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Powder Technology 420 (2023) 118376

Contents lists available at ScienceDirect

Powder Technology
journal homepage: www.journals.elsevier.com/powder-technology

Influence of rubber powder size and volume fraction on dynamic


compressive properties of rubberized mortar
Guoxiang Yang a, Yaojiang Fan a, Xing Li a, Ying Xu a, b, *
a
Institute of Geosafety, China University of Geosciences (Beijing), Beijing 100083, China
b
State Key Laboratory of Hydraulic Engineering Simulation and Safety, School of Civil Engineering, Tianjin University, Tianjin 300072, China

H I G H L I G H T S G R A P H I C A L A B S T R A C T

• Dynamic compressive properties of


rubberized mortar are investigated.
• Effects of rubber powder size and vol­
ume fraction on properties are
investigated.
• Failure process and energy absorption
capacity of rubberized mortar are
analyzed.
• Rubberized mortar has reduction in
strength but improvement in energy
absorption.

A R T I C L E I N F O A B S T R A C T

Keywords: Rubber particles taken from waste tires have been proposed as a prospective substitute for natural aggregates.
Rubber powder Although the dynamic mechanical responses of rubberized concrete have been studied considerably, rubberized
SHPB mortar without coarse aggregates is desired for laboratory constitutive study due to the uniformity requirement.
Impact load
This work uses rubber particles with sizes of 40, 80, and 120 mesh and volume percentages of 10%, 20%, 30%,
Dynamic compressive strength
Energy absorption capacity
and 40% to prepare mortar specimens. A split Hopkinson pressure bar combined with a momentum-trap device is
utilized to apply dynamic loads. Experimental results indicate that the dynamic compressive strength of
rubberized mortar increases with rubber sizes but is negatively correlated to volume fraction. The reduction in
the dynamic strength of rubberized mortar is less evident as compared to that of rubberized concrete investigated
in previous studies. Additionally, the incorporation of rubber powder with smaller size can slightly improve the
energy absorption capacity of rubberized mortar.

1. Introduction annual new tire production goes over 1.6 billion units and around 1
billion waste tires are generated. The disposal of the waste tire is a
According to the 2021 Global Tire Recycling Market Report, the worldwide environmental problem due to its non-biodegradable nature

* Corresponding author at: State Key Laboratory of Hydraulic Engineering Simulation and Safety, School of Civil Engineering, Tianjin University, Tianjin 300072,
China
E-mail address: maggie_xu@tju.edu.cn (Y. Xu).

https://doi.org/10.1016/j.powtec.2023.118376
Received 30 November 2022; Received in revised form 11 February 2023; Accepted 21 February 2023
Available online 24 February 2023
0032-5910/© 2023 Elsevier B.V. All rights reserved.
G. Yang et al. Powder Technology 420 (2023) 118376

and combustion risk [1,2]. Direct landfill of the waste tire without ratio of energy absorption needs to be re-examined.
proper treatment occupies a large area and provides breeding grounds Considering the pulse shaping, Pham et al. [34,35] and Feng et al.
for pests [3]. Furthermore, accidental burning of the exposed tires may [36] pointed out that the rubberized concrete showed higher sensitivity
produce massive toxic gases. As a result, processing the waste tire into to the loading rate and the rate-sensitivity went up with the volume
the forms of crumb rubber or powdered rubber and incorporating them percentage of the added rubber chips. The presence of the rubber chips
into the cementitious materials as a partial or complete replacement of slowed down the propagation of the cracks and exhibited progressive
mineral aggregates [4–6] is regarded as a sustainable approach in failure in comparison with the normal concrete. Besides, in order to
relieving the waste tire-related environmental concerns. enable the valid analysis of the failure and fragmentation characteristics
Rubber is a polymer material characterized by high resilience and of the dynamic compressive specimens, the momentum-trap technique
toughness, low density but desired fatigue and impact resistance. The is usually adopted to ensure the single pulse compressive loading
inclusion of rubber into cementitious materials thus may not only pro­ [37,38]. To date, this technique has not yet been used related to dy­
duce a high-performance construction material (rubberized mortar or namic compression and fragmentation research of rubberized mortar.
rubberized concrete) with superior physical and mechanical properties, In the preparation of the rubberized concrete, different sizes (i.e.,
but also ameliorate the greenness of the environment [7–10]. For chipped, crumb and powdered rubber) and percentages of rubber par­
example, by incorporating a certain percentage of the rubber crumb, the ticles were always simultaneously adopted to replace the fine and coarse
rubber mortar showed a nearly 35% reduction in the overall density, aggregates according to the ASTM standard C136 [21,39] or other
whereas a significant acoustic attenuation enhancement (~40%) was related industrial standards [7,12,20]. However, the use of chipped
resulted [11]. The rubberized mortar is thus a promising choice in rubber or crumb rubber as the replacement of the coarse aggregates may
constructing lightweight structures with remarkable noise isolation. be problematic for fabricating laboratory specimens, because of the
Güneyisi et al. [12], Kang and Jiang [13] proved that the incorporation introduction of macroscopic heterogeneity [40–42]. Furthermore, the
of crumb rubber helped reduce the shrinkage stress and thus restrict the addition of the rubber chips often leads to greater strength loss [5],
development of the shrinkage cracks within the concrete. The rubber­ preventing its application in construction applications. Therefore, this
ized cementitious composites also exhibited better abrasion resistance study focuses on the rubber mortar containing only fine aggregate to
than the conventional ones [14]. On ductility, Youssf et al. [15] study the effects of particle size and volume fraction of rubber powder
concluded that the rubberized concrete has better ductility than that of on its dynamic mechanical properties and energy absorption
plain concrete and a replacement of sand by 50% in the mixture could characteristics.
increase its impact resistance by approximately 3.5 times. Moreover, the The aim of this work is to study the influences of rubber powder size
rubberized cementitious materials also showed better performance in and volume fraction on the dynamic compressive properties and energy-
thermal insulation [2], fatigue resistance [16], and energy absorption absorbing ability of rubberized mortar. The modified SHPB apparatus
capacity [17]. containing a momentum-trap device was adopted to conduct the dy­
The above-mentioned advantages promote the rubberized cementi­ namic compressive tests. Prior to the dynamic test, the scanning electron
tious materials as an environmentally friendly civil engineering con­ microscope (SEM) was employed to identify the microstructures of the
struction alternative. However, because of the weak bond capacity prepared mortar. A high-speed camera was utilized to record the time-
between the cement matrix and rubber particles, the rubberized varying failure process during the dynamic compression. With the
cementitious materials often show an obvious reduction in strength as force balance realized, the dynamic compressive strength, failure pro­
compared with the plain concrete or mortar [3,11,18–22]. The strength cess and energy absorption capacity of the rubberized mortars were
reduction is sometimes acceptable for constructions like roadside bar­ compared and analyzed. Finally, the effects of loading rate, powder size
riers [23], road pavement [24], and insulation layers of the buildings and volume fraction of the added rubber on the dynamic failure and
[25], where high fatigue resistance and energy absorption capacity are fragmentation characteristics were carefully analyzed. This work can
more preferred. Whereas for engineering construction applications such reveal the dynamic mechanical behavior and energy-absorbing perfor­
as load-bearing beams, long-span bridge structures and the specific mance of the rubberized mortar, and has particular guiding significance
armor units, the significant decrease of the compressive strength is not for applying rubberized mortar as an alternative material in the con­
desirable. Therefore,optimized rubber inclusion proportion and gran­ struction of seismic-resistant structures.
ulometry [11], addition of the effective binder material such as silica
fume [26,27], and chemical pretreatment of the rubber surface [28,29] 2. Experimental setup
are proposed to effectively increase the cement-rubber paste bond and
thereby lessening the compressive strength reduction. 2.1. Specimen preparation and characterization
Particularly for structures in areas with strong tectonic activity or
near blasting operations, the dynamic compressive response is one of the Portland cement with 20% (by mass fraction) limestone addition was
most important indexes involved in civil engineering constructions. To adopted as the binding material in this study. Two types of aggregates, i.
date, very few efforts have been performed to study the dynamic e., the ISO 679 standard sand with an average density of 1.590 g/cm3,
compressive properties of rubberized cementitious materials using the and rubber powder with a density of 0.405 g/cm3 of different sizes (40,
SHPB system. Liu et al. [8] and Huang et al. [30] used a 70 mm-diameter 60, and 80 mesh) were adopted. The average size of the rubber powder is
SHPB system to conduct the dynamic tests of the rubberize concrete, approximately identical to that of the standard sands. Besides, a certain
concluding that the dynamic compressive strength showed obvious rate- percentage of mineral powder [43,44], silica fume [45], fly ash [46],
dependent behavior, and the dynamic fracture toughness and energy and other concrete admixtures such as antifoaming agents [47] and
dissipation capacity of concrete were significantly enhanced. Yang et al. polycarboxylate superplasticizer [48] were also added to enhance the
[31] analyzed the dynamic failure modes and energy absorption char­ density, workability, and interface bonding ability, and eventually to
acteristics of rubberized concrete under various impact loading condi­ meliorate the physical and mechanical performance of the mixtures.
tions, demonstrating that the total energy absorption of dynamic Powdered rubber with sizes of 40 mesh, 80 mesh and 120 mesh was
compression was greater than that of split tension. The enhancement in separately added to partially replace the fine sand in the mixtures by
energy absorption capability helps to absorb and dissipate the energy of 10%, 20%, 30% and 40% volume percentage. For the purpose of com­
earthquakes, reducing the risk of damage to the building and improving parison, the plain mortar without rubber particles was also fabricated,
its overall stability. However, the pulse shaping technique as suggested and the detailed composition fraction of the mixture can be found in our
for testing brittle solids [32,33] was not utilized in these studies to earlier work [49].
facilitate the stress uniformity within the specimens, the enhancement According to the mixing procedure suggested by Güneyisi et al. [12]

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G. Yang et al. Powder Technology 420 (2023) 118376

and Jalal and Mansouri [50], the solid components except the rubber contrast, the surrounding cement paste underwent a certain degree of
powder were first stirred for 5 min using a laboratory power-driven deformation during the hydration reaction, thus generating tensile stress
revolving pan mixer. Then the water containing the antifoaming at the bonding interface and alliterating the separation between the
agents and polycarboxylate superplasticizer were poured and mixed for rubber powder and the matrix. Additionally, the microstructural
5 min. Afterwards, the rubber powder with volume fraction and pre­ investigation by SEM also shows extensive micro cracks emerged from
scribed size was incorporated to the mixture, during which the mixer the vicinity of the bonding interface and developed into the interior of
kept working to avoid the rubber packing. The reason for incorporating the cement matrix, which can be ascribed to the deformation mismatch
rubber powder at the end is to prevent the adverse effect on the hy­ induced by the complex stress state between the cement paste and
dration reaction of cement [51]. Thereafter, the homogeneous mortar rubber powder during the processes of hydration. The existence of the
mixture was carefully poured into a 100 mm3 cubic mold and fully ITZs and internal micro-cracks will greatly impact the mechanical
compacted, after which all molds were wrapped with plastic film to properties of the rubberized mortar, i.e., the more the interface transi­
prevent excessive moisture loss and kept undisturbed for 24 h in an air- tion zones, the higher the porosity and the looser the structure, thereby
conditioned room at 25 ◦ C. Then the cubic blocks were demolded and leading to a worse bonding effect and a lower resultant strength.
moved to a standard curing box with a constant temperature of 25 ◦ C
and relative humidity of 50% for 28 days. Upon completion of the
curing, cylinders with size of 50 mm (in diameter) × 100 mm (in height) 2.2. Experimental apparatus
were first drilled from the cubic block. Some of the cylinders were
polished on both ends (Fig. 1a) for quasi-static compressive tests, other The quasi-static compression tests were performed using a conven­
were further cut into 50 mm in height with ends polished (Fig. 1b) for tional uniaxial servo-hydraulic testing system at a constant loading rate
dynamic tests according to the suggested methods [52]. of 0.02 mm/min, which is capable to simulate a strain rate of ~10− 6 s− 1.
Fig. 1c and d show the variations of density and acoustic velocity for To conduct the dynamic test, a modified SHPB apparatus containing the
mortar cylinders with different rubber powder sizes and volume frac­ momentum-trap device (as illustrated in Fig. 3) was adopted.
tions. Both the density and the velocity decrease with increasing the The traditional SHPB apparatus mainly includes a striker bar (0.3 m
rubber inclusion proportion, while the variation of these properties with in length and 50 mm in diameter), an incident bar (5 m in length and 50
the rubber powder size is not as that significant. This is expected because mm in diameter), a transmitted bar (2.5 m in length and 50 mm in
the rubber powders play a similar role as the air voids in the plain diameter), and a data acquisition system. The other parameters of the
mortar. Besides, although some additives (e.g., fly ash and silica fume) apparatus can be also found in the literature [38]. As mentioned earlier,
were incorporated to enhance the interface adhesion between the rubber the stress uniformity within the specimen is vital for dynamic testing of
powder and cement matrix and also act as void fillers, numerous voids (i. the material. Therefore, the pulse shaper made of C11000 copper disc
e., rubber-induced pores) can still be identified (Fig. 2) in the interfacial was adopted to filter and obtain a non-dispersive bell-shaped incident
transition zone (ITZ). This is due to the non-polar property of rubber stress wave with a relatively long rising edge, thereby allowing the stress
powders, i.e., increasing the air-trapping capacity and results in a more wave to have enough time to propagate forward and back several times
porous structure during the water evaporation process in comparison before the peak. In this way the dynamic force balance on the two ends
with the plain mortar [25,53]. Moreover, the rubber powder almost of the samples can be achieved.
maintained its original shape due to its high chemical stability. In Particularly for the dynamic compressive failure mode and frag­
mentation analysis, the achieving of the single-pulse loading is an

Fig. 1. Photos and basic physical properties of the rubberized mortar: (a) specimens for static tests, (b) specimens for SHPB tests, (c) the density and (d) the acoustic
velocity for different rubber size and rubber percentage.

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G. Yang et al. Powder Technology 420 (2023) 118376

Fig. 2. SEM images showing the microstructure of the rubberized mortar.

Fig. 3. Schematic of the SHPB apparatus with the momentum-trap device.

important issue. In a conventional SHPB test, the reflected wave has been described in our earlier work [37].
generated at the specimen surface will propagate back to the impact end, Fig. 4a displays the waveforms measured in a typical dynamic
where it transforms from tension to compression and propagates again compressive test using the momentum-trap technique. It is observed that
towards the specimen. This wave will load the specimen for the second the second loading wave consists of a compression part with very low
time. This process repeats leading to the multiple loading on the spec­ amplitude and a subsequent tension part. The tension portion of the
imen. For this reason, the energy responsible for the specimen damage is wave helps to separate the incident bar from the specimen and prevent
ill-defined, resulting in complications to the specimen failure analysis. In the subsequent compressive pulse acting on the specimen. The specimen
this work, the momentum-trap technique [54,55] was adopted to ach­ thus only undergoes a single-pulse compression during the dynamic
ieve a single loading during dynamic compression tests so as to facilitate loading, realizing the so-called soft-recovery of the specimen and thus
failure analysis. The momentum-trap system mainly consists of a hollow facilitating the accuracy of failure analysis. Fig. 4b indicates the dy­
cylinder rigid mass and a flange plate attached to the incident bar near namic stress histories for a typical dynamic compressive test. It is
its impact end as shown in Fig. 3. The working principle of the technique observed that the magnitude of stress acting on the left side of the

Fig. 4. (a) Typical stress waveforms when using the momentum-trap technique. (b) Stress equilibrium in a typical dynamic compressive test.

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G. Yang et al. Powder Technology 420 (2023) 118376

specimen (the sum of the reflected and incident wave) is almost identical studies [2,5,41,56]. Fig. 5b indicates the elastic modulus changes versus
to that of the right side (transmitted wave) from 210 μs to the peak the rubber powder size and volume fraction. It is observed that the
moment (~ 300 μs), demonstrating that the force balance has been modulus decreases with the increase of rubber volume fraction. This can
realized and the dynamic test is valid. Besides, there exists an obvious be ascribed to the soft nature of the rubber. However, it can be also
platform in the reflected wave, meaning that the constant strain rate observed that the elastic modulus of the rubberized mortar is weakly
loading is realized. With the stress equilibrium attained, the slope of the dependent on the rubber powder size.
linear part of the transmitted wave is defined as the loading rate [33]. Besides, the incorporation of rubber powder plays an adverse effect
Moreover, the dynamic compressive stress and strain can be calculated on the overall strength of rubberized mortar, mainly induced by the
using the incident, reflected and transmitted waves, weak bond interface between the cement and rubber paste, and also the
lower load-carrying capacity of the rubber powder themselves. Aver­
AE
σ (t) = (εi (t) + εr (t) + εt (t) ) (1) agely, the strength of the rubberized mortar decreases by 14.7%, 19.4%,
2As
25.2%, and 32.5% for the inclusion proportion of 10%, 20%, 30% and
C
∫ t 40%, respectively. It is noted that the observed reduction in strength is
ε(t) = (εi (t) − εr (t) − εt (t) )dt (2) much lower than those for the rubberized concrete as reported in the
Ls
literature [57–59] where a 45–60% strength reduction was observed for
0

where σ is the compressive stress applied on the specimen, ε denotes the 20% rubber proportion. Moreover, for a given inclusion proportion, the
strain on the bars with subscript i, r, t indicating the waves on three bars. strength decreases in general with the decrease of the powder size. This
As and Ls refer to the cross-sectional area and length of the specimen. A is because for a given inclusion proportion, the number of powder
and C denote the cross-sectional area and one-dimensional P-wave ve­ particles increases with the decrease of powder size. More rubber par­
locity. E is the elastic modulus of the bars. ticles mean more defects and thus decrease the overall strength of
rubberized mortar. This result contradicts with the size effect reported in
3. Experimental results and discussions the literature [21,22,57,59,60]. In those studies, the tire chips with sizes
roughly ranging from 10 to 30 mm were used to replace the coarse ag­
3.1. Compressive behaviors of rubberized mortar under quasi-static gregates, which might introduce remarkable macroscopic heterogene­
loading state ities into the specimens at the material testing scale. According to the
International Society for Rock Mechanics and Rock Engineering (ISRM)
Fig. 5 implies the static compressive strength, elastic modulus, and suggested method for testing the mechanical properties of brittle solids,
failure characteristics of the rubberized mortar with various inclusion the specimens should be uniform in petrography, intact and represen­
parameters of rubber powder. For a given powder size, the compressive tative of the testing material [61]. The diameter of the specimen should
strength approximately linearly reduces with the increase of rubber be at least 10 times of the average grain size of the brittle solids.
volume fraction (Fig. 5a), which is consistent with the results in existing Therefore, with incorporating the chipped rubber, significant stress
concentration may occur in the vicinity of the ITZs. Excessive cracks

Fig. 5. The mechanical properties and failure modes of the rubberized mortar. (a) compressive strength, (b) elastic modulus, and (c) failure modes.

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G. Yang et al. Powder Technology 420 (2023) 118376

might initiate in these areas due to the deformation mismatch between reduction compared to that of the control mortar) regardless of the
the cement matrix and rubber powder under the action of the external rubber size. As the rubber volume fraction is increased, the strength
loads, leading to premature failure of the rubberized concrete. As a reduction ratio gradually increases until an approximate 27% reduction
result, the large size rubber chip dominates the failure and results in is observed when 40% of the fine aggregated is replaced. The dynamic
reduced compressive strength. strength reduction ratio is much smaller than that of the rubberized
In this work, only the fine-grained sands were partially replaced by mortar under the static load, where a nearly 40% reduction is observed
rubber powder with relatively small particle size, the resultant mortar with the same replacement percentage (Fig. 5). Furthermore, consistent
can thus be considered as a homogenous material [62,63]. Therefore, with the static strength observation, the dynamic strength of mortar
the main failure mechanism is the debonding between the rubber par­ with a larger rubber size (i.e., 40 mesh) is larger than that of mortar with
ticle and the cement matrix. The mortar specimen with smaller rubber smaller rubber size (i.e., 120 mesh) at given loading rate and rubber
powder has more particles and greater specific surface area, thereby inclusion percentage. For example, for the mortar with 10% rubber and
leading a lower strength. The failure modes of the rubberized mortar are the loading rate of ~2000 GPa/s, the dynamic strength of mortar with
displayed in Fig. 5c, most of the specimens exhibit tensile failure mode, rubber size of 40 mesh is 80.5 MPa, whereas only 72.1 MPa for mortar
and the number of tensile cracks is positively correlated to the powder with rubber size of 120 mesh, nearly an 11% strength difference.
percentage but negatively correlated to the rubber size. This observation Compared with the larger rubber particles, the increase of surface area
confirms the failure mechanism for rubberized mortar. induced by smaller rubber powders facilitates the growth of ITZs in
cement-based matrix, thus contributes to the decrease in the compres­
sive strength [42,53,65].
3.2. Dynamic stress-strain curves and strength variations of the In order to quantitively describe the improvement in compressive
rubberized mortar strength of rubber mortar under different loading rates, the dynamic
increase factor (DIF) is introduced and defined as the ratio of dynamic
Fig. 6 shows the complete stress-strain curves of rubberized mortar compressive strength to quasi-static strength [41]. The calculated DIFs
with 40 mesh rubber powder under different loading rates and rubber of the rubberized mortar are plotted in Fig. 9. It is shown that the DIFs
percentage. It is observed that for a given rubber percentage, the dy­ linearly increase with both the loading rate and rubber volume fraction.
namic strength shows obvious rate dependency (Fig. 6a), i.e., the dy­ Although the plain mortar exhibits the highest dynamic compressive
namic strength increases with the loading rate. Besides, the dynamic strength, the greatest DIF value occurs for the rubberized mortar with
elastic modulus is almost unchanged with the loading rate. These ob­ 40% rubber powder volume percentage, demonstrating that the
servations match well with those for homogenous rock materials [64,65] rubberized mortar shows higher sensitivity to the loading rate. This
but are partially different from those for rubberized concretes [34,52]. observation matches well with the experimental results in previous
In their work, the elastic modulus slightly varied in an arbitrary manner, studies on rubberized concrete or rubberized geopolymer concrete
which again may be attributed to the inhomogeneity of the specimen. As [34,52]. In this study, it is also observed that the dynamic strength is
the rubber powder inclusion percentage increases, the dynamic strength weakly dependent on the rubber size for the rubberized mortar as shown
decreases (Fig. 6b). At the meaning time, the dynamic elastic modulus in Fig. 9b.
gradually decreases with increasing the rubber volume fraction, indi­
cating that the incorporation of the rubber powder reduces their
deformation resistance. 3.3. Energy-absorbing capacity of rubberized mortar
The dynamic compressive strength of the rubberized mortars is
depicted in Fig. 7. The dynamic strength is obviously greater than the The dynamic dissipated energy, Ws, defined as the enclosed area
corresponding static one. Regardless of the rubber powder size, the underneath the dynamic stress-strain curve of the tested specimen, can
dynamic strength approximately increases linearly with the increase of be directly calculated from the incident, reflected, and transmitted wave
the loading rate but declines with increasing the volume fraction. The data,
strength reduction is mainly due to reduced mechanical properties at the Ws = Wi − Wr − Wt (3)
ITZs. Massive microcracks may develop quickly within these regions and

accelerate the failure of the overall cement-rubber mixtures [39]. t

To better illustrate the effects of rubber powder percentage and size Wk = E0 C0 ε2k (t)dt (4)
0
on the dynamic strength, the strength against the loading rate and the
rubber size at a given rubber inclusion percentage is shown in Fig. 8. where Wi, Wr and Wt are the elastic energy carried by three stress waves.
When rubber powder volume fraction is 10%, the reduction in the dy­ The subscript k in equation represents the waves on three different bars.
namic strength of the rubberized mortar is neglectable (less than 10% To reduce the errors caused by the specimen size deviations, the

Fig. 6. Complete stress-strain curves of rubberized mortar (40 mesh) with different (a) loading rates and (b) rubber inclusion percentages.

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G. Yang et al. Powder Technology 420 (2023) 118376

dissipated energy density, wd, is introduced [66] and governed by,


Ws
wd = (6)
Vs

where Vs is the volume of the tested specimen.


Fig. 10 implies the tendency of dissipated energy density of the
rubberized mortar. Note that the dissipated energy data for plain mortar
are also plotted for comparison. According to the figure, the dissipated
energy almost linearly changes with the loading rate and exhibits an
upward trend with the rubber volume fraction. This matches well with
the observations reported by Aly et al. [67], in which the drop-weight
test was employed to reveal the energy absorption characters by the
geopolymer concrete. Therefore, the rubberized mortar requires higher
energy to fail as compared with the plain mortar [4]. The excellent
impact energy absorption capacity of rubber mortar makes it being a
promising building material, such as roadside barriers and various
pavements. Besides, given a constant rubber percentage, the rubberized
mortar with 120 mesh rubber powder assumes the highest energy ab­
sorption capacity, followed by the mortars with 80 mesh and 40 mesh
rubber powder inclusion. Moreover, it is also found that the increase
gradient of the fitting curves (dashed lines) for each mortar group are
roughly identical, indicating that the rubber powder size has little effect
on the rate sensitivity of the energy-absorption capacity. To summarize,
adding rubber powder to the cementitious material will improve its
energy absorption capacity. Although the dynamic peak strength de­
clines with the increase of volume fraction of the rubber powder (Fig. 7),
the energy absorption capacity of rubber mortar is positively correlated
with rubber content. Therefore, the rubber with a smaller size is more
preferred for constructions requiring less load-carrying capacity but
higher energy absorbing ability. In addition, the maximum increase in
energy absorption is observed in the mortars with 40% rubber inclusion.
The dissipated energy density approximately increases by 1.49 (40
mesh), 1.70 (80 mesh) and 2.01 (120 mesh) times that of the plain
mortar, respectively.

3.4. Dynamic failure patterns and fragmentation analysis

The failure modes of rubber mortar with respect to different vari­


ables are illustrated in Fig. 11. Unlike the observation of recovered
specimens from static compressive tests, the cracks on dynamically
loaded specimens are dominated by axial cracks, which is due to the
uniaxial loading with reduced end effect as compared with the static
compression. At the lower loading rate, several macroscopic tensile
cracks are observed at failure, whereas many visible cracks appear with
higher loading rate (Fig. 11a). Note that during the failure process, only
a few mortar fragments that fly away from the failed specimens are
observed, indicating that the kinetic energy carried by the flying frag­
ments is negligible and most of the input energy is consumed in the
development of the new crack surfaces. Meanwhile, the crack density at
failure evidently increases with the rubber powder volume fraction
(Fig. 11b) and decreases with increasing the rubber powder size
(Fig. 11c), which keeps up with the variation trend of the absorption
energy density. It is worth mentioning that Pham et al. [34] pointed out
that the added rubber in the concrete acts as the crack arrestor that helps
impede the propagation of the cracks. Thus, the failed rubberized mix­
tures show larger fragments and lower crack density under a similar
loading rate as compared with normal concretes. It is believed that the
larger size (5–10 mm, over 10 times that employed in our work) rubber
Fig. 7. Dynamic compressive strength of mortar with power size (a) 40 mesh, crumbs used to replace the coarse aggregates can cause bridging be­
(b) 80 mesh, and (c) 120 mesh. tween the cracks and reasonably restrict the expansion of existing
cracks. Whereas the use of rubber powder with the size roughly equal to
the fine grading sand has little crack bridging effect, and thus the
specimens with higher rubber percentage and smaller rubber size are
more likely to shatter into small pieces under dynamic loads.
Fig. 12 shows the fragment size distributions of the recovered

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G. Yang et al. Powder Technology 420 (2023) 118376

Fig. 8. Dynamic compressive strength of mortars with different rubber dimensions. (a) Rubber percentage 10%; (b) rubber percentage 20%; (c) rubber percentage
30%; (d) rubber percentage 40%.

Fig. 9. The DIF values versus the loading rate with different (a) volume percentages and rubber sizes.

specimens in the typical dynamic tests using the momentum-trap tech­ thereby leading to a higher fragmentized degree. To quantify the frag­
nique. The size distribution was measured by sieving and weighting the ment size distribution characteristics, the sieving curves of recovered
debris and is known as the fragment mass distribution [37,53], and the specimens with different loading rates and rubber inclusion parameters
sieve size was determined as 0.075 mm, 0.25 mm, 0.5 mm, 1 mm, 2 mm, are illustrated in Fig. 13. For a given rubber percentage and size, i.e.,
5 mm and 10 mm. It is observed that the percentage of larger fragments 10% rubber percentage and 40 mesh rubber size, the median diameter
significantly reduces with the increase of the loading rate. Due to the d50 of the recovered fragments, is reduced from 17.85 mm to 6.18 mm
inefficient time allowing crack propagation along the tortuous granular within the loading rate range of 1161 GPa/s to 2867 GPa/s, almost
surface under the higher loading rates, more microcracks are formed and reduced by 2/3. When the rubber percentage changes from 0% to 40% at
transgranular fracture is dominant [64,68]. Besides, as mentioned a constant rubber size and loading rate, the parameter d50 drops from
earlier, adding a higher percentage or smaller size of rubber powder 9.91 mm to 8.53 mm with a reduction of nearly 14%, whilst only a
contributes to more ITZs. These ITZs serve as weak planes to provide decrease of approximate 7% is observed when the rubber size changes
primary propagation paths for newly created cracks under impact loads, from 40 mesh to 120 mesh at a similar loading rate of ~2100 GPa/s and

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G. Yang et al. Powder Technology 420 (2023) 118376

w
w

Fig. 10. Dissipated energy density for rubberized mortar at different loading rates and rubber sizes with various rubber volume fractions.

Fig. 11. Failure snapshots of (a) rubberized mortar (20%, 40 mesh) with different loading rates (b) rubberized mortar (40 mesh, ~ 1390 GPa/s) with different
inclusion percentages and (c) rubberized mortar (20%, ~ 1550 GPa/s) with different rubber sizes.

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G. Yang et al. Powder Technology 420 (2023) 118376

Fig. 12. Recovered fragments of tested rubberized mortar with (a) different loading rates, (b) rubber percentages and (c) rubber sizes.

Fig. 13. Size distribution of recovered fragments from the rubber mortars at different loading rates and with different rubber volume fractions and sizes.

rubber percentage of 10%. Therefore, the loading rate has the most mode, energy absorption capacity and fragment size distribution char­
significant effect on the fragmentation characteristics, followed by the acteristics are comprehensively analyzed. The findings from the current
rubber volume fraction, whereas the rubber size acts a relatively limited work can be briefly summarized as follows:
role in affecting the size distribution characteristics of the recovered
fragments. (1) The dynamic compressive strength of the rubberized mortar in­
creases with the loading rate and rubber powder size but declines
4. Conclusions with increasing the rubber volume fraction. The maximum
reduction of 27% in strength is observed when the rubber per­
In this work, the dynamic compressive behavior of homogeneous centage is 40% and rubber size is 120 mesh, which is much
rubberized mortar with different rubber volume percentages and pow­ smaller than those of the dynamic strength reported for the
der sizes was studied. The SHPB apparatus in conjunction with the rubberized concrete in previous studies.
momentum-trap technique was used to conduct the dynamic compres­ (2) The dynamic increase factor linearly rises with both the loading
sion tests, based on which the dynamic strength, DIF variation, failure rate and rubber volume fraction but shows weak dependence on

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