CARRYOVER REPORT

AC Q U I SI TI O N I N F O R M ATI O N

System Name: PATROL with PDA Acquired By: Jennb

Project Name: SQT_PATrol_PDA_CM_rev D Column serial Number: 11581505610K
Sample Set Method: 090 Carryover Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
Processing Method Carryover PM, Carryover Clean Sample Kit 1 Lot Number: N070015
Report Method Name: Carryover Report Build Version: Empower 2 Software Build 2154 SPs
User Name: System Installed:
Sample Set Feature Release 5
Id: 11954 DB ID:
Result 847558692
Set Id 11966
Sample Set Name: Carryover Sample Set Start Date: 11/4/2010 9:31:58 PM

In the Carryover qualification, two pre-blank injections are performed to determine if the chromatograph is
clean enough to measure carryover. Those injections are followed by three Caffeine calibration injections at a
concentration of (0.2 ppm) which is 0.005 percent of the Challenge injection concentration (4000 ppm).

The Challenge injection is made and is followed by three post-blank injections.

Carryover is reported as a percent of the Challenge concentration. If the % Carryover of first post-blank injection
is less than 0.010% the qualification passes.

Carryover Peak Results

Carryover Carryover
SampleName Peak Type % Carryover
Specification Pass Fail
1 PostBlank1 < or = 0.010% Found 0.009 PASS

Printed 7:59:22 AM US/Eastern 11/17/2010 Page: 1 of 3

 CARRYOVER REPORT

AC Q U I SI TI O N I N F O R M ATI O N

System Name: PATROL with PDA Acquired By: Jennb

Project Name: SQT_PATrol_PDA_CM_rev D Column serial Number: 11581505610K
Sample Set Method: 090 Carryover Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
Processing Method Carryover PM, Carryover Clean Sample Kit 1 Lot Number: N070015
Report Method Name: Carryover Report Build Version: Empower 2 Software Build 2154 SPs
User Name: System Installed:
Sample Set Feature Release 5
Id: 11954 DB ID:
Result 847558692
Set Id 11966
Sample Set Name: Carryover Sample Set Start Date: 11/4/2010 9:31:58 PM
Caffeine

Caffeine
0.004 0.004 0.004

Caffeine
AU

AU

AU
0.002 0.002 0.002

0.000 0.000 0.000

0.00 1.00 2.00 0.00 1.00 2.00 0.00 1.00 2.00

Minutes Minutes Minutes

PreBlank; Vial: 12; Inj: 1 PreBlank; Vial: 12; Inj: 2 Standard; Vial: 8; Inj: 1

0.004 0.004 0.004

Caffeine
Caffeine
AU

AU

AU

0.002 0.002 0.002

0.000 0.000 0.000

0.00 1.00 2.00 0.00 1.00 2.00 0.00 5.00 10.00 15.00
Minutes Minutes Minutes

Standard; Vial: 8; Inj: 2 Standard; Vial: 8; Inj: 3 Challenge; Vial: 9; Inj: 1

Caffeine

Caffeine

Caffeine

0.004 0.004 0.004

AU

AU

AU

0.002 0.002 0.002

0.000 0.000 0.000

0.00 1.00 2.00 0.00 1.00 2.00 0.00 1.00 2.00

Minutes Minutes Minutes

PostBlank1; Vial: 12; Inj: 1 PostBlank2; Vial: 12; Inj: 1 PostBlank3; Vial: 12; Inj: 1

Printed 7:59:22 AM US/Eastern 11/17/2010 Page: 2 of 3

 CARRYOVER REPORT

AC Q U I SI TI O N I N F O R M ATI O N

System Name: PATROL with PDA Acquired By: Jennb

Project Name: SQT_PATrol_PDA_CM_rev D Column serial Number: 11581505610K
Sample Set Method: 090 Carryover Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
Processing Method Carryover PM, Carryover Clean Sample Kit 1 Lot Number: N070015
Report Method Name: Carryover Report Build Version: Empower 2 Software Build 2154 SPs
User Name: System Installed:
Sample Set Feature Release 5
Id: 11954 DB ID:
Result 847558692
Set Id 11966
Sample Set Name: Carryover Sample Set Start Date: 11/4/2010 9:31:58 PM

Peak Results
Sample Type: Unknown
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 PreBlank Unknow n 12 1 Caffeine 1.093 12212 5248 Found 0.0084
2 PreBlank Unknow n 12 2 Caffeine 1.099 11456 4924 Found 0.0079

Peak Results
Sample Type: Standard
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 Standard Standard 8 1 Caffeine 1.095 7356 3123 Found 0.0050
2 Standard Standard 8 2 Caffeine 1.095 7135 3032 Found 0.0050
3 Standard Standard 8 3 Caffeine 1.097 7278 3079 Found 0.0050

Peak Results
Sample Type: Unknown
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 PostBlank1 Unknow n 12 1 Caffeine 1.097 12752 5371 Found 0.0088
2 PostBlank2 Unknow n 12 1 Caffeine 1.093 11818 5040 Found 0.0081
3 PostBlank3 Unknow n 12 1 Caffeine 1.092 11832 4970 Found 0.0082

Printed 7:59:22 AM US/Eastern 11/17/2010 Page: 3 of 3