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SANS 6269 (2005) - Welding of Thermoplastics - HDPE
SANS 6269 (2005) - Welding of Thermoplastics - HDPE
SANS 6269:2005
Edition 1.1
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Table of changes
Change No. Date Scope
Amdt 1 2005 Amended to change the designation of SABS standards to SANS
standards with no technical changes.
Acknowledgement
The SABS Standards Division wishes to acknowledge the valuable assistance derived from
publications of the following organizations:
Foreword
This standard was approved by National Committee SABS TC 1041, Welding of thermoplastics, in
accordance with procedures of the SABS Standards Division, in compliance with annex 3 of the
WTO/TBT agreement.
Annex A forms an integral part of this document. Annex B is for information only.
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Contents
Page
Acknowledgement
Foreword
1 Scope ..................................................................................................................................... 3
4 Requirements ......................................................................................................................... 4
Annex A (normative) Test piece details and locations of test specimens for
flat sheet samples ................................................................................ 24
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SANS 6269:2005
Edition 1.1
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1 Scope
This standard describes methods of testing welded joints in a specified range of thermoplastics (see
table 1).
a) tensile test;
b) tensile-creep test;
d) peel test.
Commonly used acceptance criteria are given for each test method.
2 Normative references
The following standards contain provisions which, through reference in this text, constitute
provisions of this standard. All standards are subject to revision and, since any reference to a
standard is deemed to be a reference to the latest edition of that standard, parties to agreements
based on this standard are encouraged to take steps to ensure the use of the most recent editions
of the standards indicated below. Information on currently valid national and international standards
can be obtained from the SABS Standards Division.
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1 2
Symbol Material description
PE-HD High-density polyethylene (rigid PE)
PP-B Polypropylene block copolymer
PP-H Polypropylene homopolymer
PP-R Polypropylene random copolymer
PVC-C Chlorinated polyvinyl chloride
PVC-Hi High-impact polyvinyl chloride
PVC-U Unplasticized polyvinyl chloride (rigid PVC)
PVDF Polyvinylidene fluoride
Owing to their molecular and structural build-up, these thermoplastics have specific characteristics
in processing and in their applications. When semi-finished products of thermoplastics are being
used, especially for load-bearing members, these material characteristics have to be taken into
account, in particular in cases of simultaneous mechanical, thermal and chemical stress.
Further information on the characteristics of semi-finished products, for example pipes, plates,
sections and mouldings, can be found in DVS 2201-1, and the properties of the most common
thermoplastics for structural calculations can be found in DVS 2205-1.
4 Requirements
The appropriate test methods shall be selected according to the end usage of the particular product.
The validity of the test results depends on the conditions of manufacture of the test specimens and
on the test conditions. The results are translatable to a prediction of the final behaviour of the
product only if the conditions of test specimen manufacture and testing correspond to those of the
final product in use. Stresses induced during fabrication shall also be taken into account.
The weldability of a given combination of base and filler material should be verified with the welding
filler manufacturer.
Test piece details and locations of test specimens are provided in annex A.
Unless otherwise stated in the specification that cites this standard, and where applicable,
acceptance criteria shall be as given in 5.5 (tensile strength welding factor), 6.9 (tensile creep
welding factor), 7.5 (bending angle), and 8.8 (decohesion percentage).
5 Tensile test
5.1 Preparation of test specimens
5.1.1 The tensile test described in this subclause is based on a method described in DVS 2203-2,
which may be read in conjunction with this standard.
5.1.2 The preparation of the welded joint in the test specimen shall accurately reflect the actual
production conditions, i.e. with or without weld bead or reinforcement.
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5.1.3 A minimum of five welded test specimens shall be tested. A further five unwelded test
specimens shall also be tested. The latter five unwelded specimens serve as reference samples.
The shape and dimensions of the test specimens shall be as shown in figure 1 (a), as applicable to
the weld under test. If the specimen shown as type 1 in figure 1 (a) tears at the clamping device,
specimens according to type 2 shall be used.
5.1.4 When tensile tests are carried out on a socket-type joint, the test specimen shall comprise
one socket and two pipe components (see figure 1 (b)).
This is in order to eliminate any tendency for the specimen to deflect laterally under tension and
thus to introduce a bending moment, as would be the case if only a single pipe component were
used.
1 2 3 4 5 6 7 8
Thickness Test specimen type 1 Test specimen type 2
h b L1 L b L1 L be
≤ 10 15 120 ≥ 170 10 115 ≥ 170 20
> 10 30 120 ≥ 300 30 115 ≥ 300 40
> 20 1,5 t 200 ≥ 400 1,5 t 200 ≥ 400 80
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If, during the normal test, the fracture does not occur in the weld area, the test specimen may be
weakened in the joint by the introduction of a round hole (for example, 3 mm diameter) drilled
centrally through the weld area. In this case, the reference unwelded test specimens shall be drilled
in the same manner.
5.2 Procedure
5.2.1 Unless otherwise agreed upon or specified in the terms of delivery for the product to be
tested, the test shall be carried out at an ambient temperature of 23 °C ± 2 °C.
5.2.2 Before the test, visually inspect the test specimen, and the welded area in particular, and
note the results.
5.2.3 Condition the test specimen for a minimum of 16 h (or for 96 h in referee cases) at the testing
temperature.
5.2.4 During the test, ensure that the specimen is extended at a uniform test speed. The test
speed is the speed at which the two clamping devices move away from each other during the test.
The preferred test speed is the speed at which the yield strength of the unwelded test specimen is
reached in approximately one minute.
The recommended test speeds for the materials covered in this standard are given in table 3.
1 2
Test speed
Material
mm/min
PE-HD 50
PP, PVDF 20
PVC 10
The force to be read is the force at the instant of fracture. If the specimen is stretched beyond its
yield point, the force at yield stress shall be read and the test terminated. If necessary, the duration
of the test shall be measured and the stress-strain curve recorded. Tests where the specimens
fracture in the region of the clamping shall be disallowed.
5.3 Evaluation
The tensile welding factor fz = FV/FB is determined from the mean values of the fracture forces of the
welded test specimens (FV) and the reference test specimens (FB). If the specimens are stretched
before fracture, the force at yield stress shall be taken as the reference value.
In arbitration tests and in the case of test specimens that differ in thickness and width, the force is to
be related to the product b x h (where b = width of test piece, h = thickness of test piece) at the
centre of the test piece or directly next to the joint. The welding factor is then calculated according
to the formula:
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FV bB × h FV bB h
B B
fz = × = × ×
bV × hV F FB bV hV
B
The appearance of the test pieces after the test shall be noted, and in particular the type of fracture
and the fracture appearance shall be assessed.
d) the overall appearance of specimens before the test, and visual assessment of the weld;
h) the thickness and width of the test specimens, in millimetres (mean values);
m) the applicable of the force at fracture, the force at yield stress, or the corresponding stress
values;
p) the appearance of the test specimens after the test and visual assessment of the appearance of
the fracture; and
The mean value for the five (or more) specimens shall be at least the value shown in table 4.
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If no fracture has occurred in the test specimens, the ratio of the yield stresses in welded and
unwelded specimens shall comply with table 4.
1 2 3 4 5 6
Tensile welding factor
fZ
Welding process
PVC-HI
PE-HD PP PVC-C PVDF
PVC-U
Heated-tool welding 0,9 0,9 0,8 0,9 0,9
Extrusion welding 0,8 0,8 – – –
Hot-gas welding 0,8 0,8 0,7 0,8 0,8
Electrofusion welding 0,9 0,9 – – –
Solvent welding – – 0,8 0,9 0,9
6 Tensile-creep test
6.1 Principle of test
Creep is the occurrence of an increase in strain with time while the load remains constant.
In general, tensile-creep testing involves subjecting a test specimen, under constant ambient
conditions, to a static load that is kept constant throughout the test.
The tensile-creep test is appropriate for all joint types where environmental factors are a
consideration, for example where a pipe carries hot sulfuric acid or other dangerous chemicals, or
operates for long periods at an elevated temperature.
In the particular test described in this standard, the procedure is repeated for different load values in
order to obtain a curve of stress-versus-time points.
Specifications for gripping devices and the loading system are given in ISO 899-1.
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Unless otherwise agreed upon, the test shall be carried out in air at a constant temperature of
23 °C ± 2 °C.
NOTE By mutual agreement, the test duration may be shortened by testing at a higher temperature. The
duration of the test may also be shortened by the use of environmental reagents or media. Media that cause
specimens to swell, or bring about chemical changes, shall not be used. For PE-HD, aqueous wetting agent
solutions have proven satisfactory.
The load values selected should reflect the stress levels that the product will experience in practice.
The tensile force per unit area for the specimen can be calculated from the equation:
F = σ × A
where
The test load shall be so selected as to produce a fracture before excessively large deformations
take place.
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Use test specimens of the shape and dimensions shown in figure 1(a) for the tensile test. If the
specimen shown as type 1 tears at the clamping device, use specimens of type 2.
For each load value, prepare at least five welded and five unwelded specimens. (If statistical
analysis is to be used, increase the number of specimens to a minimum of six each.)
Since at least two load values have to be used in the test, the minimum required number of welded
and unwelded specimens is ten of each (or twelve of each if statistical analysis is used).
Before testing, condition the test specimens in the test atmosphere (temperature and humidity) until
no further dimensional changes occur.
6.6 Procedure
6.6.1 Before the test, visually inspect each test specimen, and the welded area in particular, and
note the results.
6.6.2 The test specimens have to be pre-loaded initially. Ensure that the pre-load does not exceed
5 % of the smallest test load and that it does not cause any significant strain.
6.6.3 Then so load the test specimen smoothly and steadily that the required test load is reached
within a period of 1 s to 5 s. Take the instant when the load is fully applied as time t = 0.
Allow the test to continue until fracture of the specimen occurs. Note the time to fracture and the
cross-section of the specimen. If so required, also note the elongation of the fractured specimen.
6.6.4 Although not necessary for the purpose of the test, it might sometimes be beneficial to take
intermediate readings between the application of the initial load and fracture in order to gain a better
insight into the course of the creep curve of the specimen. In this case, the first strain measurement
reading need only be taken after a period of at least ten times the period required to apply the total
test load.
For further information on this type of testing and the use of results gained from it, and for fuller
details of the test procedure, see ISO 899-1.
6.7 Evaluation
In order to determine the tensile-creep welding factor FS, the creep fracture curves for the welded
and unwelded specimens shall first be plotted on axes of stress-versus-time.
The values for the co-ordinates of points on the time axis of each curve are calculated as the
geometric mean of the time to fracture for each group of five specimens, i.e.
5 t1 × t 2 × t3 × t 4 × t 5
10
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The values for the co-ordinates of points on the stress axis of each curve are calculated from the
applied load and the final cross-sectional areas of the specimens. The stress value at fracture for
each specimen is then calculated by the formula given in 6.4, and the geometric means of each
group of five specimens are calculated.
The points obtained as above are then plotted as curves for the welded and unwelded test
specimens.
A vertical line is then drawn through both curves at a constant time value.
The tensile-creep welding factor fS is the ratio of the stress values at fracture in the welded and
unwelded test specimens at a constant time, i.e.
σ 1S σ
fS = and 2S
σ 1B σ 2B
NOTE A constant welding factor over the whole range will only result if the curves are parallel.
d) the overall appearance of specimens before the test, and visual assessment of the weld;
g) the thickness and width of the test specimens, in millimetres (mean values);
11
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n) the tensile-creep welding factor fS, with associated tensile stress value of unwelded test
specimen;
o) the permanent fracture elongation of welded and unwelded test specimens, if required;
p) the appearance of the test specimens after the test and visual assessment of the appearance of
the fracture; and
1 2 3 4 5 6
Tensile creep welding factor
fs
Process
PVC-HI
PE-HD PP PVC-C PVDF
PVC-U
Heated-tool welding 0,8 0,8 0,6 0,6 0,6
Extrusion welding 0,6 0,6 – – –
Hot-gas welding 0,4 0,4 0,4 0,4 0,4
7 Bend test
7.1 Preparation of test specimens
7.1.1 The bend test as described in this standard is based on a method described in DVS 2203-5,
which may be read in conjunction with this standard.
Dress the weld bead flat along the side in contact with the bending beam. This will generally be the
root side of the weld. Radius the longitudinal edges on the underside of test specimens, as shown
in figure 4.
12
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7.1.3 The shape and dimensions of the test specimens are given in table 6. (See also figure 5.)
In table 6, the test specimen thickness relates to the nominal thickness of the product. In the case of
pipes, depending on diameter and wall thickness, a smaller width value (b) may be used for the test
specimen, but it shall not be less than 15 mm.
Test specimens from pipe welds shall be so tested that the inside of the pipe is subjected to a
tensile stress.
In the case of test specimen thicknesses that exceed 30 mm, material shall be removed from one
side (the outer surface in the case of pipes) to a residual thickness of 30 mm.
7.1.4 in the case of a test specimen of thickness that exceeds 30 mm and that is to be tested
without dressing off, calculate the width LS between supports (figure 5) according to the formula
LS = D + d + 3 h
where
d is equal to 25 mm.
13
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7.2 Procedure
7.2.1 Unless otherwise agreed upon or specified in the terms of delivery for the product to be
tested, the test shall be carried out at an ambient temperature of 23 °C ± 2 °C. The test specimen
and testing equipment shall be set up as shown in figure 5.
1 2
Test speed
Material
mm/min
PE-HD 50
PP, PVDF 20
PVC 10
7.2.3 The bending beam shall be applied at the centre of the weld. In the case of hot-gas welded
single-V welds, the bending beam shall be applied to the weld root, whereas, in the case of
asymmetrical double-V welds, the bending beam shall be applied to the shallower side of the weld
(see figure 6).
14
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7.2.4 Start the bending process at the required test speed until fracture or crack initiation occurs,
or up to an angle of 160°. Measure the bending angle as shown in figure 5, with the test piece under
load.
The complete pressing-through of the test specimen between the supports corresponds to a
bending angle of approximately 160°. If this is achieved without crack initiation, record the result as
"> 160°".
NOTE If a better indication of the onset of cracking is required, a force-displacement curve may be recorded
and evaluated.
7.2.5 if a maximum of two test specimens from a batch of five fail the test, two new substitute test
specimens from the same test sample may be tested. No value shall then lie below the required
minimum.
A test piece, with the weld dressed-off, is bent over a rounded 6-mm-thick bar. Manual force is
applied uniformly at a speed approximating that shown in table 7 until cracking occurs or until the
two free ends of the test piece come into contact with the support bar (see figure 7).
Owing to energy requirements, this manual method is limited to test pieces of thickness up to
10 mm.
15
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d) the overall appearance of the specimens before the test, and visual assessment of the weld;
f) the thickness and width of the test specimens, in millimetres (mean values);
l) the appearance of the test specimens after the test, and visual assessment of the appearance of
the fracture, and
16
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8 Peel test
8.1 Principle
The peel test is used to assess the cohesive strength of an electrofusion-welded socket-and-pipe
assembly. The test specimen is subjected to tensile loading in such a manner as to cause a
progressive peeling of the fusion interface between socket and pipe.
The cohesive strength of the joint is characterized by the nature of the failure in the plane of the
fused material (brittle or ductile failure), and the percentage of decohesion.
8.2 Apparatus
The apparatus comprises a suitable tensile testing machine and a loading clamp.
The apparatus and test specimen are set up as shown in figure 14, and the details of the loading
clamp are shown in figure 15.
Before machining, condition the test piece for at least 6 h at an ambient temperature of
23 °C ± 2 °C.
19
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After machining, further condition the test specimens for at least 6 h at the same ambient
temperature of 23 °C ± 2 °C.
20
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The shape and dimensions of the test specimens are shown in figure 16.
Ensure that the test specimens include the minimum and maximum gaps identified by visual
examination of the test piece before machining.
Drill a hole through the socket, for attachment of the loading clamp as shown in figure 16. The
correct diameter of the hole is t/5 (where t is as shown in figure 16), with a minimum diameter of
3 mm. Also ensure that the diameter of the hole is such that no yielding occurs at that point.
8.5 Procedure
8.5.2 Measure and record the extreme overall distance y between the first and last coil winding in
the socket (see figure 17).
8.5.3 Attach the socket portion of the test specimen to the loading clamp, and clamp the pipe
portion of the specimen in the tensile testing machine, observing the alignment and minimum
distance requirements shown in figure 14.
8.5.4 Apply a tensile axial load to the specimen, at a constant speed of between 20 and
50 mm/min.
8.5.5 Continue the loading until complete separation between the socket and pipe portions has
occurred.
8.6.2 Record the location of fractures, for example in the socket or the pipe, between the windings
or at the interface.
21
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8.6.3 Measure and record the total length of brittle fracture d in the welding plane, parallel to the
pipe axis (see figure 17).
8.6.4 For each specimen, calculate the percentage of decohesion, using the following equation:
C = (d/y) × 100
where
y is the overall length between first and last winding in the socket, in millimetres.
22
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g) the time between fusion and machining of test specimens, i.e. conditioning period;
j) the overall appearance of specimens before the test, and visual assessment of the weld;
n) the appearance of specimens after the test, and visual assessment of the type and location of
the fracture;
For socket assemblies, the initial fracture may be in the brittle mode over a maximum length of y/3,
i.e. the maximum permissible decohesion is 33 %.
23
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Annex A
(normative)
The sizes shown for test pieces in figure A.1 are the minimum sizes for smaller specimens. These
dimensions have to be adjusted proportionately to cater for the larger test specimen sizes.
24
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The sizes shown for test pieces in figure A.2 are the minimum sizes for smaller specimens. These
dimensions have to be adjusted proportionately to cater for the larger test specimen sizes.
Annex B
(informative)
Bibliography
DVS 2201-1, Testing of semi-finished thermoplastics products – Part 1: Fundamentals – Guidance.
DVS 2203-1, Testing of welded joints of thermoplastics – Part 1: Test methods – Requirements.
DVS 2203-4, Testing of welded joints of thermoplastics – Part 4: Tensile creep test.
DVS 2203-5, Testing of welded joints of thermoplastics – Part 5: Technological bending test.
© SABS
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