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Lab Report PDF
Lab Report PDF
Laboratory Report
On
Coagulation and Flocculation
Lab Date: March 06th, 2024
Lab Group Number: 04
Module Leader: Reginald Kogbara
Disclaimer: This report is prepared and presented as the original work of the student and has not
been copied or plagiarized in any way. It is submitted as solely my work in partial fulfilment of the
requirement of the course GEEN-1148-M02-2023-24. I understand the university’s plagiarism
policy and accept responsibility for every plagiarism charge where existent in this document.
Table of contents
1. INTRODUCTION……………………………………………………………………….3
2. AIM………………………………………………………………………………………3
3. APPARATUS…………………………………………………………………………….3
4. EXPERIMENTAL PROCEDURE………………………………………………………6
5. COAGULATION (RAPID MIXING)…………………………………………………..9
6. FLOCCULATION (SLOW MIXING)…………………………………………………10
7. CONCLUSION AND RECOMMENDATIONS……………………………………....12
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INTRODUCTION
Access to clean and safe drinking water is essential for human health. To ensure that water is safe
for consumption, it must undergo a treatment process that involves coagulation and flocculation.
During coagulation, coagulants are added to break down colloidal particles and cause them to
aggregate into larger flocs. Flocculation induces the formation of even larger flocs, which can be
quickly removed through sedimentation or filtration, eliminating suspended particles, colloids,
and other contaminants from the water.
AIM
The aim of this laboratory is to study flocculation and coagulation mechanisms, assess their
effectiveness in reducing turbidity, and determine the settling of flocs before as well as after the
experiment.
APPARATUS
1. Flocculation Digital Jar Testing Machine
The equipment is made of six stirring units, each of which has a timer and a motor-
driven mechanism with controlled speed settings.
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2. Measuring Jars
For this experiment, four measuring jars with a 1-litre capacity are being used..
3. Turbidity Meter
It is used to calculate the turbidity of the water samples before and after the experimental
process.
4. Water Sample
Surface-flowing stormwater and tap water are collected as water samples for this
experiment.
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5. Coagulants
Aluminium and ferric (iron) chloride are common coagulants used in the jar test. Iron
chloride is the coagulant used in this experiment.
6. Weighing Machine
This machine is used to weight the amount of iron added in the water sample
7. pH Paper
pH paper is used to check the pH level of the water samples.
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EXPERIMENTAL PROCEDURE
Several steps are involved in the experimental process for the coagulation and flocculation of the
water sample.
Step 1: 250ml of surface-running stormwater water sample is taken in each measuring jar.
Step 2: Next, we need to figure out the pH values of the given tap water and stormwater
sample from figure 9
Step 3: As part of the experiment, it's important to determine the turbidity of the
water sample both before and after testing. To do this, we need to calibrate the
turbidity meter using standard samples. Align the arrow on the turbidity meter and
take readings with at least two turbidity standard samples to ensure accurate
calibration.
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Figure 10: Calibration samples alignment and test readings.
Step 4: Note the readings which are closest to the turbidity meter's standard values
are acceptable. The table below explains the turbidity values which are obtained
during the experiment. Therefore, the turbidity meter's calibration is completed. To
verify the calibration, we can repeat a few of the standard samples and compare the
results.
Step 5: To identify the turbidity value of the sample water collected in four beakers,
we need to fill the sample testing water in a cleaned cuvette (a circular cross-
sectional small container) up to the marked point. The figure below shows the
experimental procedure.
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Water Sample Turbidity readings
before settling
Beaker No. 5 2.25 NTU
Beaker No. 6 1.53 NTU
Beaker No. 7 1.72 NTU
Beaker No. 8 1.65 NTU
Tap water 0.31 NTU
Table 2: Turbidity readings of water samples before settling.
Step 6: After finding the turbidity of the water sample, coagulant is added to the
water samples in different beakers with different amounts. In this experiment, Iron
chloride is used as a coagulant and added to the water sample collected in different
beakers. The table below explains the amount of coagulant added to the sample.
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COAGULATION (RAPID MIX)
Coagulation is a chemical process that is commonly used in water and wastewater treatment
facilities to remove impurities such as suspended particles and colloids from the water. The process
involves adding coagulants such as aluminium sulfate (alum), ferric chloride or polyaluminium
chloride to the water. These coagulants work by neutralizing the electrical charges on the suspended
particles, which causes them to destabilize and come together to form larger aggregates known as
flocs.
Here, table 3, shows the quantity of coagulants added to the water sample.
These four beakers are placed below the four stirring units, the blades are immersed in the water
samples.
This experimental procedure of coagulation is a fast-mixing process, For this experiment, a timer
was used to mix the coagulation process for 1 minute. For this process, a minimum speed of 25 rpm
is required. However, for this test, the speed has been increased to 150 rpm.
The following formula can be used to calculate the velocity gradient (G-1):
G-1 = 2* TT* N
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FLOCCULATION (SLOW MIXING)
Usually, flocculation occurs after coagulation. Chemicals like alum or ferric chloride are
added during coagulation to neutralize the charges on suspended particles, which helps them
to stick together. To encourage these neutralized particles to collide and form larger flocs,
gentle mixing takes place during the flocculation stage.
However, in this case, the coagulant is mixed into the water sample at a lower speed for a
longer period.
As shown in the table below, the coagulant is added to the water sample in this experiment
at various rates.
TIME ROTATIONAL
SPEED(RPM)
5 min 100
5 min 50
5 min 20
Table 4: Slow mixing speed unit
Following the process of mixing the coagulant and water sample at varying speeds for a
certain period, the samples are set aside for approximately one hour to settle down.
After an hour, now note the turbidity readings of the water samples are shown in the table
below.
Water Sample Turbidity readings after
settling
Beaker No. 5 3.59 NTU
Beaker No. 6 2.36 NTU
Beaker No. 7 2.86 NTU
Beaker No. 8 2.92 NTU
Tap Water 0.30 NTU
Table 5: Turbidity readings after settling
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Determine the power required:
Therefore, the power required for mixing the sample is 0.000855 Watts.
Figure 15, shows the settling down of floccs at the bottom of the beaker and the colour of the water
being changed due to the dosage of coagulants added to the sample.
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CONCLUSION AND RECOMMENDATIONS
According to the results, after experimenting, the turbidity values of water samples have increased
(as shown in Table 5), following the process of settling. Ideally, after settling, the turbidity values
should be lower than the values obtained before settling (as shown in Table 2). Due to some
conditions, this may occur those are:
1. Settling time: The duration of the settling period allows sufficient time for
coagulated particles to settle out of the water. Longer settling times generally result
in lower turbidity levels as more particles are removed from the water.
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