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Composites Part B 197 (2020) 108117

Contents lists available at ScienceDirect

Composites Part B
journal homepage: www.elsevier.com/locate/compositesb

Quasi-static crushing behavior of novel re-entrant circular


auxetic honeycombs
Chang Qi a, Feng Jiang a, Alex Remennikov b, Lian-Zheng Pei a, Jun Liu c, Jun-Shan Wang c,
Xiang-Wei Liao d, Shu Yang a, *
a
State Key Laboratory of Structural Analysis for Industrial Equipment, School of Automotive Engineering, Dalian University of Technology, Dalian, 116024, China
b
Center for Infrastructure Protection and Mining Safety, University of Wollongong, Wollongong, NSW, 2522, Australia
c
Ansteel Group Beijing Research Institute Co., Ltd., Beijing, 102211, China
d
Ansteel Group Iron and Steel Research Institute, Anshan, 114021, China

A R T I C L E I N F O A B S T R A C T

Keywords: Honeycombs with re-entrant (RE) unit cells were found to have negative Poisson’s ratios (NPRs) and enhanced
Auxetic energy absorption capabilities than regular hexagon honeycombs. For further improved energy absorption ca­
Re-entrant circular honeycomb pacity, a novel re-entrant circular (REC) honeycomb configuration is proposed in this work by replacing the
Negative Poisson’s ratio
sloped cell wall of the regular re-entrant honeycomb with double circular arc cell walls, which can dissipate extra
Crushing response
Energy absorption
energy due to more formed plastic angles during the crushing process. The in-plane quasi-static crushing
response of the REC honeycomb with large deformation was investigated theoretically and numerically. The
numerical modeling methods in LS-DYNA software were validated by using the quasi-static crush test data of 3D-
printed REC honeycomb specimens. Experiment and numerical simulations both revealed that quasi-static load
can result in an “X” mode deformation of the REC honeycomb. Based on the simulated deformation profiles of the
representative unit, theoretical models were derived to predict the REC honeycomb’s crushing strength, i.e.
plateau stress. Good agreements were found between the theoretical and the numerical results within a relative
error about 9%. Parametric analyses further showed that the unit cell configuration has a great effect on the
crushing strength of the REC honeycomb. The REC honeycomb presents a varied Poisson’s ratio with the global
strain of the honeycomb; smaller radius to height ratio and length to height ratio were found to yield more
pronounced NPR effect. Moreover, compared with the regular RE honeycomb, the specific energy absorption of
the REC honeycomb is much higher due to the introduction of the double circular arc cell walls.

focusing on their superior properties owing to the NPR effect, including


the increased shear modulus [8], increased indentation resistance [9],
1. Introduction
enhanced fracture toughness [6], better energy absorption [10], vari­
able stiffness [11] and lower fatigue crack propagation [12] compared
Auxetics refer to the materials or structures showing counterintuitive
with conventional materials. With a better understanding of the mech­
deformations compared to conventional ones, i.e. the auxetics show
anisms of their mechanical advantages, the auxetics are expected to be
transverse expansion or contraction under uniaxial tension or
used in various engineering applications, such as automotive crash
compression load [1]. As such, auxetics possess negative Poisson’s ratios
safety, product packaging and structural protection [13–15].
(NPRs) in a general sense. Auxetic materials were first found in nature,
Honeycombs have been used for decades as engineering materials in
including the cancellous bone [2], the cow teat skin [3], the aquatic
aerospace, naval, electronic, and automotive industries due to their high
salamander skin [4] and some face-centered cubic (FCC) crystals [5]. In
stiffness/strength to mass ratios as well as the matured manufacturing
1987, Lakes [6] first obtained a man-made NPR foam by heat treatment
techniques [16]. In recent years, auxetic honeycombs with NPR prop­
of the polyurethane foam, and measured its Poisson’s ratio of 0.7.
erties have been extensively researched as innovative engineering
Later, Caddock et al. [7] also achieved the NPR effect in preparing
meta-materials, due to their even higher relative stiffness and strength
polytetrafluoroethylene with a microporous structure and named it as
and more efficient energy absorption [17] than traditional honeycombs.
auxetic. The auxetics have drawn lots of research efforts in recent years

* Corresponding author.
E-mail address: yangshu@dlut.edu.cn (S. Yang).

https://doi.org/10.1016/j.compositesb.2020.108117
Received 16 January 2020; Received in revised form 25 April 2020; Accepted 29 April 2020
Available online 15 May 2020
1359-8368/© 2020 Elsevier Ltd. All rights reserved.
C. Qi et al. Composites Part B 197 (2020) 108117

Nomenclature ν Poisson’s ratio


L length of REC honeycomb in x-direction
r radius of circular arcs H height of REC honeycomb in y-direction
l length of the cell walls along the x direction σ ys yield strength of base material
h height of the cell walls along the y direction ε global stain of the honeycomb in y-direction
t cell walls thickness of honeycomb H0 original height of the representative unit
s the width of the unit cell along the x direction Hf final height of representative unit
α radius to height ratio L0 original length of representative unit
β length to height ratio Lf final length of representative unit
γ thickness to height ratio σ1 stress at the loading end of specimen
θ angle between circular arc and cell walls along the x σ2 stress at the supporting end of specimen
direction uy displacement of representative unit in y-direction
ρr relative density of honeycomb Mp fully plastic bending moment of cell wall, Mp ¼ ρysbt2/4
b out-of-plane thickness of honeycomb Δθ plastic angle
V loading velocity σs quasi-static plateau stress
ρs density of base material vs steady-shock velocity
E Young’s modulus of base material εd locking strain

The NPR effect of the auxetic honeycombs can be realized by the special honeycomb (RSH) and star-arrowhead honeycomb (SAH), with the
topologies of their microstructures such as the re-entrant (RE) [18], the in-plane crushing responses explored theoretically and numerically.
chiral [19], the double arrowhead [20] and the star-shaped [21] units, Ingrole et al. [35] designed a new enhanced auxetic honeycomb based
etc. There are many studies have investigated the static mechanical on the RE honeycomb and conducted tests on 3D printed samples. In
properties of the auxetic honeycombs. A For instance, Wang et al. [22] addition, hierarchy is being introduced to energy absorbing structures
analyzed the elastic properties of RE honeycombs in two orthogonal for enhancing mechanical properties. Li et al. [36] found that the hier­
directions using a strain-based expansion homogenization method. archical tubes is a more weight-efficient energy absorber than the reg­
Alderson et al. [23] measured the Poisson’s ratio of a set of chiral ular hexagonal tubes. Fan et al. [37,38] proposed hierarchical cellular
honeycombs and anti-chiral honeycombs with 3, 4 and 6 ligaments materials, which have superior mechanical properties compared with
under small deformation based on finite element analysis (FEA) and solid-wall cellular materials. Sun et al. [39] introduced a hierarchical
experiments. Gao et al. [24] studied the mechanical properties of the core sandwich panel against the blast loading. Fang et al. [40] investi­
three-dimensional double arrowhead structures intersected by a gated the mechanical properties of a special hierarchical honeycomb
two-dimensional honeycomb with negative Poisson’s ratio through under out-of-plane loads.
theoretical, numerical and experimental analyses. As above shown, development and design of auxetic honeycomb
Study has showed that the honeycombs’ crushing behaviors under materials with enhanced mechanical properties, especially in crushing
large deformation, such as deformation mode, deformation mechanism behaviors under large deformations, has become an interesting and hot
and crushing strength, are different from those under small deformation topic that researchers are paying close attention to. In this regard, more
[25]. In some applications, metallic auxetic honeycombs are often used efforts are needed to propose and construct new auxetic honeycomb
as cores of sandwich protection structures suffered from large defor­ configurations with innovative mechanisms to achieve superior me­
mation [26]. Analyses of deformation mechanism of the auxetic hon­ chanical performances such as the enhanced energy absorption capa­
eycombs in the elastic deformation cannot satisfy the increasing bility than the conventional honeycombs. Moreover, quantitative
applications demand in advanced engineering fields. One notable relationships between the mechanical properties and the various design
property of the honeycombs under large deformation is that the crushing variables need to be revealed and established to assist the design process
strain increases without obvious increase in stress for a certain period of of such materials.
time, which is called the “plateau stage”. The average stress during this In this work, we proposed a new re-entrant circular (REC) auxetic
stage is defined as the crushing strength, which dominates the energy honeycomb configuration by replacing the sloped cell wall of the con­
absorption of the material [27]. Qi et al. [28] analyzed the in-plane ventional re-entrant (RE) unit with double circular arc cell walls, which
crushing response of the tetra-chiral honeycombs under both shows obvious NPR effect observed through experiment and finite
quasi-static and dynamic loading conditions through numerical simu­ element (FE) simulations. The FE modeling method was validated by
lations and theoretical analyses. Gao et al. [29] deduced the empirical using the quasi-static crushing test data of a REC honeycomb specimen
formula to characterize the crushing deformation modes of the obtained through 3D-printing technology. The elastic-plastic deforma­
double-arrowed auxetic honeycombs under large deformation in two tion mode and the collapse mechanism of the REC honeycombs were
in-plane directions. Fu et al. [30] investigated the nonlinear shear revealed by FE simulations. Based on the deformed profiles of the
modulus of the RE honeycomb under large deformation derived by the representative unit cells and the principle of conservation of energy,
mechanical behavior of the cell configuration verified by numerical theoretical models have been derived to predict the crushing strength of
simulations. Hu et al. [31] studied the quasi-static crushing mechanical the REC honeycomb subject to quasi-static load. With the theoretical
properties of anti-trichial honeycombs with large deformation. models, the effects of geometric parameters of the unit cell including
With the fast development of additive manufacturing (AM) methods radius to height ratio and length to height ratio on the crushing strength
such as the 3D printing technique, some innovative configurations are of the REC honeycomb were analyzed. Poisson’ ratio of the REC hon­
being devised to achieve new deformation mode, enhanced stiffness, eycomb was analyzed, and the variation of Poisson’ ratio with respect to
more obvious NPR effect or larger plateau stress region of the honey­ the global crushing strain with different radius to height ratio and length
combs. Hu et al. [32] studied the quasi-static crushing properties of to height ratio were achieved and explained in detail. Finally, Compared
re-entrant anti-trichiral honeycombs made from ABS polymer by both to the RE honeycomb with the same feature dimensions, the specific
experiments and theoretical analysis. Wang et al. [33,34] proposed a energy absorption (SEA), i.e. energy absorption per unit structural mass,
novel re-entrant auxetic honeycomb named as re-entrant star-shaped value of the REC honeycomb is higher at any global strain levels.

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C. Qi et al. Composites Part B 197 (2020) 108117

2. Materials and methods be written as


2αð1 cos θÞ � β (4)
2.1. Re-entrant circular honeycombs
For convenience in the following discussion, we name the central
Fig. 1b shows the schematic view of the in-plane crushing setup of a portion framed by a green dotted line of the unit cell as hourglass cell,
typical REC honeycomb specimen (Fig. 1a) in this work. The honeycomb and the four surroundings framed by a red dotted line as petal cells, as in
is placed on a rigid plate and vertically crushed by another rigid plate Fig. 1d. The petal cell and the hourglass cell form a hierarchical
from the top along the negative y-direction with a constant velocity V. configuration.
Geometry of the honeycomb unit cell can be uniquely defined by three Depending on the specific applications or requirements, base mate­
independent variables l, h and r, as indicated in Fig. 1d, where l is the top rials for constructing the REC honeycomb could be metallic materials
and bottom side length, h is the height of the unit cell, and r is the circle such as the aluminum alloys of traditional honeycombs, or polymers
radius of the eight arcs replacing the inclined cell walls of the RE hon­ such as the polylactic acid (PLA) widely used by 3D printers. In this
eycomb, refer to Fig. 1c. Geometrical feasibility requires that h/2<r<l/ work, both PLA and generalized metallic material were used to construct
2. The four small circular arcs have identical arch angle of θ, while θ ¼ the novel REC honeycombs. The former was used for fast preparation of
arcsin (h/2r). The width of the unit cell is s, and the cell wall is assumed the REC honeycomb specimens on a 3D printer and later the proof-of-
to be uniform with thickness t, while the out-of-plane width is b. To assist concept experimental tests, while the latter was applied in the numeri­
the derivation of the crushing strength formula in the following, non- cal models for a thorough investigation on the crushing behaviors of
dimensional parameters have been defined, the radius to height ratio such novel honeycombs under the quasi-static load.
α ¼ r/h, the length to height ratio β ¼ l/h, and the thickness to height Mechanical properties of the PLA used in 3D-printing were obtained
ratio γ ¼ t/h, respectively. We assume the honeycomb specimen has 8 � by tensile tests of dog-bone-shaped samples in our previous study [28],
15 cells, i.e., the number of cells is 8 in the x-direction and 15 in the y- as in Fig. 2a. Fig. 2b shows the engineering stress-strain curve of the PLA
direction. The overall height of the REC honeycomb in y-direction after material with Young’s modulus E ¼ 1.57 GPa and yield stress σ ys ¼ 32
the array is H, and the overall length in x-direction is L. The circular arc MPa at a failure strain about 0.02. The generalized metallic material
angle, θ, the unit cell width, s, and the relative density, ρr, of the REC constituting the REC honeycomb was assumed to be rate independent
honeycomb can be expressed as elastic perfect-plastic with mass density ρs ¼ 2700 kg/m3, Young’s
modulus E ¼ 70 GPa, Poisson’s ratio ν ¼ 0.3, and yield strength ρys ¼
1
θ ¼ arcsin (1) 130 MPa.

s ¼ 2hðβ α þ α cos θÞ (2)


2.2. Finite element (FE) modeling method
γðβ þ 4αθÞ
ρr ¼ (3) We used the nonlinear explicit FE solver LS-DYNA 971 for all the
β α þ αcosθ
simulations and performed the numerical modeling work in the com­
The geometrical restriction on the REC honeycomb unit cell can also mercial software Hypermesh® [41]. In the baseline FE model, l ¼ 6 mm,

Fig. 1. (a) 3D-printed REC honeycomb specimen; (b) schematic of a REC honeycomb specimen (α ¼ 0.6, β ¼ 1.2) under crushing load; (c) unit cell configuration of
RE honeycomb; (d) unit cell configuration of REC honeycomb.

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C. Qi et al. Composites Part B 197 (2020) 108117

Fig. 2. (a) 3D-printed dog-bone-shaped samples; (b) Engineering stress-strain curve of PLA under uniaxial tension [28].

h ¼ 5 mm, r ¼ 3 mm, t ¼ 0.2 mm, H ¼ 75 mm, L ¼ 71.2 mm, and b ¼ 5 for all interfaces [27].
mm were adopted for the unit cell (see Fig. 1b), with corresponding α, β,
and γ values of 0.6, 1.2 and 0.04, respectively. Based on the baseline
design, three geometrical configurations were first obtained by changing 2.3. Specimen and experimental set-up
the value of α between 0.54 and 0.7 with an arc radius r varying between
of 2.7 and 3.5 mm, respectively. Secondly, another three geometrical 2.3.1. Specimen
models were obtained by setting the value of β to 1.4, and 1.6, with the The proposed REC honeycomb configuration is relatively compli­
side length l of 7 and 8 mm, respectively. In these cases, the overall cated and not easily manufactured by traditional machining methods.
honeycomb’ height H is keeping a constant value of 75 mm. The For proof-of-concept and model validation purposes, prototypes of the
geometrical configurations of the seven honeycomb specimens are listed REC honeycomb were constructed by using a 3D-printer through the
in Table 1 along with their overall honeycomb’s length and relative fused deposition method (FDM), as shown in Fig. 3a. The overall ma­
densities. In addition, two specimens were obtained by changing the cell chine size of the 3D-printer is 480 � 475 � 620 mm, while the printing
wall thickness to 0.1 and 0.3 mm, corresponding to a γ value of 0.02 and platform size is 300 � 300 � 300 mm. The nozzle diameter of the 3D-
0.06, respectively. FE models of these specimens were used to explore printer is 0.4 mm, and the printing accuracy is �0.08 mm. Three spec­
the effects of geometrical parameters on the in-plane crushing response imens were printed with identical dimensions: length L ¼ 123.3 mm,
of the REC honeycombs. height H ¼ 85.6 mm, out-of-plane width b ¼ 15 mm, unit cell side length
Cell walls of the honeycomb were modeled using Belytschko-Tsay l ¼ 32 mm, cell height h ¼ 28 mm, circular radius r ¼ 15 mm, and cell
(BT) four-node shell elements with five integration points through the wall thickness t ¼ 1.76 mm, corresponding to α, β, and γ values of 0.54,
thickness. After performing a mesh convergence analysis, a mesh size of
0.3 mm was determined to be optimal, which balanced the numerical
stability, accuracy and computational efficiency. Behaviors of the
constitutive materials, i.e. the PLA and the metallic material, were
modeled using *MAT_PIECEWISE_LINEAR_PLASTICITY, in which the
experimentally obtained stress-strain curve of the PLA can be defined.
Moreover, von Mises yield surface with associated flow rule was adopted
for the post-yield behavior of the constituting material. In the models,
the out-of-plane degrees of freedom (DOF) of the specimen were con­
strained. The bottom rigid plate was fixed and the top plate was given a
vertical constant velocity of V, as shown in Fig. 1b. The AUTOMA­
TIC_SURFACE_TO_SURFACE algorithm was adopted for contact be­
tween the honeycomb specimen and the rigid plates. In addition, the
AUTOMATIC_SINGLE_SURFACE algorithm was defined to account for Fig. 3. (a) 3D printing process of REC honeycomb specimen through FDM; (b)
self-contact of the honeycomb walls. The contact friction was neglected Uniaxial compression test setup of 3D-printed REC honeycomb specimen.

Table 1
Geometric parameters of the REC honeycombs.
Circular radius and cell height ratio α Cell side length and cell height ratio β

0.54 0.6 (baseline) 0.7 1.4 1.6

Geometric configuration

Honeycomb’s length L (mm)


66.4 71.2 75.3 76.2 101.2
Relative density ρr 0.174 0.153 0.185 0.133 0.119

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C. Qi et al. Composites Part B 197 (2020) 108117

1.14 and 0.06, respectively. The constitutive material of the specimens is


the PLA, whose stress-strain curve is depicted in Fig. 2b.

2.3.2. Quasi-static crushing test set-up


We performed quasi-static crushing test of the 3D-printed REC
honeycomb specimen by using a universal testing machine, as shown in
Fig. 3b. The specimen was placed on a fixed flat steel plate and com­
pressed by a top steel plate at a loading speed of 4 mm/min. Compres­
sion was along the same direction as tension of the dog-bone-shaped
samples to avoid anisotropy of the PLA material. The crushing force
level was recorded by a sensor in the loading plate. A high-definition
digital camera was used to monitor the deformation process of the
specimen. To obtain repeatable and reliable results, three specimens of
identical dimensions were tested respectively.

3. Results and discussion

3.1. Experimental results and model validation

For the purpose of numerical model validation, FE model of the


tested specimen was developed to simulate the quasi-static crushing
response. Fig. 4 shows the snapshots of specimen deformation during the
crushing process along with the simulated profiles at the same moment.
Due to the consistent deformation of three tested specimens, only one
specimen is showed in Figs. 4 and 5. During the early stage of loading
with a vertical displacement up to 7.5 mm, the specimen showed mainly
elastic deformation. Further crushed, the curved walls of the specimen
began to bend and rotate about the connecting points with the hori­
zontal walls. It is noted that the arcs along the diagonal lines experi­
enced larger deformations than others and formed two deformation
bands, as depicted in Fig. 4e and f. Accordingly, the central cell
deformed the most with its two large arcs in contact with each other,
seen in both the experiment and the simulation. Meanwhile, such a
unique deformation pattern caused the cells in the bilateral regions to
move towards the center of the specimen, resulting in an obvious NPR
effect, as shown in Fig. 4e. Further crushing resulted in the gradual
bending and collapse of more curved walls, as well as the initiation of
bending deformation of the horizontal walls, and the specimen shrank
more obvious as seen in Fig. 4h with a displacement of 30 mm. Finally,
most cells collapsed and self-contacted along with material ruptures at
several joint areas due to stress concentration, as in Fig. 4i–l. The
numerically obtained deformation patterns of the specimen at different
strain levels match the experimental results quite well, as seen in Fig. 4.
The force-displacement history of the specimen measured during the
quasi-static crushing test is depicted in Fig. 5. At first very small
displacement before 3 mm, the REC honeycomb specimens were crushed
to eliminate the unevenness caused by the printing errors, resulting in a
first small peak in the force-displacement curves. In the ideal FE model,
the starting time of loading was set to be delayed a little to avoid the
unevenness of the tested specimens. In addition, the deviation of three
curves is caused by the printing accuracy. Three specimens have the
same macro-dimension with some small print defects. Print defects of
some cell walls with different thickness in the plastic hinges results in
the different of the peaks and trends. Fig. 4. Deformed profiles of 3D-printed REC honeycomb specimen under quasi-
Three experimental crushing force is biased within a certain range, static crushing (V ¼ 4 mm/min) with crushing displacements of: (a) 0 mm in
featuring a short elastic deformation period with a maximum peak force experiment; (b) 0 mm in FEA; (c) 7.5 mm in experiment; (d) 7.5 mm in FEA; (e)
about 1450 N followed by a plateau stage with a load level about 1000 16 mm in experiment; (f) 16 mm in FEA; (g) 30 mm in experiment; (h) 30 mm
N. This justifies the cellular material characteristics of the 3D-printed in FEA; (i) 40 mm in experiment; (j) 40 mm in FEA; (k) and (l) enlarged view of
the rupture region, 40 mm in experiment.
REC honeycomb. Good agreement between the numerical and the
experimental force-displacement curves was observed in both force
levels and corresponding displacements. Therefore, the FE modeling 3.2. Quasi-static crushing response of REC honeycombs
methods herein are assumed valid and can be used in the following
study. This study aims to examine the quasi-static crushing behaviors of the
newly proposed REC honeycomb, including the deformation pattern, the
plateau stress, the Poisson’s ratio and the energy absorption capabilities.
These information will provide a basis for further engineering

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C. Qi et al. Composites Part B 197 (2020) 108117

constitutive material properties.

3.2.1. Numerical results


In this work, we used the explicit finite element method to solve
quasi-static problem. Considering the quasi-static loading velocity in the
experiment is significantly low, to conduct an economically-efficient as
well as accurate analysis, both mass effect and analysis time should be
reduced. Refer to the work of Zou et al. [42], when the impact velocity is
lower than the steady-shock velocity vs, the deformation mode of the
honeycomb can be regarded as quasi-static mode. The steady-shock
velocity vs is given by
pffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
vs ¼ 2σ s εd =ρs (5)

where ρs is the density of the basic material; εd is the locking strain; and
σ s is the quasi-static crushing strength. For the baseline REC honeycomb
(α ¼ 0.6, β ¼ 1.2, γ ¼ 0.04), the locking strain of εd ¼ 0.71 can be
Fig. 5. Comparison of three experimentally, one numerically and one theo­ determined by the energy absorption efficiency method [43], and the
retically obtained crushing force-displacement curves of 3D-printed PLA-based steady-shock velocity can be obtained as vs ¼ 18.9 m/s. The crushing
REC honeycomb specimen. velocity of V ¼ 1 m/s is lower than the steady-shock velocity vs, so we
assumed that this load can be regarded as quasi-static crushing load.
applications of such materials. Towards this end, FE models of the REC Fig. 6 shows the FE simulated deformation patterns of the REC
honeycombs were developed based on the validated numerical methods. honeycomb with different geometrical parameters at different strain
In addition, to assist quick estimation in the design practice, the crushing levels under the crushing velocity of V ¼ 1 m/s along the y direction. The
strength, i.e. the plateau stress of the REC honeycomb was derived green dashed frame refers to the boundary of the initial model. In gen­
theoretically as a function of the unit cell dimensions and the eral, a non-uniform deformation distribution is observed from the

Fig. 6. FE simulated deformations of REC honeycombs (equal γ ¼ 0.04) under quasi-static crushing (V ¼ 1 m/s) at different strain levels with different geometrical
parameters: (a) α ¼ 0.6, β ¼ 1.2 (baseline); (b) α ¼ 0.54, β ¼ 1.2; (c) α ¼ 0.6, β ¼ 1.6.

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C. Qi et al. Composites Part B 197 (2020) 108117

beginning of the loading throughout the whole process till the specimen the circular arcs which require a much higher force level. Therefore, the
is fully compacted. The deformation of the baseline model (α ¼ 0.6, β ¼ stress increases rapidly until the specimen is fully compacted, corre­
1.2, γ ¼ 0.04) first occurs mainly in the upper and centric regions of the sponding to Stage C in Fig. 7. Generally, honeycomb with higher plateau
specimen at a global strain of 0.25, where the dominating mechanisms stress can absorb more energy. We’ve focused on Stage B and derived the
include the shrinking of local hourglass cells to the center, the bending theoretical formulation for plateau stress prediction of the REC
of circular arc cell walls and the rotation of the petal cells about the honeycomb.
joints without too much compression. This results in a so-called “X”
mode deformation pattern shown in Fig. 6a. As the global strain in­ 3.2.2. Theoretical analysis of plateau stress
creases to 0.5, the unit cells form two obvious “X” shaped bands before To derive the theoretical crushing strength of the REC honeycomb
the collapse of rest cells. Three most collapsed regions locate in the subject to the quasi-static load, i.e., the plateau stress, an ideal profile of
upper, the middle and the lower parts of the specimen, respectively. The one representative unit was established for theoretical analysis (see
re-entrant essence of the REC honeycomb causes lateral gathering of the Fig. 8e and f), according to the collapse processes of typical cell
unit cells toward the center, resulting in the NPR deformation of the extracted from the FE result (Fig. 6a) in Section 3.2.1, as shown in
original rectangular specimen. Further crushed, most of the unit cells are Fig. 8a–d. Arraying such representative units along both x and y-di­
compacted at a global strain of 0.75. Fig. 6b and c shows the deformed rections can reproduce the total REC honeycomb. The representative
profiles of the REC honeycomb specimens with α ¼ 0.54, β ¼ 1.2 and α unit has an original width L0 ¼ s and an original height H0 ¼ h (Fig. 8e).
¼ 0.6, β ¼ 1.6, respectively. Clearly, the unit cell configuration shows a The length of the cell walls l, circular arcs radius r and cell wall thickness
great effect on the deformation pattern of the REC honeycomb. In the t are assumed to be constants during the crushing process. The constit­
current case, the initiation and the evolution of deformation bands are uent material was assumed to be rate independent rigid perfect-plastic in
different in the three specimens with different unit cell configurations. the theoretical analysis considering the negligible elastic stage as in
Moreover, compared with the baseline, the specimen with a smaller Fig. 7.
circular arc radius shows larger lateral contraction and more obvious At the beginning of the collapse process, the unit cell remain at their
NPR effect (refer to Fig. 6a and b). On the other hand, a larger side original positions with no deformations shown in Fig. 8e. After that, the
length of the unit cell than the baseline results in the “bulge effect” of the top cell wall moves downward toward the bottom one under the
specimen on both sides and less NPR effect, as shown in Fig. 6c. crushing, and the arc wall ACB bends an angle of Δθ until the cell
Fig. 7 shows the quasi-static crushing stress-strain curves of typical approach the densification state, as shown in Fig. 8f. At this state, the
REC honeycombs, which can be divided into three stages, corresponding collapsed cell height is Hf. The relative displacement along the y-di­
to the three distinct deformation mechanisms. Stage A is the linear rection of the representative unit from the initial position to densifica­
elasticity, where the stress increases linearly with elastic strain, corre­ tion state is:
sponding to the elastic bending deformation of the arc walls. After
uy ¼ H0 Hf ¼ h 2t 4rsin2 ðθ = 2Þ (6)
reaching the material yield stress, plastic hinges form at both ends of the
arc walls. Before the hourglass cells fully compacted and all petal cell As shown in Fig. 8f, the bended circular arc wall A’C’B’ forms one
contacting, the stress oscillates around a certain value and forms the plastic hinge at A’ point while the middle part of the arc A’C’B’ deforms
plateau stage, i.e., Stage B in the stress-strain curve of the REC honey­ very small and almost keeps constant curvature. Therefore, we assume
comb. In Stage B, the deformation of the unit cell is out of sync, that the plastic angle is formed by the arc wall around the joint A point
including the cells those have not undergone plastic deformation, those as shown in Fig. 8f:
have been contacted, and those are in-between state, as shown in Fig. 6.
The cells with larger deformation constitute the “X” shaped bands, Δθ ​ ¼ ​ π=2 θ (7)
resulting in the non-uniform deformation of the overall REC honey­ According to the theory of energy conservation, the external work is
comb. With a larger strain, more cells came into contact, and the “X” equal to the plastic energy dissipation. Due to the quasi-static load, the
shaped bands become thicker gradually until these bands mix together. kinetic energy caused by inertial effect can be neglected in this case,
The evolution of the “X” shaped bands causes the stress oscillation in refer to the work of Wang at al [29]. There are 16 plastic angles form at
Stage B as in Fig. 7. Eventually, cell walls contact with each other and the ends of 8 arc walls. Considering the same 16 plastic angles marked
the compressive densification occurs. Once the arc walls of the cells are by 16 small red circles in Fig. 8e, that reads
tightly packed, further crushing results in the collapse and flattening of
L0 bσ s uy ¼ 16Mp Δθ (8)

where Mp is the plastic bending moment of the arc walls. In the case of
rigid perfect-plastic beams with a rectangular cross section, Mp ¼ σysbt2/
4. By using Eqs. (6)–(8) and the definitions of α ¼ r/h, β ¼ l/h and γ ¼ t/h,
the quasi-static plateau stress σ l of the REC honeycomb can be obtained
as

σys γ2 ðπ 2θÞ
σs ¼ � � (9)
ðβ α þ α cos θÞ 1 2γ 4αsin2 ðθ=2Þ

The calculation process is transparent. Some important mechanical


indexes of the REC honeycombs are listed in Table 2, containing the
bending moment, the plastic angle, the displacement of representative
unit in y-direction, the theoretical plateau stress, the numerical crushing
strength and the relative error. The starting and ending strains of the
plateau stage are uniformly taken as 0.05 and 0.5 to avoid the effect of
elasticity and densification. The plateau stress of the REC honeycomb
under the quasi-static crushing load as in Eq. (9) is only related to the
yield strength of the constitutive material and the parameters of the unit
Fig. 7. Typical stress-strain curves of REC honeycombs under quasi-static
configuration. Fig. 9 shows the FE simulated global stress-strain re­
crushing (V ¼ 1 m/s). sponses of the REC honeycombs with different parameters, along with

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C. Qi et al. Composites Part B 197 (2020) 108117

Fig. 8. Collapse process of one representative unit of the baseline REC honeycomb under quasi-static crushing: (a) initial configuration (FE model); (b–c) the collapse
processes; (d) densification (FE model); (e) initial configuration (theoretical model), and (f) idealized densification (theoretical model).

Table 2
Numerical and theoretical mechanical indexes of the REC honeycombs.
Radius to height ratio α Length to height ratio β Thickness to height ratio γ

0.54 0.6 (baseline) 0.7 1.4 1.6 0.02 0.06


3
Plastic bending moment Mp (10 N⋅m) 6.50 6.50 6.50 6.50 6.50 1.63 14.63
plastic angle Δθ 0.39 0.59 0.78 0.59 0.59 0.59 0.59
Displacement of representative unit in y-direction uy (mm) 1.24 1.92 2.50 1.92 1.92 2.12 1.72
Numerical crushing strength (MPa) 0.699 0.670 0.678 0578 0.467 0.160 1.571
Theoretical crushing strength by Eq, 9 (MPa) 0.752 0.682 0.652 0.562 0.477 0.154 1.714
Relative error (%) 7.45 1.82 3.84 2.80 2.27 3.48 9.08

the corresponding plateau stresses predicted by the theoretical model of length, relatively speaking, the number of plastic angles in same area of
Eq. (9). In all the cases, the numerical crushing strength fluctuates along region becomes more, helping to increase the crushing strength; the
the theoretical predictions. Good agreement between the theoretical and number of plastic angles is more sensitive to the crushing strength than
numerical predictions can be observed from Table 2 with the maximum the strain to densification, resulting in the length to height ratio is more
relative errors about 9%. In addition, the theoretical predicted mean sensitive to the crushing strength than the radius to height ratio.
crushing force of 1073.8 N by multiplying the crushing area and Eq. (9)
is compared with the experimental value, as shown in Fig. 5. The 3.3.2. Poisson’s ratio
theoretical mean crushing force is close to the three experimental During the crushing process, the REC honeycombs laterally shrink in
crushing forces. Therefore, it is evident that the theoretical formulation varying degrees, as shown in Fig. 6. The lateral displacement of the REC
Eq. (9) provides a good estimation of the quasi-static crushing strength honeycomb is non-uniform along the y direction because of the overall
for the REC honeycomb. non-homogeneous deformation. To calculate the numerical Poisson’s
ratio of the REC honeycomb, 16 red points uniformly along the right
lateral side of the REC honeycomb are trailed considering the symmetry
3.3. Discussions of the specimens, as shown in Fig. 1b. The displacement of the 16 red
points along the x direction at different global strain are recorded. The
3.3.1. Crushing strength lateral strain of the REC honeycomb is then calculated by the double
Fig. 10 shows the theoretically predicted variation of REC honey­ average lateral displacement of these trailed points and the overall
comb’s quasi-static crushing strength with different parameters, con­ length of honeycomb along the x direction L. Fig. 11 shows lateral
taining radius to height ratio α, length to height ratio β and thickness to displacement-strain curves of five typical red points recorded in Fig. 1b.
height ratio γ. With the larger thickness to height ratio γ, the crushing Due to the overall non-homogeneous deformation, five curves have
strength become larger. It can be explained by that the larger thickness different trends and the maximum lateral displacements of these point
to height ratio means larger relative density of the REC honeycomb as in are similar. Point “A” is crushed first, reaching the maximum lateral
Eq. (3), helping increasing the crushing strength. In addition, smaller displacement first. Point “C” is farthest from “X” shaped band, resulting
radius to height ratio α and length to height ratio β tend to show larger in the lateral displacement of the Point “C” decreases most slowly.
crushing strength, and the length to height ratio β has a greater impact Fig. 12 shows Poisson’s ratio and global crushing strain curves of
on crushing strength than the radius to height ratio α. This can be REC honeycomb with different radius to height ratio α and length to
explained as follows: smaller α value means smaller circular arc radius height ratio β. As speculated by the deformation, the REC honeycomb
and the petal cells closer to the circle, which can earlier enter the presents a negative Poisson’s ratio at any global strain. Different from
densification while producing the same number of plastic angles, help­ the traditional definition of the Poisson’s ratio in the elastic range, the
ing to increase the crushing strength; smaller β means smaller cell side

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C. Qi et al. Composites Part B 197 (2020) 108117

Fig. 10. Theoretical quasi-static crushing strengths of REC honeycombs with


different parameters.

Fig. 11. Displacement along the x direction of five typical lateral points trailed
in the simulated deformation profile of the baseline REC honeycomb under the
quasi-static load.

α ¼ 0.6, 0.25 of α ¼ 0.7, 0.24 of β ¼ 1.4 and 0.22 of β ¼ 1.6. This


upward trend of the Poisson’s ratio with increased global strain can be
explained by the non-uniform overall deformation mode. At the early
global strain, few cells deformation first and has entered the densifica­
tion stage, forming the “X” shaped bands, while most cells have not
occurred significant deformation, as shown in Fig. 6. These deformed
cells caused a sudden laterally shrink, resulting in the trough of the
Poisson’s ratio. With the global strain increased, more and more cells go
into the densification stage, resulting in the Poisson’s ratio converging to
a certain value, i.e. the Poisson’s ratio at the honeycomb fully densified.
In addition, smaller radius to height ratio α and length to height ratio β
tends to show smaller Poisson’s ratio, indicating more obvious NPR ef­
fect. These can be explained as follow: smaller α means larger arch angle
θ, and larger deformable angle for the hourglass cells to laterally shrink,
helping to increase lateral displacement of the honeycomb; smaller β
indicates smaller cell length l and the overall honeycomb’s length L,
Fig. 9. FEA predicted quasi-static (V ¼ 1 m/s) stresses of REC honeycombs meaning in the case of equal lateral displacement, the lateral strain is
corresponding plateau stresses predicted by theoretical analysis with different increased, helping to increase the Poisson’s ratio.
parameters: (a) variable α; (b) variable β; (c) variable γ.
3.3.3. Comparisons with the RE and REC honeycombs
Poisson’s ratio of the REC honeycomb varies with the global strain. The The REC honeycomb is proposed by replacing the sloped cell wall of
Poisson’s ratio first shows minimum value at the early global strain of the regular RE honeycomb with double circular cell walls. It is signifi­
crushing as shown in Fig. 12, and the minimum Poisson’s ratio is about cant to compare these two kinds of honeycombs to highlight the special
1.0. With the increased strain, the Poisson’s ratio gradually increases advantage of this design. Therefore, FE models of RE honeycomb were
until converges to a certain value, which is 0.35 of α ¼ 0.54, 0.32 of also established. The macro scale of the honeycomb, the number of cells,

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C. Qi et al. Composites Part B 197 (2020) 108117

Fig. 12. Poisson’s ratio vs. global crushing strain of REC honeycomb under quasi-static load with (a) different α; (b) different β.

geometrical parameters of the single cell and the simulation setting is cell causes the obvious NPR effect of the RE and the REC honeycombs.
same to the baseline REC honeycomb. Considering the same thickness of Due to the same configuration size of the hourglass cell in these two
the cell walls, the relative density of two kinds of honeycombs are kinds of honeycombs, the final convergent value of Poisson’s ratio at the
different, which is 0.101 of the RE honeycomb and 0.153 of the baseline global strain about 0.8 is equal about 0.32.
REC honeycomb. Fig. 13 gives the FE simulated deformations of RE Specific energy absorption (SEA) is the energy absorption per unit
honeycombs under quasi-static load. Combining the deformation of the mass. A higher value of SEA represents the better energy absorption
baseline REC honeycomb as shown in Fig. 6b, the RE honeycomb shows effect. Fig. 15 shows the SEA-strain curves of the REC honeycomb and
the same macroscopical deformation pattern with the “X” mode under other typical auxetic honeycombs with the same macro scale, the same
the quasi-static load. The difference is that only one “X” shaped band is single cell geometries and wall thickness (t ¼ 0.2 mm) under quasi-static
formed during the crushing process, and the “X” shaped band is load. It is noted that SEA value of the REC honeycomb is higher than the
distributed under the honeycomb. star and the tetra-chiral honeycombs before the global strain of 0.62 and
Fig. 14a shows the stress-strain curves of the RE and REC honey­ 0.73. In addition, the SEA value of the REC honeycomb is higher than
combs under the quasi-static load. The numerical crushing strength of that of the RE honeycomb at any strain levels. With the increased strain
the RE honeycomb is compared with the theoretical plateau stress level, the discrepancy becomes larger. The SEA value of REC honeycomb
derived by Hu et al. [27], and the good agreement between the nu­ is 48.2% more than that of RE honeycomb at the global strain of 0.4,
merical and theoretical predictions verifies the FE model of the RE while the SEA value of REC honeycomb is 90.9% more than at the global
honeycomb. The curve of the REC honeycomb shows three distinct strain of 0.8. It is cleared that the hierarchical REC honeycomb was able
stages, containing the elastic stage, the plateau stage and the densifi­ to absorb more energy through plastic deformation than the regular
cation stage, while there are only elastic and plateau stages can be counterpart under the same quasi-static load. Due to the introduction of
observed in the curve of the RE honeycomb before the global strain of structural hierarchy, the unit cell under the quasi-static load deforms in
0.8. In addition, the plateau stress of the REC honeycomb is much higher two steps. Firstly, the hourglass cell shrinks laterally until the cell
than the RE honeycomb. On the one hand, the sloped cell wall was approach the provisional densification state. Secondly, the petal cell
replaced with double circular arc cell walls, resulting in the double flattened until the cell walls fully contacted. The circular arc walls in the
plastic hinges numbers, significantly increasing the plateau stress. On petal cell is more prone to produce plastic deformation, and produce
the other hand, the structural hierarchy results in the petal cells flat­ double numbers of plastic hinges than one slope cell wall, both help to
tened after the hourglass cells shrinking, and the stress of the REC enhance the energy absorption of the REC honeycomb.
honeycomb rises very quickly after the plateau stage.
Fig. 14b shows the Poisson’s ratio-strain curves of the RE and REC 4. Conclusions
honeycombs under the quasi-static load. The REC honeycomb tends to
show smaller Poisson’ ratio at the early strain, meaning more obvious The in-plane quasi-static crushing behaviors of a novel re-entrant
NPR effect. Refer to Fig. 6b, there are two “X”-shaped bands in the REC circular (REC) auxetic honeycomb devised from re-entrant honeycomb
honeycomb and only one “X”-shaped band in the RE honeycomb, which under large deformation, has been investigated through experimental,
means the REC honeycomb tends to form more “X”-shaped band and theoretical and numerical methods. Parametric studies, including radius
toward to the overall deformation, resulting in the more lateral to height ratio, length to height ratio and thickness to height ratio were
displacement at the early strain. The inward contraction of the hourglass carried out to reveal the influence of cells’ configuration on the crushing

Fig. 13. FE simulated deformations of the RE honeycomb under the quasi-static load.

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C. Qi et al. Composites Part B 197 (2020) 108117

Fig. 14. Stress-strain and Poisson’s ratio-strain curves of RE honeycomb and the baseline REC honeycomb under the quasi-static load.

● The REC honeycomb tends to show more obvious NPR effect than the
RE honeycomb at the early strain, and show the same Poisson’s ratio
when the honeycombs come into the densification stage. The
crushing strength and the specific energy absorption (SEA) of the
REC honeycomb is higher than the RE honeycomb at any global
strain levels.

Declaration of competing interest

The authors declared that they have no conflicts of interest to this


work.

Acknowledgments

This work was supported by the Ansteel Group Beijing Research


Institute Co., Ltd. under contract No.BWJ2019-13, and the National
Natural Science Foundation of China (nos. 51475069 and 51475070).

Fig. 15. SEA-strain curves of the RE honeycomb, the star honeycomb, the tetra-
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