ay Designation: E415 14 Standard Test Method for Analysis of Carbon and Low-Alloy Steel by Spark Atomic Emission Spectrometry" 1. Scope 14 Thies mato covers he shia eternton 30 alloying ond resid let carton a Towa ‘ose by spark stone cision vacou sperm te ss acing ages shows (Na. met gnc * at ‘Seach ees mci 1.2 This test met covers aba of specimens ving Sameer ada eas aloe The pak Nag stan pening. The specimen hicks can vary sige ‘coring 10 the ign of the gecomeler stan, Bi & ‘sets btw 10m a8 oon he ee fun a be 13 This tet method eaves he ine contol anys a ‘ro an tesa operations el he aap of woe Ite His dng for shikai a fog Specimen Beker performance xpd whe sls ‘ral ul pci ofr call coon soa, Hower Honea pe 14 This snd does ox prot to aes al of te sefy concern ety aod with ma. fe reponse ur of hi sana! etal app Prt oes and heats pacts dane te ae I of eur oso pre se, 2 Referenced Documents 211 ASTM Sundae? 138 Teminlogy Relating w Amiyical Chany fo Mots Or a Keats Moa EMS Practice for Esblsing and Contling Atomic "Enso Secochemcl Arya Cues, EIS) Test Methods ue Chea Anas of Caton Sts {Low-Alloy Stel, Seon Ele Sl gt to, a ‘rot fon 0s Pracice fr Using Cooled Atmosphere a Spee IDI Test Mend oe Detrntion of Caton Sl, "Nargen, and Orypen in Sco, Nike, nl Cobalt ‘Alloy by Vrous Carbon a! Fn Tig 11325 tie for Veto ard Uso Cnt Cha Specocericl Anas lat Pate for Condi w Insherry Stay © tres Guide fr Inert td Ue of Ress fom Tntratesry Teng of Chena Asis MatosGh ens 18D Practise for Sampling te non for Deteina- thon of Chemeal Conpstine 19M Pate foe Reqering Rests fom Metts of (Choma Analy ‘ASTM NN? Ma a Prescton of Data and Conte ‘Chart Amis 111 or defn tems asl is est meta ero ‘emonogy E13, 4 Summary of Test Method 41 A capacitor dluge ie pode Rewer the Ma ound foc af the dak sien comes shaped Soe Te daca teminaelat pedi Sn tine nerf slete on ito a pet ‘ned an he late ant ener th aye Tae records The os seine Hic fase, ‘arto toga a in ie nthe ec ‘kre The orp fhe aan yn ‘evn evs fy enacting he spestometer a In he sp che with argon 5 Sites and Use 51 Thiet metre pecan of nts aod ays ply tosh a for Strut lh conposion! seieains ttn Sa oe atl lb ms cae pefrag secon ory promower acy sod Tehri ened tt work wl pred na oy cope hoy. Song Doses Li Rare Pace £1806 fo deve ad pra 0 ssn don ma ee 2 Eston Sec, ape of roving ial po aoa spat spe ST! ae 3 Spr Chamber aol id wih sg, The souk camber sal mou dy pes ‘Mihae prove wih asp sun oble Arn fi we sone estos of a om “31 Fallow the namics meommendton for chasing ei chante (un nts opt ‘yay el te dine cosy 0), Fle ool {Tojo ar Cen ens owao (ite tn oie fem sane meaty da Spey nowt when cy. 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The tipo syn al beacon with Price EAD, 7 Reagents and Materia 7.1 Gomer Eleces—The cnr cecrades can te ste va age dl oe ar pod {anf shovm experimental ta eave pression nd at ‘imo rca ty eter en 5 a 6S tn epi en thinset mance) a pally SS machined 90" or IX ane "LL Abuck dep wil colton he ipo the cle Ths dept sald be removed Paes specimens ply thief Ig monet san rede th evel Isa he eps ado waste sgh amos a nso Bence species: Bb. The eae of ‘Sceple exc o aed vares toma as ‘nt aan shold fe sash nec abt Livers oem 72. ner Ga, Ago, core wit Price Ea, Reference Materia Cored Reference Mae (CRM) These wal abe mt Natal Ista Studs ad echlogy (NIST) er sources an pm lo pt of the ms {rv sunges ine 1 'They be ed era the Spostomet forthe slew tres oo ae the Fextrmane ofthe ot th. i ot spanner oe Era ca ae ie py oe {CMe an poston sample pep by the sani roses icone is fe mt Cea no's tr example, sf ation may we to BeQy ens oct wih asm refrence rials nde y noma pec anges ore yest Ne 12 Referee terial kM} ae ase fom ‘nape supers se canbe despa in home, RM ae ‘ply ese o coal (erin am if ra tan ‘is the pectometor "Thos eon atl al fe Impenman aod erin apes sorpestons of ch lame econo rd cera 9. Preparation f Species and Refeene Materials 9.1 The apc and efrne ra mute pred inthe sme mane.“ specie at fen age sale ‘con mst eof sli se snl ices er repeat fine peopel the spectrometer san 1-0 Sena ‘tet specs i aly! pte 92 Eset speinens ze fe fom voi pis in he repo ob xc (No) stl gr th sae wh {AML + wal Stand oN es TABLE 20m Aneya i igo Dit baie lode (et oy) he ial gr wth dry above ft dc ane ‘nding as (oe example [Dg ay te a or oe nl pin its ‘use eruci ned by ch 921 Reference atria an pecs nt efi sry van aie fie Be ei osc ie uti ep my lh 10.1 Program te spectometer acon he ner stan is sl i the sai! eso ch leet liste in abe. alpen ay be sd Tor pen lene er eae ikl depentng on hema rn tango an the nial ses tae ‘noi ce rhea a a ps 10.2 Tet te pstning of te yen ence io ir tht pea radian cig the spine chm te This she dane aly as fen ea a ‘mamtain poe ete sit sar. ello te ant tier’ ommend proce The bry wll ne the fags of posing the alee saMy esrs—14 Siesta esos: 1, Exciaton and spose 1 lec! Parameter: 1L Txeton parame se normally stabi by theyre Th allowing anges eis tel phn nd newer uments my 2 om Ds. 1112 Whom purmetr acs are establish, mann ‘tem cacy, The vari a power supply voluge ll ose and peters hel win = 2% WL} fino Cede iar eat frat shal be af ounsloriy wigs he cancer dag ‘The following stings veil ilies and newer AA Or etc Parner Escation wis, on ‘whch hep armor enn TI and 113 a ‘lhe may Rew provided at cat be sown exp ‘neal at ule pecan ad aecuuy ar out. te flowing anges ate ne nly aoe: TILL Sle brand expose pti sty of volavaton ate during specimen excitation. Once ‘Shia obin he parameters cost T22 A hpiegy gon steer esi the aly pap Molar ge ipriies,ogen. ox} 0, ‘breton or war vp eter nthe pss om apeoperty pcp pce ald Ye mid 113 Bleciade Syvem-—The specimen, electrically epee so lee THe apport eco 2 Ah egston or sr a eo which ha he ocho 90° 120" ale eo Use he 3 fm, 3mm (=r) altel sp. Cao Us ‘Sur lest wth wo to xcetions wing he ope Ine conn descr Ian 12 14 Photomliper PetatTe sensi othe po- ‘oot smal ais and ty te spe ‘Serimanufcerbe te partway lee THs The rane of anode cae potas era es tue shal be sete, at 0 Vt 1000 V Se tinh el ange te ae eer too serie 0 Tene forthe comet concentration range sl ster Foti. The pres on he caps may fe read Gras oa sumber of ec redn systray be ‘Sloped whch ii ear or fg nto othe foveal wch ray be pied ive erer 1 12, Calieton, Standardéation, and Veriton 121 Cala —Using the condo given in 1.1 = 11 cox calivantan otal eee aes a {ros seq, bliss sean vl nnda Yor ein (8 vee Be ed ‘calranevn ap is ara ny vere) Thee $a eas he cian frac element spn he ‘eed concmaton rage Etc exch elvan, i a ‘bn samp and erir two fortes and ae Be Sere vale. Ifthe spcoaee Ys abd ste ery repent wih ia onc soqencr a tt Mes Uist he verges of the dt foreach pois dtr Seni hrves a ted he oposite neta Snare or rtoe E05, 122 Sandanistion-Following the manufacturer's srcommeniaion samirne on ti tuo aye Tris Kor aud a regs ave ied ke Tenssseny cots eer y satin ts onl on he ‘alt ry spp sits crectone Standard {roe done yin verison ts hat eaings have 123 Vein Mei that ras stand ois lsd sation an T'S Alyce sconce wth Sato 1.1 ss dot al win he conse a1, tom ant wrath henson ‘ny he maui Tanz Each hry sll daeine the oeey of sctcation cesar tel ast anal Type ‘iho the canal inte each i 2A, perm 2 “beatin and open veriicton Repeat sara 3 ‘crys wrest are within tna ie cr es ‘Et er for inset robe 124 Qvaliy Cony! contol i accor ds wih ASTALRINE 7, race 1309, quant ‘samy col pose 13, Fctaton ad Radon Mesurements clin snd 0 that econ vl ping on 3 oes Soros 6m (28) fm be eg fe peinGy esis 14 ow Oi cetin cme,» pgety x cin BS a Sea a el ‘acc py eis cine i ‘Stems mary ase ccd wos me eect cmon mytext 182 ce specimen dle a rept te average of the dapewe rests 14, Caestion 14. Unig the average rents bind in 13.2, clea thes fn a th clemans ort taylors cle 2 15. Precision and Bias 154 PresionUp cpt abate coopeetd in pr fouming his xt edhe apt end the sts rr ‘i sanimarv In Tale 3 Aldo! data or within- Iahrtry varity of ret, one hy anying tee Specimens of oe ail ctr brn i acne shih source enon sete ia ths mete, to Tate Otros yeni renter ese vay sing the same set abd esto cmt, “ABLE Sate! Woman (Ts tod E415 Exes Sy)@y esrs—14 ct nes MM ayers MOAI A aro Tiracqnas Rte A Bo Pe 1 "ABLE «Vr aot Win ail Labrie NBS 22)Gy eais-14 1.1 Prt for Celcam and Niongen—Up w sgt lara copes in amin hyo tee Sppronimae ole forth expected easy in, Rs {ierang o Ow NNO cl an fe eal nt ‘he illowing egunion which Ca the apse ean eve = Viera OF] o 15.1.2 Fer mitogen, the repo ink, ts angina vale of 0.000 thoushout he rane of ass nope 152 Blast la tee spines ta previosly had en atnyod by chemical tcbaigics fa sore atone Tabor wet sealed flowing he cron tis ot ‘thd The dt ae gv in Tale Not. 152. Blarfor Calc and Noone bis hi st retbod at cena san Tacs ay be ug by ‘aarng te seeped ferns ees with the antiet ‘Store obsined by meray texting eT 16 Keywords 16. cabo lowly we spk tami isin spectre als pecuomeuyQy ests {ABLE sae emo or Caen aa trogen TABLE inva or Clu ng Noon ‘ ‘ioe come. i eos ooLy ens om em