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Keywords: In cryogenic machining, employing internal supply cooling through the tool not only diminishes tool wear and
Cryogenic machining enhances workpiece machining quality but also offers the benefits of reduced liquid nitrogen consumption and
Cooling supply method more precise cooling. These advantages are particularly noteworthy for efficiently machining challenging ma
Chip formation mechanism
terials. However, prevailing research on internal supply cooling through tools predominantly concentrates on
Titanium alloys
aspects such as tool wear and surface integrity, with a relatively limited exploration of material removal
mechanisms. The material removal process stands as a crucial factor influencing cutting stability and surface
smoothness. Thus, this study focuses on the Ti-6Al-4 V alloy, utilizing numerical modeling to investigate the
impact of liquid nitrogen cooling methods on the cutting deformation zone. In addition to its benefits for
difficult-to-machine materials, internal supply cooling through the tool presents a promising avenue to enhance
machining efficiency. Consequently, this study strategically selected the Ti-6Al-4 V alloy as the research subject,
employing numerical modeling to delve into the influence of liquid-nitrogen cooling methods on the cutting
deformation zone. Furthermore, employing a combination of cutting experiments and simulations, we analyzed
the evolution of temperature fields and microstructures within the deformation zone to elucidate the chip for
mation mechanism under liquid nitrogen cooling conditions. The outcomes of this investigation reveal that in
comparison to liquid nitrogen external supply cooling, internal supply cooling through the tool effectively re
strains chip serration, thereby contributing to an enhancement in machining quality. The analysis demonstrates
that, under conditions of internal supply cooling through the tool, chip formation is predominantly influenced by
the adiabatic shear effect induced by low temperatures. In contrast, under external supply cooling conditions,
susceptible to the low-temperature embrittlement effect, the chip’s free surface tends to undergo brittle cracking.
This shift in the chip formation mechanism toward the co-dominance of adiabatic shear and brittle cracking
results in a more pronounced serration of the chips. This study establishes a theoretical foundation and guides the
industrial application of cryogenic machining.
1. Introduction they are increasingly being utilized in civilian sectors such as biomedical
engineering, the petrochemical industry, and rail transportation for
Titanium alloys are characterized by a high specific strength, applications such as heat exchangers, distillation towers, artificial joints,
excellent toughness, superior corrosion resistance, and stable mechani and artificial teeth (Muthaiah et al., 2022). However, titanium alloys
cal performance at low temperatures. Consequently, they have found belong to the category of difficult-to-machine materials, exhibiting
widespread applications in the aerospace and defense industries and challenges such as high cutting temperatures, low cutting efficiency,
deep space exploration (Chakraborty et al., 2022). For instance, tita rapid tool wear, difficulty in chip evacuation, and poor surface quality
nium alloys constitute approximately 15% of the total mass of the (Lu et al., 2020). These issues significantly impede the further devel
Boeing 787 and approximately 9% of that of the C919 (Liu et al., 2022a). opment and application of Ti alloys. To ensure the continued use of Ti
Additionally, as the applications of titanium alloys continue to advance, alloys in modern industries, it is important to explore efficient
* Corresponding author at: School of Mechanical Engineering, Dalian University of Technology, Dalian 116024, China.
E-mail addresses: hbliu@dlut.edu.cn, 15554135712@163.com (H. Liu).
https://doi.org/10.1016/j.jmatprotec.2024.118377
Received 25 November 2023; Received in revised form 7 March 2024; Accepted 8 March 2024
Available online 10 March 2024
0924-0136/© 2024 Elsevier B.V. All rights reserved.
J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Table 1
Material parameters of Ti-6Al-4 V alloy. The relevant parameters are used for subsequent analytical calculations and simulation modeling.
Parameter Notation Numerical source Parameter Notation Numerical source
satisfy the orthogonal cutting method proposed by Buda, the material coated carbide inserts (TiAlN coating, cutting edge length 4 mm) with a
was cut into 3 mm × 30 mm × 100 mm sheets using laser cutting. rake angle of 4◦ , a clearance angle of 7◦ and a tool cutting edge angle of
0◦ . The external supply cooling method is set up as follows: Liquid ni
trogen is injected directly onto the workpiece after passing through the
2.2. Experimental equipment and methods storage tank, external piping, and nozzle (2 mm in diameter and about
40 mm from the workpiece) in order to ensure that the workpiece to be
An orthogonal cutting method is used to simplify the subsequent machined can be cooled continuously. For both liquid nitrogen supply
calculation steps. In other words, only one cutting edge was involved in methods, the flow rate was 45 L/h and the liquid nitrogen pressure was
the cutting, and the inclination angle of the cutting edge was 0◦ , which set at 0.4 MPa. The parameters were determined according to Tahma
ensured that the direction of the cutting speed was perpendicular to the sebi’s study (Tahmasebi et al., 2019), which concluded that the best
cutting edge. This method equates the complex cutting problem to a cooling effect was achieved at a liquid nitrogen pressure of 0.4 MPa.
simple 2D strain problem, which is convenient for studying the chip After the liquid nitrogen supply equipment was fixed, the titanium
formation mechanisms. alloy sheet was fixed on the fixture for orthogonal cutting. At the same
This experiment was carried out on the self-developed CVM650 time, a force gauge (Kistler 9257B) was installed under the fixture to
cryogenic machine tool, which can not only cool by supplying liquid monitor the stability of the cutting process and the tool condition. In
nitrogen inside the tool, but also prepare liquid nitrogen by itself, as order to make the experimental setup clearer, we provide a schematic
shown in Fig. 1. At the same time, we have independently developed the diagram of the site and schematic diagram of the cutting, the positioning
matching cryogenic internal cooled spindle, toolholder and tool. of the workpiece and the tool in Fig. 2. The cutting parameters for this
In this experiment, for the method of internal supply cooling through experiment are shown in Table 2.
the tool, the specific setup is as follows, after the liquid nitrogen is At the end of the experiment, the chips were collected under different
output from the storage tank, it reaches the tool through the conveying cutting conditions. One part of the chips was resin inlaid and then
pipeline, the internally cooled spindle, and the internally cooled tool sequentially sanded, polished, etched (Kroll reagent, 40 s), and placed
shank in turn, and then the workpiece is cooled accurately. The length of under an ultrafield microscope (VHX-600E, Japan) to observe the degree
the tool selected for this experiment is 150 mm, the diameter is 16 mm, of serration and distribution of shear bands of the chips. The other part
and there is a liquid nitrogen channel with a diameter of 5 mm inside the was ultrasonically cleaned with alcohol and then placed under a scan
body of the tool, which reaches the front of the tool after passing through ning electron microscope (Q45, USA) to observe the microstructural
the channel, and finally the liquid nitrogen is sprayed to the machining features of the chip with the specific viewing orientation shown in Fig. 2.
area by the jet hole with a diameter of 2 mm (mainly spraying the rake
face of the cutter, which also affects the flank face of the cutter). In this 2.3. Modeling of cutting simulation
case, the distance between the jet hole and the insert is about 10 mm,
and the angle between the jet hole and the horizontal plane is 60◦ . The Utilizing experimental and analytical methods to explore cutting
tool is shown in Fig. 2(c). In addition, the milling cutter is equipped with mechanisms can achieve higher physical accuracy, but issues such as
low efficiency, inconvenience, and difficulty in obtaining some data
exist. Therefore, this experiment is further combined with cutting
simulation (Liu et al., 2022b). In this experiment, the ABAQUS/Explicit
software was used as the basic platform, and a 2D cutting model was
established using the thermal-displacement coupling model. To ensure
the stability of the cutting process, the first-order linear quadrilateral
cell CPE4RT was chosen. The model was divided from top to bottom into
removal, separation, and material matrices. Mesh accuracy is the key to
improving the simulation accuracy (Aydın, 2023). To obtain better
calculation results, we set the mesh of the removal and separation layers
smaller, whereas the mesh of the workpiece matrix was set larger. In
addition, to prevent mesh distortion at the moment of contact between
the tool and workpiece, we set a certain tilt angle for the removal layer.
After several pretests, further changes in the size and number of meshes
did not affect the experimental results.
Previous studies concluded that the Johnson–Cook constitutive
Fig. 1. Cryogenic machine tool CVM650. Self-developed cryogenic machine model has wide applicability in simulations (Imbrogno et al., 2017).
tools that enable cryogenic internal supply cooling through the tool. Therefore, this model was selected for the simulation. Its expression is as
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 2. Experimental program and principle of cryogenic machining. (a) Diagram of the equipment used for the cutting test, observation diagram, tool movement
diagram and workpiece positioning diagram. (b) Schematic diagram of cryogenic internal supply cooling through tools. (c) Internally cooled tool used for this cutting.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 3. Schematic diagram of heat transfer imposition. (a) External supply cooling. (b) Internal supply cooling through the tool. The difference in the applied position
of convective heat transfer was utilized to differentiate the liquid nitrogen supply cooling method, and the convective heat transfer coefficient of liquid nitrogen was
set to 75000 W⋅m− 1⋅K− 1.
Fig. 4. Stress distribution in the chip deformation area. (a) External supply cooling. (b) Internal supply cooling through the tool. The cutting speed is 300 m/min, the
undeformed chip thickness is 0.1 mm and the tool rake angle is 4◦ .
and two shear stress components, as shown in Fig. 7. In the experimental shear stresses can be mutually converted, so τxy and τyx are equal. The
section, we clarified that this experiment involved orthogonal cutting; normal stress in the z direction was obtained using Eq. (3). The stress
therefore, the cube was not subjected to force in the x-direction, and its state of the cube in the first deformation zone is shown in Fig. 7(b).
value could be set to 0. At the same time, from the plane state analysis, ( ) σ
the normal stress in the y-direction and the shear stress in the z-direction σz = v σx + σy = (3)
2
are also 0. This means that τxz, τyz, τzx, and τzy are all equal to 0. The
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 5. Schematic diagram of chip analysis model. (a) Modeling of serrated chips. (b) Enlarged diagram of the shear band. Fig. (b) is a magnification of the shear
band AONM in Fig. (a).
The stress state of the cube can be obtained using Eq. (4).
⎡ ⎤ ⎡ ⎤
σ x τxy τxz 0 τ 0
σ ij = ⎣ τyx σy τyz ⎦ = ⎣ τ σ 0 ⎦ (4)
τzx τzy σz 0 0 σ/2
Fig. 6. Simulation results of stresses in the first deformation zone. The pink The hydrostatic pressure, P, of the hexahedron can be obtained using
color of the graph shows the condition of external cooling, the green color Eq. (6).
shows the condition of internal supply cooling through the tool, the positive σ1 + σ2 + σ3 σ
values are tensile stresses and the negative values are compressive stresses. The P= = (6)
3 2
values are taken from the case of a cutting speed of 300 m/min.
The equivalent stress (σ), equivalent strain (ε), and equivalent strain
rate (ε̇) of the hexahedron are further calculated using the following
equation:
Fig. 7. Force diagram analysis of a cube. (a) Generalized model. (b) Actual stress state. By extracting the tiny cubes in the shear zone and analyzing their stress state,
the equivalent stress, strain, and strain rate can be deduced.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
⎧ √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅
⎪
⎪ 1[ ] 3σ 2 1
⎪
⎪
⎪ &σ = (σ 1 − σ2 )2 + (σ2 − σ 3 )2 + (σ 3 − σ1 )2 = + 3τ2 μ= √̅̅̅̅̅̅̅̅ (11)
⎪
⎪ 2 4
⎪
⎪ √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ 1 + 1.328 vakrc ρc
⎪
⎨ 1[ ] 3ε2 γ2
&ε = (ε1 − ε2 )2 + (ε2 − ε3 )2 + (ε3 − ε1 )2 = + (7) From Eq. (11), it can be seen that the heat distribution coefficient is
⎪
⎪ 2 4 3
⎪
⎪
⎪
⎪ √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ √̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ proportional to the cutting speed, i.e., the heat distribution coefficient
⎪ 2
will increase after the cutting speed is increased, and when the cutting
⎪ [ ] 2
⎪
⎪ 1 2 2 2 3ε̇ γ̇
⎩ &ε̇ = (ε̇1 − ε̇2 ) + (ε̇2 − ε̇3 ) + (ε̇3 − ε̇1 ) = +
2 4 3 speed is at a higher value, the theoretical value of μ is close to 1.
Theoretically, when cutting at high speeds, the time for the radiative
In orthogonal cutting, the values of the normal strain and normal
transfer of the cutting heat to the outside environment is significantly
strain rate are much smaller than the values of the shear strain and shear
shortened, and the heat loss in the cutting process is reduced, which
strain rate. Therefore, the equivalent strain and strain rate can be
ultimately leads to an increase in the heat distribution coefficient.
expressed by the following equations:
The cutting process is a deformation process involving large tem
√̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅
3ε2 γ2 γ perature gradients, high strains, and large strain rates, therefore, the
&ε =
4
+ ≈ √̅̅̅
3 3 (8) flow stress τ of the processed material needs to be represented by the
Johnson–Cook model, whose expression is shown in Eq. (1). In the
&
previous calculations, we expressed the equivalent strain and equivalent
√̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅̅ strain rate in Eq. (8)(9). In that equation, the strain γ and strain rate γ̇ are
ε̇ =
3ε̇2 γ̇2
+ ≈ √̅̅̅
γ̇
(9) then expressed in Eqs. (12) and (13), respectively.
4 3 3 cosγ0
γ= (12)
(2) Temperature sinφcos(φ − γ0 )
During the metal-cutting process, with the rapid movement of the
vcosγ0
tool, an adiabatic temperature increase occurs in the processed material γ̇ = (13)
under strong extrusion, resulting in a rapid increase in temperature in Scos(φ − γ 0 )
the shear zone. The interaction between the high temperature and high
Where γ0 denotes the rake angle of the tool, φ denotes the shear angle in
strain rate causes the material to undergo adiabatic shear thermoplastic
cutting, and the expression is shown in Eq. (14). v denotes the cutting
instability, resulting in the formation of jagged chips. The temperature
speed and S denotes the width of the adiabatic shear band, which can be
distribution in the shear zone is plotted in Fig. 8.
calculated using Eq. (15).
In the first deformation zone, owing to the extremely short plastic
deformation time, the generated cutting heat cannot be emitted into the φ = arctan
cosγ0
(14)
environment in time. Therefore, the temperature in the first deformation ξ − sinγ 0
zone can be expressed as the sum of the initial and adiabatic temperature Where ξ denotes the deformation coefficient of the material. In
increases, as shown in Eq. (10). Komanduri’s (Komanduri and Von Turkovich, 1981) previous study, it
∫γ was concluded that the value of ξ is approximately 1 for high-speed
μη 0 τdγ
T = T0 + ΔT = T0 + (10) machining of titanium alloys.
ρc
√̅̅̅̅̅̅̅
12 2m′cos(φ − γ 0 )kT0
Where T0 is the initial temperature of the workpiece, ΔT is the tem S= (15)
θτ0 cosγ0 v
perature generated under adiabatic conditions, ρ is the density of the
material, c is the specific heat capacity of the material, μ is the heat
Where k is the material thermal conductivity, T0 is the initial deforma
distribution coefficient, γ is the shear strain of the material, τ is the flow
tion temperature of the material, m′ and θ are the material constants, and
stress of the material, and η is the Taylor Quinney coefficient, which is
τ0 is the material reference shear stress.
usually taken as 0.9.
By applying Eqs. (10)–(15), the ideal cutting temperature in the
The heat distribution coefficient μ means the proportion of heat
primary deformation zone can be calculated. However, the above dis
capable of generating a temperature rise after taking into account the
cussion did not consider the cooling aspect. Therefore, to differentiate
heat losses in the first deformation zone, and the formula for this value
between the two supply methods, it is necessary to ensure that the
was proposed by Loewen (Loewen and Shaw, 1954) and is shown in Eq.
cutting experiments begin immediately after liquid-nitrogen spraying
(11).
starts, without the need for pre-cooling of the workpiece to prevent
complete infiltration of the material by liquid nitrogen owing to pro
longed exposure. Based on these assumptions, we recalculated the
temperature after the introduction of liquid nitrogen as follows.
In cryogenic machining, liquid nitrogen is supplied through the tool
in two main ways: external supply cooling and internal supply cooling.
External supply cooling uses external piping to spray liquid nitrogen
onto the machining area to achieve cooling. This method provides
continuous cooling of the workpiece material but does not provide real-
time cooling of the cutting tool. Internal supply cooling through the tool
implies that liquid nitrogen is delivered and sprayed through the in
ternal cavity of the tool to its tip, providing real-time cooling of the
insert with minimal impact on the workpiece. Fig. 9 illustrates these two
cooling methods.
Based on Fig. 9, we conclude that the temperature distribution of the
chip is influenced by the application method of liquid nitrogen; its
impact mechanism is illustrated in Fig. 10. During external supply
Fig. 8. Schematic diagram of the temperature field of the chip. S is the width of cooling, liquid nitrogen continuously cools the workpiece, resulting in
the shear band, φ is the shear angle, and γ0 is the rake angle of the tool.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 9. Different ways of supplying liquid nitrogen. (a) External supply cooling. (b) Internal supply cooling through the tool. Liquid nitrogen is ejected from an
internal channel that protects the tool while minimizing the continuous irritation of the workpiece from the liquid nitrogen.
Fig. 10. Schematic diagram of heat exchange under different supply methods. (a) External supply cooling. (b) Internal supply cooling through the tool. In condition
(a), the cooling source generated by the liquid nitrogen exchanges sufficient heat with the workpiece surface. And in condition (b), liquid nitrogen continuously cools
the tool surface, which in turn exchanges heat with the tool-chip contact surface.
the free surface of the chip consistently being at an extremely low Therefore, these two cooling methods can be distinguished. Firstly,
temperature (-196◦ C). Furthermore, because the free surface is far from under the conditions of external supply cooling, due to the strong
the tooltip, its exposure to thermal shock effects is minimal. In contrast, convective heat transfer capacity of liquid nitrogen, the temperature
during internal supply cooling through the tool, the workpiece is less near the free surface remains close to − 196◦ C. At the tooltip away from
affected by liquid nitrogen, and the low temperature primarily in the free surface, the temperature is primarily the result of the heat
fluences the contact surface between the tool and chip, leading to a generated by plastic deformation and is the sum of the initial tempera
temperature reduction in that region. ture and the adiabatic temperature rise, as expressed in Eq. (16). Under
Fig. 11. Schematic diagram of heat field distribution. Depending on the method of liquid nitrogen supply, under external supply cooling, the free surface of the chip
is always at a very low temperature, while the tool-chip contact surface is at normal temperature. In the case of internal supply cooling through the tool, the liquid
nitrogen continuously cools the tool, which in turn lowers the temperature of the tool-chip contact surface, while the free surface is at normal temperature.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
the condition of internal supply cooling through the tool, although heat From Fig. 12, it can be inferred that after the tool contacts the chip,
exchange occurs with the air, the convective heat transfer capacity of the segment AC experiences compressive forces, leading to a shear defor
air is close to zero and can be ignored. Therefore, the temperature near mation along the AC direction. To clarify the deformation of segment AC
the free surface is approximately the same as that in the first deforma after the application of liquid nitrogen, a comprehensive analysis of the
tion zone. However, the tooltip away from the free surface is constantly strain rate and temperature for this region must be conducted, consid
subjected to strong cooling by liquid nitrogen, and the temperature at ering the information from Section 3.2.
this location is the sum of the actual temperature and the temperature of From the perspective of material deformation, when the deformation
the liquid nitrogen, as expressed in Eq. (17). Simultaneously, the results environment reached the critical strain rate, segment AC underwent an
shown in Fig. 11 can be obtained by calculating using this expression. ASD. The variation in the adiabatic shear deformation is closely related
⎧ ∫γ to the adiabatic shear band. Dodd and Bai (Dodd and Bai, 1985) indi
μη 0 τdγ
⎪
⎪
⎪ &T 0 + + Tc (Tool − chip contact area) cated that the width of the adiabatic shear band is closely related to the
⎪ ρc
⎪
⎪
⎪ ∫ strain rate and temperature. Specifically, as the deformation tempera
⎪
⎪
ture decreases and the cutting speed increases, the width of the adiabatic
γ
⎪
⎨ μη 0 τdγ
T0 + ( Shear zone area ) (16)
ρc shear band becomes narrower, as shown in Eq. (18).
⎪
⎪ ∫
⎪
⎪ γ √̅̅̅̅̅̅̅̅
⎪
⎪ μη τ dγ
⎪ 0 1 λT ∗
⎪
⎪
⎪
T0 +
ρc
(Free surface area) S= (18)
⎩ 2 τ∗ ε̇∗
Fig. 12. Illustration of chip formation mechanism. The first deformation zone is subject to tensile / compression, the free surface is affected by tensile stress, and
tensile fracture occurs when it reaches the fracture limit. The bottom of the chip is subjected to compressive stress and reaches the critical deformation condition,
adiabatic shear deformation occurs.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
From Fig. 12, it can be inferred that, after the tool contacts the chip, mode toward a predominantly brittle fracture, with crack propagation as
the OC segment is subjected to tensile forces; consequently, tensile the main mechanism.
fracture may occur. Therefore, investigating whether the material un Based on the previous temperature field modeling analysis, we
dergoes fracture under cutting conditions is crucial for understanding observed that under the condition of external supply cooling of liquid
the deformation in this region. Material toughness is a major factor that nitrogen, liquid nitrogen mainly affects the tensile deformation zone. If
influences material fracture. During the cutting process, the material at the strain rate is sufficiently high and the temperature is sufficiently low,
OC is always subjected to the coupling effect of temperature and strain the free surface may crack, leading to brittle fracture. Therefore, under
rate. Therefore, it is necessary to combine previous analyses to explore external supply cooling conditions, the chip formation mechanism may
the fractures at this location. In previous studies, we used Eq. (19) to shift to the dominant roles of adiabatic shear and periodic cracking. In
represent the material brittleness, indicating that the material brittle contrast, internal supply cooling through the tool maintains a relatively
ness is directly proportional to the yield strength and inversely pro high free-surface temperature, and cracking is generally less likely to
portional to the material fracture toughness. occur.
In summary, we outlined the chip formation mechanisms under
f (ε̇, T)
B = ∫ εf (19) different liquid-nitrogen cooling methods. First, for the external supply
f (ε, ε̇, T)
0 cooling during cutting, when liquid nitrogen was applied to the free
surface of the chip, the plasticity of the free surface decreased because of
where B is the brittleness of the material and ε, ε̇, and T represent the
the low-temperature effect. However, the Ti-6Al-4 V alloy has good
strain, strain rate, and temperature of the material, respectively.
mechanical properties at low temperatures, and its free surface does not
The above equation indicates that the temperature and strain rate are
undergo tensile cracking at relatively low speeds. As the cutting speed
the main factors influencing material brittleness. Previous studies have
increased, the coupling effect of low temperature and high strain rate
experimentally demonstrated that the material yield strength increases
further increased the brittleness of the free surface, making it more
with decreasing temperature or increasing strain rate. Under high-
prone to tensile cracking. At this point, the chip formation mechanism
strain-rate dynamic loading conditions, plastic metal materials exhibit
shifts from the traditional adiabatic shear deformation to the coexis
a specific strain-rate effect that distinguishes them from static loading
tence of adiabatic shear and periodic cracking. Under conditions of in
tests, resulting in significant changes in their mechanical properties and
ternal supply cooling through the tool, liquid nitrogen was ejected from
fracture behavior. Generally, with an increase in strain rate, both the
the tooltip, and the radiative range of the cooling medium was mainly at
yield strength and ultimate tensile strength of the material increase.
the tooltip and the tool-chip separation surface, reducing the cutting
However, the increase in yield strength is greater than the increase in
temperature near the tooltip. According to the analysis, a decrease in
tensile strength, leading to the yield strength ratio of the material
temperature in the compression zone of the first deformation region
gradually approaching 1 (McCammon and Rosenberg, 1957). In the
increases the sensitivity of the adiabatic shear behavior, promoting the
context of materials science, changes in the yield-strength ratio affect
occurrence of adiabatic shear effects. At this time, the chip formation
the toughness and brittleness of materials. A higher yield strength ratio
mechanism was enhanced by the low-temperature-induced adiabatic
indicates greater brittleness, and when the yield strength ratio ap
shear deformation behavior. In summary, Fig. 14 shows the two mech
proaches 1, the material undergoes full embrittlement. However, as the
anisms of chip formation.
temperature decreases, the resistance to dislocation motion in the metal
crystals increases, making it difficult for dislocations to occur. This leads
4. Results and discussion
to an increase in the YS of the material. Lower temperatures result in
weaker atomic thermal vibrational forces, causing the material to
4.1. Analysis of the effect of cooling conditions on the degree of chip
transition from tough to brittleness (Stepanov et al., 2015). The effects of
serration
temperature and strain rate on the mechanical properties of the material
are shown in Fig. 13; lower temperatures and higher strain rates led to
Serrated chip morphology is a crucial indicator for describing chip
more pronounced material brittleness. According to relevant studies in
formation and serves as a vital reference for guiding process parameter
materials science, an increase in material brittleness shifts the fracture
optimization, tool design, and material selection. From the perspective
of improving machining efficiency, a higher serration level makes chips
easier to clear, contributing to a reduction in specific cutting energy.
However, excessive serration can intensify tool and workpiece vibra
tions, hindering the improvement in surface quality. However, a lower
serration implies that the chips are more prone to entanglement and
adhesion, leading to potential surface scratches. Therefore, under
standing and controlling the serration of chips is paramount for guiding
cutting optimization.
In the field of machining, some scholars consider the appearance of
serrated chips to indicate that the material has entered the high-speed
machining phase (Chen et al., 2021). Generally, the formula for calcu
lating chip serration is represented by Eq. (20). Fig. 15 (a) shows a
schematic diagram of the calculations.
H− h
Gs = (20)
H
where H is the height at the top of the chip tooth, and h is the height of
the root of the chip tooth.
To investigate the influence of cooling conditions on the serration
level of chips, we observed the microscopic morphology of chips
Fig. 13. Relationship between tough-brittle properties and temperature & collected after corrosion using an ultra-field microscope. The results are
strain rate. A decrease in temperature or an increase in strain rate enhances the shown in Fig. 15 (b). As can be seen from the graph, the level of serration
brittleness of the material and promotes fracture.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 14. Schematic diagram of chip formation mechanism under different cooling methods. Under external supply cooling conditions, when the cutting speed is high,
the coupled effect of low temperature and high strain rate leads to brittle tensile fracture of the free surface of the chip, which transforms the chip formation
mechanism into a combination of brittle cracking and adiabatic shear.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 18. Comparative validation of strain rates. Based on Eqs. (8), (9), (12),
(13) and (14), the strain rates inside the chip obtained at different cutting
speeds are calculated. The error bars represent the range of error between the
strain rate values obtained at different time points during the simulation and
the mean value, and their length is determined by the standard deviation.
parameters, strains, strain rates, and other parameters into Eq. (10), the
actual temperature in the shear zone can be obtained for specific pa
rameters. Considering that the experimental setup could not directly
measure the temperature distribution in the shear zone, we used a
simulation to validate the accuracy of the proposed temperature model.
After completing the simulation, the temperature distribution in the
shear zone was extracted using the built-in features of ABAQUS. The
results are shown in Fig. 19. From Fig. 19, it can be observed that under
the condition of external supply cooling with liquid nitrogen, the free
surface of the chip remained in an ultralow-temperature environment,
whereas the cutting edge was in a high-temperature state. Conversely,
under the conditions of internal supply cooling through the tool, the
temperature of the free surface was relatively high and the temperature
Fig. 17. Width of adiabatic shear band. The width of the shear band obtained
of the cutting edge was relatively low.
by analyzing Eq. (15). The shear band width decreases with increasing cut
To further explore the temperature environment of the chip, the
ting speed.
cutting temperatures at points A, B, and C were obtained, as shown in
Fig. 20 (a), and their averages were calculated. Subsequently, these
within the unit area became more intense, and consequently, the
values were compared with the results obtained from the analytical
serration of the chips became more pronounced. Liu (Liu et al., 2018)
calculations. The comparison results are shown in Fig. 20(b) and Fig. 20
also noted that the width of the shear band decreased with increasing
(c), respectively. From Fig. 20, it can be observed that, on the one hand,
cutting speed. Moreover, based on a transmission electron microscopy
the cooling method with liquid nitrogen affects the distribution of cut
analysis, as the width of the shear band decreased, the grains inside the
ting temperatures, and the distribution pattern aligns with the predicted
band transformed from columnar to equiaxed, which further facilitated
one. Specifically, under external supply cooling, the temperature of the
the formation of serrated chips.
free surface was low, whereas, under internal supply cooling through the
Based on the results shown in Fig. 17, by further combining Eqs. (8),
tool, the temperature at the cutting edge was low. The numerical error in
(9), (12), (13), and (14), the strain rates inside the chips under different
the obtained temperature did not exceed 25%, and the changing trend
cutting speeds can be calculated. The results were compared with the
remained consistent. The main reason for this error is that frictional
simulation data, as shown in Fig. 18, with an error of less than 20%. The
heating may alter the temperature in the cutting area, which was not
figure shows that the cooling conditions have a minor impact on the
considered in this study. However, with an increase in the cutting speed,
strain rate, which is closely related to the cutting speed. As the cutting
the heat in the shear zone increases. This is because with an increase in
speed increased, the strain rate also increased rapidly. The reason for the
cutting speed, the heat generated by plastic deformation increases, but
discrepancy between the simulation and actual results is two-fold. First,
the heat dissipation time is significantly shortened, ultimately causing
in actual machining, the temperature inside the shear band is not con
the cutting temperature to increase continuously. The high consistency
stant, and the cooling effects lead to fluctuations in the strain rate in
between the simulation and analytical results confirmed the accuracy of
some areas. Second, the sampling position of the strain rate can affect
the temperature prediction model proposed in Section 2.
the accuracy of the numerical value.
Considering the comprehensive analysis of the temperature and
(2) Analysis of the cutting temperature
strain-rate fields, under the condition of external supply cooling with
In cryogenic machining, changes in the temperature field become
liquid nitrogen, cooling is mainly applied to the free surface, which re
more complex owing to variations in the supply of liquid nitrogen. In the
mains at an extremely low temperature. This can easily lead to cracking
previous chapters, we established a temperature field modeling method
on the free surface if coupled with the high strain rates induced by
for different liquid-nitrogen supply methods. By substituting the cutting
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 19. Simulation results of cutting temperature. (a) Simulation plot of cutting temperature for different cooling conditions and cutting speeds. (b) Distribution of
cutting temperature under different conditions. Extraction of the temperature inside the shear zone of Fig. (a) yields Fig. (b).
cutting. Chip formation under these conditions may involve adiabatic numerous cracks appeared on the free surface of the chip, and no
shearing and periodic cracking. The temperature at the cutting edge was obvious dents were observed on the detached surface of the chip.
relatively low under the condition of internal supply cooling through the Combined with the transverse profile, it was found that the adiabatic
tool. As analyzed in the previous sections, when the critical strain rate is shear phenomenon coexisted with cracks that appeared on the top of the
reached, the adiabatic shear effect becomes more sensitive with chip and gradually converged to the shear zone after the cracks
decreasing temperature. To some extent, this promoted chip serration. extended, indicating that the material at the free surface reached the
However, the effect of serration was not as significant as that of fracture limit and brittle fracture occurred. However, according to the
cracking. SEM image in Fig. 21, adiabatic shear deformation still occurs at the
bottom of the chip. Based on the aforementioned analysis, owing to the
4.3. Analysis of the microstructure inside chips favorable low-temperature mechanical properties of the Ti-6Al-4 V
alloy, low temperatures only reduce its plastic deformation ability
To validate these inferences further, we observed the microstructure without inducing a ductile-to-brittle transition. When the cutting speed
of the chips. First, experimental observations revealed that under any was low, the free surface exhibited plastic behavior without brittle
liquid-nitrogen cooling cutting conditions, adiabatic shear bands could cracking. However, at higher cutting speeds, the combined effect of high
be observed in the AC segment, as shown in Fig. 21. The presence of strain rates and low temperatures led to the formation of tensile cracks
ASBs indicates the adiabatic shear deformation of the chips during on the free surface, which extended toward the bottom of the chip.
cryogenic cutting. In materials science, it is believed that when the strain Additionally, because of the plastic deformation caused by material
rate of material deformation exceeds a certain threshold, materials are plasticity and friction effects, extremely high cutting temperatures are
prone to thermal plastic instability, which leads to adiabatic shear generated, and the thermal softening effect leads to plastic deformation
deformation. Therefore, in machining, this theory is more suitable for at the bottom of the chip, independent of the cutting speed.
describing the chip deformation process. In other words, at the moment Fig. 23 shows the microstructure of the chips under the condition of
of contact between the tool and material, the material in the cutting zone internal supply cooling through the tool. Regardless of the cutting speed,
undergoes significant plastic deformation owing to the compressive the free surface of the chip remained smooth without crack distribution.
action of the tooltip. At extremely high strain rates, localized adiabatic Upon examining the cross-section, there were signs of ductile tearing at
shear occurs, forming regularly distributed adiabatic shear bands on the the bottom of the chip, accompanied by numerous ductile dimples.
chips and ultimately resulting in the observed periodic serrated Combined with the phenomenon shown in Fig. 21, it is considered that
morphology. in internal supply cooling through the tool, cooling occurs on the contact
To further analyze the formation of chips, we employed scanning surface of the tool and chip and does not affect the free surface of the
electron microscopy (SEM) for the direct observation of the unembed chip. Therefore, cracks did not appear on the free surface of the chips.
ded chips. A schematic of these observations is shown in Fig. 2. The Additionally, adiabatic shear plastic deformation remains the primary
microstructures of the chips were observed from different angles, and cause of chip formation owing to the high-temperature thermal soft
the results are summarized in Figs. 22 and 23. ening effect.
Fig. 22 shows the microstructure of the chip under the external The microscopic structural changes discussed in this section align
supply cooling conditions. From the longitudinal profile in Fig. 22(a), it with the assumptions made in Section 3 and are consistent with the
can be observed that at lower cutting speeds, the free surface of the chip temperature analysis presented in Section 4.2. Therefore, by synthesiz
is relatively smooth, with some folds when enlarged, and there are still ing the results, the mechanism of chip formation under different cooling
obvious dimples on the chip separation surface. Combined with the conditions can be inferred.
transverse profile, no brittle fracture occurred on the surface, indicating
that the material had not reached the tensile fracture limit at low strain 4.4. Analysis of chip formation mechanisms
rates. Combined with the adiabatic shear band observed in Fig. 21, the
chip formation mechanism at this point was dominated by the adiabatic Based on the analysis of theoretical and experimental phenomena,
shear. However, as the cutting speed increases, the chip formation we compared the effects of two different liquid nitrogen supply methods
mechanism changes. As shown in the longitudinal section of Fig. 22(b), on chip formation. From the modeling and simulation perspectives, the
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 20. Comparison of theoretical temperature and simulation temperature. (a) Position of temperature acquisition in chip simulation. (b) The cutting speed is
120 m/min. (c) The cutting speed is 300 m/min. The error bars represent the range of error between the cutting temperature values obtained at different time points
during the simulation and the mean value, and their length is determined by the standard deviation.
traditional adiabatic shear theory cannot explain the chip formation of the tool and intense plastic deformation of the material rapidly
mechanism in the cryogenic machining of titanium alloys. In cryogenic increased the temperature at the tooltip, generating a considerable
machining, the machined material undergoes deformation at high strain amount of cutting heat. Under the combined effects of thermal softening
rates and constantly experiences intense cooling from the liquid nitro and strain strengthening, an adiabatic shear zone was formed, extending
gen. Therefore, the chip formation mechanism in cryogenic machining is from the tooltip to the free surface. Second, as the tool moves further,
expected to differ from that of machining. The chip formation mecha the formed chip continues to climb under the push of the leading tool
nism in cryogenic machining is summarized in Fig. 24. face, intensifying the shear slip within the chip. At this stage, the tool’s
Mode 1 shows the chip formation process with internal supply compression and friction load on the already-formed shear zone further
cooling through the tool. Under these conditions, no surface cracks were affected the degree of serration. Finally, the chip flows rapidly along the
observed from the low-speed stage to the high-speed stage. However, an leading edge, causing intense plastic deformation at the bottom of the
obvious adiabatic shear band appeared, indicating that the formation of chip under strong friction. The chip was formed after completing these
serrated chips was mainly dominated by adiabatic shear. According to three steps.
the figure, the process of forming a serrated chip under the conditions of In addition, observations of the microscopic morphology revealed
internal supply cooling through the tool can be summarized in three that under external supply cooling conditions with liquid nitrogen, no
stages. Initially, the tool contacts the workpiece material at an extremely cracks were observed on the free surface when the cutting speed was
high speed, exerting a positive compressive force on the material. low. Therefore, the chip formation pattern remained, as illustrated in
Combined with strain hardening due to the high strain rate, a hardened mode 1. Mode 2 represents another pattern: under external supply
zone formed near the chip contact surface. Simultaneously, the friction cooling conditions with liquid nitrogen, adiabatic shear deformation
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 21. SEM image of a serrated chip after corrosion. When viewed after etching with Kroll’s reagent, the location drawn by the yellow line is the adiabatic shear
zone of the chip.
occurs at the tooltip at higher cutting speeds. Simultaneously, owing to methods have advantages in terms of improved machining efficiency
the coupling of the low temperature and high strain rate, a ductile-to- and reduced cutting energy consumption compared to dry machining.
brittle transition occurs on the free surface of the chip, leading to However, the method of internal supply cooling through the tool sup
cracking. The extension of the adiabatic shear deformation at the tooltip presses the degree of serration of the chips compared to external supply
synchronizes with the extension of the brittle cracks on the free surface, cooling; therefore, this method is more advantageous for ensuring cut
resulting in serrated chip formation. ting stability and improving machining quality.
Based on the analysis presented in this section, it is evident that
cryogenic machining can increase the serration of chips, making them 5. Conclusion
more conducive to fragmentation and removal. Experiments have also
found that under conditions of internal supply cooling through the tool, In this study, the chip formation mechanism of cryogenic machining
the serration of chips is relatively low. Therefore, it was necessary to was investigated based on stress triaxiality, and the influence law of the
examine these findings. First, both liquid-nitrogen supply methods result liquid nitrogen supply mode on the chip morphology was explored,
in a more pronounced serration of chips compared with dry cutting, which fills the gap in the material removal mechanism through internal
which facilitates chip breakage. When chip serration is more pro supply cooling through the tool. This study focused on the stress dis
nounced, the contact length between the tool and chip is reduced, tribution in the main shear zone, based on which the chip fracture
thereby lowering the frictional heat and, to some extent, inhibiting tool problem in the first deformation zone was defined as a material-damage
wear (Bermingham et al., 2011). Yılmaz et al (Yılmaz et al., 2018). also challenge under the mixed action of tensile/compressive stress. At the
noted that when materials encounter difficulties in chip breaking, same time, computational models of the temperature field and strain
entangled chips can affect continuous processing, leading to decreased rate field applicable to different liquid nitrogen cooling modes are
efficiency and posing safety risks to operators. Wang’s (Wang et al., established through comparative analysis, and the mechanism of chip
2015) research indicated that when materials undergo a transition from formation under liquid nitrogen cooling conditions is revealed by
ductile to brittle behavior, brittle chips can reduce cutting energy con combining it with an analysis of the influence of loading conditions on
sumption. However, when the degree of chip serration is excessively the deformation state of the material. The main conclusions are as
high, it can negatively impact the tool life and surface quality. Guo (Guo follows.
et al., 2021) and Yu (Yu et al., 2020) suggested that excessive chip
serration can cause fluctuations in cutting forces, affecting tool vibra 1. In cryogenic machining, the formation of chips is not controlled by a
tion, and leading to a decline in machining quality. Zhang et al (Zhang single stress component, with tensile stress acting on the location
et al., 2021). also emphasized that while removing material brittleness near the free surface of the chip, and compressive stress acting on the
may increase efficiency, plastic removal is key to ensuring quality. Based area near the chip contact surface of the tool. From the perspective of
on the above analysis, we conclude that both liquid-nitrogen cooling chip formation, when the temperature decreases or the strain rate
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 22. Microstructure of Ti-6Al-4 V under liquid nitrogen external supply cooling conditions. (a) The cutting speed is 120 m/min. (b) The cutting speed is 300 m/
min. As the cutting speed increases, the free surface is subjected to the coupling effect of low temperature and high strain rate, brittle tensile fracture occurs and
cracks appear.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 23. Microstructure of Ti-6Al-4 V under internal supply cooling conditions through the tool. (a) The cutting speed is 120 m/min. (b) The cutting speed is 300 m/
min. The change in cutting speed has very little effect on the free surface, which is extremely smooth.
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J. Li et al. Journal of Materials Processing Tech. 327 (2024) 118377
Fig. 24. Formation process of chips in cryogenic machining. When the cutting speed is low, the chip formation mechanism under both liquid nitrogen supply
methods is Mode 1. When the cutting speed is higher, the chip formation mechanism with liquid nitrogen external supply cooling changes to Mode 2.
increases, under the action of tensile stresses, brittle fracture, and combination of simulation modeling and experiments, revealing the
crack initiation on the free surface of the chip are promoted, and influence of the liquid-nitrogen supply mode on the chip formation
under the action of compressive stresses, the plastic deformation of mechanism, which provides a theoretical reference for the industrial
the adiabatic shear is promoted. application of cryogenic machining. In future research, on the one hand,
2. Differences in the way liquid nitrogen is supplied affect the tem it is necessary to explore the effect of liquid nitrogen cooling on the tool
perature field distribution during the cutting process. Under external wear mechanism to further promote the process optimization of tita
supply cooling conditions, the liquid nitrogen applied to the work nium alloys, on the other hand, it is necessary to research the low-
piece resulted in a lower free-surface temperature of the chip, which temperature dynamic mechanical properties of the material, and to
made the chip more susceptible to brittle fracture. In contrast, under further deepen the chip formation mechanism based on the dynamic
conditions of internal supply cooling through the tool, liquid nitro fracture mechanism of the material.
gen can be cooled precisely to the tip region, and the temperature at
the tool-chip interface is much lower when the chip is more sus CRediT authorship contribution statement
ceptible to shear slip and maintains plastic removal of the chip.
3. The results of the cutting experiments showed that the method of Jie Zhang: Software. Shaowei Jiang: Investigation. Jianming Li:
internal supply cooling through the tool reduced chip serration by Writing – original draft. Yueshuai Zuo: Validation. Haibo Liu: Writing
15.75% compared to conventional external supply cooling. This – review & editing. Yang Wang: Methodology. Yongqing Wang:
reduction in serration is advantageous in terms of the stability of the Formal analysis.
cutting process and improved machining quality.
4. In conventional external-supply cooling cutting, the continuous
Declaration of Competing Interest
impact of liquid nitrogen leaves the workpiece at a low temperature.
When the cutting speed is high, the coupling effect of low tempera
The authors declared that they have no conflicts of interest to this
ture and high strain rate often leads to the tough-brittle transition of
work. We declare that we do not have any commercial or associative
the material. Under tensile stress, the free surface of a chip is prone to
interest that represents a conflict of interest in connection with the work
brittle cracking, leading to chip formation dominated by periodic
submitted
cracking and adiabatic shear effects. Removal of the material
through a mixed tough-brittle fracture form produces more pro
Acknowledgements
nounced serrated chips, which exacerbates cutting vibrations and is
not conducive to ensuring machining quality.
The authors gratefully acknowledge the financial support from the
5. Under the condition of internal supply cooling through the tool,
National Natural Science Foundation of China (No. U20B2033), the
liquid nitrogen precisely cools the tool through the internal channels,
Changjiang Scholar Program of Chinese Ministry of Education (No.
which protects the tool while simultaneously reducing the cryogenic
Q2021053, T2017030), the Fundamental Research Funds for the Central
stimulation of the workpiece by liquid nitrogen. When the cutting
Universities (DUT22LAB505).
speed is high, which is affected by the coupling effect of the low
temperature and high strain rate, the material in the tool-chip con
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