Method: Apple Juice W2024 Page 1 Date: 2024-01-18 3:29:54 PM

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Analysis Begun

Start Time: 2024-01-18 3:18:18 PM Plasma On Time: 2024-01-18 3:17:29 PM

Originator: Optima 8300 Technique: ICP Continuous
Spectrometer: Optima 8300 , S/N No Serial # Autosampler:

Sample Information File:

Results Data Set: MANDEEP and beer
Results Library: U:\ICP Results Database\Results.mdb

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Batch ID:
Sequence No.: 1 Autosampler Location:
Sample ID: Calib Blank 1 Date Collected: 2024-01-18 3:18:37 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Calib Blank 1
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Y 371.029 1272551.9 3940.35 0.31% 100.0 %
Ca 422.673† 4961.0 172.79 3.48% [0.00] mg/L
Mn 257.610† 5657.7 116.76 2.06% [0.00] mg/L
K 766.490† 2052.0 78.99 3.85% [0.00] mg/L
Cu 324.752† 2710.4 210.14 7.75% [0.00] mg/L

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Batch ID:
Sequence No.: 2 Autosampler Location:
Sample ID: Standard 1 Date Collected: 2024-01-18 3:21:52 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Standard 1
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Y 371.029 1300546.2 15388.76 1.18% 102.2 %
Ca 422.673† 322406.7 651.93 0.20% [5.003] mg/L
Mn 257.610† 247101.3 177.28 0.07% [2.004] mg/L
K 766.490† 119295.7 572.57 0.48% [9.005] mg/L
Cu 324.752† 152152.1 384.77 0.25% [1.994] mg/L

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Batch ID:
Sequence No.: 3 Autosampler Location:
Sample ID: Standard 2 Date Collected: 2024-01-18 3:22:57 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Standard 2
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Y 371.029 1278537.7 6057.52 0.47% 100.5 %
Ca 422.673† 666405.1 830.43 0.12% [10.007] mg/L
Mn 257.610† 480254.4 516.03 0.11% [4.007] mg/L
K 766.490† 276128.3 701.54 0.25% [21.012] mg/L
Cu 324.752† 317238.7 352.70 0.11% [3.999] mg/L
Method: Apple Juice W2024 Page 2 Date: 2024-01-18 3:29:54 PM

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Batch ID:
Sequence No.: 4 Autosampler Location:
Sample ID: Standard 3 Date Collected: 2024-01-18 3:23:54 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Standard 3
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Y 371.029 1272317.7 6798.60 0.53% 99.98 %
Ca 422.673† 999931.5 1568.26 0.16% [15.010] mg/L
Mn 257.610† 1007769.2 564.51 0.06% [8.015] mg/L
K 766.490† 389030.2 1370.76 0.35% [30.017] mg/L
Cu 324.752† 466819.9 1784.04 0.38% [5.998] mg/L

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Batch ID:
Sequence No.: 5 Autosampler Location:
Sample ID: Standard 4 Date Collected: 2024-01-18 3:24:53 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Standard 4
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Y 371.029 1308202.9 9960.71 0.76% 102.8 %
Ca 422.673† 1315352.8 3747.85 0.28% [20.014] mg/L
Mn 257.610† 1471823.1 1356.35 0.09% [12.022] mg/L
K 766.490† 497171.9 1687.95 0.34% [39.022] mg/L
Cu 324.752† 604598.8 2140.39 0.35% [7.998] mg/L

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Batch ID:
Sequence No.: 6 Autosampler Location:
Sample ID: Standard 5 Date Collected: 2024-01-18 3:25:48 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Standard 5
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Y 371.029 1291903.7 6255.05 0.48% 101.5 %
Ca 422.673† 1665430.7 6165.33 0.37% [25.017] mg/L
Mn 257.610† 1717294.6 1250.21 0.07% [14.026] mg/L
K 766.490† 651726.9 2490.24 0.38% [51.029] mg/L
Cu 324.752† 785014.5 4082.56 0.52% [9.997] mg/L

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Calibration Summary

Analyte Stds. Equation Intercept Slope Curvature Corr. Coef. Reslope

Ca 422.673 5 Lin, Bracketing -6573.2 66650 0.00000 0.999884
Mn 257.610 5 Lin, Bracketing 1195.1 122700 0.00000 0.999766
K 766.490 5 Lin, Bracketing 8210.2 12610 0.00000 0.999910
Cu 324.752 5 Lin, Bracketing -427.8 77640 0.00000 0.999174

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Batch ID:
Sequence No.: 7 Autosampler Location:
Method: Apple Juice W2024 Page 3 Date: 2024-01-18 3:29:55 PM

Sample ID: Sample001 Date Collected: 2024-01-18 3:26:53 PM

Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Sample001
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Y 371.029 1302187.5 102.3 % 0.62 102.3 % 0.62 0.61%
Ca 422.673† 490233.9 7.454 mg/L 0.0255 7.454 mg/L 0.0255 0.34%
Mn 257.610† 512852.6 4.169 mg/L 0.0153 4.169 mg/L 0.0153 0.37%
K 766.490† 279963.5 21.55 mg/L 0.041 21.55 mg/L 0.041 0.19%
Cu 324.752† 555470.4 7.160 mg/L 0.0168 7.160 mg/L 0.0168 0.23%

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Batch ID:
Sequence No.: 8 Autosampler Location:
Sample ID: Sample002 Date Collected: 2024-01-18 3:27:48 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Sample002
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Y 371.029 1283995.2 100.9 % 0.18 100.9 % 0.18 0.17%
Ca 422.673† 482065.3 7.331 mg/L 0.0183 7.331 mg/L 0.0183 0.25%
Mn 257.610† 517669.8 4.208 mg/L 0.0121 4.208 mg/L 0.0121 0.29%
K 766.490† 280567.4 21.60 mg/L 0.122 21.60 mg/L 0.122 0.56%
Cu 324.752† 560412.2 7.224 mg/L 0.0357 7.224 mg/L 0.0357 0.49%

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Batch ID:
Sequence No.: 9 Autosampler Location:
Sample ID: Sample003 Date Collected: 2024-01-18 3:28:40 PM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Mean Data: Sample003
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Y 371.029 1305890.0 102.6 % 0.31 102.6 % 0.31 0.31%
Ca 422.673† 480078.4 7.301 mg/L 0.0197 7.301 mg/L 0.0197 0.27%
Mn 257.610† 509157.6 4.139 mg/L 0.0080 4.139 mg/L 0.0080 0.19%
K 766.490† 276541.8 21.28 mg/L 0.046 21.28 mg/L 0.046 0.21%
Cu 324.752† 551290.9 7.107 mg/L 0.0253 7.107 mg/L 0.0253 0.36%