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Clinker
Clinker
Clinker
(14.139.34.2) VALID UP
Indian Standard
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ICS : 91.100.10
© BIS 2015
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FOREWORD
This Indian Standard was adopted by the Bureau of Indian Standards, after the draft finalized by the Cement and
Concrete Sectional Committee had been approved by the Civil Engineering Division Council.
In India, Portland cement clinker has been regularly supplied to various independent units ranging from large
grinding stations to mini cement plants to produce all common varieties of cement used in construction. In view
of global competitiveness of Indian cement manufacturing, clinker is also exported to different countries.
At present, the concerned Indian Standard specifications for cement, for quality requirements of clinker, refer to
the chemical requirements prescribed for cement in the Indian Standard specifications for ordinary Portland
cement. In view of the increased use of clinker as tradable commodity and in order to provide a common standard
reference for this material, these specifications are laid down to cover requirements of clinker as a separate
standard.
The composition of the technical committee responsible for formulation of this standard is given in Annex B.
This standard lays down minimum requirements expected from clinker to the used for manufacture of various
types and grades of cements. However, depending upon the special intended requirements of a particular type or
grade of cement, the manufacturer may design for appropriate additional requirements of clinker, if so desired
subject to compliance of the minimum requirements specified in this standard.
For the purpose of deciding whether a particular requirement of this standard is compiled with, the final value,
observed or calculated, expressing the result of a test or analysis shall be rounded off in accordance with IS 2 : 1960
‘Rules for rounding off numerical values (revised)’. The number of significant places retained in the rounded off
value should be the same as that specified value in this standard.
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IS 16353 : 2015
Indian Standard
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PORTLAND CEMENT CLINKER — SPECIFICATION
1 SCOPE consisting of lime (CaO), and silica (SiO2) with smaller
proportions of alumina (Al2O3) and iron oxide (Fe2O3).
This standard covers various requirements such as,
manufacture, chemical and physical requirements, 5 CHEMICAL REQUIREMENTS
storage and transportation of Portland cement clinker
used to produce cement meeting relevant Indian The Portland cement clinker shall conform to the
Standard specifications. chemical requirements given in Table 1, when tested
in accordance with the methods given in IS 4032. For
2 REFERENCES the purpose, the representative clinker shall be ground
to pass 150 μm IS sieve and tested.
The following standards contain provision which
through reference in this text, constitute provisions of 6 PHYSICAL REQUIREMENTS
this standard. At the time of publication, the editions
indicated were valid. All standards are subject to 6.1 For checking its conformity, the cement produced
revision, and parties to agreement based on this out of the clinker shall conform to the requirements
standard are encouraged to investigate the possibility given in Table 2. For the purpose, the clinker shall be
of applying the most recent editions of the standards ground to a fineness of 220 ± 25 m2/kg [when tested
indicated below: as per IS 4031 (Part 2)] with appropriate quantity of
gypsum to obtain cement having not more than 3.5
IS No. Title percent SO3.
456 : 2000 Code of practice for plain and
reinforced concrete (fourth revision). 6.2 In order to regulate the quality of clinker supplied in
650 : 1991 Specification of standard sand for terms of its particle size, the purchaser and the supplier
testing of cement (second revision) may mutually decide the accepted particle size
4031 Methods of physical tests for distribution of clinker. As a general guidance, the particle
hydraulic cement size distribution given in Table 3 may be followed.
( Part 2 ) : 1999 Determination of fineness by specific
7 TRANSPORTATION OF CLINKER
surface by Blaine air permeability
method (second revision) 7.1 Portland cement clinker shall be supplied duly
( Part 3 ) : 1988 Determination of soundness (first covered in trucks or suitable railway wagons or in ships
revision) or barges of suitable capacity. The supplier and the
( Part 5 ) : 1988 Determination of initial and final purchaser shall ensure that clinker is transported in
setting times (first revision) environmental friendly manner minimizing dust
( Part 6 ) : 1988 Determination of compressive pollution and spillage of clinker.
strength of hydraulic cement (other
7.2 For exports, clinker shall be supplied in suitable
than masonry cement) (first revision)
vessels with covered top to avoid any contact with
4032 : 1985 Methods of chemical analysis of
moisture or sea water, supplier shall ensure that clinker
hydraulic cement (first revision)
is transported to water front or loading terminals in
4845 : 1968 Definitions and terminology relating
environmentally friendly manner.
to hydraulic cement
3 TERMINILOGY 8 STORAGE
For the purpose of this standard, the definitions given Portland cement clinker shall be stored in such a
in IS 4845 shall apply. manner as to permit easy access for proper inspection
and to protect it from deterioration during storage. It
4 MANUFACTURE shall be stored in proper storage area to protect it from
Portland cement clinker consisting mainly of calcium entry of moisture or any other contamination; and can
silicates, aluminates and ferrites shall be obtained by be stored in covered gantry or silo. If stored in an open
heating to incipient fusion, a pre-determined and area, it shall be ensured to place it on PCC floor and
homogenous mixture of materials principally covered with tarpaulin to avoid loss of quality.
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IS 16353 : 2015
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(Clause 5)
Sl Characteristic Requirement
No.
(1) (2) (3)
i) Ratio of percentage of lime to percentages of silica, alumina and iron oxide, when calculated by the formula: 0.66 – 1.02
CaO
2.8 SiO 2 + 1.2 Al2O3 + 0.65 Fe2O3
ii) Ratio of percentage of alumina to that of iron oxide, Min 0.66
iii) C3S, percent by mass1), Min (see Note 1) 35
iv) C3A, percent by mass1) (see Note 1) 3-12
v) C3S+C2S, percent by mass1), Min (see Note 1) 70
vi) Total sulphur content calculated as sulphuric anhydride (SO3), percent by mass, Max 2.7
vii) Free lime, percent by mass, Max 3.0
viii) Chloride content, percent by mass, Max 0.1
(see Note 2)
ix) Magnesia, percent by mass, Max 6.0
x) Alkali content, percent by mass expressed as sodium oxide (Na2O), Max (see Note 3)
xi) Total loss on ignition, percent by mass, Max 1.5
xii) Insoluble residue, percent by mass, Max 1.0
1)
Optional.
NOTES
1 The tricalcium silicate (C3S), tricalcium aluminate (C3A) and dicalcium silicate (C2S) contents are calculated by the formulae:
C3S = 4.07 (CaO-Free CaO) - 7.60(SiO2) - 6.72(Al2O3) - 1.43(Fe2O3)
C3A = 2.65 (Al2O3) - 1.69 (Fe2O3)
C2S = 2.87 (SiO2) - 0.75 (C3S)
2 The requirement of chloride content in the cements to be used for prestressed concrete structure shall be 0.05 percent by mass, maximum.
3 Alkali-aggregate reactions have been noticed in aggregates in some parts of the country. On large and important jobs where concrete is
likely to be exposed to humid atmosphere or wetting action, it is advisable that the aggregate be tested for alkali-aggregate reaction. In
the case of reactive aggregates, the use of cement with alkali content below 0.6 percent expressed as sodium oxide (Na2O) that is,
equivalent alkalies (Na2O+0.658 K2O), is recommended. Where, however, such cements are not available, use of alternative means
may be resorted to for which a reference may be made to 8.2.5.4 of IS 456. If so desired by the purchaser, the manufacturer shall carry
out test on Portland cement clinker for alkali content and report the result.
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IS 16353 : 2015
Standard Mark may be granted to manufacturers or for test shall be taken as described in 11 and shall be
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producers may be obtained from the Bureau of Indian tested in the manner described in the relevant clauses
Standards. of this standard.
ANNEX A
(Clause 11.2)
SAMPLING AND CRITERIA FOR CONFORMITY FOR CLINKERS
A-1 SCALE OF SAMPLING the bulk storage shall be divided into number of sub-
lots depending upon the mass of the lot, in accordance
A-1.1 Lot with Table 4.
The quantity of clinker from the same manufacturing Table 4 Number of Sub-lots into which a Lot is to
unit and offered for inspection at one time not be Divided
exceeding 2 000 t shall constitute a lot. (Clauses A-2.1, A-3.2 and A-4.2)
The samples shall be selected and examined for each Sl Mass of the Lot Number of Sub-Lots
lot separately for ascertaining their conformity to the No. t
requirements of this standard. (1) (2) (3)
i) Up to 100 2
A-2 SAMPLING FROM BULK STORAGE (SILOS) ii) 101 to 200 3
iii) 201 to 300 4
A-2.1 Sub-lots iv) 301 to 500 5
v) 501 to 1 000 6
For the purpose of sampling, the quantity of clinker in vi) 1 001 to 2 000 7
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IS 16353 : 2015
A-2.2 Gross Sample a ship or barge shall be divided into a number of sub-
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lots depending upon the mass of lot, in accordance with
The gross sample shall be taken from a sub-lot by
Table 4.
taking increments at regular intervals when the Portland
cement clinker is being charged into the bulk storage
A-4.3 Gross Sample
or is being discharged from the bulk storage. If there
is more than one opening for charging or discharging, The gross sample shall be taken from a sub-lot with
the increments shall be taken from each opening. the help of suitable sampler by taking increments at
Increments shall be taken from each sub-lot and each regular intervals when Portland cement clinker is being
increment shall weigh at least 2 kg. It shall be ensured loaded into or discharged from the ship or the barge.
that the quantity of sample so collected is sufficient Increments shall be taken from each sub-lot and each
for tests prescribed in this standard. increment shall weigh at least 2 kg, and the mass of
gross sample shall be minimum 24 kg.
A-3 SAMPLING FROM WAGONS OR TRUCKS
A-3.1 This method shall apply when Portland cement A-5 REDUCTION OF GROSS SAMPLE
clinker in bulk is received in wagons or trucks.
A-5.1 Equal quantities of the material shall be taken
A-3.2 Sub-lots from each of the gross sample representing the sub-lot
into which the lot has been divided and mixed together
For the purpose of sampling, the quantity of Portland
to constitute a composite sample representing the lot
cement clinker in wagons or trucks shall be divided
as a whole. The mass of the composite sample shall be
into a number of sub-lots depending upon the mass of
about 24 kg.
the lot, in accordance with Table 4. The sub-lots shall
consist of approximately equal number of wagons or A-5.2 The composite sample shall be divided into 3
trucks. Minimum two trucks/wagons shall be selected equal parts; one for the purchaser, another for the
at random from each sub-lot. supplier and the third to be used as a referee sample,
The referee sample shall be used in case of a dispute
A-3.3 Gross Sample
between the purchaser and the supplier. Each of these
The gross sample shall be taken from a sub-lot with parts shall then be placed in a suitable container and
the help of a suitable sampler by taking increments of labelled with full identification particulars, such as
not less than 2 kg from 6 evenly distributed points in supplier’s name, lot number, sub-lot number, date of
each selected wagon or truck and the mass of gross sampling, etc.
sample shall be minimum 24 kg.
A-6 NUMBER OF TESTS AND CRITERIA FOR
A-4 SAMPLING FROM SHIPS AND BARGES CONFORMITY
A-4.1 This method shall apply when clinker in bulk is
A-6.1 A composite sample shall be tested for all the
received in ships or barges.
requirements specified in this standard.
A-4.2 Sub-lots
A-6.2 All the test results shall satisfy the requirements
For the purpose of sampling, the quantity of clinker in of the standard to declare the conformity of the lot.
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IS 16353 : 2015
ANNEX B
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(Foreword)
COMMITTEE COMPOSITION
Cement and Concrete Sectional Committee, CED 2
Organization Representative(s)
Delhi Tourism and Transportation Development Corporation Ltd, SHRI JOSE KURIAN (Chairman)
New Delhi
ACC Ltd, Mumbai SHRI S. A. KHADILKAR
SHRI RAMAN S ADANAND PARULEKAR (Alternate)
Ambuja Cements Limited, Mumbai SHRI J. P. D ESAI
SHRI C. M. DORDI (Alternate)
Association of Consulting Civil Engineers (India), Bangalore SHRI AVINASH D. S HIRODE
SHRI K. K. MEGHASHYAM (Alternate)
Atomic Energy Regulatory Board, Mumbai SHRI L. R. BISHNOI
SHRI SAURAV ACHARYA (Alternate)
Builders’ Association of India, Mumbai REPRESENTATIVE
Building Materials and Technology Promotion Council, New Delhi SHRI J. K. PRASAD
SHRI C. N. JHA (Alternate)
Cement Manufacturers’ Association, Noida D R K. C. N ARANG
DR S. K. H ANDOO (Alternate)
Central Public Works Department, New Delhi SHRI A. K. GARG
SHRI RAJESH KHARE (Alternate)
Central Soil and Materials Research Station, New Delhi SHRI M URARI R ATNAM
SHRI S. L. G UPTA (Alternate)
Central Water Commission, New Delhi DIRECTOR (CMDD)(N&W)
DEPUTY DIRECTOR (CMDD) (NW&S) (Alternate)
Conmat Technolgies Pvt Ltd, Kolkata DR A. K. C HATTERJEE
Construction Chemicals Manufacturers’ Association, Mumbai SHRI S AMIR S URLAKER
SHRI UPEN P ATEL (Alternate)
CSIR-Central Building Research Institute, Roorkee SHRI S. K. S INGH
CSIR-Central Road Research Institute, New Delhi DR RAKESH K UMAR
DR R ENU M ATHUR (Alternate)
CSIR-Structural Engineering Research Centre, Chennai DR K. RAMANJANEYULU
SHRI P. SRINIVASAN (Alternate)
Delhi Development Authority, New Delhi CHIEF ENGINEER (QAC)
DIRECTOR (MATERIAL MANAGEMENT) (Alternate)
Engineers India Limited, New Delhi SHRI S. CHATURVEDI
SHRI P. K. MITTAL (Alternate)
Fly Ash Unit, Department of Science and Technology, New Delhi SHRI CHANDER M OHAN
Gammon India Limited, Mumbai SHRI VENKATARAMANA N. HEGGADE
SHRI MANISH MOKAL (Alternate)
Hindustan Construction Company Ltd, Mumbai D R CHETAN HAAZAREE
SHRI MANOHAR CHERALA (Alternate)
Housing and Urban Development Corporation Limited, New Delhi SHRI D EEPAK BANSAL
Indian Association of Structural Engineers, New Delhi SHRI M AHESH TANDON
SHRI GANESH JUNEJA (Alternate)
Indian Concrete Institute, Chennai SHRI VIVEK NAIK
SECRETARY GENERAL (Alternate)
Indian Institute of Technology Madras, Chennai DR DEVDAS M ENON
DR M ANU SANTHANAM (Alternate)
Indian Institute of Technology Roorkee, Roorkee PROF V. K. GUPTA
DR BHUPINDER SINGH (Alternate)
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Organization Representative(s)
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Indian Roads Congress, New Delhi SECRETARY G ENERAL
DIRECTOR (Alternate)
Institute for Solid Waste Research & Ecological Balance, DR N. BHANUMATHIDAS
Visakhapatnam SHRI N. K ALIDAS (Alternate)
Lafarge India Pvt Ltd, Mumbai MS M ADHUMITA B ASU
Military Engineer Services, Engineer-in-Chief’s Branch, MAJ GEN AJAY ANAND
Army HQ, New Delhi SHRI MAN S INGH (Alternate)
Ministry of Road Transport & Highways, New Delhi REPRESENTATIVE
National Council for Cement and Building Materials, Ballabgarh SHRI V. V. A RORA
DR M. M. ALI (Alternate)
National Test House, Kolkata SHRI B. R. M EENA
SHRIMATI S. A. KAUSHIL (Alternate)
Nuclear Power Corporation of India Ltd, Mumbai SHRI ARVIND S HRIVASTAVA
SHRI RAGHUPATI ROY (Alternate)
OCL India Limited, New Delhi DR S. C. AHLUWALIA
Public Works Department, Govt of Tamil Nadu, Chennai SUPERINTENDING ENGINEER
EXECUTIVE ENGINEER (Alternate)
Research, Design & Standards SHRI R. M. S HARMA
Organization (Ministry of Railways), Lucknow SHRI V. K. YADAVA (Alternate)
The India Cements Limited, Chennai DR D. VENKATESWARAN
SHRI S. GOPINATH (Alternate)
The Indian Hume Pipe Company Limited, Mumbai SHRI P. R. B HAT
SHRI S. J. SHAH (Alternate)
The Institution of Engineers (India), Kolkata DR H. C. VISVESVARAYA
SHRI S. H. J AIN (Alternate)
The National Institute of Engineering, Mysore DR N. SURESH
SHRI H. N. RAMATHIRTHA (Alternate)
The Ramco Cements Ltd, Chennai SHRI BALAJI K. M OORTHY
SHRI ANIL KUMAR P ILLAI (Alternate)
Ultra Tech Cement Ltd, Mumbai DR S UBRATO C HOWDHURY
SHRI ASHOK K. TIWARI (Alternate)
Voluntary Organization in Interest of Consumer Education, SHRI M. A. U. K HAN
New Delhi SHRI H. WADHWA (Alternate)
In personal capacity (B-803, Gardenia Building, Film City Road, SHRI A. K. J AIN
Malad (E),Mumbai)
In personal capacity (36, Old Sneh Nagar, Wardha Road, Nagpur) SHRI L. K. JAIN
In personal capacity (EA-92, Maya Enclave, Hari Nagar, New Delhi) SHRI R. C. WASON
In personal capacity (E-1, 402, White House Apartments, SHRI S. A. R EDDI
R.T. Nagar, Bangalore)
BIS Directorate General SHRI J. ROY CHOWDHURY, Scientist ‘F’ and Head (Civil Engg)
[Representing Director General (Ex-officio)]
Member Secretaries
SHRI S ANJAY P ANT
Scientist ‘E’ (Civil Engg), BIS
and
SHRI S. ARUN KUMAR
Scientist ‘C’ (Civil Engg), BIS
Organization Representative(s)
In personal capacity (E-1, 402, White House Wardha Road, Nagpur) SHRI S. A. R EDDI (Convener)
20 Microns Ltd, Mumbai SHRI ATIL PARIKH
SHRI S UNIL M ISTRY (Alternate)
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Organization Representative(s)
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ACC Ltd, Mumbai SHRI S. A. K HADILKAR
SHRI RAMAN SADANAND P ARULEKAR (Alternate)
AIMIL Ltd, New Delhi DR V. M. SHARMA
SHRI AMAN KHULLAR (Alternate)
Ambuja Cements Limited, Mumbai SHRI J. P. D ESAI
SHRI C. M. DORDI (Alternate)
Building Materials and Technology Promotion Council, New Delhi SHRI J. K. PRASAD
SHRI C. N. JHA (Alternate)
Cement Corporation of India Ltd, New Delhi SHRIMATI SARASWATHI D EVI
MS BIBHA KUMARI (Alternate)
Cement Manufacturers’ Association, Noida DR D. VENKATESWARAN
SHRI S. K. SAXENA (Alternate)
Central Electricity Authority, New Delhi SHRI Y. K. S HARMA
SHRI M OHAN KUMAR (Alternate)
Central Pollution Control Board, Delhi SHRI J. S. KAMYOTRA
SHRI P. K. G UPTA (Alternate)
Central Public Works Department, New Delhi SHRI A. K. GARG
SHRI RAJESH KHARE (Alternate)
Central Soil and Materials Research Station, New Delhi SHRI M URARI RATNAM
SHRI U. S. VIDYARTHI (Alternate)
CSIR-Central Building Research Institute, Roorkee SHRI S. K. S INGH
CSIR-Central Road Research Institute, New Delhi SHRI J. B. SENGUPTA
Dalmia Cement (Bharat) Limited, New Delhi DR K. C. NARANG
SHRI C. S. S HARMA (Alternate)
Elkem South Asia Pvt Ltd, Navi Mumbai SHRI BRAJESH M ALVIYA
SHRI S URENDRA S HARMA (Alternate)
Fly Ash Unit, Ministry of Science and Technology, New Delhi SHRI CHANDER M OHAN
Gammon India Limited, Mumbai SHRI AVINASH Y. MAHENDRAKAR
SHRI M ANISH M OKAL (Alternate)
Gujarat Engineering Research Institute, Vadodara SHRI J. C. C HAUDHARY
SHRI R. H. F AFER (Alternate)
Hindustan Construction Company Limited, Mumbai SHRI AVINASH HARDE
DR CHETAN H AZAREE (Alternate)
Indian Concrete Institute, Chennai DR ANANT M. P ANDE
SECRETARY GENERAL (Alternate)
Institute for Solid Waste Research & Ecological Balance DR N. BHANUMATHIDAS
(INSWAREB), Visakhapatnam SHRI N. K ALIDAS (Alternate)
Lafarge India Limited, Mumbai SHRI M. K. C HAUDHARY
SHRI YAGYESH KUMAR GUPTA (Alternate)
Maharashtra Engineering Research Institute, Nasik SCIENTIFIC R ESEARCH OFFICER
ASSISTANT RESEARCH OFFICER (Alternate)
Military Engineer Services, Engineer-in-Chief Branch, Army HQ, BRIG S. B. VAJRAMATTI
New Delhi SHRI S UBODH KUMAR CHOPRA (Alternate)
Ministry of Commerce & Industry, New Delhi INDUSTRIAL ADVISER
SENIOR DEVELOPMENT OFFICER (Alternate)
Ministry of Road Transport & Highways, New Delhi SHRI A. K. PATHAK
SHRI O. P. S HRIVASTAVA (Alternate)
National Council of Cement and Building Materials, Ballabgarh DR M. M. ALI
DR S. H ARSH (Alternate)
National Hydroelectric Power Corporation Limited, Faridabad SHRI A. K. J AIN
National Test House, Kolkata SHRI D. V. S. PRASAD
DR MOITRAYEE DEVI (Alternate)
NTPC Ltd, New Delhi SHRI M ASOOM ALI
OCL India Limited, New Delhi DR S. C. AHLUWALIA
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Organization Representative(s)
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Public Works Department, Govt of Tamil Nadu, Chennai JOINT CHIEF ENGINEER (IRRIGATION )
EXECUTIVE ENGINEER (Alternate)
Ready Mixed Concrete Manufacturers’ Association, Mumbai SHRI VIJAYKUMAR R. KULKARNI
Tamil Nadu Minerals Limited, Chennai SHRI M. B HOOPATHI
SHRI S. KANNADASAN (Alternate)
Tata Steel Ltd, Jamshedpur REPRESENTATIVE
The Ramco Cements Ltd, Chennai SHRI BALAJI K. M OORTHY
SHRI ANIL KUMAR P ILLAI (Alternate)
Ultra Tech Cement Ltd, Mumbai DR S UBRATO CHOWDHURY
DR M. R. KALGAL (Alternate)
In personal capacity (IV/17, President’s Estate, New Delhi) SHRI K. H. BABU
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BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods
and attending to connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission in writing of BIS. This does not preclude the free use, in the course of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue of
‘BIS Catalogue’ and ‘Standards : Monthly Additions’.
This Indian Standard has been developed from Doc No.: CED 02 (7922).