URANIUM DUST SEPARATION SYSTEM ISAAC CORGATELLI EMILY MACK JOSEPH NORMAN YING YANG VALUE PROPOSITION • Every year there is more need for clean, reliable energy • Some new advanced nuclear reactor designs are safer and more economically feasible • Manufacturing of fuel for these designs creates mixed glass and metallic uranium waste • Project is to create a system to separate useful uranium from glass and zirconium oxide • Team will provide analysis for upscaling for use in the industry THE WASTE PRODUCT • Fuel is cast in quartz tubes coated in zirconium oxide powder • Quartz tubes are broken off from the fuel pins, generating waste product • Final waste product consists of quartz shards, zirconium oxide, and fine particles of uranium/zirconium alloy
Manufacturing Process
Waste Product Example
DESIGN REQUIREMENTS • Design needs to fully process material batch within 15 minutes • Must separate out 95% of surrogate material by weight • Process must be dry to avoid criticality safety concerns • Process must require no human input besides loading and unloading of material SEPARATION METHODS • Mass separation: • Difficult due to dry process preference • Complicated by uranium tracking requirements • Would require extensive material pre- processing • Magnetic separation: • Has been studied previously for use with this waste product • Does not require precise particle size control • More commercially available MAGNETISM
• Three types of magnetism: ferromagnetism,
paramagnetism, and diamagnetism • All materials are weakly diamagnetic • Iron, cobalt, and nickel are ferromagnetic • Many other materials are paramagnetic • Paramagnetism manifests as extremely weak magnetic attraction • Uranium is relatively highly paramagnetic
Specific magnetic susceptibilities
MAGNETIC ROLLER CONCEPT • Combats gravity effect on material • Only requires slight stream separation FLUX ANALYSIS
Individual Magnet Linear Halbach Array
Linear N-S Array Radial N-S Array
MATERIAL SURROGATE • Because real Uranium cannot be used in our case, a surrogate material must be used for testing • Surrogate should imitate the magnetic properties of Uranium. • Zirconium Oxide and Quartz tubes are easily obtainable
Quartz Tube
Titanium Granules Surrogate Material
• 0.5x susceptibility of uranium • Equivalent volume of metal • Nontoxic in mixture • Potentially pyrophoric • Glass is size classified ZrO2 Powder PREVIOUS DESIGN
• Permanent magnets invert to
separate material sitting on top • Recycling bin carries material back up to magnets for continuous processing • Changed design due to difficulty of tuning and suboptimal magnet utilization ROLLER DESIGN • Machine allows for continuous recycling of material over the bare magnet roller • Construction from polycarbonate and 3D printed parts provides valuable proof of concept before upscaling to industry ROLLER MACHINE OPERATION 3D PRINTING MACHINING • Lexan (polycarbonate) used for structure • High strength and clear for easy viewing • Side plates machined by UI facilities and all other plated machined in the ME machine shop PURCHASED PARTS • 280 ½’’ N52 magnet cubes • Glass test tubes • Titanium sponge: 800g, 0.5-1mm • 1/2" x 24" x 48" Lexan • 3 DC motors • Vibrating motor • Items from our BOM MOTOR CONTROL / WIRING
• An emergency switch controls the entire circuit for safety.
• Two 12V-2A-150RPM-5.09kgf⋅cm DC Gear Motors control the ring and magnet, respectively. • Three 24V-5A-120W Power Supplies control three motors. • A 24V-30W Vibration Motor shakes the plate, which causes the mixture to fall along it. FINAL SOLIDWORKS DESIGN • Includes motor mounts and alignment for sprockets • Brush mounted behind roller to remove any residual material after each cycle • Contact surfaces of ring are rubber and sandpaper tape for optimum grip FINAL PRODUCT
• Powered by three separate
24V power supplies • All shafts ride on purchased roller bearings • All blue parts are 3D printed PLA • Clear parts are machined Lexan or plexiglass TESTING PROCEDURE • Tests were performed with multiple weight batches of surrogate material • Material is loaded onto the vibrating platform via the cutout on the side plate • Optimal results were found with smaller batch sizes due to less material clogging
Final Surrogate Material
OPERATION HEAVY LOAD OPERATION SEPARATION RESULTS • Tests with 0.5 – 1mm titanium granules yield approximately 95% separation by weight • Zirconium Oxide is present in final product • Significant glass shards make it into the separated product due to bouncing CHALLENGES
• WORKING WITH N52 MAGNETS
• FINDING USEABLE AND ACCURATE MATERIAL SURROGATE • TUNING SYSTEM TO MINIMIZE LOSS OF MATERIAL FROM BOUNCING • SHIPPING DELAYS ON ESSENTIAL COMPONENTS REMAINING ISSUES / FUTURE WORK • MATERIAL LOSS FROM BOUNCING • WARPING IN LEXAN STRUCTURE • FINE TUNING OF ROLLER SPEED -1.5 RPM RING -17 RPM ROLLER • SMART CONTROLS AND AUTOMATED RECOVERY MONITORING • FUTURE WORK SHOULD FOCUS ON USE OF INDUSTRIAL ROLLERS WITH CASCADING DESIGNS PLAN FOR IMPLEMENTATION • Scaling up for use in industry would require modifications to design to eliminate material loss • Existing industrial separators would likely work well with modification • Cascading design would allow for multiple passes and continuous processing BUDGET Budget Overview