Date: 3 ) !

2 o 2 4 Page No
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Observation Inference
Experiment

PrelhmuDary test.

coloun andd appeaance B]ue caloun May be Loppen present

test
when the Subs Aance Blue in coldwhite May be coppen pxesent
heated and cooled. Ln hot

3 Flame test
The Substance is made Blue isgeen Mcy be Coppen peSent
Into a paste
daop of con. Hcl . A smal.
Lamount. of Ihe past. is
Intxocuced nto Hhe flame
sing a xod.

BOTOD Trifluoride test

The subs tance is made coloun Absence bo xote
nto a Paste by mixig
The pinch of Ca E and conHyscy
rhy paste is introduce d into he flame
 Expt.No. Date Page No. 2I
S.No Experiment Observation Inference

Ethy Borate test

Thesub stance is womed ND gneen edpd flame Absence of baxate
uaiIhtwodnops ap con. Ha SO4
and few dnops of etfhanal hen
Vapou iS gnited.

Action of Hcl
Small amount of chanactenis tic
the Substance Aheate chagge Absence
Sulphide
f canbonote

two ps o cil Hel

Action of Con. H9.SO4

small amount of fhecolour less gos tuns lime wden Presence os oxalate
Substance is treatel i lh milky Gas come out from
twodnops of Con. H2sO4 lime waten buans uith blue
and then cuanmed. flame iç ignted

Chromy chloxide test

The subs ~ance is heatedRe ornge opuns condensingPresence f chioziole
(uito khacry and con, Hasa to red oils dops To tis ad!
acetic acid and lead acetate

Date Page No
Expt. No.

Experiment Observation Inference

S.No.

Yellow Precipitate is obtaunel

A white Sublamae iS Presence of mMoniwm

The Substanceis beate
in a dy kest tube forme&

Action of NaOH
Presence of anonium
Jhe substane is Locted coloun less gas wuth pungent
ith NaOHSoltion Smell giving dense white fumes
wth con. Hc)

Ash test.
pinkblue, geen Absence of Mg Al
1he Substance is txete
and
olown
tuilh di) HNOZ, cnd cobalt
nikxato, A çiltenpapen i s
ippedin thisSolution
and heated in he bunsen
Laune The colon of fhe
ash is notel.
 SNo. Experiment Observation Inference

PRePARATION SoDI M CAR BoNArE ExIRACT

About mie n boilel with
osodium canbonate in 20 ml distillel wnten when rhe volume Te duces to tuo
txdit is coled and fillered. The filtened fillxatel known
cantonate Contains VanioWs CniOns as theix Sc um Salt The filtxate
is analzed foY anionS anl the resicdue is cncuys edfar e presence of Cations

TEST WiIH SODum CARBuNATE

colow extxact Blue Colown Paesence of Coppen

2 A ttle of he ext act A

cwncy uhite precipitate Presence of chlori le
soluble in NHOH

ill eff envescence stops

boiled and Cooled Then AghO,
is adel

A ittle ofIhe extract is. NO white Precipitate insoluble Absence f suphate

aidified uith dl He) boilel in con Hcl is abtalned
Lcosled and add Bacla Solutio

Date Paue No
Expr.No

Experiment Observation Inference

SNO.

LA little f the extyact isA white Precipi Lde Psesence af oxalate

acidiçed th dil acetic acinsoluble in amMonium OEalte

boiled cooled and Cacls and ox alic acid solution but

Solution soble in cil Hc and di HAo

BYOwn test
Absence
bxouwn
xing
acidif1ed ifh clil Heso and
mìxed with feeshly pxepas ed
Feso Soltion To fhis mix tund
Con. Haso4 is add along the
Side of the test Lube with

ANALYs1so£ BASIc RADLcALs

PRE PARAToN Of SoL UTION

The cat ion on aysiscan be Cam i e out uith the Te s iclue of Socdium
Cantongte er txct Ihe residue dissolved Solvent Cwaten ax iLHd
Con Hc conHNO 3-4 2qua
andtaken as test solution
 Date Page No 25
Expt No,

S.No. Experiment Observation Inference

T a) take c Small amount NO )bite preciptate Absence of Jaad

LOf origina) solut ion cif uits

hot Con Hel)and cald wao
and ccol it b apuaten
and centxifgad
b) rke a Sclamount. NO ohite precipikate Absence Lead
aprigin al Solutio cit
water ) and ad cilHe|!
and centri Pged.
To the above solut ion ad Black Precipitate Pxecence of cuzt

bomel add Nas and

Centxif uged
Take o Small amont of NO bxOun and wbite Absence of on
preciptate olwmun um

min Afte Cacaling add sli

Smel of mmonia.

Date
Page No.
Expt. No.
Inference
Observation
S.No.
Experirnent

No chanactonistic Absence of zn, Ni, o

To the above Solution
and mn
add aS and centxifgod change
Absence of Ba SY an
white precip1tate
Take o Small amount of Ca
Solution adl Sald
NHc add excess
Solution falloued by Solid
CauH) Cog and centxifuged
Presence of ammoDrOM
shiteues formed wben
amount of lhe
A Small oipped
SubstCnce
treteA bng the glass xodmouth of
in Hcl nean the
is eolved
Jhe test tube
beated e s

CATLONS.
ANAusis O GROUp

uith NeuHCoole&and Conkeifugoo

is boiled
lhe oup pxecipitate il Aso Heat ed caole

and centaifused
 Date Page No 27
EXDt No
Observation Inference
Experiment
SNo.

Centxifugpd. solution is taken Spot plate and excess

A tle of
olue coloun fosmtion
f liqor ammonia is aclded A deep
Presence of coppen is Confmedl.

CATIo NS

Ammoniun isLonfiYmed
the A cenless gas ifh
TO little of
Solutian he smell of am monia uning
and heatel tet
JHmus ko blue and
Paducinq den se white fume
Sxong Tod dipped in
ConHl is ob taine.

Date : Page NO.

No

ExptNo
Inference
Observation
S.NO.
Experiment

Recoxt Salt mic Ewne contains

The guen. noyaani

Acid Radicals

Sumple YaLcdical aloricAe

antexfexinq xadical Cxalote

Rosic Radicals

Qmnoniun