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Cement and Concrete Research 69 (2015) 10–18

Contents lists available at ScienceDirect

Cement and Concrete Research


journal homepage: http://ees.elsevier.com/CEMCON/default.asp

Electrical resistance tomography to monitor unsaturated moisture flow


in cementitious materials
Milad Hallaji a, Aku Seppänen b, Mohammad Pour-Ghaz a,⁎
a
Department of Civil Construction and Environmental Engineering, North Carolina State University, Raleigh, NC 27695, USA
b
Department of Applied Physics, University of Eastern Finland, Kuopio, Finland

a r t i c l e i n f o a b s t r a c t

Article history: Traditionally the electrically-based assessment of the moisture flow in cement-based materials relies on two- or
Received 18 April 2014 four-point measurements. In this paper, imaging of moisture distribution with electrical resistance tomog-
Accepted 12 November 2014 raphy (ERT) is considered. Especially, the aim is to study whether ERT could give information on unsaturat-
Available online 20 December 2014
ed moisture flows in cases where the flow is non-uniform. In the experiment, the specimens are monitored
with ERT during the water ingress. The ERT reconstructions are compared with neutron radiographs, which
Keywords:
Concrete (E)
provide high resolution information on the 2D distribution of the moisture. The results indicate that ERT is
Electrical Resistance Tomography (ERT) able to detect the moisture movement and to show approximately the shape and position of the water front
Image Analysis (B) even if the flow is nonuniform.
Transport Properties (C) © 2014 Elsevier Ltd. All rights reserved.

1. Introduction in cement-based materials. In the majority of previous studies, a set of


electrode pairs was embedded in the cement-based material, and im-
The durability of reinforced concrete structures is related to the abil- pedances between pairs of electrodes were measured. For example,
ity of concrete to impede the ingress of water and aggressive agents McCarter et al. [22,24,27–29] monitored water ingress in concrete spec-
(e.g., [1,2]). Therefore, the water transport rate in concrete is often imens by measuring the impedance between electrode pairs embedded
used as a measure of the durability. Advanced methods have been de- at different depths. They showed that the impedance measured de-
veloped to monitor the moisture movement in unsaturated cement- creases significantly as the water front enters the “influence zone” of
based materials including nuclear magnetic resonance (NMR) spectros- the electrode pair. Due to the diffusive nature of the electric current,
copy [3–5], methods based on attenuation of electromagnetic radiation however, the impedance between the electrodes changes even by the
(e.g. gamma-ray [6–8], X-ray [9,7,10–13] and neutron [14–21] imag- moisture content change far from the height of the electrode pair. Con-
ing), and electrically-based methods [22–27]. sequently, the inference of the water front location based on such mea-
Each of the aforementioned methods has advantages and limita- surements is not a straightforward task.
tions. While NMR, gamma-ray, X-ray, and neutron imaging have a To estimate the location of the water front based on pairwise imped-
high resolution, they are generally limited to small specimens (from a ance measurements, both experimental and numerical calibration strat-
few millimeters to a few centimeters, depending on the equipment egies have been proposed. McCarter et al. [22,24,29] proposed a method
and source intensity) due to large energy requirements for imaging in which the rate of impedance change is monitored as a function of
large specimens. In addition, gamma-ray, X-ray and neutron imaging time, and the arrival of the water front at the height of the electrode
are invasive methods and are mainly limited to laboratory due to the re- pair is taken as the time at which the rate of impedance change is at
quired facilities. For example, neutron imaging (radiography/tomogra- maximum. Rajabipour et al. [26] derived an analytical function based
phy) requires a neutron source, such as a nuclear reactor. Electrically- on finite element simulations to relate the impedance between embed-
based methods, in contrast, have a low spatial resolution, but they are ded electrode pairs to the water front position. It is noted that the im-
noninvasive, inexpensive and rapidly performed. pedance measurements from horizontally aligned electrode pairs can
Various electrically-based methods, such as electrical impedance provide estimates for the water front location only if the water front is
spectroscopy (EIS) [26,28] and single frequency alternating current approximately horizontally aligned, i.e., the water flow is one-
measurements [28], have been used for monitoring unsaturated flow dimensional (1D). This assumption is not always valid; the water flow
can be non-uniform for example due to the spatial variation of the
porosity.
Electrical resistance tomography (ERT) is an imaging modality
⁎ Corresponding author. Tel.: +1 919 515 2235; fax: +1 919 515 7908. which could provide a robust tool for monitoring the moisture flow in
E-mail address: mpourghaz@ncsu.edu (M. Pour-Ghaz). concrete. In ERT, the three-dimensional (3D) distribution of the

http://dx.doi.org/10.1016/j.cemconres.2014.11.007
0008-8846/© 2014 Elsevier Ltd. All rights reserved.
M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18 11

electrical resistivity is imaged using a set of current injections and elec- 2.1. Materials
trode potential measurements. ERT has been used for monitoring the
water infiltration in soil [30–34]. Buettner et al. [35,36] have also stud- To facilitate simultaneous ERT and neutron radiography measure-
ied the feasibility of ERT for monitoring the water ingress in concrete. ments, several constraints had to be addressed. First, the neutron imag-
Stacey [37] applied ERT for monitoring moisture movement in Berea ing requires a nuclear reactor laboratory, and the allowable time for
sandstone. While the studies of Buettner and Stacey showed the poten- carrying out the experiment in this facility was limited. To reduce the
tial of ERT for monitoring the moisture flow in concrete and sandstone, duration of the test, highly porous cement paste was used to facilitate
the results of ERT were not corroborated by other techniques. Recently, a rapid water ingress. The rapid moisture movement, on the other
duPlooy et al. [38] used ERT to monitor (essentially) 1D water ingress in hand, constrains the time allowed for acquiring a neutron image: if
concrete slabs. One face of each slab was exposed to water for 23 days, the neutron exposure time is long, the moisture distribution changes
and ERT measurements were performed using electrodes attached to considerably during the exposure and causes artifacts in neutron im-
the wetted side of the slab. The results were in agreement with destruc- ages. To reduce the neutron exposure time, relatively thin samples
tive tests and the estimates from electrical capacimetry and ground were used in the experiment. Furthermore, the initial moisture content
penetrating radar. of the material had to be high enough; the electrical resistivity of a very
The objective of this study is to investigate whether ERT could give dry cementitious material is high, and this may cause problems in ERT
feasible information on the distribution of moisture in cases where the imaging [39]. It is also noted that enough contrast in conductivity, and
water flow is non-uniform. To this end, ERT imaging of moisture flow hence in moisture content, is necessary for the water movement to be
is experimentally compared with high resolution neutron radiography. detectable by ERT. The exact threshold for this contrast depends on
Both a horizontally uniform (1D) and a nonuniform (2D) water source many factors including the pore size distribution of the material, sensi-
are used, resulting in different shapes of the water front; in the 2D tivity of and the noise in measurements, and sample and electrode size.
case, the water front is not even approximately horizontally aligned. Establishing this contrast ratio requires experimental and computation-
al investigations. Finally, many setup accessories were made of Teflon or
aluminum, because they are almost “transparent” to neutrons and thus
2. Materials and methods do not cause artifacts in radiographs.

Two cement paste specimens were used in the experiment. A water 2.1.1. Cement paste material
reservoir was mounted on top of each specimen. ERT and neutron radi- Specimens used in this work were made of type I ordinary portland
ography measurements were simultaneously carried out during water cement (OPC, Type I) with a water-to-cement ratio (w/c) of 0.60. The
ingress. The entire top surface of the first specimen was exposed to plain cement paste and high w/c were selected in order to produce a
water, while in the second specimen the water reservoir covered only highly porous material. ERT measurements can be performed on con-
about one third of the top surface. The aim of this setting was to induce crete and mortar as well [38–40]. However, the feasibility of ERT to
a 1D water flow in the first specimen and a 2D flow in the second one. monitor moisture movement in concrete needs to be experimentally in-
Photographs of the two specimens 60 min after the addition of water vestigated in the future.
are shown in Fig. 1. The dark surface areas indicate the wetted regions,
and qualitatively the difference between the two flows is clear: in the 2.1.2. Sample preparation
first case (Fig. 1a) the water front is nearly horizontal, whereas in the The cement paste was mixed according to ASTM C305 and was cast
second case (Fig. 1b) water forms a curved plume which grows radially. in a 7.6 × 7.6 × 30.5 cm steel mold. The steel mold rested on a 7.6 cm ×
Although the photograph in Fig. 1a (and especially the neutron radio- 30.5 cm face during casting. After casting, the mold was wrapped in a
graphs in Section 3) shows that the water front in the first specimen is wet cloth and a layer of plastic. The specimen was demolded after
not exactly horizontal, we refer to this test case as the 1D flow case 18 h. To reduce the porosity gradient from top to bottom of the speci-
and the corresponding water source as the 1D source. Respectively, men (due to possible segregation in the high w/c cement paste) a
the attributes of the second specimen (Fig. 1b) are referred to as the 0.50 cm thick layer from the top of the prism was cut using wet saw
2D flow and the 2D source. and discarded. Next, the cement paste prism was sliced into 1.37 cm

Fig. 1. Photographs of the specimens 60 min after adding water: a) specimen with 1D water source; b) specimen with 2D water source.
12 M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18

thick square disks, resulting in 7.6 × 7.1 × 1.37 cm square disk speci- 2.1.3. Water reservoirs
mens. The accuracy of the cutting procedure was approximately ± Water reservoirs were mounted on top of the specimens using a thin
0.1 cm. The disks were moved to an oven at 50 °C for 5 h, and then layer of pure silicon caulk. The reservoirs were made of Teflon. In the 1D
sealed in two layers of plastic bag and placed inside an environmental source, the reservoir covered the entire top surface of the specimen,
chamber at 23 °C temperature for 21 days to achieve a relatively uni- while in the 2D source, the width of the reservoir was only 26 mm.
form moisture content throughout the specimen. Fig. 2b and c schematically illustrate the locations and sizes of the
The initial moisture content was made approximately uniform to water reservoirs with dotted lines.
investigate the feasibility of using ERT to monitor moisture transport
in controlled conditions, and to simplify the comparison of ERT images 2.1.4. Electrodes
and neutron radiographs. In a case of nonuniform initial moisture con- Surface mounted electrodes were placed at the perimeter surfaces of
tent, ERT imaging becomes a slightly more challenging task. However, the specimens. The electrodes were made by applying a thin layer of
ERT is not limited to cases where the initial moisture content is uniform; colloidal silver paint directly to the surface of the cement paste, and
it is possible to account for the effect of the inhomogenous initial condi- then applying a layer of conductive silver-filled epoxy on top of the
tion in ERT computations [41]. silver paint. The silver paint layer was intended to smoothen the cement
After conditioning, the two large surfaces of the specimens were paste surface to get a better electrical contact. Electrodes were connect-
sealed with a thin transparent tape (packing tape) to avoid evaporation ed to the measurement unit by force contacting aluminum screws to the
during the test. Fig. 2a shows a photograph of the 2D specimen. The surfaces of the mounted electrodes.
exact dimensions of both 1D and 2D specimens are shown in Fig. 2b A total of 15 electrodes were mounted on the 1D flow specimen
and c respectively. Note that during the experiment the specimens (5 electrodes at each side except the top) as shown in Fig. 2b. In the
were placed with the longer dimension vertically. Therefore, the casting case of the 2D flow specimen, 19 electrodes were mounted, as shown
direction – top to bottom during casting – was horizontal. The casting in Fig. 2c. The lengths of the electrodes were 8.0 mm in vertical direction
direction for the 1D specimen was from right to left and for the 2D spec- and covered the entire thickness of the specimen. Specimen dimensions
imen from left to right. and the electrode numbering are shown in Figs. 2b and c. The

Fig. 2. (a) Photograph of the specimen with a stripe water source (2D flow), (b) schematic illustration of the specimen with uniform water source (1D flow), (c) schematic illustration of
the specimen with stripe water source (2D flow).
M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18 13

photograph in Fig. 2a shows the 2D flow specimen after the electrodes the electrical resistivity inside the object is reconstructed. In addition to
were mounted. The spaces between the electrodes on the perimeter monitoring water ingress in concrete [35,36,38], ERT has been proposed
surface were sealed with a transparent tape to avoid evaporation. for detecting damage and other structural defects in concrete [39,40,
42–44]. In [41,45–48], surface breaking cracks in concrete were detect-
2.1.5. ERT measurement fixture ed with ERT applied on conductive films on the surface of concrete
For simultaneous ERT and neutron radiography measurements, the elements.
fixture shown in Fig. 3 was designed. The fixture and all connections A variety of computational methods for the image reconstruction in
were made of aluminum, while the parts in contact with the aluminum ERT has been developed [49]. In this paper, a standard difference imaging
screws attached to electrodes were made of Teflon. A 5 mm thick alumi- approach [50] is adopted. In difference imaging, a temporally varying
num sheet covered with a 2 mm thick Teflon sheet was installed at the object is imaged on the basis of the difference between ERT measure-
back of the fixture to improve the stability of the fixture and the speci- ments corresponding to two time instants. The difference data is used
mens. A steel mesh was secured to the back plate using aluminum for reconstructing the change of the resistivity between the two instants.
tape. The openings and the sizes of the wires provided a scale to cali- The difference reconstruction is conventionally based on a global linear-
brate the dimensions of the neutron radiographs. A triangular alumi- ization of the non-linear observation model of ERT, and consequently,
num water reservoir was mounted on the fixture. The neutron image the reconstructions are often qualitative in nature especially if the tem-
of the water triangle was used for determining the dependence be- poral variation of the resistivity is large or if the linearization point is
tween the optical density values of the neutron images and the moisture poorly selected. On the other hand, difference imaging is relatively tol-
content (see Section 2.3). erant to modeling errors, and hence widely used in many ERT applica-
In this work, the electrodes were placed all around the specimen. tions. In this study, the specimen before the start of the water ingress
However it is also possible to perform ERT measurements on samples was used as the reference state for difference imaging. The software
with only a single accessible side (e.g., slabs) [39]. In field applications used in the ERT reconstructions was based on Matlab implementations
of ERT to such geometries the use of more advanced computational by Vauhkonen et al. [51,52].
methods such as domain truncation might become necessary. Since in this study the electrodes on the perimeter surface covered
the entire thickness of a specimen, the ERT measurements did not
2.2. Electrical resistance tomography imaging carry information on the (possible) variation of the electrical resistivity
in the direction perpendicular to the two large surfaces of the speci-
In electrical resistance tomography (ERT), electric currents are mens. In other words, the setting only allowed for 2D ERT imaging. On
injected into an object through electrodes attached on the object's sur- the other hand, the neutron radiographs are also 2D images, and
face, and corresponding to each current injection, a set of electrode po- hence, 2D ERT reconstructions were sufficient for the comparisons
tentials are measured. Based on these measurements, the distribution of aimed at in this study. It is also worth noticing that the thin sample ge-
ometry was determined by the neutron radiography; if the specimens
had been thicker, a longer neutron exposure would have been needed.
ERT, by contrast, is not limited to 2D geometries; in most applications
3D ERT is used [53].
For simultaneous ERT and neutron radiography imaging, the ERT fix-
ture (Fig. 3) was positioned inside a neutron chamber. The ERT mea-
surement equipment was connected to the fixture with 3-meter-long,
shielded, high quality, low resistance cables. An in-house developed
equipment set [48,41] was used in the ERT measurements. The equip-
ment consisted of a current supply, a voltmeter, a manual switch system
and a computer for the data collection. A sinusoidal alternating current
(AC) with an amplitude of 2.0 mA and a frequency of 1 kHz was used in
all measurements. The frequency was chosen based on electrical imped-
ance spectroscopy (EIS) measurements. The frequency was kept as low
as possible to avoid inductance effects due to the long cables connecting
electrodes to the ERT measurement unit, and on the other hand, the fre-
quency had to be high enough to avoid electrode polarization effects.
With the selected frequency, the imaginary component of the imped-
ance was negligible. The same frequency was used by McCarter [27] to
monitor moisture penetration in concrete.
For ERT, 31 current injections were applied in the 1D flow case, and
39 injections in the 2D flow case. The currents were injected between
electrodes 2–14, 3–13, 4–12, 5–11 and electrodes i − j, i = {1,15}, j =
{1,…,N}, i ≠ j, where N is the number of electrodes (N = 15 in the 1D
flow case, and N = 19 in the 2D flow case). Corresponding to each cur-
rent injection, the electric potentials on all electrodes were measured
against a common ground, which was connected to one of the current
carrying electrodes. This resulted in a total of 465 potential measure-
ments in the 1D flow case and 741 measurements in the 2D flow case.
Since the current injections and potential measurements were switched
manually, collecting one data set took approximately 4 min. It is noted,
however, that for an automatic ERT system carrying out the same mea-
surements would take less than 1 s.
Fig. 3. ERT measurement fixture. 1. Aluminum frame, 2. steel mesh, 3. teflon frame, 4. spec-
For both samples, the first set of ERT measurements was carried out
imen with 2D moisture flow, 5. water reservoirs, 6. back plate, 7. water triangle, and 8. before water was added to the reservoir. These data sets were used as
specimen with 1D moisture flow. reference measurements in the difference imaging. After adding
14 M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18

water, multiple ERT measurements were performed on each specimen. the conversions, the optical intensity images were smoothed by low
For each specimen, a set of three ERT measurements are shown in this pass filtering, to reduce the effects of randomness in the radiation and
paper. In the case of the specimen with the 1D water source, the times attenuation.
of the measurements were 23 min, 32 min and 15 h 50 min. Here, the The above-described analysis of the neutron images differs slightly
reported times indicate the instants of completing an ERT measurement from the analysis made in studies [12,55–58] where the neutron attenu-
cycle, counted from the instant of adding water to the reservoir. The cor- ation coefficient of water, μw, was determined experimentally, and Beer's
responding times for the specimen with the 2D water source were Law was used for converting the neutron intensities to water contents. A
17 min, 28 min and 16 h 30 min. The measurement times were chosen different analysis was used, because in the present experiment, the
to match with the times of neutron radiography exposures, although an water contents were high, up to 0.40. Due to the well-known beam
exact match was not possible, due to long measurement times and some hardening effect, the Beer's law is applicable only for thin layers of
preparations that were required between the measurements. water, typically less than 1 mm total water thickness [59], which corre-
sponds to a water content of 0.073 in the present specimen geometry.
2.3. Neutron radiography
3. Results and discussion
The experiment was carried out at the PULSTAR nuclear reactor of
North Carolina State University. The neutron beam is comprised of ther- The results of the 1D and 2D water flow cases are shown in Figs. 4
mal neutrons with a nominal kinetic energy of approximately 0.05 eV. and 5, respectively. In both figures, the results of neutron radiography
The diameter of the beam at the imaging plane is 48 cm. The collimation are illustrated in the left column and the ERT reconstructions in the
ratio L/D is variable from 100 to 150 (where L is the distance between right column. The (finishing) time of the neutron exposure/ERT mea-
aperture and imaging plane and D is the diameter of the entrance aper- surements is shown under each image. Note that due to the rather
ture). The neutron flux at the image plane is approximately 1.8 × long durations of the neutron radiography (9 min) and ERT measure-
106 n cm−2 s−1. A conventional X-ray film using a Gadolinium convert- ments (4 min), it was not possible to exactly match the times of the im-
er screen and a vacuum cassette was used. The dimensions of the film ages. Since ERT measurements were faster than neutron radiography,
were 35.5 cm × 43.2 cm, covering the entire EIT fixture. The maximum multiple ERT measurements were performed during the experiment
resolution of the images using the film is approximately 33 μm [54]. and the ERT measurements that most closely matched the time of neu-
Based on a series of trial measurements, 9 min was identified as a tron radiography measurements were used for comparison. However,
feasible duration of the neutron exposure. The trial measurements since the water penetration slowed down approximately 8 min after
were also used for assessing the length of a transition period right the exposure to water, the radiograph–ERT image pairs in each row in
after adding water, during which the flow rate was high: after approxi- Figs. 4 and 5 are comparable despite the time lags between the images.
mately 8 min the water movement was slow enough to obtain clear ra- All six neutron images in Figs. 4 and 5 are represented in a mutual
diographic images with 9-minute neutron exposure. colorscale. The black and white color, respectively, correspond to the
A total of four neutron radiographic images were taken. The first maximum and minimum water content change Δw over all six neutron
image was taken before adding water to the reservoirs. This radiograph images. The ERT images are shown in individual colorscales, i.e. the min-
was used as a reference for the rest of the neutron images (see below). imum and maximum value of each ERT reconstruction is taken as the
The second neutron exposure started 10 min after adding water and minimum and maximum limit of the colorscale in each ERT image, re-
was completed 9 min later. This radiograph is referred to as the spectively. This choice is made, because the difference in ERT recon-
19 min image hereafter. Correspondingly, the neutron exposures for structions considered in this paper are qualitative in nature. The use of
the next two images were completed 35 min and 16 h after the addition a common colorscale for all six ERT images would render the contrast
of water. To avoid water depleting during the experiment, more water in some of the images extremely low, because the range of values varies
was added to the reservoirs after the second neutron exposure. Howev- between the images. Hence, the ERT reconstructions in Figs. 4 and 5 can-
er, the water reservoirs of both specimens got empty between the third not be interpreted in terms of absolute moisture content. Instead, they
and fourth neutron exposures. only provide qualitative information on how the moisture is spatially
To quantify the moisture movement, the radiographs were inter- distributed.
preted in terms of the moisture content based on the neutron images Qualitatively, a large negative resistivity change Δρ depicted with
of a triangular water reservoir (Section 2.1.5) as follows (cf. [55]). The red color in the ERT reconstructions should indicate a high water con-
neutron images of the triangular water reservoir (Section 2.1.5) provid- tent change Δw depicted with black in the neutron images. Respective-
ed neutron data of a linearly increasing thickness t of water. The water ly, a positive resistivity change should indicate the decrease of the water
thickness t was converted to volumetric moisture content w (corre- content. Note, however, that the occurrences of the positive resistivity
sponding to the thickness of the specimens ts) simply by division change are most probably reconstruction artifacts — in a setup where
w = t/ts. The pixel-wise optical density I in the neutron radiographs is water ingresses to porous medium, the change of the resistivity with re-
linearly proportional to the local intensity of the neutron flux. To ap- spect to the initial state is expected to be non-positive. Correspondingly,
proximate the dependence between w and I, a sixth order polynomial the negative values in Δw are probably artifacts — caused by imperfect
w = f(I) was fitted to I vs. w values. This low order approximate alignment of the neutron images corresponding to the initial state and
model provided an adequate fit to the data. the subsequent states.
In the cement paste, the attenuation is not solely caused by the
water component, and consequently, the polynomial approximation 3.1. 1D source case
w = f(I) determined using the water triangle observations cannot be di-
rectly used for converting the pixel-wise optical density I to the volu- The water ingress into the 1D specimen is shown in the neutron im-
metric moisture content w of the cement paste. However, the change ages in Fig. 4 (left column). In the 19 min image, the water front has
of the volumetric moisture content, Δw, can be estimated by subtraction moved approximately 2.0 cm from top of the specimen. After 35 min,
Δw ¼ w−winit , where winit ¼ f ðI init Þ and w ¼ f ðI Þ, respectively, are ob- the distance is about 2.6 cm, as evidenced by the boundary between
tained from the neutron data of the sample at the initial state and after the red and yellow color. These images also reveal a nonuniform pene-
wetting. Here, winit ¼ winit þ wc and w ¼ w þ wc , where winit and w are tration of water. Clearly, water flows slightly faster on the right hand
the actual water contents and wc can be interpreted as an equivalent side of the specimen. Moreover, the water content is higher (compared
water content, i.e., a water thickness that causes neutron attenuation to other wetted region) at the corners of the specimen, especially at the
equal with the attenuation caused by a completely dry specimen. Before top right corner. In the 16 h image, water has penetrated further. Again,
M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18 15

19 min 23 min

35 min 32 min

16 h 15 h 50 min
Fig. 4. Neutron radiography image (left column) and ERT images (right column) of the specimen with one-dimensional (1D) water source. The times of the neutron exposures/ERT mea-
surements are shown under the images.

water flow has been slightly faster on the right hand side of the speci- neutron–32 min ERT). Further, the 15 h 50 min ERT image clearly
men, and also this image shows the highest water content around the shows that the moisture has moved downwards.
top corners. As noted above, water in the reservoir depleted between It is worth noticing that 23 min and 32 min ERT images include
35 min and 16 h. In the absence of the external water source, the mois- wide green areas indicating a small negative change of the resistivity
ture gradient within the specimen has decreased. in positions where Δw is zero and no change of the electrical resistivity
The nonuniform penetration of water and the high water content at is expected. These errors in the reconstructions are partly due to
the corners of the specimen are probably caused by 1) a porosity gradi- smoothness-promoting regularization used in the solution of the
ent within the sample due to the high w/c and segregation, and 2) dam- ERT inverse problem and partly due to the linearization made in
ages at the corners, induced by cutting the samples. Although measures the difference imaging approach — and also due to the ill-
were taken to minimize damages, they may have occurred as the mate- posedness of the ERT inverse problem. Nevertheless, the movement
rial had a high w/c and the samples were sliced after only 18 h of curing. of the water front is very clearly indicated by ERT images in Fig. 4.
The ERT reconstructions in Fig. 4 (right column) capture the mois- The ERT images also reveal the nonuniformity of the flow: ERT
ture movement relatively well. In the 23 min ERT image, the area of shows correctly that the movement of the water front is fastest on
the low resistivity (high negative resistivity change) corresponds well the right hand side of the specimen. Also, the highest changes in
to the wetted area in the 19 min neutron image (Fig. 4, first row). The the electrical resistivity are detected at the highest moisture content
same applies to the pair of images in the second row (35 min region — the top corners of the specimen.
16 M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18

19 min 17 min

35 min 28 min

16 h 16 h 30 min
Fig. 5. Neutron radiography image (left column) and ERT images (right column) of the specimen with two-dimensional (2D) water source. The times of the neutron exposures/ERT mea-
surements are shown under the images.

3.2. 2D source case extent that at 16 h it covers the entire width of the specimen, and the
moisture is concentrated towards the top left corner of the specimen.
The neutron radiographs in Fig. 5 (left column) illustrate the mois- The ERT reconstructions are shown in the right column in Fig. 5. The
ture movement in the specimen with 2D (strip) water source. The 17 min and 28 min images illustrate the 2D flow well. The position and
shape of the plume in the 19 min and 35 min neutron images is similar shape of the plume is approximately tracked: The widths of the areas of
to that observed visually in the 60 min photograph (Fig. 1b). The size of low resistivity in the 17 min and 28 min ERT images correspond well to
the plume has increased between 19 min and 35 min. Although the the widths of the wetted areas in the 19 min and 35 min radiographs.
water source was in the middle of the top surface of the specimen, The depth of the plume is more difficult to assess based on the ERT im-
water has moved nonsymmetrically; the plume is off-centered and ages, because of the smoothness of the images discussed above. Howev-
slightly inclined towards the left. This is again probably due to the po- er, a slight growth of the plume can be detected based on the 17 min and
rosity gradient within the specimen. The 16 h neutron image shows 28 min ERT images. Moreover, these images show the non-symmetry of
that the depletion of the water reservoir has again resulted in the de- the moisture distribution: resembling the corresponding neutron radio-
crease of the moisture gradient by diffusion within the specimen. More- graphs, the low resistivity areas (depicted with red) are inclined to-
over, the diameter of the plume has further increased with time to the wards the left. Finally, the 16 h 30 min ERT reconstruction indicates
M. Hallaji et al. / Cement and Concrete Research 69 (2015) 10–18 17

that the moisture has concentrated around the top left corner of the or recommendations expressed in this paper are those of the author(s) and
specimen — a phenomenon shown also by the 16 h neutron image. do not necessarily reflect the views of the National Science Foundation.
It is worth noticing that the three ERT images in Fig. 5 are represent-
ed in different colorscales. This choice was made because of the qualita- References
tive nature of the difference reconstructions; in 17 min and 28 min ERT
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