Orgo Lab 6 Report

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You can never shift equilibrium toward product so you cant get 100% yield

One potential source of error for purity determination could arise from impurities affecting the IR
spectrum, where impurities not adequately accounted for or identified might manifest as
additional peaks, while errors in sample preparation, handling during analysis, or variations in
instrument calibration could also influence the accuracy of purity assessment.

Conclusion: Did you achieve your purpose? Regarding the achievement of the purpose, the
purpose was to synthesize an ester through esterification. To determine if this goal was
accomplished, we must consider the formation of the desired ester product, which can be
assessed based on the appearance and mass of the product obtained. By comparing the initial
amounts of acetic acid and 1-butanol with the final mass of the product, we can evaluate the
efficiency of the reaction and whether the theoretical yield was achieved.

How did azeotropic distillation assist in the significant formation of product. Azeotropic
distillation played a crucial role in facilitating the significant formation of the product. Azeotropic
distillation is a method used to remove water from reaction mixtures by forming an azeotrope, a
mixture of two or more liquids that boils at a constant temperature and composition. In this
experiment, water, butanol, and ester formed an azeotrope, allowing the removal of water from
the reaction mixture and shifting the equilibrium of the esterification reaction towards the
formation of the desired ester product. This process ensured the completion of the reaction and
increased the yield of the ester product. Therefore, azeotropic distillation assisted in achieving a
higher yield of the desired ester product.

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