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358
 ANEXO A

RESULTADOS ANALÍTICOS

PARÂMETROS FÍSICO-QUÍMICOS

359
ANEXOS

360
 ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C1

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm mL min L/h
3-8-05 22:00 24,4 95 7,43 0
4-8-05 22:00 25,3 100 7,42 0 650 80,0 487,5
5-8-05 22:00 25,2 90 7,68 -1 210 30,0 420,0
7-8-05 22:00 25,3 94 7,61 -1 123 20,0 369,0
9-8-05 22:00 24,7 88 7,55 -1 210 30,0 420,0
11-8-05 22:00 24,7 90 7,61 0 220 38,0 347,4
13-8-05 22:00 25,4 84 7,60 20 285 39,0 438,5
15-8-05 15:00 25,8 84 7,28 55 620 75,0 496,0
17-8-05 11:00 25,2 91 7,60 58 125 40,0 187,5
19-8-05 19:00 25,7 85 7,55 31 180 26,0 415,4
21-8-05 15:00 25,1 92 7,64 29 215 35,0 368,6
23-8-05 10:00 24,9 89 7,53 64 270 45,0 360,0
25-8-05 15:00 25,6 105 6,99 3 255 36,0 425,0
29-8-05 15:00 25,0 89 7,75 19 235 31,8 444,1
31-8-05 10:00 24,0 80 7,65 48 275 37,3 442,4
2-9-05 10:00 23,9 93 7,69 47 222 30,0 444,0
5-9-05 15:00 24,0 94 7,60 63 305 41,7 439,1
7-9-05 9:00 22,9 93 7,56 66 340 40,0 510,0
9-9-05 0:00 23,4 92 7,80 83 207 30,0 414,0
12-9-05 9:00 22,2 96 7,81 112 250 35,0 428,6
16-9-05 9:00 23,8 105 7,80 122 230 32,0 431,3
19-9-05 9:00 22,5 112 7,47 138 310 30,0 620,0
26-9-05 9:00 21,8 100 7,80 171 215 30,0 430,0
30-9-05 9:00 23,3 108 7,51 2 395 148,0 160,1
3-10-05 9:00 22,1 96 7,74 11 285 35,0 488,6
11-10-05 10:00 22,4 94 7,77 51 240 30,0 480,0
17-10-05 9:30 20,6 106 7,56 24 215 30,0 430,0
28-10-05 12:00 20,3 114 7,64 11 190 30,0 380,0
4-11-05 13:00 18,5 123 7,47 43 215 30,0 430,0
18-11-05 10:00 18,0 117 7,55 71 280 40,0 420,0

361
ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C1

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm mL min L/h
25-11-05 10:00 17,7 113 7,16 62 215 30,0 430,0
29-11-05 10:00 17,4 108 7,24 69 205 30,0 410,0
2-12-05 10:00 17,9 109 7,33 53 190 30,0 380,0
6-12-05 10:00 18,1 108 7,29 99 210 30,0 420,0
9-12-05 10:00 18,3 108 7,39 114 190 30,0 380,0
13-12-05 15:00 18,9 101 7,47 97 180 30,0 360,0
16-12-05 12:00 18,0 100 7,41 128 160 30,0 320,0
20-12-05 10:00 17,3 101 7,39 102 195 30,0 390,0
27-12-05 10:00 16,3 125 7,45 93 180 45,0 240,0
3-1-06 10:00 17,4 94 7,34 134 210 30,0 420,0
17-1-06 10:00 16,2 95 7,14 198 210 30,0 420,0
24-1-06 10:00 16,0 93 7,38 53 215 30,0 430,0
27-1-06 10:00 16,8 92 7,10 133 220 30,0 440,0
2-2-06 15:00 18,1 97 7,24 207 240 30,0 480,0
7-2-06 15:00 18,0 107 7,18 223 240 30 480,0
10-2-06 10:00 17,6 90 7,17 236 235 30 470,0
17-2-06 15:00 18,5 99 7,28 272 235 30 470,0
24-2-06 15:00 17,1 107 7,29 247 230 30 460,0
3-3-06 9:00 17,4 102 7,32 334 230 30 460,0
10-3-06 10:00 17,5 100 7,26 445 190 30 380,0
17-3-06 16:00 19,5 99 7,19 789 260 30 520,0
24-3-06 16:00 20,0 91 7,35 733 245 30 490,0
30-3-06 9:30 0 175 30 350,0
31-3-06 16:00 20,9 100 7,23 13 320 30 640,0
3-4-06 15:00 320 30 640,0
4-4-06 9:00 365 30 730,0
4-4-06 11:00 320 30 640,0
5-4-06 10:00 20,2 97 7,25 30 325 30 650,0
6-4-06 9:00 18 325 30 650,0
7-4-06 9:00 18 315 30 630,0

362
 ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C1

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm mL min L/h
10-4-06 9:00 17 220 30 440,0
11-4-06 14:00 19,5 105 7,49 18 225 30 450,0
12-4-06 9:00 19 220 30 440,0
18-4-06 9:00 40 210 30 420,0
20-4-06 9:00 18,6 96 7,40 45 210 30 420,0
21-4-06 9:00 58 210 30 420,0
21-4-06 11:00 258 205 30 410,0
21-4-06 9:00 114 210 30 420,0
26-4-06 10:00 1 395 60 395,0
26-4-06 17:00 5 210 30 420,0
27-4-06 9:00 0 215 30 430,0
28-4-06 9:00 193 205 30 410,0
1-5-06 9:00 155 430 60 430,0
3-5-06 9:00 134 420 60 420,0
4-5-06 9:00 115,0 460 60,0 460,0
5-5-06 9:00 19,3 111 7,34 114 190 30 380,0
8-5-06 9:00 340 395 60 395,0
9-5-06 9:00 360 400 60 400,0
10-5-06 9:00 381 415 60 415,0
11-5-06 9:00 370 425 60 425,0
12-5-06 9:00 363 425 60 425,0
15-5-06 9:00 99 75 60 75,0
16-5-06 9:00 277 165 30 330,0
17-5-06 9:00 379 170 30 340,0
19-5-06 9:00 442 225 30 450,0

363
ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C2

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm ml min L/h
3-8-05 22:00 24,3 92 7,37 0
4-8-05 22:00 25,0 96 7,58 520 80,0 390,0
5-8-05 22:00 25,6 97 7,81 190 30,0 380,0
7-8-05 22:00 25,3 94 7,66 -1 186 30,0 372,0
9-8-05 22:00 24,6 93 7,66 -1 245 40,0 367,5
11-8-05 22:00 24,6 93 7,65 240 40,0 360,0
13-8-05 22:00 25,4 87 7,86 0 170 28,0 364,3
15-8-05 15:00 25,8 88 7,47 26 470 75,0 376,0
17-8-05 11:00 25,2 94 7,69 20 251 40,0 376,5
19-8-05 19:00 25,5 87 7,80 9 190 30,0 380,0
21-8-05 15:00 25,0 87 7,70 8 225 35,0 385,7
23-8-05 10:00 24,7 81 7,80 22 280 45,0 373,3
25-8-05 15:00 25,5 87 7,61 1 194 36,0 323,3
29-8-05 15:00 25,2 84 7,79 8 200 31,8 378,0
31-8-05 10:00 24,0 77 7,65 27 245 37,3 394,1
2-9-05 10:00 23,7 81 7,77 22 170 30,0 340,0
5-9-05 15:00 24,1 88 7,90 39 260 41,7 374,3
7-9-05 9:00 23,2 85 7,50 55 245 40,0 367,5
9-9-05 0:00 23,4 88 7,81 -1 236 30,0 472,0
12-9-05 9:00 22,4 90 7,81 9 215 35,0 368,6
16-9-05 9:00 23,7 97 7,74 19 207 32,0 388,1
19-9-05 9:00 22,6 99 7,51 33 205 30,0 410,0
26-9-05 9:00 21,9 89 7,69 56 185 30,0 370,0
30-9-05 9:00 23,2 94 7,47 -2 315 148,0 127,7
3-10-05 9:00 22,2 92 7,64 -2 210 35,0 360,0
11-10-05 10:00 22,4 90 7,64 11 195 30,0 390,0
17-10-05 9:30 20,7 99 7,42 3 180 30,0 360,0
28-10-05 12:00 20,8 107 7,40 -1 185 30,0 370,0
4-11-05 13:00 18,6 115 7,37 15 185 30,0 370,0

364
 ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C2

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm ml min L/h
18-11-05 10:00 17,9 103 7,22 40 260 40,0 390,0
25-11-05 10:00 17,8 105 7,30 26 150 30,0 300,0
29-11-05 10:00 17,5 108 7,13 38 260 30,0 520,0
2-12-05 10:00 17,9 107 7,28 27 170 30,0 340,0
6-12-05 10:00 18,0 106 7,24 45 180 30,0 360,0
9-12-05 10:00 18,6 103 7,43 54 160 30,0 320,0
13-12-05 15:00 18,7 95 7,30 51 150 30,0 300,0
16-12-05 12:00 18,0 99 7,27 60 170 30,0 340,0
20-12-05 10:00 17,2 99 7,28 39 154 30,0 308,0
27-12-05 10:00 16,2 113 7,24 30 165 45,0 220,0
3-1-06 10:00 17,7 94 7,25 50 175 30,0 350,0
17-1-06 10:00 16,3 95 7,14 107 245 30,0 490,0
24-1-06 10:00 16,2 93 7,42 32 220 30,0 440,0
27-1-06 10:00 17,0 91 7,11 106 255 30,0 510,0
2-2-06 15:00 18,3 91 7,20 135 255 30,0 510,0
7-2-06 15:00 18,2 91 7,05 136 260 30 520,0
10-2-06 10:00 17,6 88 7,02 157 255 30 510,0
17-2-06 15:00 18,8 99 7,14 209 255 30 510,0
24-2-06 15:00 17,0 103 7,24 171 265 30 530,0
3-3-06 9:00 17,5 98 7,20 289 255 30 510,0
10-3-06 10:00 17,6 96 7,10 463 260 30 520,0
17-3-06 16:00 19,5 98 7,23 462 210 30 420,0
24-3-06 16:00 19,5 105 6,91 (1)
27-3-06 9:00
29-3-06 9:30 0 270 30 540,0
30-3-06 9:30 0 290 30 580,0
30-3-06 14:00 0 295 30 590,0
31-3-06 16:00 20,7 92 7,26 162 300 30 600,0
3-4-06 15:00 245 30 490,0
4-4-06 9:00 280 30 560,0

365
ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C2

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm ml min L/h
4-4-06 11:00 285 30 570,0
5-4-06 10:00 20,2 94 7,14 298 235 30 470,0
6-4-06 9:00 333 285 30 570,0
7-4-06 9:00 304 215 30 430,0
10-4-06 9:00 379 205 30 410,0
11-4-06 14:00 19,8 101 7,56 416 200 30 400,0
12-4-06 9:00 455 205 30 410,0
18-4-06 9:00 656 205 30 410,0
19-4-06 9:00 682 215
20-4-06 9:00 18,8 97 7,49 704 210 30 420,0
21-4-06 9:00 738 200 30 400,0
21-4-06 11:00 739 208 30 416,0
21-4-06 9:00 887 185 30 370,0
26-4-06 10:00 -7 145 60 145,0
26-4-06 17:00 -35 65 30 130,0
27-4-06 9:00 -1 45 30 90,0
28-4-06 9:00 216 30 30 60,0
1-5-06 9:00 71 20 60 20,0
3-5-06 9:00 55 15 60 15,0
4-5-06 9:00 40
5-5-06 9:00 19,3 98 7,67 29 5 30 10,0
8-5-06 9:00 11 8 120 4,0
9-5-06 9:00 5 5 120 2,5
11-5-06 9:00 -1 2 120 1,0
15-5-06 9:00 103 95 60 95,0
16-5-06 9:00 299 195 30 390,0
19-5-06 9:00 389 215 30 430,0
22-5-06 9:00 526 210
25-5-06 9:00 651 225 30 450,0

366
 ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C2

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm ml min L/h
26-5-06 9:00 638 245 30 490,0
29-5-06 9:00 426 110 30 220,0
30-5-06 9:00 558 180 30 360,0
31-5-06 9:00 606 215 30 430,0
1-6-06 9:00 596 225 30 450,0
2-6-06 9:00 22,7 105 6,70 536 225 30 450,0
5-6-06 9:00 613 195 30 390,0
6-6-06 9:00 624 225 30 450,0
7-6-06 9:00 604 230 30 460,0
8-6-06 9:00 573 235 30 470,0
9-6-06 9:00 521 245 30 490,0
12-6-06 9:00 536 205 30 410,0
13-6-06 9:00 556 205 30 410,0
14-6-06 9:00 589 210 30 420,0
19-6-06 9:00 435 220 30 440,0
20-6-06 9:00 410 215 30 430,0
21-6-06 9:00 437 180 30 360,0
22-6-06 9:00 494 185 30 370,0
23-6-06 9:00 517 210 30 420,0
26-6-06 9:00 532 220 30 440,0
27-6-06 9:00 516 220 30 440,0
28-6-06 9:00 486 225 30 450,0
29-6-06 9:00 458 220 30 440,0
30-6-06 9:00 470 200 30 400,0
3-7-06 9:00 217 65 30 130,0
4-7-06 9:00 439 150 30 300,0
5-7-06 9:00 509 195 30 390,0
6-7-06 9:00 519 210 30 420,0
7-7-06 9:00 504 230 30 460,0
10-7-06 9:00 518 215 30 430,0

367
ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C2

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC µS mm ml min L/h
28-7-06 10:00 24,9 89 6,73 520 220 30 440,0
14-7-06 9:00 26,3 111 7,18 485 230 30 460,0
18-7-06 9:00 405 225 30 450,0
4-8-06 10:00 25,8 119 6,59 610 295 40 442,5

(1) limpeza o filtro da coluna C2

368
 ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C3

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC S mm ml min L/h
3-8-05 22:00 24,5 95 7,60 0
4-8-05 22:00 25,1 97 7,60 24 325 80,0 243,8
5-8-05 22:00 24,6 98 7,70 20 135 30,0 270,0
7-8-05 22:00 25,1 95 7,66 -80 229 38,0 361,6
9-8-05 22:00 24,7 95 7,61 -244 240 46,0 313,0
11-8-05 22:00 24,5 95 8,01 150 60,0 150,0
13-8-05 22:00 25,2 92 7,96 -339 180 45,5 237,4
15-8-05 15:00 25,7 90 7,65 -330 305 75,0 244,0
17-8-05 11:00 25,0 102 7,53 -324 170 40,0 255,0
19-8-05 19:00 25,4 92 7,52 -350 180 38,0 284,2
21-8-05 15:00 25,1 91 7,48 -441 190 35,0 325,7
23-8-05 10:00 24,8 87 7,64 -384 175 45,0 233,3
25-8-05 15:00 25,4 90 7,43 -248 220 36,0 366,7
29-8-05 15:00 25,0 86 7,64 -272 165 31,8 311,8
31-8-05 10:00 24,1 84 7,51 -342 180 37,3 289,5
2-9-05 10:00 23,7 84 7,55 -346 150 30,0 300,0
5-9-05 15:00 24,2 89 7,60 -357 185 41,7 266,3
7-9-05 9:00 23,1 87 7,48 -444 190 40,0 285,0
9-9-05 0:00 23,4 89 7,55 -335 146 30,0 292,0
12-9-05 9:00 22,2 87 7,68 -306 165 35,0 282,9
16-9-05 9:00 23,6 96 7,60 -330 170 32,0 318,8
19-9-05 9:00 22,7 97 7,64 -379 130 30,0 260,0
26-9-05 9:00 21,9 91 7,62 -268 155 30,0 310,0
30-9-05 9:00 23,1 92 7,35 -245 445 148,0 180,4
3-10-05 9:00 22,2 89 7,77 -364 155 35,0 265,7
11-10-05 10:00 22,5 86 7,59 -225 200 30,0 400,0
17-10-05 9:30 20,7 93 7,33 -84 215 30,0 430,0
28-10-05 12:00 20,3 99 7,39 80 180 30,0 360,0
4-11-05 13:00 18,6 109 7,33 158 170 30,0 340,0

369
ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C3

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC S mm ml min L/h
18-11-05 10:00 17,9 103 7,09 88 275 40,0 412,5
25-11-05 10:00 17,9 107 7,21 -51 230 30,0 460,0
29-11-05 10:00 17,8 103 7,16 -99 225 30,0 450,0
2-12-05 10:00 17,9 105 7,15 -123 220 30,0 440,0
6-12-05 10:00 17,2 100 7,23 -123 210 30,0 420,0
9-12-05 10:00 18,5 100 7,25 -36 220 30,0 440,0
13-12-05 15:00 18,7 95 7,11 -46 215 30,0 430,0
16-12-05 12:00 18,2 96 7,12 -43 225 30,0 450,0
20-12-05 10:00 17,2 95 7,07 -12 240 30,0 480,0
27-12-05 10:00 16,3 109 6,99 -125 320 45,0 426,7
3-1-06 10:00 17,7 94 7,21 -166 155 30,0 310,0
17-1-06 10:00 16,4 92 7,13 66 215 30,0 430,0
24-1-06 10:00 16,2 89 7,26 196 220 30,0 440,0
27-1-06 10:00 17,1 91 7,08 208 195 30,0 390,0
2-2-06 15:00 18,5 94 7,13 103 170 40,0 255,0
7-2-06 15:00 18,4 94 7,11 22 170 50 204,0
10-2-06 10:00 17,6 90 7,07 143 165 30 330,0
17-2-06 15:00 19,0 93 7,15 224 155 35 265,7
24-2-06 15:00 17,8 99 7,25 245 180 60 180,0
3-3-06 9:00 17,6 104 7,28 -287 165 240 41,3
10-3-06 10:00 18,2 102 7,31 417 155 540 17,2
17-3-06 16:00 19,0 121 6,94 -152 175 150 70,0
24-3-06 16:00 20,2 102 7,12 68 205 60 205,0
29-3-06 9:30 1 145 30 290,0
30-3-06 14:00 0 150 30 300,0
31-3-06 16:00 20,9 91 7,15 226 160 30 320,0
3-4-06 15:00 130 30 260,0
4-4-06 9:00 135 30 270,0
5-4-06 10:00 20,4 92 7,08 293 170 40 255,0
6-4-06 9:00 47 135 30 270,0

370
 ANEXOS

PARÂMETROS FÍSICO-QUÍMICOS – COLUNA C3

Parâmetros físico-químicos Caudais

Data / Hora Temp Condutiv pH Nível Saída
ºC S mm ml min L/h
7-4-06 9:00 67 115 30 230,0
10-4-06 9:00 294 135 30 270,0
11-4-06 14:00 19,8 91 7,52 236 150 40 225,0
12-4-06 9:00 253 105 30 210,0
18-4-06 9:00 206 85 30 170,0
19-4-06 9:00 208 85
20-4-06 9:00 18,8 95 7,40 209 85 30 170,0
21-4-06 9:00 209 85 30 170,0
21-4-06 9:00 288 80 30 160,0
26-4-06 10:00 -5 95 60 95,0
26-4-06 17:00 -25 45 30 90,0
27-4-06 9:00 1 40 30 80,0
28-4-06 9:00 -83 25 30 50,0
1-5-06 9:00 -307 40 60 40,0
3-5-06 9:00 -334 30 60 30,0
4-5-06 9:00 -379,0 30
5-5-06 9:00 19,3 96 7,39 -409 14 30 28,0
8-5-06 9:00 -486 41 120 20,5
9-5-06 9:00 -507 39 120 19,5
11-5-06 9:00 -548 37 120 18,5

371
ANEXOS

372
 ANEXOS

ANEXO B

RESULTADOS ANALÍTICOS

METAIS PESADOS

373
 ANEXO C

MICROSCOPIA ELECTRÓNICA

IMAGENS DE VARRIMENTO

391
ANEXOS

392
 ANEXOS

393
ANEXOS

394