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Composite Structures: Sciencedirect
Composite Structures
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A R T I C LE I N FO A B S T R A C T
Keywords: In this study, stiff stab-resistant materials for riot shields were developed by using fiber reinforced polymer
Stab resistance composites (FRPs) made of three different types of fibers: carbon, glass and p-aramid. The stab resistance of the
Hybrid composite FRPs were investigated with respect to the thickness and types of reinforced fibers according to the U.S.A.
Micro-CT National Institute of Justice (NIJ) standard. Hybrid composites were then developed to compensate for the
Fiber reinforced polymer (FRP)
weaknesses of each FRP, and the stacking sequences were optimized. The mechanisms of the stab resistance and
the blade penetration for each FRP were investigated via static stab compressive tests. Additionally, the failure
mode and fracture topography after the stab resistance tests were obtained using a micro-CT scanner.
1. Introduction reinforced polymer composites (FRPs). To obtain the rigidity for stiff
structures such as shields and helmets, the interfacial bonding strength
Over the centuries, general armor made of wooden and metallic between the fiber and the matrix of the composite is crucial. However,
materials has been used for personal protective equipment (PPE) [1]. the main disadvantage of UHMWPE-reinforced polymer composites is
With the increased severity in gun control legislation, both police of- that they have poor interfacial bonding strength [15,16].
ficers and the public are easily exposed to the threat of stabbing by For this reason, most research on stab-resistant FRP has focused on
incisive weapons. Thus, stab-resistant PPE has been gradually issued and used aramid fiber reinforced polymers (AFRP). Woven p-aramid
[2]. fabrics have been frequently used for PPE because of their excellent
There are two types of stab-resistant PPE: stiff and flexible [3]. For toughness, tensile properties and cutting resistance [17]. Knife pene-
both the flexible and stiff types of stab-resistant PPE, high performance tration occurs at two distinctive steps [18]. First, the knife tip pene-
fibers, such as p-aramid fiber and ultra high molecular weight poly- trates the surface of the target material. Then, the inner object is cut by
ethylene (UHMWPE) fiber, have been issued to reduce the weight of the the knife’s edge. Consequently, the penetration and cutting by the knife
PPE and improve the agility of the user [4,5]. Flexible PPE, which in- blade should be considered to improve the stab resistance. However,
cludes vest, gloves, pants, and other clothes, mainly requires a light both p-aramid fiber and AFRP have relatively poor compressive
weight and comfortableness when worn. Commercial stab-resistant strength and hardness.
vests are made of 20–50 sheets of multiple layers of p-aramid or Carbon fiber reinforced polymer composites (CFRP) have been in-
UHMWPE fiber fabrics [6,7]. Research on stab-resistant PPE has been creasingly developed using novel techniques because of their out-
highly concentrated on flexible PPE based on the shear thickening fluid standing properties, which include a high specific strength and stiffness,
and fabric laminates, with few studies having reported on stiff stab- design flexibility, etc. [19]. When CFRP is used as stiff-type stab-re-
resistant materials [8–10]. sistant PPE, the increase in hardness helps to restrict the penetration of
Stiff PPE, which includes riot shields, have been typically fabricated the knife tip, which is the first step of the stab mechanism [18] during
with polymeric, metallic and ceramic plates [11,12]. Until now, riot stabbing.
shields fabricated with polycarbonate or asbestos plates mainly protect In this study, stab-resistant FRPs were fabricated with three dif-
from clubbing and thrown objects [13]. However, these materials are ferent types of fibers: carbon, glass and p-aramid fibers. The stab re-
easily destroyed and penetrated by a stabbing assault [14]. These low sistance tests were performed according to the U.S.A. National Institute
mechanical problems can be solved by using high-performance fiber of Justice (NIJ) standard 0115.00. The stab resistances of the FRPs were
⁎
Corresponding author.
E-mail address: minkook@kist.re.kr (M. Kim).
https://doi.org/10.1016/j.compstruct.2019.111690
Received 30 August 2019; Received in revised form 25 October 2019; Accepted 6 November 2019
Available online 09 November 2019
0263-8223/ © 2019 Elsevier Ltd. All rights reserved.
J. Cheon, et al. Composite Structures 234 (2020) 111690
investigated with respect to the thicknesses and types of reinforced fi- The specimens were located on the backing materials, which consisted
bers. Additionally, hybrid composites were developed, and a stacking of four layers of 6 mm neoprene sponge, a single layer of 30 mm closed-
sequence was optimized to compensate for the weaknesses of each FRP. cell polyethylene foam and two layers of 6 mm rubber. For the stab
The use of two types of fibers in a suitable combination can not only resistance test, an engineered knife blade P1 impactor, which has one
improve the mechanical properties of composite, but also result in cutting edge, was manufactured using a BS4659 BO1 tool steel (West
performance synergy on fracture and flexural toughness [20,21]. The Yorkshire Steel Co Ltd, U.K.) according to the NIJ standard. The total
mechanism of the stab resistance and blade penetration through the length of the blade was 100 mm, the length of the cutting edge was
FRP was investigated via static compressive tests using the stab blade. 33 mm, and the thickness of the blade was 2 mm. Fig. 1 shows a
Finally, the failure mode and fracture topography after the stab re- schematic diagram of the stab resistance test setup and the knife blade
sistance tests were obtained using a micro-CT scanner. P1 impactor. The impact energy of the stab resistance tests was de-
termined to be 24 J based on protection level 1 of the NIJ standard. To
satisfy protection level 1, the penetration depth should be less than
2. Experimental
7 mm under an impact energy of 24 J. The total drop mass and impact
velocity of the stab resistance test were 2.6 kg and 4.31 m/s, respec-
2.1. Materials and fabrication
tively. During the stab resistance test, the velocity, force, displacement
and energy of the impact were measured using a CEAST data acquisi-
In this paper, three different types of plain woven fibers, namely, E-
tion system (DAS 64 K, Instron, U.S.A.), and the penetration depth was
glass (1180 plain weave, SK chemical, Republic of Korea) para-aramid
calculated from the time-displacement results.
(SNA1622, SAENAL Tech Tex, Republic of Korea) and carbon (C120
plain weave, SK chemical, Republic of Korea), were used to reinforce-
2.3. Static stab compressive test and three-point bending test
ment the stab-resistant composites. Diglycidyl ether of bisphenol-A type
epoxy resin (YD-128, Kukdo Chemical, Republic of Korea) was used as
To analyze the stab penetration process in the FRPs, a static stab
the matrix with a polyoxypropylene diamine-type hardener (D-230,
compressive test was also performed using a material testing machine
Kukdo Chemical, Republic of Korea). The composite specimens were
(Instron 5567A, Instron, U.S.A.). The knife blade, P1, was mounted on
fabricated via the hand lay-up method with the standard autoclave
the compressive zig and the FRP specimen was placed below the blade,
process for the epoxy resin (30 mins dwelling at 80 °C and 2 h curing at
as shown in Fig. 2. Then, the knife was penetrated into the FRP spe-
125 °C under 7 bars). 6, 9, 12, 15, 18, and 24 layers for each fiber fabric
cimen with a compressive speed of 10 mm/min. The FRP specimen was
were laminated and are represented as follows: [C6] to [C24] for the
held using a donut-shaped component 25 mm in diameter with 5 mm
CFRP, [A6] to [A24] for the AFRP and [G6] to [G24] for the glass fiber
thick jigs, which were fabricated with glass fiber reinforced polymer
reinforced polymers (GFRP).
composite to prevent bending.
Carbon/aramid and carbon/glass hybrid composites were also fab-
The flexural strength and stiffness of the FRPs and the hybrid
ricated with the same materials and process. For the hybrid composites,
composites were measured by a three-point bending test following
total 16 plies of carbon and aramid or carbon and glass fabric were
ASTM D790. The span length and width were six times and twice the
laminated in a 1:1 ratio (8 plies each) with following stacking sequence:
thickness of each FRP, respectively. The width of each specimen was
[C8/A8], [C4/A8/C4], [A8/C8], [A4/C8/A4] for carbon/aramid hybrid
fixed to 13 mm and the span to depth ratio was 16:1. According to
composites and [C8/G8], [C4/G8/C4], [G8/C8] and [G4/C8/G4] for
ASTM D790, the test speed was calculated with the thickness and span
carbon/glass hybrid composites. [C8/A8] indicates that the carbon layer
length of each FRP. For three-point bending test specimens of the CFRP,
was on the blade falling top side and the aramid layer was on the back
AFRP and GFRP, 16 layers of each fabrics were laminated identically to
side. CFRP with stacking sequence [C16] was also fabricated to compare
the hybrid composites.
with the hybrid composites results of stab resistance test and three-
point bending test.
2.4. Damage detection with the Micro-CT
Table 1 shows the properties [22] and parameters of each reinforced
fiber and fabricated composite. The specimens were cut using a water
To identify the damaged area and volume of each FRP after the stab
jet cutting system (T500-3015, TOPS waterjet, Republic of Korea).
resistance test, the penetrated area and the volumetric geometry for the
FRP were detected using a micro-CT scanner (SKYSCAN 1172, Bruker,
2.2. Stab resistance test U.S.A.). The specimens for the damaged FRP were prepared in a square
shape (20 mm × 20 mm) to improve the resolution of the micro-CT
The stab resistance test of the FRP specimens was performed based images. The medium camera pixels (2 k × 1 k) had a 9.0 μm resolution
on U.S.A. National Institute of Justice (NIJ) standard 0115.00 [23] with a source power of 10 W, and the specimens were rotated from 0° to
using a drop tower impact test machine (CEAST 9350, Instron, U.S.A.). 180° to capture the CT images every 0.4°. For the CFRP, AFRP and
carbon/aramid hybrid composites, the CT images were captured
Table 1 without filtering X-rays. However, the CT images for the GFRP were
Parameters of the each reinforced fibers and fabricated composites. captured with an Al-filter because the penetration of X-rays made de-
Properties of the reinforced fabrics tection insufficient.
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J. Cheon, et al. Composite Structures 234 (2020) 111690
100 mm
12 mm 38 mm
8º
9º
15º 15 mm
2 mm
NIJ Standard-0115.00 (P1-Type Blade)
33 mm
(a)
Composite
Neoprene Sponge
(4 Plies, 24 mm)
Polyethylene Foam
(1 Plies, 30 mm)
Rubber
(2 Plies, 12 mm)
(b)
Fig. 1. Schematic diagram of (a) knife blade P1 and (b) the stab resistance test set-up.
reinforced fiber type. Negative (minus) values indicated that the P1 AFRP had a relatively better stab resistance due to high density of the
blade impactor was blocked and could not penetrate the FRP specimen. glass fiber, as shown in Fig. 3-(b). To satisfy protection level 1 of the NIJ
With the same thicknesses and areal densities, the CFRP had the most standard (penetration depth < 7 mm), at least 12 plies of carbon fab-
favorable stab resistance. rics or 15 plies of glass and aramid fabrics should be laminated. Based
The GFRP had a relatively better stab resistance in terms of thick- on these thicknesses, the CFRP should be thicker than 2.6 mm, the
ness compared to the AFRP. However, in terms of the areal density, the AFRP should be thicker than 3.9 mm, and the GFRP should be thicker
10 mm/min
Donut-shaped Steel Jig
Bolt
Composites
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J. Cheon, et al. Composite Structures 234 (2020) 111690
Specimens
-10 Thickness (mm) -10
Areal density (g/cm2)
0 1 2 3 4 5 6 7 0.1 0.3 0.5 0.7 0.9
0 0
20 20
30 30
GFRP
GFRP
40 40
CFRP
CFRP
50 50
AFRP
AFRP
60 60
70 70
(a) (b)
Fig. 3. The penetration depth of the FRPs with respect to the thickness and the reinforced fiber type; (a) function of the thickness, (b) function of the areal density.
than 3.2 mm. increased and the knife blade impactor penetrated the FRP specimens.
The impact force-displacement curves of the stab resistance tests are The impact force required for penetration increased proportionally to
shown in Fig. 4. The initial values of the impact force fluctuated due to the specimen thickness. If the force required to penetrate the specimen
the vibration caused by the compression of the soft backing materials. was greater than the maximum impact force that can be exerted by the
After the backing materials were fully compressed, the impact force drop weight impact test, the specimen was not penetrated. The
1 1
Impact force (kN)
0.8
[G15]
0.8 [C12]
[G12]
[C9]
0.6 0.6
[G9]
0.4 [C6] 0.4
[G6]
0.2 0.2
0 0
0 20 40 60 80 0 20 40 60 80
Displacement (mm) Displacement (mm)
(a) (b)
1.4
[A24]
1.2 [A18]
Impact force (kN)
1 [A15]
0.8 [A12]
[A9]
0.6
0.4 [A6]
0.2
0
0 20 40 60 80
Displacement (mm)
(c)
Fig. 4. The impact force-displacement curves of the stab resistance tests; (a) CFRP, (b) GFRP and (c) AFRP.
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J. Cheon, et al. Composite Structures 234 (2020) 111690
3 [C24] 3
2.5 2.5
2 [C18] 2
[G24]
1.5 [C15] 1.5
[G18] [G9]
[C12]
[G6]
1 1 [G15]
[G12]
0.5 [C9] 0.5
[C6]
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Displacement (mm) Displacement (mm)
(a) (b)
3
[A24]
2.5
Compressive force (kN)
[A18]
2
1.5
[A15]
1 [A12]
0.5 [A9]
[A6]
0
0 10 20 30 40 50 60
Displacement (mm)
(c)
Fig. 5. The static stab compressive test results with respect to the reinforced fiber and thickness of FRP; (a) CFRP, (b) GFRP and (c) AFRP.
maximum impact force was determined by the impact test setup and the FRP are pushed by the spine of the blade and compressed in the plane
mechanical properties of the FRP specimens. The maximum impact direction. – The stab compressive load is then increased again. (5)
force of the CFRP, AFRP and GFRP under the NIJ standard test were Friction and residual stress dominant step: The size of the crack and the
1260 N, 1130 N and 1078 N, respectively. If the blade impactor pene- damage area is maximized through the ricasso section of the knife.
trated the FRP specimen, the maximum displacement was increased by Then, the body of the blade slides through the penetrated hole of the
the length of the penetrated blade. FRP – the compressive load then decreases.
Fig. 7 shows the flexural test results of the FRP with respect to the
reinforced fibers. As expected, the CFRP had the highest flexural stiff-
3.1.2. Mechanism of the knife penetration ness and strength, followed by the GFRP and then the AFRP. As the
To analyze the mechanism of the blade penetration through the thickness of the specimen increased, the compressive load also in-
FRP, static stab compressive tests were performed. Fig. 5 shows the creased equally, but showed different behaviors depending on the type
static stab compressive test results with respect to the reinforced fiber of reinforced fiber. In particular, the CFRP showed a high increase rate
and thickness of the FRP. The mechanism of the FRP stab resistance can and value for the compressive load at the beginning of compression, as
be clearly explained by the static compressive and gradual penetration shown in steps (1) & (2) in Fig. 6. Because the CFRP has a relatively
of the blade. high flexural stiffness and strength, the stab compressive load is also
The blade penetration process though the FRP can be divided into 5 higher than the AFRP and GFRP. In contrast, the AFRP initially showed
steps, as shown in Fig. 6: (1) Surface hardness and flexural stiffness a low stab compressive load (similar to the GFRP, even if the tensile
dominant step: the fibers on the surface begin being cut by the blade tip stiffness was much larger than the GFRP) due to the low compressive
and the FRP specimen is globally banded by the compressive load of the properties of aramid fiber [25–27]. However, the AFRP had an espe-
blade – the stab compressive load sharply increases by the flexural cially high stab compressive load in the later step of the crack and
stiffness and hardness of the FRP. (2) Compressive properties dominant penetration propagation (steps 3 & 4) due to the abrasion and cutting
step: the lower part compresses out of the plane direction – the stab resistance of the aramid fibers [28,29] as shown in Fig. 6-(c).
compressive load also increases to reach the maximum point. (3) Cut- When the first peak value of static stab compressive load in an early
ting resistance dominant step: the blade impactor penetrates the FRP by step was higher than the maximum impact force of the stab resistance
cutting the reinforced fiber using the cutting edge. The bending and test, the FRPs blocking the blade and not being penetrated (penetration
compressive stress out of plane direction are then released by the fiber depth < 0). As a result, CFRP has the advantages on high flexural
cutting, and the stab compressive load is decreased by the stress release stiffness, compressive strength and surface hardness in order to prevent
of the cut fiber plies. (4) Cutting resistance dominant step: after the the beginning of blade tip penetration. After penetration begins (pe-
blade breaks through the FRP, the penetration crack (hole) in the da- netration depth > 0), the high cutting and abrasion resistance prop-
maged area is widened in the in-plane direction by cutting the re- erties of AFRP help prevent crack propagation and blade penetration
inforcement using the blade cutting edge. The surrounding parts of the
5
J. Cheon, et al. Composite Structures 234 (2020) 111690
Increase of
compressed
area
(4) (5)
Fig. 6. The blade penetration and stab resistance mechanism of the FRP.
from the cutting. the [C15], [G15] and [A15] were 0.7 mm, 4.6 mm and 6.5 mm, respec-
tively.
The CFRP showed a wide damaged area and brittle failure, and the
3.1.3. Failure mode carbon fibers were broken by the impact instead of being cut by the
Fig. 8 shows images of the top surface, cross-section and bottom blade. With a smallest penetration depth (0.7 mm), the bottom surface
surface of the 15 plies of laminated CFRP – [C15], GFRP – [G15] and was also widely fractured by the tensile stress from the impact. The
AFRP – [A15] after the stab resistance tests. The penetration depths of
6
J. Cheon, et al. Composite Structures 234 (2020) 111690
50 Flexural stiffness 800 disking failure mode, as shown in Fig. 8-(c). The aramid fibers were
Flexural strength 700 then torn by the cutting. The deformed area returned from the dishing
1 mm 1 mm 1 mm
7
J. Cheon, et al. Composite Structures 234 (2020) 111690
carbon/aramid hybrid composites and the structural stability is main- fibers were laminated on the falling surface of blade, had better stab
tained after the crushing with the impactor [31–33]. resistance performances compared to the CFRP. The hybrid composite
To satisfy protection level 1 of the NIJ standard, a total of 16 plies, 8 with the [C8/A8] and [C4/A8/C4] stacking sequences where carbon fi-
plies of CFRP and AFRP or 8 plies of GFRP, were laminated for the bers were laminated on the falling surface of the blade had a better stab
hybrid composites. The stacking sequences of the carbon/aramid hy- resistance performance compared to the CFRP. Specifically, the [C8/A8]
brid composites were controlled at [A8/C8], [A4/C8/A4], [C8/A8] and hybrid composite had the best stab resistance without penetration. The
[C4/G8/C4], and at [G8/C8], [G4/C8/G4], [C8/G8] and [C4/G8/C4] for hybridized aramid fiber under the CFRP layer increased the impact
the carbon/glass hybrid composites. The thicknesses and areal densities energy absorption and resistance to being cut by the blade.
of the carbon/aramid hybrid composites were 4.25 mm and 5200 g/m2, Additionally, the high surface hardness of the CFRP also prevented the
respectively, and for the carbon/glass hybrid composites they were blade tip from digging into the hybrid composite.
3.25 mm and 5480 g/m2, respectively. However, the hybrid composite with aramid fibers laminated on the
surface had a lower stab resistance performance. If the AFRP layers
3.2.1. Stab resistance of the hybrid composites were located on the inner side (compressive side) of the bending, the
Fig. 9 shows the penetration depth of the carbon/aramid and flexural property was relatively low, as shown in Fig. 10-(b), and the
carbon/glass hybrid composite via the stab resistance test with an im- surface hardness of the hybrid composite was also reduced. Therefore,
pact energy of 24 J. The penetration depth of the CFRP, [C16], was the blade tip easily began to penetrate the hybrid composite.
1.4 mm. The carbon/glass hybrid composite had a lower stab resistance
(higher penetration depth) for all stacking sequences compared to 3.2.2. Failure mode of the carbon/aramid hybrid composites
[C16], even though it was thicker than the CFRP, as shown in Fig. 9-(a). Fig. 12 shows the cross section and bottom surface images of the
The glass fiber had no benefits in mechanical properties, and there was carbon/aramid hybrid composites after the stab resistance tests. The
little difference in fracture mechanism under stab impact. greatest difference between the CFRP and the hybrid composite was the
However, the flexible strength largely decreased by hybridization delamination between the AFRP and CFRP. This delamination further
with glass fiber and aramid, as shown in Figs. 10 and 11. Figs. 10 and absorbed the stab impact energy and mitigated the progression of pe-
11 shows the flexural stiffness & strength and flexural stress–deflection netration cracking by the blade.
curve of the hybrid composites, respectively. The composite with only Moreover, hybridization with the AFRP provided a significant im-
carbon fiber, [C16], showed brittle fracture. In the case of hybrid provement in the damage area and fiber breakage reduction in the
composite, the bending strength decreased drastically however the CFRP, as shown in Fig. 12-(c) and (d). The AFRP reinforced under the
crack did not propagated rapidly and showed ductile fracture. And the CFRP prevented damage of the bottom layer, which was fractured by
flexural toughness of composites were improved by the hybridization. the tensile stress from the impact, and prevented the plugged out
The penetration depth of the carbon/glass hybrid composites were broken carbon fiber from being pushed out by the blade. The AFRP had
higher than CFRP and there was no performance improvement by the a higher cutting and abrasion resistance, and it effectively prevented
hybridization because of the flexural strength decrease. Unlike aramid propagation of the blade crack. However, when the CFRP was on the
fiber, glass fiber had no resistance to cutting and could not obtain hy- bottom layer or the supporting AFRP layer was too thin, the bottom
brid effect to increase stab resistance. CFRP layer was damaged by the impact or the supporting AFRP layer
In case of carbon/aramid hybrid composites, where the carbon was pushed back by the broken CFRP layer, as shown in Fig. 12-(a) and
50 500 50 500
Flexural stiffness Flexural stiffness
Flexural strength
Flexural strength (MPa)
40 400
Flexural strength (MPa)
Flexural stiffness (GPa)
30 300 30 300
20 200 20 200
10 100 10 100
0 0 0 0
[G81C8] [G4C28G4] [C4G38C4] [C84G8] [A81C8] [A4C28A4] [C4A38C4] [C84A8]
(a) (b)
Fig. 10. Flexural stiffness and strength of the hybrid composites; (a) carbon/glass hybrid composites, (b) carbon/aramid hybrid composites.
8
J. Cheon, et al. Composite Structures 234 (2020) 111690
Fig. 11. Flexural stress-deflection curve of the hybrid composites; (a) carbon/glass hybrid composites, (b) carbon/aramid hybrid composites.
(b). AFRP should be thicker than 3.9 mm, and the GFRP should be thicker
The AFRP layer closed the penetration cracks by reducing the per- than 3.2 mm. The CFRP showed a wide damaged area with fiber
manent destruction of the carbon fibers and restoring it after stab im- breakage by the impact and the broken fiber protruded due to the
pact. This crack closing by the AFRP could improve its resistance to blade. Contrary, the damaged area of the AFRP was relatively narrow
repeated stab impacts and maintain the structural stability after the stab and the main fracture was generated by fiber cutting.
impact. Finally, the stacking sequences of the carbon/aramid and carbon/
The carbon/aramid hybrid composite had a better stab resistance glass hybrid composites were optimized to compensate for the weak-
compared to the CFRP and AFRP. For the best stab resistance of the nesses of each fibers. The carbon/aramid hybrid composites, where the
hybrid composite, CFRP with a high stiffness and hardness should be carbon fibers were laminated on the falling surface of blade, had better
located on the surface where the blade falls, and AFRP, which has an stab resistance performances compared to the CFRP. And the hy-
excellent cutting resistance and impact energy absorption, should be bridization provided a significant improvement in the damage area and
located on the back side. The hybrid composite with this stacking se- fiber breakage reduction of the CFRP.
quence [C8/A8] had the best stab resistance performance.
9
J. Cheon, et al. Composite Structures 234 (2020) 111690
1 mm 1 mm
1 mm
1 mm 1 mm
10
J. Cheon, et al. Composite Structures 234 (2020) 111690
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