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New
Series
Numerical Data
and Functional Relationships
in Science and Technology
GROUP II VOLUME 31
Molecules
and
Radicals
Magnetic
Properties of
Paramagnetic
Compounds
SUBVOLUME F
MATERIALS.SPRINGER.COM
123
Landolt-Bo€rnstein: Numerical Data and Functional
Relationships in Science and Technology – New Series
Volume 31F
Landolt-B€ornstein
Numerical Data and Functional Relationships
in Science and Technology
New Series
Geophysics (Group V)
Some of the group names have been changed to provide a better description of their contents.
A. Gupta
Editor
Magnetic Properties of
Paramagnetic Compounds
Subvolume F
Authors
R.T. Pardasani P. Pardasani
Department of Chemistry Department of Chemistry
School of Chemical Sciences University of Rajasthan
and Pharmacy, Central University of Jaipur, India
Rajasthan
Bandar Sindri, Ajmer, India
In continuation to our efforts to update the magnetic susceptibility data of paramagnetic compounds, a new
Volume II/31F is presented herewith covering literature partly from 1991–2000. Since most of the
researchers these days consult the literature online, a new pattern is being introduced with effect from
this volume. All the magnetic properties of each individual substance are listed as a single document which
is self explainable and allowing search in respect of substance name, synonyms, common vocabulary, and
even structure. It is hoped that a new pattern will facilitate greater accessibility of magnetic data and
enhance the use of Landolt-B€ ornstein.
The editor wishes to express her thanks to the authors R.T. Pardasani and Pushpa Pardasani for this
excellent volume. The encouraging support of Dr. Wolfgang Finger from Springer is gratefully
acknowledged.
v
Contents
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Part I La . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Magnetic properties of polymeric mixed metal lanthanide-copper complex with
diglycolic acid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Magnetic properties of chains of centered lanthanum cluster with some distortion . . . . . . . . . 14
Part II Ti . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Magnetic properties of low-valent, titanium(II) complex with iron carbonyl
betenyliolene ligand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Magnetic properties of titanocene hydride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Magnetic properties of titanocene anionic dihydride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Magnetic properties of dimeric titanocene oxide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Magnetic properties of permethyltitanocene telluride . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Magnetic properties of mononuclear titanium(III) chloro complex with cyclic triamine . . . . . 27
Magnetic properties of mononuclear titanium(III) thiocyanato complex with
cyclic triamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
Magnetic properties of mononuclear titanium(III) isocyanato complex with
cyclic triamine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Magnetic properties of heterometallic Ti(III)–Al(III)2 complex with Schiff base ligand . . . . . . 33
Magnetic properties of hexacyanotitanate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Magnetic properties of mononuclear anionic titanium(III) aryloxide chloro complex with
TMEDA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Magnetic properties of mononuclear anionic titanium(III) aryloxide chloro complex with
TMEDA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Magnetic properties of titanium(III) chloro complex supported by benzamidinate ligand . . . . 41
Magnetic properties of titanium(III) complex supported by benzamidinate ligand . . . . . . . . . 43
Magnetic properties of titanium(III) alkyl complex supported by benzamidinate ligand . . . . . 45
Magnetic properties of titanium(III) alkyl complex supported by benzamidinate ligand . . . . . 47
Magnetic properties of heterodinuclear titanium(III)-lithium(I) complex supported
by dicyclohexyl amide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
Magnetic properties of titanium(III) complex supported by di(isopropyl) amide . . . . . . . . . . . 51
Magnetic properties of titanium(III) phenyl supported by di(isopropyl) amide . . . . . . . . . . . . 53
Magnetic properties of titanium(III) complex supported by di(trimethylsilyl) amide . . . . . . . . 55
vii
viii Contents
Part III Zr . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Magnetic properties of zirconium(III) complex with cyclopentadienyl unit with
pendant phosphine donors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
Magnetic properties of zirconium-lithium cluster . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
Part IV V. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
Magnetic properties of edge-bridged open fifteen electron vanadocene complex . . . . . . . . . . . 83
Magnetic properties of vanadium(III) chloro complex with chelating
silylamino(disilylamido) ligand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
Magnetic properties of vanadium(III) hydrocarbyl complex with chelating
silylamino(disilylamido) ligand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86
Magnetic properties of monomeric V(III) chloro complex supported by
dicyclohexyl amide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
Magnetic properties of monomeric V(III) chloro complex supported by
bis-(trimethylsilyl)amide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
Magnetic properties of dimeric V(III) chloro complex supported by dicyclohexyl amide . . . . . 90
Magnetic properties of monomeric V(III) borohydride complex supported by
bis(trimethylsilyl)amide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92
Magnetic properties of tetranuclear vanadium(III) complex . . . . . . . . . . . . . . . . . . . . . . . . . . 94
Magnetic properties of tetranuclear vanadium(III) complex . . . . . . . . . . . . . . . . . . . . . . . . . . 96
Magnetic properties of asymmetric trinuclear vanadium(III) complex
(having [M3O2]6+ core) with oxime . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98
Magnetic properties of dinuclear vanadium(III) amide complex containing a
vanadaazacyclobutane ring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100
Magnetic properties of dimethyl vanadium(III) complex with trimethylsilyl amide . . . . . . . . . 101
Contents ix
Part V Nb . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 281
Magnetic properties of mixed-dicyclopentadienyl niobium complex . . . . . . . . . . . . . . . . . . . . . 283
Magnetic properties of mixed-dicyclopentadienyl niobium complex . . . . . . . . . . . . . . . . . . . . . 285
Magnetic properties of three dimensional bimetallic, copper(II)-niobium(V)
pyrazine complex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 287
Magnetic properties of iodo bridged niobium complex of mesitylene . . . . . . . . . . . . . . . . . . . . 288
Magnetic properties of dinuclear, nitride bridged heterobimetallic niobium-lithium
complex with amide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 290
Magnetic properties of chloro bridged dinuclear mixed-valence niobium(II,III)
complex with substituted amine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 292
Part VI Ta . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 293
Magnetic properties of mixed-dicyclopentadienyl tantalum complex . . . . . . . . . . . . . . . . . . . . 295
Magnetic properties of mixed-dicyclopentadienyl tantalum complex . . . . . . . . . . . . . . . . . . . . 297
Magnetic properties of 17-electron tantalum-centered radical containing carbonyl
and 1,2-bis(diphenylphosphino)ethane ligands . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 299
Magnetic properties of mixed ligand molybdenum(V) complex with dithioacid and propyl
dithioacid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 487
Magnetic properties of mixed ligand molybdenum(V) complex with dithioacid and butyl
dithioacid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 489
Magnetic properties of mixed ligand molybdenum(V) complex with aminothiol and propyl
dithioacid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 491
Magnetic properties of mixed ligand molybdenum(V) complex with aminothiol and butyl
dithioacid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 493
Magnetic properties of oxomolybdenum(V) complex with dimethylene-
bis-2-benzimidazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 495
Magnetic properties of oxomolybdenum(V) complex with tetramethylene-
bis-2-benzimidazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 496
Magnetic properties of oxomolybdenum(V) salt with 2-(20 -quinolyl)benzimidazole . . . . . . . . . 497
Magnetic properties of oxomolybdenum(V) complex with 2-(20 -quinolyl)benzimidazole . . . . . 499
Magnetic properties of oxomolybdenum(V) salt with 2-(20 -quinolyl)benzimidazole . . . . . . . . . 500
Magnetic properties of oxomolybdenum(V) complex with 2-(20 -quinolyl)benzimidazole . . . . . 502
Magnetic properties of tricyanomethanide complex of oxomolybdenum(V) . . . . . . . . . . . . . . . 503
Magnetic properties of tricyanomethanide complex of oxomolybdenum(V) . . . . . . . . . . . . . . . 505
Magnetic properties of tricyanomethanide complex of oxomolybdenum(V) . . . . . . . . . . . . . . . 507
Magnetic properties of oxomolybdenum(V) complex with Schiff base
(derived from isonicotinic acid hydrazide) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 509
Magnetic properties of dimolybdenum(III) complex with triphenylphosphine . . . . . . . . . . . . . 511
Magnetic properties of (pentamethylcyclopentadienyl)-molybdenum(IV) chloride . . . . . . . . . . 512
Magnetic properties of (pentamethylcyclopentadienyl)-molybdenum(IV) iodide . . . . . . . . . . . 514
Magnetic properties of μ-cyanide bridged dimolybdenum(V) complex with
substituted amido ligand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 515
Magnetic properties of tetrachlorophosphonium decachlorodimolybdate . . . . . . . . . . . . . . . . 517
Magnetic properties of molybdenum(V) complex with salicylaldehyde-S-
methylisothiosemicarbazone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 519
Magnetic properties of molybdenum(V) complex with salicylaldehyde-S-
methylisothiosemicarbazone (solvated) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 521
Magnetic properties of cyanide-bridged array of molybdenum atoms based on salene-iron
complex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 523
Magnetic properties of heterobimetallic cobalt-molybdenum, sulfido-iodo cluster . . . . . . . . . . 525
Magnetic properties of heterobimetallic cobalt-molybdenum, sulfido-bromo cluster . . . . . . . . 527
Magnetic properties of heterobimetallic cobalt-molybdenum, sulfido-chloro cluster . . . . . . . . 529
Magnetic properties of heterobimetallic cobalt-molybdenum,
sulfido-phenylthiolato cluster . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 531
Contents xix
Part IX W . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 545
Magnetic properties of cyclopentadienyl tungsten(IV) complex with 4,40 -dimethyl-2,20 -
bipyryridyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 547
Magnetic properties of cyclopentadienyl tungsten(IV) complex with 4,40 -dimethyl-2,20 -
bipyryridyl . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 549
Magnetic properties of cyclopentadienyl tungsten(IV) cationic complex with
4,40 -dimethyl-2,20 -bipyryridyl as tetraphenylborate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 551
Magnetic properties of tungsten(IV) 3,5-dimethylphenoxide complex with triamidoamine
ligand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 553
Magnetic properties of tungsten(IV) 3,5-dimethylphenyl complex with
triamidoamine ligand . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 554
Magnetic properties of cyclopentadienyl N,N-dienthyldithiocarbamate tungsten complex . . . . 555
Magnetic properties of cyclopentadienyl O,O0 -diethyldithiophosphate tungsten complex . . . . 557
Magnetic properties of cyanide-bridged array of tungsten atoms based on
salene-iron complex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 559
Magnetic properties of cyanide-bridged array of tungsten atoms based on
salene-iron complex . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 561
Part X Mn . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 563
Magnetic properties of bis(trans-phenylacetynyl)-manganese(II) . . . . . . . . . . . . . . . . . . . . . . . 565
Magnetic properties of bis(trans-trimethysilylacetynyl)-manganese(II) . . . . . . . . . . . . . . . . . . 567
Magnetic properties of 1,10 ,2,20 -tetraisopropyl-3,30 ,4,40 ,5,50 -hexamethyl-manganocene(II) . . . . 569
Magnetic properties of manganese(II) complex with nitronyl nitroxide radical . . . . . . . . . . . . 571
Magnetic properties of azide bridged manganese(II) complex with 4,4’-dimethyl-
2,2’-bipyridine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 573
Magnetic properties of manganese(II) complex with dicyanamide and pyrazine ligands . . . . . 575
Magnetic properties of manganese(II) complex with 1,2-bis(4-pyridyl)-ethene . . . . . . . . . . . . . 577
Magnetic properties of di-μ-(1,3)-N3-bridged manganese(II) complex with
1,2-bis(4-pyridyl)-ethane . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 579
xx Contents
Part XI Re . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 937
Magnetic properties of rhenium(II) isocyanide complex with diphenylphosphinoethane . . . . . 939
Magnetic properties of rhenium(II) complex with cyano and diphenyl-
phosphinoethane ligands . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 940
Magnetic properties of rhenium(III) complex with 2-(4-chlorophenylazo)-1-
methylimidazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 941
Magnetic properties of rhenium(III) complex with 2-(4-chlorophenylazo)-1-
methylimidazole . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 943
Magnetic properties of rhenium(IV) chloro complex that contains tri-amidoamine ligand . . . 945
Magnetic properties of rhenium(II) complex with phthalocyanine . . . . . . . . . . . . . . . . . . . . . . 947
Magnetic properties of tetrachlorophosphonium decachlorodirhenate . . . . . . . . . . . . . . . . . . . 949
Magnetic properties of tetrachlorophosphonium hexachlororhenate . . . . . . . . . . . . . . . . . . . . 951
Magnetic properties of mixed valence Re(I)C4Re(II) radical cation . . . . . . . . . . . . . . . . . . . . . 953
Introduction
General remarks
Volumes II/31B–I compliment and extend the “Magnetic Susceptibility Data” which was published as a
new volume II/31A titled “Magnetic Properties of Paramagnetic Compounds” in 2012 [1]. The literature
covered here extends partly from 1991 to 2000. Significant developments during this period have been:
(i) A new class of paramagnetic pharmaceutical substances called magnetic resonance imaging (MRI)
contrast agents. These pharmaceuticals function to provide contrast between diseased and normal tissue
and/or show the status of organ function and blood flow [2]; (ii) Magnetic properties of rare earth metal
molecular compounds and their interpretation in the free-ion approximation [3, 4]; (iii) Design and
synthesis of molecular devices based on metal-complex subunits within a supramolecular assembly with
unique magnetic and electronic properties [5]; (iv) Exploration of long range neighbor magnetic exchange
interactions [6].
The susceptibility data have again been mostly reported at room temperature and the studies down to
0.0 K have oftenly been reported in the form of figures (as curves of χ M vs. T or μeff vs. T or χ MT vs. T ).
Throughout the volume the data have been reported in CGS units, commonly abbreviated as cgs or cgs-emu
and represented as cm3 mol1. The SI units wherever reported have been changed into the cgs units by the
following conversion factor:
χM SI m3 mol1 ¼ 4π 106 χM cgs cm3 mol1
The sign convention used throughout this volume is that negative value of J signifies antiferromagnetic
coupling i.e. where the ground state has minimum multiplicity. All over the files ‘c’ after numbers stands
for corrected value of magnetic moment and paramagnetic susceptibility after making diamagnetic
corrections.
Organization of files
With the objective to collate the enormous amount of information on magnetic susceptibility parameters of
a very large number of a variety of skeletons and present it in a form that can readily be retrieved and used,
a new pattern is being introduced with volumes II/31B–I keeping in view that now a majority of research
groups look at the scientific data electronically. All the magnetic properties of each individual substance are
being documented as a single file and every single document is self-explainable. Each file is comprised of
Title of the document listing searchable and common vocabulary as well as synonyms, Name of the
substance according to IUPAC system and its abbreviated formula, CAS-number (wherever available),
Gross formula, Properties – listing all properties reported using a standard SpringerMaterials term (see next
section) and the Structure – a completely drawn structure of the molecule and/or ligand as well as a separate
molefile of the compound is provided to allow even structure searches. The magnetic data have been
presented in the form of table. It is followed by additional remarks such as susceptibility equations,
exchange parameters, etc. and figures with captions showing curves of χ M vs. T or μeff vs. T or χ MT vs. T,
wherever appropriate. Temperature and pH dependence, if reported, is indicated in the remarks column. As
far as possible the reference is made to the original literature.
The files are listed under their central metal ion or atom (transition metal, lanthanide or actinide).
The transition elements are listed by the group in which they occur in the periodic table starting with
Group IV (Ti, Zr, Hf) and proceeding until Group I (Cu, Ag, Au) followed by lanthanides and actinides.
La, Ti, Zr, V, Nb, Ta, Cr, Mo, W, Mn and Re are published in volume II/31F.