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Chem Journal
Chem Journal
JR ic ~
\
Experiment No. 11
s1f' p h ' ·c acid 00 it.
Aim: To identify the given substance by the action of ilute
d, atch glass atchbox d .
Apparatus: Test tube, test tube holder, test tube stan 1~ , e1Ivery tube
, .•a e P,.aper.
Procedure:
,
dilute
(
smell of rotten eggsis)
evo :ved .\' - . /
sulphide.
2. Test the gas with a filter pa er ~ - :fl\e baper hlfhed silvery !:JYli/ogen sulphide gas is
bla k~ confirmed.
soaked in lead acetate solution.
whe n wa~ dilute sulphuric acid.
Deduction: The substance gal hyd roge n su~ · hide gas
-......:....,;,0, • Fe 0~ H 2S t
Reaction: FeS + H2S04
i&e.
Result: The give n unk now n subs tanc e ii a met a ulpb
*
RW.IAb Mpnual-cum-Pr:::,
Experiment No. 12
j\irn: To identify the given b
su stance by the ac . .,...
j\pparatus: Test tube, test tub h hon of ~mte , sulphuric acid on it.
e older, watch 1
substances required: Give nkn g ass, m tchbox, _delivery tube, etc.
nu own sub t · ( - \
paper. s ance, dilutes - lphun7c
aci , lime water,. potassium dicbromate
procedure: ~ /
SI No. Experiment
1. Add the given substance to a Bris~ cence of ~
test tube having bout 2 lhl cqltfurl~~-;, -~domless as
of dilute sulph ·c acid. /,,,, is ~o rved. (._
l
2. Pass the gas through lim 1tme j ter turned Jllie~ oxide.
water taken in another test
tube using a delivery tube. It'.?· )
3. Test the gas with a filter_ No o)jaracteristic ,
Carbon dioxide gas is
cop-fumed.
paper soaked in potassium" chan'ge.
dichromate solution. \ ~
Deduction: The substance gave carbo~ ~ J w ! {warmed with dilute sulphuric acid.
Reaction: Nalco, + H;SQ•.,.,, \ > Na2so. + H,O + co, t
Result: The given u i i . , . ,...... own su~stance is a metal carbonate.
)
()
Expe rime nt No. 13
Aim: To identify the given substance by the action of
' lute sulphuric acid on it.
tube holder, test tube stanl watch g}ass, matchb ox, dehve .
A aratus: Test tube, test
. . ry tub
pp \uric at id blue d e, etc
bstan ces required: Given unknown substance, dtl e sulpJ ' an red litrn .
Su Us pap
et' Sttj
Procedure: P\.
sulphuric acid.
Deduction: The substance ga~ gas ~ ~ed with dilute sulphuric acid.
***
24
nb Unrnvu-cwn-P_roct iC~
j $periJnent No. 14
I SI No.
1.
Experiment
Add the given substance
to a test tube conta,inin~ Brisk te.fferv~~~nce C?f a
J
Inference
~ e gas may be sulphur
dilute sulphuric acid. \ _ c~lo~rl ss gas ~1t~ the smell of-" aioxi~~
burnin sulphur 1s,,obs
2. Pass the gas throu ~ '
Lim ~ d ilky. The. gas may be sulphur
water taken in another
test tube using a delivery illoxide.
tube. ~--/
Dedu~tion: The subs~ ~ t i r dir ~-gas when warmed with dilute sulphuric acid.
B. Te
.
sting the giv en su
b\
sta nc e:
I
cle
,,
7
at\ w
.. atc h
',~
g1
;
ass ....
j
Ad d a few dro
.
ps of cone. HCl to it and mi X With
Take the given substance A in a ,;<, n'l~ :;f!J? a 1·Itt1e of the paste to a non-luminous Bunsen fla
rste. Ii, -_ouuce
a clean glass rod to get a fin)! ;' w c1:e
ned as me liJ.tion ed be for e. No te the observations in a table. No
using a platinum , ~ ~ ce B no w by making a paste of it, as mentio
ne:
abov e!- r f st su bs tan
the platinum wire\~~ mentioJ?-ed d D.
pro edure~(( r substances C an
above. Then re1 /at, ~ 7 Metal ion present
SI No. Suti tancl
Sodium (Na+)
1.
Potassium (K+)
Lilac
Ca lcium (Ca2+)
Brick red (fugitive)
2
Copper (Cu +)
4.
***
SI No. Experiment
'
(ii Pe rim en t No . 18
.01 : To id en tif y the given s ub stance b
,41
tu be , tes t tub h Y the action of h eat on .1t.
_.pparatus: Te st e older t tub e stanct(a
~ ' est matchbov"' watch glass, de liv .
ery tub e, etc.
ec au tio ns :
J'r
Th e test tube should n ot be overh
(1 ) . . br ea k eated and ont 1_ .
. tee tu be should be used.
Othe rw ise , tt m ay y a ha ra glass t B oros1I
. }
) He at th e te st tu be at the f tp of a non l . f
(2
tu be co m es in - uminous Bunsefl'flame .
(J) If a ho t te st contac ith
t W break.
.
e sh ou ld no t b co ld surfaces ot mo isture ' it may r
(4) The gi ve n su bs ta
nc .
e touched by h and s~ 1t may b,e po iso n~ .
proc ed ur e:
SI Ex pe rb ne Inference
Observation
I. H ea t a pi nc h of th e give J"he cr o~,olate .p ro wn subs
tance M ay be•.\ead dioxide.
si~ --/
su bs ta nc e in a dr y Bo ro ~ efi p-ale yellow.
{
te st tube. A colourless, odourless ga
s is The gas ma y be
evo\v~ oxygen.
d re d · ic change. The gas is neutral.
2. I~ tro du ce m oi st bl ue fan N? chara
e ga
lit m us pa pe r str ip s to\h~ ;.; .
g rekindled. The gas is oxygen.
3. In tro du ce a fa in t gl ow in
sp lin t to th e ga s.
\ Presence of oxygen
{h ro ug h ; ka lin e f ~e pyrogallol solution first
4. Pa ss th e ga s gas is confirmed.
io nY .~ i tu.med br ow n and then dark
py ro ga llo l sol ut
g a , , 'b;d f'n to black.
in an ot hef te stf ub e us in
delivery tu'be. ~
~ wi~h Th e residue is lead
co ol 4 '~e.~ 11J w residue fu~e monoxide (litharge).
5. A llo w t{ e te st qi1"e-to gl as s of the te st tu be g1vm
g 1t a
~ \ br ow n appearance.
~ n1
Reactlo
I
1
2Pb i 2
(c oc ol afe brown
)
- ..=--= --=.-\ -~ ), 2P b0
( \ llo
~ ~(ye w)
+ 0 2t
dioxide.
.te br o,.,wn su bs ta nc e is le
ad
Result:
rr i( )- . - '
.vue g1vell\1!-,-~ .
nk no w n_ph oc-o!@
)- ' ......__,, *
I
I
Experiment No. 19
action of heat on it.
Aim: To identify the given substance by the
tub
tube stan d, matchbox, watch glass, delivery e, etc
Apparatus: Test tube , test tube holder, test
I ·
Precautions: shoul
and only a f ard glass cJfy Borosil t~st tube
(1) The test tube sho uld
Otherwise, it may break.
not be ove rheated
f )d be u&erj
us Bunse flaJl1.e. I ·
ino
(2) Heat the test tube at the tip of a non
tact
-lum
with cold
1
surfaces or moisture, it niay break.
(3) If a hot test tube com es in con
The give n sub stance sho uld not be tou ched b .han ds; it ma:0pe poison ous.
(4)
Procedure:
Experiment Observation
SI No. ; .
Heat a pinch of the give ~ The colour of the substance ~ye PPer(ID
I. \
substance in a dry Borosil f\ st chai~ge d from Jight gre en to black. oxide.
{ A colourless, odourless gas is The gas may be
tube.
e',olveo~ carbon dioxide.
;
Introduce moist blue and red Blue litmus turned red. No change The gas is acidic.
2.
as.J .• o~ ed in red litmus.
litmus paper strips to~
The gas is carbon
3. Pass the gas through lime
water taken in another 1$r dioxide.
tube using a delivciy.-rube.
Presence of carbon
!ntroduc~ ~ l~er pap er~ aked .)ro cha
4. racteristic change.
~ dioxide gas is
m potassmm tch romate
confirmed.
l~
solution ~ther1as. l
(grJ n) ..
ate .
een,amorphous substance is copper carbon
.. A ~ ,
Res 1t: The given,._____ o
1
ara er stt
.t\PP ' e tube stand matchbo)'-, watch glass, delivery tube, etc.
1 s·
fon
precau • /
l) The tes t tub e sho uld not b
rheated and o I Borosil te~ tube Jshould be used.
( Otherwise, it ma y hr k e ove n Ya gla ss
ea .
) He at the tes t tub e at the tip 0 f ·
,'
(2 a non -.Iumin ous Bun se '"'-flam .
tes t tub e com es in c t act With cold urf:
(3) If a hot . on s aces ot
I
mo
.
tsture, it m~y bre ak. \
sta nce sho uld t b
(4) The giv en sub O
o e touched b - h and s-,t' 1t
.
y
'
be poisonous
du re· .-- -- ma
1 //' ./ . ~
proce ·
SI No. Ex per im ent Inference
Observation
1. He at a pin ch of the giv en b: ~ esidue may be
he 9olsmr of the substance
sub sta nce in a dry Bo ros il te . t \ chaefg~ from ~ hite to yellow. a metal' bx-ide.
/ Th e gas ma y be
tube. A coi ourless, ohourless gas is
als o-e'Wlve'"~ carbon dioxide.
2. Pass the gas through µme L. e wa ter tur ned mi ky.. .J Th e gas is car bon
water taken in anothet etube dioxide.
using a delivery tube. .
Pre sen ce of car bon
3. Introduce potassium
dio xid e gas is
di chr om ate
confirmed.
+ CO 2 t
Reaction: Zn (yellow when hot and
- Ycwi white when cold)
I
morphous substance is zinc carbona
te.
Resul · ow n whi .
I
Experiment No. 23
Aim: To identify the given substance by the action of ; eat on it.
Precautions: (
Apparatus: Test tube, test tube holder, test tube stan matchbbx, watch glass, delivery tub
e,etc
. J\JO
( l) The test tube should not be overheated and
Otherwise, it may break. .
only a ard glass
(2) Heat the test tube at the tip of a non-lurnmous Bunse flam . 7 Borosil test tub h
./.
(3) If a hot test tube comes in contact with cold surfaces r mJ isture, i'. .~ break. .
~ J
e s OUld '--
'1': ~
~pl
fr•
(1 )
(4) The given substance should not be touched b_y..h.,rj ; 1t mayt ,. .,L~r \
e p01s.:o~m, . . "__
(2
Procedure: f \
Observation
r, 171 ~ (3
(L
I'
SI No. Experiment Inference
I. Heat a pinch of the give
substance in dry Borosil
tube.
t', )7he colol)Iless ,cJ..eliquescen
~ryst'1s turned y~llow o!Y1'e ating
ktid a reddish brJwn gas turning
blu/ iittfuls-red1s"-e-,a!~ .
f Th ~low )
substance-may be
ZnO orPbO.
The gas may be
0 Tlie s o i u ~ed black.
nitrogen dioxide.
~
. .d
d1ox1
freshly prepared solution of e gas is
ferrous sulphate. I confirmed.
[PW Lab ~
iiperJJJJI:'..... .... ~- - .
u
Exp erim ent No. 25
Aim : To identify the given substance by the
action of ~ at.-on it.
App arat us: Test tube, test tube holder, test tube
stan '
matchb'ox, watch glass d 1.tvery tub
e
I
Precautions:
(1) The test tube shou ld not be over heat ed and
Otherwise, it may break.
only a ard ass i Borosil t st tube
~
r
should be
~
e, etc.
tube .
The gas may be
nitrogen dioxide.
of nitrogen
2. Pass the gas thro ug . ence
Pres .
d1ox1de gas is
prep ared solu tion of
sulp hate .
confirmed.
3. Allo w the he yell ow resid ue fuse d with the The residue is lead
~ s of the test tube givi ng it a monoxide.
down.
~ wn appe aran ce.
2 2Pb~ + 4N0 2t +
Reaction:
ale yellow) (reddish brown)
(whi
(tttabManual--cum-!°3
£$peTI
'Jllent No. 26
.
z
fh .
-ro ident ify the given substance by the acf
~11as
ion o eat on 1t.
·JJJ: J.'
,>I psratus: Test tube, test tube holder, lest tube stand
fmatcbbo • watch glass, delivery tube, etc.
l'AP dons:
be used.
Borosil ter\: tube,)should
recau
fhe test
(1) other wisetu~e s hould
, ,t may not. be overheated and only a
break
~
am .. /
fleat the test tube at the tip of a non-luminous Bunse
ture, it m!ty break.
(Z) If a hot test tube comes in contact With cold surfaces O mo(s
it may lie poison · ,• ., ~, ;
(J) The give n subs tance shonJd not be touched b chands, C l~
'1 .
(4)
.::_~ iiL -...1..____j~ _:~ ~~ ;:: :~- -- .
procedurrie:=__ __ __j_~ _ _J~ . .:::::::::,,._.JL_
L t - ~- --- i~~ ~~ ~~ --,
- - -~E~x~p~e~n~·m~e~n~ ~:
t ~cllbsla
Infer ~--;-~
:~ence
nce is a/
w'e'll .
SI1No- sub ~. Th~ whdite
Heat a pinc h of the ao/"e did nO\ melt but
· give n subs tanc e in a dry n efense w~ te fu~ fume's'
are due to NH, an
po ited as wllite sahd on HCl gases formed.
Boro sil test tube.
e
ti·on·· NH4CI ~ J
Reac
chloride.
Result: The 0£(whit
oive . c
n e)unknown wh1te
.
ce--is ammonium
***
Expe rime nt No. 27
it.
Aim: To identify the given substance by the action of heat on
.
ox, watch glas s, d ehver
Apparatus: Test tube, test tube holder, test tube stanc i(m atchb y tub
Precautions:
I \ e, etc.
i lass cjly Borosil test tube
( 1) The test tube shoul d not be overh eated and only a ard
)I.
(3) If a hot test tube come s m conta ct with cold surfa ces
or mqisture, it nl,y break.
may be poiso~
(4) The given subst ance shou ld not be touch ed by_ha nd( it
~
1
Procedure: 'Y ../ •
Aim: To identify the sources of polluti s in and aro und you r locality.
o
Procedure: Visit the water bodie~
- our Ity suc h as lakes, rivers, pon ds, we ll,
h~ fu l materials that mi~ th-t rese wa etc. Find out the
tf bodies. Som e causes ?f ~at ~r po~luti
with the water body, di mpmg of garbag on ar~ sewage mixing
e afldJ)olythene bag s, etc. In It, dis pos
mg che mic al poisons such
as industrial wastewa~e\ ~ d so Of·i f
bul ate the inf orm atio n you col lec ted .
SI No . Na me of wa ter bod y
Ki nd of pol lut ant s
1.
4. --C.
r
\
O **1