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Certificate of Analysis
Product Name: Acetic acid
glacial, puriss., meets analytical specification of Ph. Eur.,
BP, USP, FCC, 99.8-100.5 %
Product Number: 27225
Batch Number: SHBL6735
Brand: Sigma-Aldrich
CAS Number: 64-19-7
Formula: CH3CO2H
Formula Weight: 60.05
Quality Release Date: 15 SEP 2017
Date retested: 28 JAN 2021
Recommended Retest Date: JUL 2024

TEST SPECIFICATION RESULT

ASSAY 99.8 - 100.5 % 100.2 %
FREEZING POINT ≥ 15.6 DEG C (CONGEALING) COMPLYING
RESIDUE (EVAPORATION) ≤ 0.01 % < 0.01 %
APPEARANCE COMPLYING COMPLYING
REDUCING SUBSTANCES COMPLYING COMPLYING
KMNO4 RED. MATTER (AS HCOOH):
≤ 0.01 % < 0.01 %

REDUCING SUBSTANCES COMPLYING COMPLYING

KMNO4 RED. MATTER (AS HCOOH):
≤ 0.01 % < 0.01 %

RESIDUAL SOLVENTS COMPLYING COMPLYING

HEAVY METALS ≤ 0.0002 % (AS PB)  0.0002 %
MISCELLANEOUS TESTS IDENTITY USP: COMPLYING COMPLYING
ALUMINIUM ≤ 0.00005 % < 0.00005 %
COPPER ≤ 0.0005 % < 0.0005 %
IRON ≤ 0.0002 % < 0.0002 %
LEAD ≤ 0.00005 % < 0.00005 %
ZINC ≤ 0.0005 % < 0.0005 %
CHLORIDE (CL) ≤ 0.0002 % (COMPLYING) < 0.0001 % (COMPLYING)
SULFATE (SO4) ≤ 0.0005 % (COMPLYING) < 0.0001 % (COMPLYING)
REMARKS IDENTITY, ASSAY AND IMPURITIES ARE COMPLYING TO THE MONOGRAPHS
OF THE ABOVE MENTIONED PHARMACOPEIAS/CODICES

Claudia Mayer
ManagerSigma-AldrichQualitywarrantsControlthatatthe time of the quality release or subsequent retest date this product conformed to the information contained in this publication. The current

Steinheim,specificationsheetGermanymaybe available at Sigma-Aldrich.com. For further inquiries, please contact Technical Service. Purchaser must determine the suitability of the product
for its particular use. See reverse side of invoice or packing slip for additional terms and conditions of sale.

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