Short Area Report

Data file: 2023082901.dx

Data File Directory D:\CDSProjects\Warfarin sodium Project Name: Warfarin sodium Tablets
Tablets\Results\Intermediate\202
30829\20230829-1.rslt
Sample name: Blank Operator: Asefa Ketema
Instrument: SANSHENG HPLC Injection date: 2023-08-29 11:26:00-07:00
Inj. volume: 20.0 Location: P1-A-1
Acq. method: Assay.amx Type: Sample
Processing method: Assay.pmx Sample amount: 0.00
Manually modified: None

VWD1A,Wavelength=283 nm

0.005

-0.005

-0.01
mAU

-0.015

-0.02

-0.025

-0.03

0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 2.2 2.4 2.6 2.8 3 3.2 3.4 3.6 3.8 4 4.2 4.4 4.6 4.8 5
Time [min]

Assay.rdl [Rev. 1] Printed: 2023-08-29 11:59:12-07:00 Page 1 of 5

 Short Area Report
Data file: 2023082902.dx
Data File Directory D:\CDSProjects\Warfarin sodium Project Name: Warfarin sodium Tablets
Tablets\Results\Intermediate\202
30829\20230829-1.rslt
Sample name: API #1 Operator: Asefa Ketema
Instrument: SANSHENG HPLC Injection date: 2023-08-29 11:31:49-07:00
Inj. volume: 20.0 Location: P1-A-2
Acq. method: Assay.amx Type: Sample
Processing method: Assay.pmx Sample amount: 0.00
Manually modified: None

VWD1A,Wavelength=283 nm
1.844

280
260
240
220
200
180
160
mAU

140
120
100
80
60
40
20
0
0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 2.2 2.4 2.6 2.8 3 3.2 3.4 3.6 3.8 4 4.2 4.4 4.6 4.8 5
Time [min]

Signal: VWD1A,Wavelength=283 nm
RT [min] Type Width [min] Area Height Area%
1.844 BV 0.39 1075.2 259.44 100.00
Sum 1075.2

Assay.rdl [Rev. 1] Printed: 2023-08-29 11:59:12-07:00 Page 2 of 5

 Short Area Report
Data file: 2023082903.dx
Data File Directory D:\CDSProjects\Warfarin sodium Project Name: Warfarin sodium Tablets
Tablets\Results\Intermediate\202
30829\20230829-1.rslt
Sample name: API #2 Operator: Asefa Ketema
Instrument: SANSHENG HPLC Injection date: 2023-08-29 11:37:36-07:00
Inj. volume: 20.0 Location: P1-A-3
Acq. method: Assay.amx Type: Sample
Processing method: Assay.pmx Sample amount: 0.00
Manually modified: None

VWD1A,Wavelength=283 nm
1.843

280
260
240
220
200
180
160
mAU

140
120
100
80
60
40
20
0
0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 2.2 2.4 2.6 2.8 3 3.2 3.4 3.6 3.8 4 4.2 4.4 4.6 4.8 5
Time [min]

Signal: VWD1A,Wavelength=283 nm
RT [min] Type Width [min] Area Height Area%
1.843 BV 0.39 1074.8 260.14 100.00
Sum 1074.8

Assay.rdl [Rev. 1] Printed: 2023-08-29 11:59:12-07:00 Page 3 of 5

 Short Area Report
Data file: 2023082904.dx
Data File Directory D:\CDSProjects\Warfarin sodium Project Name: Warfarin sodium Tablets
Tablets\Results\Intermediate\202
30829\20230829-1.rslt
Sample name: new #1 Operator: Asefa Ketema
Instrument: SANSHENG HPLC Injection date: 2023-08-29 11:43:22-07:00
Inj. volume: 20.0 Location: P1-A-4
Acq. method: Assay.amx Type: Sample
Processing method: Assay.pmx Sample amount: 0.00
Manually modified: None

VWD1A,Wavelength=283 nm
1.843

260
240
220
200
180
160
mAU

140
120
100
80
60
40
20
0
0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 2.2 2.4 2.6 2.8 3 3.2 3.4 3.6 3.8 4 4.2 4.4 4.6 4.8 5
Time [min]

Signal: VWD1A,Wavelength=283 nm
RT [min] Type Width [min] Area Height Area%
1.843 BV 0.31 1032.2 249.84 100.00
Sum 1032.2

Assay.rdl [Rev. 1] Printed: 2023-08-29 11:59:12-07:00 Page 4 of 5

 Short Area Report
Data file: 2023082905.dx
Data File Directory D:\CDSProjects\Warfarin sodium Project Name: Warfarin sodium Tablets
Tablets\Results\Intermediate\202
30829\20230829-1.rslt
Sample name: new #2 Operator: Asefa Ketema
Instrument: SANSHENG HPLC Injection date: 2023-08-29 11:49:08-07:00
Inj. volume: 20.0 Location: P1-A-5
Acq. method: Assay.amx Type: Sample
Processing method: Assay.pmx Sample amount: 0.00
Manually modified: None

VWD1A,Wavelength=283 nm
1.843

260
240
220
200
180
160
mAU

140
120
100
80
60
40
20
0
0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 2.2 2.4 2.6 2.8 3 3.2 3.4 3.6 3.8 4 4.2 4.4 4.6 4.8 5
Time [min]

Signal: VWD1A,Wavelength=283 nm
RT [min] Type Width [min] Area Height Area%
1.843 BV 0.31 1032.6 250.47 100.00
Sum 1032.6

Assay.rdl [Rev. 1] Printed: 2023-08-29 11:59:12-07:00 Page 5 of 5