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Separation of mercury from its aqueous solution through supported liquid membrane using
environmentally benign diluent
March 2010 · Journal of Membrane Science 350(1):395-401

DOI:10.1016/j.memsci.2010.01.016
Authors:
Kabita Prabirkumar Saha Aloke

Chakrabarty Indian Institute of Technology Guwahati Kumar
Ghoshal
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Citations (79) References (22)
Abstract
This paper presents an experimental investigation on Discover the

the facilitated transport of mercury through flat sheet world's research
supported liquid membrane (SLM) containing
25+
trioctylamine (TOA) as carrier and coconut oil, an
environmentally benign solvent, as diluent. Co-transport million
members
mode of mercury transfer was studied using aqueous
solution of NaOH as the strip phase. Various polymeric 160+
supports were tested in order to select the best SLM million
configuration. The SLM combination “PVDF–TOA– publication
coconut oil” shows encouraging results and it was pages
stable for a period of 98h. The fundamental parameters,
2.3+
such as feed phase pH and concentration, strip phase
billion
concentration, carrier concentration, etc., affecting the Join for free
citations
transfer of mercury through the SLM were studied. It
was observed that the extraction of mercury increases
with increase in NaOH concentration in the strip phase,
and becomes steady at a 0.3M NaOH. The extraction
process depends on feed phase pH and maximum
extraction was achieved at a pH of 1. The carrier
concentration had marginal effect on extraction as
about 91% separation of mercury was achieved without
any carrier in the SLM. Even at the most favourable
operating condition (viz., 0.3M NaOH, 4% TOA and pH
1), extraction of mercury was achieved up to 95%.
Coconut oil showed better performance in the
separation of mercury compared to other organic
solvents such as dichloroethane and heptane.
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Citations (79) References (22)
... These organic chemicals are harmful to living organisms and

environment [11,16]. Due to the recent greater stringent
environmental regulations [17] , studies on extraction methods
have directed to the more eco-friendly diluents (green diluents)
such as vegetable oils [16]. The bio-degradability, nontoxicity, non-
volatility, and inflammability with the other green features of the
vegetable oils, like palm, sunflower, cotton, coconut, corn, and
peanut oils make them a strong competitor for the traditional
diluents [15][16][18][19]. ...
... Several studies were carried out to investigate the effectiveness
of using vegetable oil as a green diluent with various extractants
[12, [15][16] [17] [18][19]. [11] examined the efficiency of using
some vegetable oils (sunflower, corn, and palm oil) as a diluent in
the formation of LEM consisting of Aliquat 336 (carrier), Span 80
(surfactant) and NaOH (internal phase). ...
Zirconium and Hafnium Separation by Novel Green Emulsion Liquid

Membrane Containing an Environmentally Benign Diluent
Article Full-text available
Mar 2020
Zeinab H Ismail · H. F. Aly
View
... This elevation is attributed to the heightened benzene ring

concentration, resulting in increased hydrogen bonds and
interactions formed between phenol and copoly(eugenol-DVB) 8%.
Consequently, a greater number of phenol complexes were formed
in the membrane phase, leading to an enhanced phenol transport
[36, 37, 38]. Nevertheless, at higher concentrations of the carrier,
specifically at 0.02 M and 0.025 M, there was a decrease in phenol
transport into the receiving phase. ...
Investigating Phenol Transport Using Copoly(Eugenol-DVB) 8% as a

Carrier with the Supported Liquid Membrane Method
Dec 2023
Windi Antika · Anisa Rahmawati · Rinawati Rinawati · Agung
Abadi Kiswandono
View Show abstract
... The methods used for the elimination of organic pollutants

include precipitation, filtration, ion exchange, flotation, reverse
osmosis, electrolysis, and membrane separation [18,19].
Furthermore, these technologies consume a lot of energy and
produce hazardous sludge or other waste products that need to be
disposed of [20] . Sometimes, these processes may recreate lethal
metal sludge. ...
Schiff-Based Modified Bentonite Clay Composites for Wastewater
Treatment: Experimental and DFT-Based Analysis
May 2023
Sadaf Mutahir · Fakhira Yaqoob · Muhammad Asim Khan ·
Bader Huwaimel
View Show abstract
... This is due to the fact that MWCNTs result in smaller pore sizes
than without MWCNTs. Because the support cannot hold the
organic carrier for an extended period of time, larger pore size
polymeric membranes have a higher tendency to leach [100] . The
presence of CNTs in the system, on the other hand, caused
membrane instability due to the hydrophilicity derived from CNT
polar groups [97]. ...
Sustainable and effective contaminants transport beyond stability

barrier of supported liquid membrane: How crucial and vital is the…
Article
Oct 2022
Mohd Hazarel Zairy Mohd Harun · Abdul Latif Ahmad
View Show abstract
... Liquid membrane techniques are used for separation of trace

quantity of solute from a solution, e.g., the removal of metal ions
from the wastewater [1][2][3] [4] . The other applications of LM
technique include but are not limited to removal of organics from
wastewater [5][6][7][8], recovery of bio-actives compounds from
plants [9][10][11], separation of biologically important products such
as various antibiotics from the fermentation broth, and bioactive
catechin from tea leaves [12][13][14]. ...
Study of the supported liquid membrane for the estimation of the

synergistic effects of influential parameters on its stability
Jan 2016
Aman Kumar · Mriganka Manna · Aloke Kumar Ghoshal ·
Prabirkumar Saha
View

from the wastewater [1][2][3] [4] . The other applications of LM
technique include but are not limited to removal of organics from
wastewater [5][6][7][8], recovery of bio-actives compounds from
plants [9][10][11], separation of biologically important products such
as various antibiotics from the fermentation broth, and bioactive
catechin from tea leaves [12][13][14]. ...

Mar 2016
Aman Kumar · Aloke Kumar Ghoshal · Mriganka Manna ·
Prabirkumar Saha
View
... Sulaiman et al. [17] claimed that the viscous palm oil helps to
stabilize the SLM support which inhibits the loss of the LM phase
within the pores of the PVDF support. Similar observations were
reported by previous studies, where the high capillary force of the
viscous solvent in the membrane support could reduce the
displacement of liquid membrane from the membrane support
matrix [22] [23] . However, the viscous palm oil resists the
permeation of nickel in the organic phase. ...
Prediction of Nickel Removal using Diffusion Model in Flat Sheet

Supported Liquid Membrane
Dec 2021
Kissan Vithilingam · Raja Norimie Raja Sulaiman · Norasikin
Othman
View Show abstract
... Several techniques are available for removal of Hg(II), including

chemical precipitation, coagulation ion exchange, chemical
reduction, membrane filtration, electrochemical separation, reverse
osmosis, biological treatment, solvent extraction, and adsorption
(Chakrabarty, Saha, & Ghoshal, 2010; Hanif et al., 2016;López-
Maldonadoa, Oropeza-Guzmana, Jurado-Baizaval, & Ochoa-Terán,
2014;López-Munoz, Aguado, Arencibia, & Pascual, 2011;Sharma,
Sharma, & Arya, 2015;Zheng et al., 2019). Till now, one of the
useful and cost-effective technique for Hg(II) removal from water
wastes is adsorption (Gisi, Lofrano, Grassi, & Notarnicola, 2016). ...
Fabrication of thiophene-chitosan hydrogel-trap for efficient

immobilization of mercury (II) from aqueous environs
Article
Aug 2020 · CARBOHYD POLYM
Santu Maity · Nabanita Naskar · Biswajit Jana · Jhuma
Ganguly
View
... In this context liquid membrane (henceforth referred as LM)

technology is proved to be very promising technology to separate
chromium from wastewater. Interested readers may go through the
published literatures of this research group regarding separation of
heavy metals using LM based techniques (Chakrabarty et al.,
2009 (Chakrabarty et al., , 2010a (Chakrabarty et al., ,
2010bBhatluri et al., 2013Bhatluri et al., , 2014Bhatluri et al., ,
2015Bhatluri et al., , 2015bBhatluri et al., , 2017. Use of
environmentally and physiologically benign vegetable oils in the
organic phase of the LM is one of the major and crucial merits of
these works, which makes the process green in nature. ...
Removal of hexavalent chromium from wastewater using supported

liquid membrane: Synthesis of chromium‐iron complex through…
Article
Apr 2020
Supriyo Mondal · Prabirkumar Saha
View Show abstract
... The result is likely to be coherent with the required amount of

carrier and stripping agent to transport higher amount of succinic
acid. This result also could be related to the complex formation that
control the external mass transfer of low solute concentration
(Chakrabarty et al., 2010) . Hence, the extraction rate at high
concentration is lower than that at low initial succinic acid
concentration. ...
Development of Vegetable Oil-Based Emulsion Liquid Membrane for

Downstream Processing of Bio-Succinic Acid
Article
Nov 2019 · FOOD BIOPROD PROCESS
Norela Jusoh · Raja Norimie Raja Sulaiman · Norasikin
Othman · Hilmi Abdul Rahman
View Show abstract
... According to those standards, the concentrations of mercury in

drinking water have to be very low and in most cases the level of
mercury in water and especially ground water higher than accepted
concentrations [8]. To reduce the concentration from water, some
separation processes have been used including; ion exchange [9],
solvent extraction [10], adsorption [11], precipitation [12] and
membrane separation [13] . In recent years the adsorption of
mercury onto mesoporous silica to treat the drinking water from
high concentration of mercury, has proved to be a valuable
separation/preconcentration technique [14]. ...
Adsorption, Kinetic and Thermodynamic Studies for Mercury

Extraction from Water Samples Using Mesoporous Silica
Article
Jan 2019
Salah Ali Mahgoub Idris
View
... Several studies using liquid membrane methods have been

developed by several researchers to handle various pollutants,
including mercury metal separation [2] , strontium separation from
[13], permeation of gas [13], CO2/N2 separation [3], arabinitol and
perseitol transport [5], cesium transport [6], and phenol transport
[7,8,16]. Separation using liquid membrane method, one of which is
polymer inclusion membrane (PIM) always involves a carrier
compound. ...
Copoly Eugenol Crosslinked Dialylphthalate 8% as a Carrier in

Phenol and Pb(II) Metal Transport
Oct 2019
Agung Abadi Kiswandono · Sutopo Hadi · Mudasir · M Irfan
View Show abstract
... TOA is cationic carrier frequently used for the extraction of metal
ions. This carrier as an extractant can be applied for the transport
of Cd ions through a BLM [165], the extraction and concentration of
Cd from F. Tajabadi and M. Ghambarian Talanta 206 (2020) 120145
zinc plant leach solutions by ELM [10], the simultaneous separation
of Hg and lignosulfonate from aqueous solution using SLM [166]
and the separation of Hg from its aqueous solution through SLM
[167] . Aliquat 336 is another cationic carrier commonly applied for
the separation of a wide variety of metallic and organic compounds.
...
Carrier-mediated extraction: Applications in extraction and

microextraction methods
Article
Jul 2019 · TALANTA
Fateme Tajabadi · Mahnaz Ghambarian
View Show abstract
... Several physical and chemical treatments are used or have been
proposed to remove these Hg species. Removal processes include
methods to eliminate particle-bound Hg (e.g., filtration) and to
adsorb dissolved Hg species (e.g., activated carbon treatment, ion
exchange, amalgamation, chemical precipitation, electrodeposition,
reverse osmosis, photochemical methods, flotation, mechanical
filtration, membrane separation, and selective liquid-liquid
extraction) (Biester et al., 2000;Mahmoud and Gohar,
2000;Huttenloch et al., 2003;Kostal et al., 2003;Chojnacki et al.,
2004;Olkhovyk and Jaroniec, 2005;Smuleac et al., 2005;Oehmen
et al., 2006;Evangelista et al., 2007;F abrega and Mansur,
2007;Lopes et al., 2007;Park et al., 2007;Vieira et al.,
2007; Chakrabarty et al., 2010) . The efficacy of any treatment
process depends on the speciation of Hg, water quality parameters,
and sorbent properties. ...
Impact of mercury speciation on its removal from water by activated

carbon and organoclay
Article
Apr 2019 · WATER RES
Ke Gai · Astrid Avellan · Thomas P Hoelen · Gregory V Lowry
View Show abstract
... Techniques to remove Hg are highly dependent on the speciation

of Hg, such as organic and inorganic mercury (Saleh,
2015a,b;Saleh et al., 2017a,b,c,d;Saleh et al., 2018). In recent
years, an abundant of techniques including adsorption (Vafaei
Molamahmood et al., 2018), precipitation and membrane
separation (Chakrabarty et al., 2010; Zhang et al., 2018b),
reduction (Fan et al., 2018) and ion exchange (Rajamohan and
Rajasimman, 2017) have been employed to remove Hg(II). Among
them, adsorption is considered simpler and more efficient (Adio et
al., 2017;Hadi et al., 2015). ...
Selective removal behavior and mechanism of trace Hg(II) using

modified corn husk leaves
Article
Mar 2019 · CHEMOSPHERE
Guo Lin · Tu Hu · Shixing Wang · Xiong Chao
View
... Studies on mercury removal from water involve a great variety of

techniques such as: reverse osmosis [11], coagulation [12], solvent
extraction [13], micellar enhanced ultrafiltration (MEUF) [14],
complexation-filtration [15,16], supported liquid membranes (SLM)
[17, 18] , ion exchange resins [19], adsorption on solid substrates
[20][21][22][23][24] and bioremediation using living macroalgae
[25]. However, only two of these techniques stand out: solvent
extraction and ion exchange resins. ...
Modelling the mercury removal from polluted waters by using

TOMAC microcapsules considering the metal speciation
Article
Feb 2018 · CHEM ENG J
Ana M. Borreguero · Adriana Leura · Juan Francisco
Rodríguez · Manuel Carmona
View Show abstract
... The transport process in SLM is a combination of two

simultaneous steps, including extraction and reextraction. The first
one is sharing the substrate between the aqueous source and the
organic membrane phases by interaction of substrate with the free
carrier in membrane (formation of substrate-carrier), and the
second step is sharing the substrate between the membrane and
the receiving phases by dissociation of the entity form [30]. On the
other hand, it should be noted that the technique of supported liquid
membranes is used for the extraction of organic compounds [31]
[32][33][34][35][36][37] and also the metal ions [38][39][40][41][42]
[43][44][45][46][47][48][49][50] [51] [52][53][54][55]. ...
Review on Mechanism of Facilitated Transport on Liquid Membranes

Jun 2017
Tarik Eljaddi · lebrun laurent · Miloudi Hlaibi
View Show abstract
... Mercury is one of the heavy metals which are considered being
toxic, persistent and non-biodegradable in the environment [1, 2].
The persistence phenomenon is considered as a sign of worry
when it is subjected to human body. ...
Mercury Extraction in Presence of Cobalt Using Hollow Fiber

Supported Ionic Liquid Membrane
Jan 2017
Mahmudul Hasan Khan Neon · Jayakumar Natesan
View Show abstract

from the wastewater123 4 . The other applications of LM technique
include but are not limited to removal of organics from
wastewater5678, recovery of bio-actives compounds from
plants91011, separation of biologically important products such as
various antibiotics from the fermentation broth, and bioactive
catechin from tea leaves121314. Among the various configurations
of the LM, the SLM is the most widely applicable technique in
commercial scale owing to certain advantages including
requirement of very less amount of solvent, requirement of low
footprint, low capital investment and higher flux of the solute
[10,11]. ...

Article
Mar 2016
Aman Kumar · Mriganka Manna · Aloke Kumar Ghoshal ·
Prabirkumar Saha
View Show abstract
... Hence, it is evident that mere solution diffusion is not enough for
LS transport; some facilitation is required for it. On the other hand,
it was observed that coconut oil could be used as an important
alternative for solvent in lieu of toxic organic solvent (Chakrabarty
et al., 2010b) . It was also observed that LS is highly soluble in
coconut oil even without any carrier agent. ...
Chapter Five. Liquid – Membrane Filters

Chapter
Dec 2015
Aloke Kumar Ghoshal · Prabirkumar Saha
View Show abstract
Mercury elimination from synthetic petroleum produced water using

green solvent via liquid-liquid extraction: Experimental, effective…
Article
Apr 2023
Kanyanat Duangchan · Wikorn Punyain · Vanee Mohdee · Ura
Pancharoen
View
Sustainable Green Synergistic Emulsion Liquid Membrane

Formulation for Metal Removal from Aqueous Waste Solution
Chapter
Dec 2022
Norul Fatiha Mohamed Noah · Norasikin Othman · Norela
Jusoh · Raja Norimie Raja Sulaiman
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Mechanisms of Mercury Ions Separation by Non-toxic Organic Liquid

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Nov 2022 · J IND ENG CHEM
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Selective mercury adsorption and enrichment enabled by phenylic

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Home Transition Metal Chemistry Mercury

March 2010 · Journal of Membrane Science 350(1):395-401

Kabita Prabirkumar Saha Aloke

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Citations (79) References (22)

This paper presents an experimental investigation on Discover the

To read the full-text of this

Citations (79) References (22)

... These organic chemicals are harmful to living organisms and

Zirconium and Hafnium Separation by Novel Green Emulsion Liquid

... This elevation is attributed to the heightened benzene ring

Investigating Phenol Transport Using Copoly(Eugenol-DVB) 8% as a

View Show abstract

... The methods used for the elimination of organic pollutants

View Show abstract

Sustainable and effective contaminants transport beyond stability

View Show abstract

... Liquid membrane techniques are used for separation of trace

Study of the supported liquid membrane for the estimation of the

... Liquid membrane techniques are used for separation of trace

Study of the supported liquid membrane for the estimation of the

Prediction of Nickel Removal using Diffusion Model in Flat Sheet

View Show abstract

... Several techniques are available for removal of Hg(II), including

Fabrication of thiophene-chitosan hydrogel-trap for efficient

... In this context liquid membrane (henceforth referred as LM)

Removal of hexavalent chromium from wastewater using supported

View Show abstract

... The result is likely to be coherent with the required amount of

Development of Vegetable Oil-Based Emulsion Liquid Membrane for

View Show abstract

... According to those standards, the concentrations of mercury in

Adsorption, Kinetic and Thermodynamic Studies for Mercury

... Several studies using liquid membrane methods have been

Copoly Eugenol Crosslinked Dialylphthalate 8% as a Carrier in

View Show abstract

Carrier-mediated extraction: Applications in extraction and

View Show abstract

Impact of mercury speciation on its removal from water by activated

View Show abstract

... Techniques to remove Hg are highly dependent on the speciation

Selective removal behavior and mechanism of trace Hg(II) using

... Studies on mercury removal from water involve a great variety of

Modelling the mercury removal from polluted waters by using

View Show abstract

... The transport process in SLM is a combination of two

Review on Mechanism of Facilitated Transport on Liquid Membranes

View Show abstract

Mercury Extraction in Presence of Cobalt Using Hollow Fiber

View Show abstract

... Liquid membrane techniques are used for separation of trace

Study of the supported liquid membrane for the estimation of the

View Show abstract

Chapter Five. Liquid – Membrane Filters

View Show abstract

Mercury elimination from synthetic petroleum produced water using

Sustainable Green Synergistic Emulsion Liquid Membrane

View Show abstract

Mechanisms of Mercury Ions Separation by Non-toxic Organic Liquid

View Show abstract