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1 s2.0 S0957582023003762 Main2
1 s2.0 S0957582023003762 Main2
1 s2.0 S0957582023003762 Main2
A R T I C L E I N F O A B S T R A C T
Keywords: In textile industries, a lot of wastewater are discharged which are one of the major environmental pollution
Textile industry problems, because they release undesirable dye effluents. Owing to re-dyeing procedures performed to meet
Re-dyeing customized color specifications, environmental pollution is a serious problem because of the emission of large
Right-first-time
volumes of wastewater. To solve the environmental problems caused by re-dyeing, the right-first-time (RFT) %,
Exhaustion rate meter
Multi-layer perceptron-based prediction
which is the rate at which the target quality is obtained with just one dyeing, must be increased by considering
the dyeing conditions that affect product quality. Here, this study suggests a framework for cleaner production of
textile dyeing process using novel exhaustion-rate meter (NERM) and multi-layer perceptron-based prediction
model to solve the environmental problems caused by re-dyeing procedure by controlling the exhaustion-rate
outliers. The proposed NERM measures the exhaustion-rate based on absorbance of the dyeing solution and is
composed of measuring and analysis section. The dyeing solution absorbance is metered in the measuring
component through a detector, which performs high-resolution measurement (0.3–1.5 nm full width at half
maximum) via a 25-μm slit in the 200–1100-nm wavelength range; the absorbance is then converted to the
exhaustion-rate based on Beer’s law in the analysis section. Using the NERM, an exhaustion rate dataset ac
cording to the Na2SO4 and Na2CO3 consumption is acquired and a surrogate model that augments the exhaustion
rate data is developed. The MLP-based prediction model is then developed using the augmented data to control
the real-time exhaustion-rate outliers. As a results, the model performance as regards Na2SO4 and Na2CO3
prediction is indicated by R2 values of approximately 0.985 and 0.998, respectively, and root mean squared
errors (RMSE) of approximately 1.477 and 1.000, respectively. In addition, the effectiveness of the proposed
framework is demonstrated through application to several scenarios in which the real-time exhaustion rate
outliers are detected.
* Corresponding authors.
E-mail addresses: sungsu@cnu.ac.kr (S. Lim), kjh24@yonsei.ac.kr (J. Kim).
1
Soohwan Jeong and Jonghun Lim contributed equally to this work as first authors.
https://doi.org/10.1016/j.psep.2023.05.009
Received 22 July 2022; Received in revised form 30 March 2023; Accepted 2 May 2023
Available online 8 May 2023
0957-5820/© 2023 The Authors. Published by Elsevier Ltd on behalf of Institution of Chemical Engineers. This is an open access article under the CC BY-NC-ND
license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
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S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
1.2. Contribution
2. Process description
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S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
are a mixture of dyes, metals and other pollutants and it are high in of a measuring section to measure the dye absorbance at regular time
colour, pH, suspended solids (SS), chemical oxygen demand (COD), intervals and an analysis component to analyze and display the
biochemical oxygen demand (BOD), metals and salts. Table 1 is the measured data on a monitor. The measuring section is composed of a
typical characteristics of dyeing wastewater according to difference filter, a pump, a circulation line through which the dye is circulated, a
references. lamp as a light source, and a detector. The filter removes impurities such
Table 1 shows the textile dyeing wastewater contains high environ as fiber particles from the extracted dye to measure the absorbance of
mental pollutants. In addition, most of these wastewater persist in the the dye itself, and the pump continuously circulates the dye through the
environment as a result of their high stability to light, temperature, circulation line. The circulate line is made of a material that allows
water, detergents, chemicals, soap and other parameters such as bleach measurement in the ultraviolet/visible range at a wavelength range of
and perspiration. Thus, the wastewater from dyeing process causes 200–750 nm. This material has high heat resistance, pressure resistance,
significant water pollution. Therefore, if the re-dyeing is required, the chemical resistance, and 0.55-mm penetration length. A pulsed xenon
wastewater is significantly increased compared to a one-time dyeing. To lamp is used as the light source to allow stable measurements over a
solve the problems associated with re-dyeing, it is necessary to improve wavelength range of 220–750 nm. The detector can measure the dye
the right-first-time (RFT) %, which is the rate at which the target quality solution at a high resolution of 0.3–1.5-nm full width at half maximum
is obtained with just one dyeing, this can be achieved by considering the using a 25-μm slit over a wavelength range of 200–1100 nm. The
dyeing conditions that affect product quality. analysis component converts the real-time spectrum of the dye
measured in the measuring section to the exhaustion-rate and displays
3. Methodology the result in real time.
The dye adsorption rate in the proposed NERM is calculated as fol
In this section, we describe the types of dyes used in the dyeing lows. Generally, when a single dye is used for cotton fabrics, the dye
process (Section 3.1) and the NERM developed to measure the real-time concentration can be determined by measuring the dye absorbance. The
exhaustion behavior (Section 3.2). The actual data measured with this relationship between the dye absorbance and concentration is expressed
meter are applied to an artificial neural network to derive surrogate by Beer’s law as follows (Fernández-Pérez et al., 2019):
models for data augmentation (Section 3.3). Using these surrogate
A=ε×l×C (1)
models, we develop the abovementioned MLP-based prediction model to
control the exhaustion-rate outliers; this model predicts and adjusts the Where,
additional Na2SO4 and Na2CO3 input amounts in response to the specific A = Absorbance.
conditions that do not follow the optimal exhaustion-rate curve (Section ε = Molar attenuation coefficient.
3.4). Finally, the model performance evaluation is discussed (Section l = Optical path in length.
3.5). C = Concentration of the attenuating species.
The absorbance and concentration of a mixture containing n types of
3.1. Dyeing materials dye can be expressed by the following equation:
A 100% cotton fabric was used as the dyeing substrate. The neutral An = k1 × C1 + k2 × C2 + ⋯ + kn × Cn (2)
salt and alkali were Na2SO4 and Na2CO3, respectively, both of which
were extra-pure reagents. In the dyeing process, Na2SO4 was first added Where,
in 10%, 30%, 30%, and 30% proportions at 3-min intervals, and Na2CO3 k = ε × l.
was added in a single batch at the 40-min mark. Novacron Blue ECR (NB When there is no interaction between the dyes, the absorbance
ECR) was used as the reactive dye, the chemical structure of which is spectrum of the mixed dyes is calculated as the sum of the absorbance
shown in Fig. 3 (Lingeswari and Vimala, 2019). spectra corresponding to the concentration of each dye:
[An ] = [k1 ⋯kn ] × [Cn ] (3)
3.2. Novel exhaustion-rate meter (NERM)
When the dye concentration is low, it can be easily estimated from its
linear relationship with the absorbance. However, the relationship di
The NERM was developed to satisfy the two most important factors
verts from Beer’s law when the dye concentration is high, and the in
influencing dyeing quality, i.e., the color difference and dyeing unifor
dividual spectrum of the n dyes combined is then applied to Eq. (3) to
mity, and ultimately, to improve the RFT. The developed NERM mea
calculate the dye concentration at a certain point in time. Finally, the
sures the final exhaustion-rate as well as the real-time exhaustion
dye concentration at a specific time is substituted into the following
behavior of the dye, such that the RFT can be increased through optimal
equation to determine the exhaustion-rate of each dye:
control.
Fig. 4 is a simplified diagram of the developed NERM, which consists [Cn ]
[En ] = 1 − (4)
[Cn,0 ]
Table 1
Typical characteristics of dyeing wastewater according to difference references. Where,
References Ghaly et al. (2014), Kehinde and Hussein Unit
En = Total dye concentration.
Ghaly & Ananthashankar Aziz (2014) (2013) Cn = Dye concentration at specific time.
(2013) Cn,0 = Initial dye concentration.
Colour 50–2500 50–2500 - Pt-
Co
pH 6–10 6.95–11.8 5.5–10.5 - 3.3. Prediction model to control exhaustion-rate outliers
SS 15–8000 15–8000 100–5000 mg/
l
This section describes the development of the proposed prediction
COD 150–12,000 150–30,000 150–10,000 mg/
l model to control the exhaustion-rate outliers. This prediction model
BOD 80–6000 80–6000 100–4000 mg/ provides operators with guidelines to control the dyeing process when
l the real-time exhaustion rate does not follow the optimal exhaustion-
Metals and <7105 437–2242 610–2175 mg/ rate curve. Specifically, the model suggests additional Na2SO4 and
salt l
Na2CO3 inputs when an outlier which does not follow the optimal
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S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
exhaustion-rate curve arises. The MLP regression algorithm is used to ordinary linear functions, a linear estimation function, y = wT x + b,
determine the relationship between the exhaustion rate and certain must be considered. In the MLP approach, an activation function is
conditions (time, temperature, and Na2SO4 and Na2CO3 input amounts). introduced to the linear estimation function to solve nonlinear
Fig. 5 shows the development procedure of the suggested MLP-based functions.
prediction model to control the exhaustion-rate outliers. Each section Fig. 7 shows the MLP calculation process. Here, x1 …xn are input
of the figure is discussed in the following subsections. In detail, Section vectors, ω1 …ωn are weights corresponding to each input vector, and b
3.3.1 describes the overall concept of MLP application to regression represents the bias. The weighted summation based on the input vectors
analysis. Section 3.3.2 describes the data generation (Fig. 5, Step 1) and weights is applied to the activation function, f, and the result be
through the NERM and the data preprocessing (Fig. 5, Step 2), and comes the input for the subsequent hidden layer or output unit. In the
Section 3.3.3 describes the construction process of a surrogate model MLP approach, a back-propagation procedure is usually performed by
that predicts the exhaustion rate under certain conditions using the reversely differentiating the activation function from the output layer to
preprocessed data (Fig. 5, Step 3). Section 3.3.4 explains the exhaustion- the input layer, to reduce the error between the value from the final
rate data extraction processes for numerous cases using different con output layer and the actual output value. The commonly used activation
structed surrogate models; the development of the prediction model to functions are ReLU, sigmoid, and tanh (Eq. (5)):
control the exhaustion-rate outliers is also described (Fig. 5, Steps 4 and
ReLU(x) = max(0, x)
5). Finally, Section 3.3.5 presents the regression model performance
indicators. 1
sigmoid(x) =
1 + exp( − x)
3.3.1. Multi-layer-perceptron (MLP) regression algorithm
MLP is a machine learning method in which computers form an exp(x) − exp(− x)
artificial neural network similar to the human brain. Recently, MLP has tanh(x) = (5)
exp(x) + exp(− x)
demonstrated superior performance in various industries by processing
not only structured, but also unstructured data related to computer Regarding the MLP experiment, we used Python 3.7.7 version, ten
vision, voice recognition, natural language processing, signal process sorflow 2.1.0 version, keras 2.8.0 version, and additionally scikit-learn
ing, etc(J. J. Lee et al., 2021; Y. Lee et al., 2021; Mikolov et al., 2013; 0.23.2 version.
Roh et al., 2021; Sangeetha and Prasad, 2006; Sukanya and Sunny,
2019). 3.3.2. Data generation and preprocessing
Generally, an MLP structure consists of an input layer, hidden layer, For the experiments performed in this study, a total of 615 data
and output layer. This structure is referred to as a deep neural network points were extracted using the NERM. Four data attributes were
when there are three or more hidden layers, as shown in Fig. 6. To solve considered: time, temperature, Na2SO4 input amount, and Na2CO3 input
amount. There were time, ranging from 0 to 120 min at 3-min intervals,
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S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
Fig. 5. Development procedure of suggested multi-layer perceptron (MLP)-based prediction model to control exhaustion-rate outliers.
and the temperature varied to certain set values over time. Three the corresponding data were eliminated. The remaining dataset after
Na2SO4 input amounts were considered, i.e., 10, 30, and 50 g, along preprocessing contained 41 (time) × 3 (Na2SO4) × 4 (Na2CO3) = 492
with five Na2CO3 input amounts, i.e., 0, 5, 10, 15, and 20 g. Data pre data elements.
processing was largely performed in two steps. In the first step, any data Data normalization was performed because the scale of each attri
unnecessary for the regression model learning process were removed. In bute value in the dataset varied widely; that is, 0–120 min; 30–60 ◦ C;
the second step, data normalization was performed because the units 10, 30, and 50 g; 5, 10, 15, and 20 g; and 0.0–0.957% for the time,
varied by data attribute according to different value scales, which hin temperature, Na2SO4 input, Na2CO3 input, and final exhaustion attri
dered the learning process. butes, respectively. Among the various normalization techniques, the z-
In the dyeing process, the Na2CO3 fixes the dye onto the fabric by score normalization method was chosen to robustly process the data in
forming covalent bonds between the two. In the experiments performed the presence of outliers. In the z-score normalization approach, the
herein, no trend was observed for an Na2CO3 input amount of 0 g; thus, mean and standard deviation of the values for the same attribute are
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S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
differences between the predicted and real values of the model. molecules already absorbed by the fabric were becoming fixed through
covalent bonding, while the dye molecules in the solution were also
∑
n
(yi − ̂y i )2 being simultaneously absorbed by the fabric. This process is referred to
MSE = i=1
(10) as “secondary exhaustion.” Section 4.2 describes the surrogate model
n
constructed using the data measured by the proposed NERM.
Here, MSE is obtained by calculating the mean following addition of
the square of the differences between the predicted and real values of the
model, which can be considered as the mean of the area of the differ 4.2. Performance of surrogate model for data augmentation
ences. Given this difference from MAE, the presence of an outlier yields a
large MSE value. This section reports the performance evaluation of the surrogate
√̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ model constructed using the MLP-based regression analysis described in
√∑
√n Section 3.3.3. The training and test datasets were split at a 0.75:0.25
√ (yi − ̂y )2 ratio to build the regression model, and RMSE and R2 were used as
√
RMSE = i=1 (11) performance indicators. To demonstrate the MLP performance, well-
n
known regression analysis methods, i.e., lasso, ridge, and support vec
As apparent from the equation, RMSE is the square root value of MSE tor regression, were applied to identical datasets. Each model was sub
and, thus, its interpretation is simplified by reconverting the unit of the jected to 100 regression experiments and the training and test data were
error indicator to that of the real value. Although similar to MAE, RMSE randomly varied each time. The performance of each regression model
is more robust. This is because, for MAE, the total sum is divided by n; was compared in terms of R2 and RMSE. Table 2 lists the mean and
√̅̅̅
however, for RMSE, the total sum is divided by n. Thus, a penalty is standard deviation values obtained for the 100 experimental results for
applied in the case of a large error. each model.
∑
n From Table 2, the MLP regression exhibited the highest performance
y i )2
(yi − ̂ and the smallest error, with MAE, MSE, RMSE and R2 values of 0.007,
SSR SSE
2
R = = 1− i=1
= 1− ∑ n (12) 0.001, 0.016 and 0.994, respectively.
SST SST
(yi − y)2 Fig. 9 shows a comparison between the actual exhaustion-rate values
i=1
of dataorigin (x-axis) and the predicted values obtained from the MLP-
Here, the total sum of squares (SST)is expressed as y − y and indicates based regression model (y-axis). The solid red line is the y = x trend
the total deviation, the regression sum of squares (SSR) is expressed as line. The values generally fall on this line, indicating the high perfor
y − y and indicates the deviation described by the regression equation,
̂ mance of the MLP regression model.
and the error sum of squares(SSE) is expressed as y − y and indicates the Fig. 10 shows the exhaustion-rate behaviors over time for different
deviation that is not described by the regression equation. The other Na2CO3 and Na2SO4 input amounts, where the solid lines ( − ) indicate
performance indicators can vary widely in value depending on the data the actual values and the triangles () indicate the predicted values from
scale, making performance evaluation based on absolute values difficult; the SMNa2SO4 surrogate model. Fig. 10(a)–(d) correspond to the cases for
however, R2 indicates the performance of a regression model in relative which the Na2CO3 input amounts were 5, 10, 15, and 20 g, respectively.
values and, thus, the interpretation is intuitive. It is apparent that the regression-based surrogate model was in good
agreement with the exhaustion behavior over time. Hence, the surrogate
4. Results & discussion model defined using the actual dataset can be considered reliable.
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Table 2
Performance of each model.
Regression model MAE MSE RMSE R2
Lasso regression 0.068 ± 0.005 0.013 ± 0.003 0.110 ± 0.015 0.726 ± 0.040
Ridge regression 0.068 ± 0.006 0.012 ± 0.003 0.273 ± 0.020 0.723 ± 0.037
Support vector regression 0.125 ± 0.025 0.105 ± 0.045 0.066 ± 0.017 0.902 ± 0.035
MLP regression 0.007 ± 0.002 0.0001 ± 6.06E − 05 0.016 ± 0.006 0.994 ± 0.004
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Fig. 10. Actual and predicted using SMNa2SO4 values for real-time exhaustion behaviors for different Na2CO3 and Na2SO4 input amounts.
Fig. 11. Plot of predicted vs. actual values for Na2SO4 inputs. Fig. 12. Plot of predicted vs. actual values for Na2CO3 inputs.
Through this model, solutions that conform to the optimum exhaustion economic improvement and provide valuable insight of cleaner pro
behavior can be suggested directly; thus, proper and immediate control duction in textile dyeing process. In this work, the outliers which
is possible and the need for re-dyeing is prevented. Thus, since the re- incurred according to the Na2CO3 and Na2SO3 input amounts is only
dyeing procedure is prevented through the suggested framework by considered. However, the other operating conditions such as dye ratio in
increasing right first time %, it will have great environmental and the dyeing solution, input time of Na2CO3 and Na2SO3, etc. are also
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S. Jeong et al. Process Safety and Environmental Protection 175 (2023) 99–110
Table 3
Conditions for scenarios of Fig. 13.
Table 5
Classification Scenario 1 Scenario 2
Conditions for scenarios of Fig. 14.
Time (min) 21 24
Classification Scenario 3 Scenario 4
Temperature (℃) 30 30
Na2SO4 input (g) 50 30 Time (min) 54 78
Na2CO3 input (g) 10 20 Temperature (℃) 59 60
Optimal exhaustion rate 0.682 0.702 Na2SO4 input (g) 10 30
Exhaustion-rate outlier 0.58 0.55 Na2CO3 input (g) 20 10
Optimal exhaustion rate 0.849 0.917
Exhaustion-rate outlier 0.75 0.82
Table 4
Na2SO4 inputs determined from PMNa2SO4.
Table 6
Classification Scenario 1 Scenario 2
Na2CO3 inputs determined from PMNa2CO3.
Time (min) 21 24
Classification Scenario 3 Scenario 4
Temperature (℃) 30 30
Na2CO3 input (g) 10 20 Time (min) 54 78
Exhaustion-rate outlier 0.58 0.55 Temperature (℃) 59 60
Predicted Na2SO4 input (g) 25.877 11.051 Na2CO3 input (g) 20 10
Suggested additional Na2SO4 amount (g) 24.123 18.949 Exhaustion-rate outlier 0.75 0.82
Predicted Na2SO4 input (g) 9.896 6.174
Suggested additional Na2SO4 amount (g) 10.104 3.826
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