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DOC NO.

: FC/F/05
CENTRE FOR RESEARCH IN ADVANCED FLUID AND PROCESSES REV: 01
UNIVERSITI MALAYSIA PAHANG EFFECTIVE DATE:
LEBUH PERSIARAN TUN KHALIL YAAKOB, 26300 KUANTAN, PAHANG 01/01/2023
PHONE: +609-431 5058 | EMAIL: fluidcentre@ump.edu.my

EQUIPMENT REQUISITION FORM


STUDENT’S INFORMATION

NAME: …………………………………………………………………………………………………………………

ID NO: …………………………………………………………………………………………………………………

EQUIPMENT FOR TESTING (Please tick (√) the applicable box)


SEM DSC

  Hitachi TM3030Plus  Jeol JSM-IT200  Ramping: Initial Temperature: …………


  Surface imaging Final Temperature: ………….
 EDX:  Elemental Analysis  Temperature Program (if any):
 Mapping ………………………………………………...
 Line ………………………………………………...
  Coating  Non-coating  Heating Rate: ……………………………...
 Type of sample:  Powder / Fiber / Solid  Gas:  Nitrogen
 Metal  Gas flow rate: ……………………………...
 Film  Type of sample:  Solid  Liquid
 Etc: ……………………

FTIR TGA

 Method:  ATR  KBR (for powder only)  Ramping: Initial Temperature: …………
 Spectrum:  Absorbance  Transmittance Final Temperature: ………….
 Library:  Yes  No  Temperature Program (if any):
 Spectrum:  Overlay  Stacking ………………………………………………...
 Type of sample: ………………………………………………...
 Powder  Solid  Liquid  Heating Rate: ……………………………...
 Gas:  Nitrogen  Oxygen  Air
 Gas flow rate: ……………………………...
 Type of sample:  Solid  Liquid

UV-VIS NIR ICP-OES

 Wavelength:  Absorbance  Standard 1:


 Transmittance As, K, La, Li, Mn, Ni, Sr, Zn, Ba, Mg
 Reflactance (solid/ film)
 Standard 2:
 Wavenumber:  Scan From: …….... to ……....
K, Si, Al, B, Ba, Na, Ag
 Scan at ……....
 Scan at ……....  Standard 3:
 Scan at …….... As, Tl, Cd, Pb, Se
 Type of sample:  Solid  Liquid
DOC NO.: FC/F/05
CENTRE FOR RESEARCH IN ADVANCED FLUID AND PROCESSES REV: 01
UNIVERSITI MALAYSIA PAHANG EFFECTIVE DATE:
LEBUH PERSIARAN TUN KHALIL YAAKOB, 26300 KUANTAN, PAHANG 01/01/2023
PHONE: +609-431 5058 | EMAIL: fluidcentre@ump.edu.my

EQUIPMENT REQUISITION FORM


ROTARY EVAPORATOR
 Standard 4:
 Temperature: ……………………………… Ag, Al, B, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe,
Ga, In, K, Li, Mg, Mn, Na, Ni. Pb, Sr, Tl, Zn
 Rotational Speed: ………………………...
 Type of sample:  Liquid  Type of sample:  Aqeous  Oil

VISCOMETER FLASH POINT

 Speed: ……………………………………...  Expected Flash: …………………………..


 Time: ………………………………………...  Type of sample: …………………………..
 Data Point: …………………………………
 Type of sample: …………………………...

INCUBATOR SHAKER FURNACE

 Time: …………………………………………  Ramping: …………………………………..


 Temperature: ………………………………  Isothermal: …….. C …….. hour
 Type of sample: ……………………………  Program: …………………………………...
…………………………………...

 Type of sample: …………………………..

X-RAY PHOTON SPECTROSCOPY (XPS) TRANSMISSION ELECTRON MICROSCOPE


(TEM)

  Survey scan   Standard Imaging


  Survey with narrow scan   Cryo-TEM Imaging
Expected elements: .......................................   Ultra-cryo Microtome
  Mapping
  Line

X-RAY DIFFRACTION (XRD) X-RAY FLUORESCENE (XRF)

 Analysis:  Results:  Elemental  Oxide


 Phase Identification  Quantification  Type of sample:
 Method:  Powder  Liquid
 Default  Method:
 Custom (please fill in the parameter below)  Loose powder  Liquid
 Start angle (°) : …………………….
 End angle (°) : …………………….
 Step size (°) : …………………….
 Time per step (s) : …………………….

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