CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N

System Name: BSM_SM_SQD2 Acquired By: sqte

Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 060 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1907 Result Set Id 2478
Sample Set Name: Carryover SSM Sample Set Start Date: 12/21/2010 1:50:20 PM EST

In the Carryover qualification, three pre-blank injections are performed to determine if the chromatograph is
clean enough to measure carryover. T hose injections are followed by three Sulfadimethoxine calibration injections
at a concentration of (5 ppm) which is 0.005 percent of the Challenge injection concentration (100000 ppm).

T he Challenge injection is made and is followed by three post-blank injections.

Carryover is reported as a percent of the Challenge concentration. If the % Carryover of first post-blank injection
is less than or equal to 0.005% the qualification passes.

Carryov er Peak Results

Carryover Carryover
SampleName Peak Type % Carryover
Specification Pass Fail
1 PostBlank1 < or = 0.005% Found 0.004 PASS

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 CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N

System Name: BSM_SM_SQD2 Acquired By: sqte

Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 060 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1907 Result Set Id 2478
Sample Set Name: Carryover SSM Sample Set Start Date: 12/21/2010 1:50:20 PM EST

2x106 2x106 2x106

Intensity

Intensity

Intensity
0 0 0
1.00 2.00 1.00 2.00 1.00 2.00
Minutes Minutes Minutes

PreBlank; Vial: 2:F,8; Inj: 1 PreBlank; Vial: 2:F,8; Inj: 2 PreBlank; Vial: 2:F,8; Inj: 3
2x106 2x106 2x106
Sulfadimethoxine

Sulfadimethoxine
Sulfadimethoxine
Intensity

Intensity

Intensity

0 0 0
1.00 2.00 1.00 2.00 1.00 2.00
Minutes Minutes Minutes

Std 0.005%; Vial: 2:E,8; Inj: 1 Std 0.005%; Vial: 2:E,8; Inj: 2 Std 0.005%; Vial: 2:E,8; Inj: 3
2x106 2x106 2x106
Sulfadimethoxine

Sulfadimethoxine
Intensity

Intensity

Intensity

0 0 0
1.00 2.00 1.00 2.00 1.00 2.00
Minutes Minutes Minutes

Stock 100 ng/µL; Vial: 2:F,5; Inj: 1 PostBlank1; Vial: 2:F,6; Inj: 1 PostBlank2; Vial: 2:F,6; Inj: 1

Printed 7:36:10 PM US/Eastern 4/26/2011 Page: 2 of 4

 CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N

System Name: BSM_SM_SQD2 Acquired By: sqte

Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 060 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1907 Result Set Id 2478
Sample Set Name: Carryover SSM Sample Set Start Date: 12/21/2010 1:50:20 PM EST

2x106
Sulfadimethoxine
Intensity

0
1.00 2.00
Minutes

PostBlank3; Vial: 2:F,6; Inj: 1

Printed 7:36:10 PM US/Eastern 4/26/2011 Page: 3 of 4

 CARRYOVER REPORT

A C Q U I S I TI O N I N F O R M A TI O N

System Name: BSM_SM_SQD2 Acquired By: sqte

Project Name: SQT_E_BSM_SM_SQD_data Column serial Number:
Sample Set Method: 060 Carryover SSM Sample Kit 1 Expiration Date:
Processing Method SMDO PM Sample Kit 1 Lot Number:
Report Method Name: Carryover RM Build Version: Empower 2 Software Build 2154 SPs
User Name: System Sample Set Id: 1907 Result Set Id 2478
Sample Set Name: Carryover SSM Sample Set Start Date: 12/21/2010 1:50:20 PM EST

Peak Results
Sample Type: Unknow n
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 PreBlank Unknown 2:F,8 1 Sulfadimethoxine 1.500 Missing
2 PreBlank Unknown 2:F,8 2 Sulfadimethoxine 1.500 Missing
3 PreBlank Unknown 2:F,8 3 Sulfadimethoxine 1.500 Missing

Peak Results
Sample Type: Standard
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 Std 0.005% Standard 2:E,8 1 Sulfadimethoxine 1.365 295250 105670 Found 0.0050
2 Std 0.005% Standard 2:E,8 2 Sulfadimethoxine 1.366 287810 106157 Found 0.0050
3 Std 0.005% Standard 2:E,8 3 Sulfadimethoxine 1.364 285814 102969 Found 0.0050

Peak Results
Sample Type: Unknow n
SampleName Sample Type Vial Injection Name RT Area Height Peak Type % Carryover
1 PostBlank1 Unknown 2:F,6 1 Sulfadimethoxine 1.352 240909 85954 Found 0.0042
2 PostBlank2 Unknown 2:F,6 1 Sulfadimethoxine 1.353 62470 20324 Found 0.0011
3 PostBlank3 Unknown 2:F,6 1 Sulfadimethoxine 1.353 26848 10199 Found 0.0005

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