.1. Ensure a copy of this procedure is presented to the radiography contractor prior
to the JSA meeting.
5.2.3. Inform the Q-Chem RPO / Designate regarding the expected arrival of any
radioactive materials at the Q-Chem premises.
5.2.4. Ensure the JSA has been completed before the issuance of a PTW.
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• Ensure the JSA is communicated during the toolbox talk to the affected
employees.
5.3.1. Meet all procedural and documentation requirements as per the radiation
protection procedure.
5.3.2. Meet all requirements as stated on the Radiation Clearance Certificate (RCC).
5.4.1. Be familiar with all emergency response procedures related to radiation safety
at Q-Chem.
5.4.2. Ensure they have received radiation safety training before working with
radioactive materials / equipment.
5.4.3. Wear an electronic radiation dosimeter (where applicable) at all times when
entering or working in a designated radiation area.
5.5.1. Ensure proper storage (where applicable) and maintenance of all equipment &
instruments containing radioactive sources.
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5.5.4. Ensure all radiation safety signage / labelling requirements are fulfilled within
their affected areas.
5.5.6. Consult with the Q-Chem RPO / Designate when necessary or if requiring
clarification on matters pertaining to radiation safety.
5.6.2. Liaise with the contractor RPO during any emergency situations that may arise
during industrial radiography work on the Q-Chem premises.
5.7.1. Where applicable; schedule and conduct medical screening and surveillance for
Q-Chem Classified Radiation Workers and anyone requiring surveillance in an
emergency situation.
5.7.2. Maintain all employee medical records as per Q-Chem Medical Records Policy.
5.8.1. Contact the Q-Chem RPO / Designate when receiving any items containing
radioactive materials
5.9. Training
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6. REFERENCES
ATTACHMENT
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APPENDICIES
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MESAIEED SITE
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NOTE: The following P.A. Announcement SHALL be made 15 minutes before the
scheduled Radiography begins.
ALL CLEAR!
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RADIOACTIVE MATERIALS
Tel:
Fax:
NAME:
Tel Office:
Tel Home:
Bleep:
Mobile Phone:
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F1. Description
Portable devices containing sealed sources of radioactive material are also typically
used in Positive Material Identification (PMI) programs.
F2. Licensing
1. Specific License
• The manufacturer, model number, isotope, activity and authorized use must be
listed on the user’s specific license before the manufacturer shall distribute the
device.
• The licensee may be authorized by the licensing agency to install and remove
fixed devices. Refer to the site specific license and read the conditions of the
license.
2. General License
• The manufacturer can distribute the device without the user having a license.
The licensing agency regulations may require the user to acknowledge the
possession of the device depending on the isotope and activity of the device.
Typically most licensing agencies allow 30 days from the receipt date of the
device for the user to make this acknowledgment in writing to the agency.
Check with local regulations to ensure compliance with this requirement.
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F3. Procurement
The following steps are required to purchase a device containing radioactive material:
• The site RPO must be notified of any plans to purchase a device before
initiating the purchase.
The RPO notification must include the device manufacturer, model number,
isotope, activity, and intended use.
• The RPO shall initiate all license amendments to add radioactive materials.
Applying or amending a specific license may take several months.
The RPO or designee must survey, perform a leak test on each device, and complete a
Radioactive Shipment / Receiving Form (Attachment 8) or equivalent if dictated by a
local regulation, on the same shift or day the shipment arrives at the licensee’s site.
Devices not going immediately into service shall be secured to prevent unauthorized
removal. Devices in temporary storage shall have a “CAUTION RADIOACTIVE
MATERIALS” sign posted and be stored in a designated storage area, keeping in mind
personnel exposure needs to be As Low As Reasonably Achievable (ALARA).
1. At intervals not to exceed six months, each device containing radioactive material
shall be visually inspected and inventoried.
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1. Sealed source wipe tests shall be performed per the device registry (Attachment 3
– Radiation Source List for details) for each device containing radioactive material.
• The registry can be obtained from the manufacturer, to determine the interval
for performing sealed source wipe tests.
2. The wipe of a sealed source shall be performed using a wipe test kit or method
[see Attachment 10 – “Sealed Source Wipe Sampling Standard” HSE-SAF-STD-
00-0015] approved by the licensing agency or authority having jurisdiction.
3. The wipe sample shall be taken from the nearest accessible point to the sealed
source where contamination might accumulate.
1. If entry is required into a vessel or piece of equipment that has a device containing
a radioactive source, the radioactive source must be considered a source of energy
and the device shutter must be placed in the closed position.
3. The following two methods shall be utilized to confirm that the device shutter is
closed properly:
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• A portable survey meter detector shall be placed in the beam path to confirm
the radiation reading has decreased to background levels and levels are below
acceptable limits.
2. If the licensee does not have procedures for removing devices containing
radioactive material, the device shall NOT be removed.
3. A licensed third party contractor shall be contacted to perform the removal process
using authorized procedures.
1. All devices containing licensed radioactive material shall be stored in a manner that
limits radiation exposure to members of the general public and prevents
unauthorized removal of the devices from the storage location.
3. This area and all sources kept within shall be included in the documented semi-
annual inspection.
2. The shipment must be packaged, labelled, and have all paperwork completed in
accordance with all applicable local regulations.
3. The RPO must survey the shipment and complete the Radioactive Shipment /
Receiving Form (Attachment 8) or equivalent if dictated by a local regulation.
4. The shipping form should accompany other required shipping papers such as the
Bill-of-Lading (BOL) containing the proper regulatory shipping description.
5. The licensee must receive a letter of transfer from the company receiving and
possessing the radioactive material.
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1. The maximum exposure limit for a Radiation Worker is 50 000 µSv/yr [50 mSv/yr].
• If a radiation worker declares her pregnancy to the RPO, the exposure limit is
5000 µSv for the term of the pregnancy.
The exposure limit for members of the general public is 1000 µSv/yr [1
mSv/yr]. Each licensee is required to document that members of the general
public shall not exceed this exposure limit. Refer to “How to Determine
Annual Radiation Exposure” (see Appendix I).
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G1. Description
Various types of analytical instruments or machines use X-ray radiation for material
testing. Two common types of analytical instruments are X-ray fluorescence (XRF)
machines and X-ray diffraction (XRD) machines. The difference and their respective
levels of threat are described below:
G2. Registration
1. Registration of X-ray producing machines may not be required by all agencies. Any
registration requirements must be verified by the RPO with the local regulatory
agency having jurisdiction.
2. The RPO is responsible for initiating the registration process in accordance with the
following requirements as appropriate:
• Amend the registration to include any new X-ray machine within 30 days of
initial operation.
G3. Procurement
The following steps are required to purchase / ease any new X-ray producing
machines:
2. The RPO shall be provided with or determine / document as part of the purchasing
/ leasing process, all information relating to the proposed procurement, including
the following:
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• The manufacturer,
• Equipment Model,
G4. Receiving
The RPO shall document receipt of the radiation-producing machine immediately upon
delivery and perform an inspection using the X-ray Machine Inspection Form
(Attachment 6) or equivalent if dictated by a local regulation.
G5. Storage
X-ray machines which must be stored until placed into service shall be stored in a
designated storage area secured to prevent unauthorized removal.
G6. Installation
1. The RPO shall be notified by the facility representative when the manufacturer is
scheduled to install (start-up) the machine.
3. The RPO shall survey and inventory the machine as soon as it is available for
operation by personnel using the X-ray Inspection Form (see Attachment 6).
2. All maintenance/repair work shall be documented and reviewed with the RPO.
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1. A readily visible warning light labelled with the words "X-RAY ON" must be
illuminated only when the tube is energized.
• The light must be fail-safe (i.e., failure of the light bulb must shut down the X-
ray machine).
2. Each X-ray machine must be labelled with the following signs bearing the radiation
symbol and the words:
3. The entrance to each X-ray room or area must be conspicuously posted with a sign
bearing the radiation symbol and the words "CAUTION - X-RAY EQUIPMENT."
4. Each registrant shall post in a place for all workers to read a “Notice to Employees.”
G9. Inspections
1. At intervals not to exceed 12 months, all X-ray machines shall be visually inspected
and inventoried by the RPO or designee.
• “Caution X-Ray Equipment” signs are posted at all the entrances; and
3. All inspections shall be performed using the X-ray Machine Inspection Form (see
Attachment 6) or equivalent if dictated by a local regulation.
Written authorization must be obtained from the RPO prior to the shipment offsite or
relocation onsite of an X-ray machine.
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The following requirements apply only to the X-ray diffraction machines, since these
machines utilize an open beam configuration:
• All unused ports must have a shutter that cannot be opened unless a collimator
or a coupling is connected to the port.
• The operator shall measure X-ray radiation levels and ensure the levels are at
background in the beam path prior to placement of any body part in the path or
vicinity of the beam.
G12. Training
2. The X-ray machine safety class shall at a minimum include the following:
• Radiation warning and safety devices incorporated into the radiation machine;
All records documenting compliance with this procedure must be maintained in the
RPO’s office or a location as designated by the RPP.
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H1. Description
Q-Chem does not own radiography sources and hence does not have a license for
these materials. However, the RPO must maintain copies of the licenses of all
radiography companies who are approved to work at Q-Chem. sites. Applicable
radiography regulations, including federal, state and local regulations, are to be listed
in the contractual agreement with the company providing radiography services.
Exposure monitoring around a radiography job requires knowledge of the source size,
type, location, and collimator. Monitoring shall be performed with a Radiation survey
meter as described in the main text of this document.
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In determining the annual radiation exposure for radiation workers, the three steps identified
below must be followed to calculate the total number of times a device would have to be
operated in a year to exceed the allowable limit (e.g., 500 mR/yr).
If it is unlikely the actual shutter operation occurrences shall not exceed the calculated
shutter operation occurrences, the licensee is exempt from personnel radiation monitoring.
If the actual shutter operation occurrences do exceed the calculated shutter operate
occurrences, the licensee is not exempt from personnel radiation monitoring and must
monitor each radiation worker that operates the devices.
Determining annual exposure to the general public is based on the commonly understood
practice that a member of the general public would not get closer than one foot when
walking or working by a radioactive device. The one-foot survey result is used to confirm
that general public annual radiation exposures are below 100 mR/yr. If this assumption is
not correct, then other measurements shall be collected before proceeding with the
calculation.
In determining the annual radiation exposure for members of the general public, follow the
two steps below to calculate the total number of hours a member of the general public could
be present and not exceed the allowable limit (e.g., 100 mR/yr).
The calculated occupancy hours must be less than the actual occupancy time for a member
of the general public. If the actual occupancy time is greater than calculated occupancy
time, then additional restrictions (barricades or signs) must be installed to reduce the actual
occupancy time for members of the general public.
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J1. Description
In refineries and petrochemical plants, sludge build-up containing decay products from
the Uranium-238 decay chain may be present. The boiling point of Radon falls
between ethane and propylene and Radon shall be concentrated during distillation in
these streams. As the radon gas travels through various systems, its decay products
(lead and polonium) plate out on equipment. While the equipment is in service, the
radiation risk from these deposits is insignificant; however, precautions must be taken
to avoid skin contact, inhalation, and/or ingestion of the decay products when
equipment is opened for maintenance.
Certain states regulate NORM as part of their radiological control programs. These
states also grant facilities a general license for NORM when it is discovered at a site.
Some states do not have any regulatory guidance regarding NORM.
• Embryo / foetus in a declared pregnant woman: 5000 µSv for the pregnancy.
2. Once this equipment is opened, an internal survey shall be performed to verify that
the surface contamination limits are not exceeded.
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J5. Instrumentation
1. A Ludlum Model 3 with a Model 44-2 gamma scintillator readout in micro Roentgen
per hour (µR/hr), or equivalent, is required to detect the low levels of gamma
radiation that may be emitted from a piece of equipment.
2. A Ludlum Model 3 (or Bicron Surveyor 50) with a Model 44-9 pancake detector
readout in counts per minute (cpm) or equivalent is required to detect alpha, beta
and gamma radiation that may be emitted from a piece of equipment.
J6. Surveys
1. When performing external surveys using the gamma scintillator, the following shall
be considered:
• The most sensitive part of the detector is the flat front end.
• The instrument also picks up radiation from all sources in the area (level
gauges, radiography cameras, etc.).
Users of the gamma scintillators must know where other radiation sources
are located.
2. These readings are best used to help identify suspect areas of concern.
• The gamma scintillation detector shall pick up the low level gamma rays that
are penetrating the equipment wall.
When the gamma radiation is present on the outside of the equipment wall,
there is good chance that the alpha and beta radiations are also present on
the inside of this equipment.
3. When performing internal surveys using the pancake detector, the following shall
be considered:
• When using the open window, the detector is detecting alpha, beta, AND
gamma radiations.
• By turning the detector over and using the back side, the detector shall only
detect gamma radiation.
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• The survey meter reads a total contamination in counts per minute (cpm). This
reading must be converted to disintegrations per minute (dpm). Refer to the
instrument manufacturer’s operations manual for performing this conversion.
• This instrument shall also pick up any radiography being performed in the area.
NORM regulations may vary from state to state. Each facility shall verify with the
agency that regulates radiation any applicable NORM limits. If there are no NORM
limits, use the following:
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J10. Decontamination
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1. 01-03-2008 Changes to include Corporate Policy requirements; including the Section 4.13
following:
• Naturally Occurring Radioactive Materials (NORM) assessment
& measurement in process sludges of Ethylene Unit
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