Form No : ILD - LAB - CAL - 002D

Date Rev. : 3-Dec-12

Rev No. : 2

PT. INDOLAMPUNG DISTILLERY

GC CALIBRATION REPORT
GC PORT : 1.1 FLOW (Kpa)
COLUMN : GP-54 CARRIER (Nitrogen) : 110 Kpa
HYDROGEN : 50 Kpa
AIR : 70 Kpa
TEMPERATURE PROGRAM (oC) TIME PROGRAM (MINUTE)
INJECTOR : 230 o
C INITIAL : 180 o
C INITIAL : 9 minute
DETECTOR : 230 o
C RATE 1 : 5 o
C/minute FINAL 1 : 20 minute
FINAL 1 : 210 o
C FINAL 2 : 0 minute
RATE 2 : 0 o
C/minute
FINAL 2 : 0 o
C
RATE 3 : o
C/minute
FINAL 3 : o
C
WORKING STANDARD : Aet-OH
CALIBRATED BY : Sant/Sani
APPROVED BY : Riski/Muhkibin
DATE OF CALIBRATED : Mar 27, 14
DATE OF APPLIED : Mar 27, 14
DATE OF NEXT CALIBRATED : Apr 27, 14
REMARK :

Once
injection RSD (%)
RSD (%) AREA
PURITY TV (ppm) (Ci) Deviation max (ppm) (%) I II III
Ethanol 1.75 100.00 2 100 2 432717 409840 430524
Acrolein 0.00 #DIV/0! 0 80 3 0 0 0
Acetaldehyde 0.00 #DIV/0! 0 70 3 0 0 0
Acetone 0.00 #DIV/0! 0 60 4 0 0 0
Isopropanol 0.00 #DIV/0! 0 50 4 0 0 0
Acetic acid 0.00 #DIV/0! 0 40 5 0 0 0
n-Propanol 0.00 #DIV/0! 0 20 7 0 0 0
Acetal 0.00 #DIV/0! 0 10 8 0 0 0
Diacetyl 0.00 #DIV/0! 0 0 0 0
Ethyl acetate 0.00 #DIV/0! 0 0 0 0
Isobutanol 0.00 #DIV/0! 0 0 0 0
n-Butanol 0.00 #DIV/0! 0 0 0 0
Acetoin 0.00 #DIV/0! 0 0 0 0
Isoamyl alcohol 0.00 #DIV/0! 0 0 0 0
n-Amyl alcohol 0.00 #DIV/0! 0 0 0 0
Isopropanol 1.00 358482 347651 354091
0

Ai/A(ISTD) RSD (%)

PURITY I II III max-min max Control AVG Ci/C(ISTD) RF
Ethanol 1.2071 1.1789 1.2159 0.0370 2 OK 1.2006 1.7500 0.6861
Acrolein 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetaldehyde 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetone 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isopropanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetic acid 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
n-Propanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetal 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Diacetyl 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Ethyl acetate 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isobutanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
n-Butanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetoin 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isoamyl alcohol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
n-Amyl alcohol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isopropanol 1.0000 1.0000 1.0000 0.0000 0 OFF SPEC 1.0000 1.0000 1.0000
 Form No : ILD - LAB - CAL - 002D
Date Rev. : 3-Dec-12
Rev No. : 2

PT. INDOLAMPUNG DISTILLERY

GC CALIBRATION REPORT
GC PORT : 1.1 FLOW (Kpa)
COLUMN : GP-54 CARRIER (Nitrogen) : 110 Kpa
HYDROGEN : 50 Kpa
AIR : 70 Kpa
TEMPERATURE PROGRAM (oC) TIME PROGRAM (MINUTE)
INJECTOR : 230 o
C INITIAL : 180 o
C INITIAL : 9 minute
DETECTOR : 230 o
C RATE 1 : 5 o
C/minute FINAL 1 : 20 minute
FINAL 1 : 210 o
C FINAL 2 : 0 minute
RATE 2 : 0 o
C/minute
FINAL 2 : 0 o
C
RATE 3 : o
C/minute
FINAL 3 : o
C
WORKING STANDARD : Aet-OH
CALIBRATED BY : Habib
APPROVED BY : Riski/Muhkibin
DATE OF CALIBRATED : Jun 8, 14
DATE OF APPLIED : Jun 8, 14
DATE OF NEXT CALIBRATED : Jul 9, 14
REMARK :

Once
injection RSD (%)
RSD (%) AREA
PURITY TV (ppm) (Ci) Deviation max (ppm) (%) I II III
Ethanol 1.75 100.00 2 100 2 372958 357335 362318
Acrolein 0.00 #DIV/0! 0 80 3 0 0 0
Acetaldehyde 0.00 #DIV/0! 0 70 3 0 0 0
Acetone 0.00 #DIV/0! 0 60 4 0 0 0
Isopropanol 0.00 #DIV/0! 0 50 4 0 0 0
Acetic acid 0.00 #DIV/0! 0 40 5 0 0 0
n-Propanol 0.00 #DIV/0! 0 20 7 0 0 0
Acetal 0.00 #DIV/0! 0 10 8 0 0 0
Diacetyl 0.00 #DIV/0! 0 0 0 0
Ethyl acetate 0.00 #DIV/0! 0 0 0 0
Isobutanol 0.00 #DIV/0! 0 0 0 0
n-Butanol 0.00 #DIV/0! 0 0 0 0
Acetoin 0.00 #DIV/0! 0 0 0 0
Isoamyl alcohol 0.00 #DIV/0! 0 0 0 0
n-Amyl alcohol 0.00 #DIV/0! 0 0 0 0
Isopropanol 1.00 315923 306721 307315

Ai/A(ISTD) RSD (%)

PURITY I II III max-min max Control AVG Ci/C(ISTD) RF
Ethanol 1.1805 1.1650 1.1790 0.0155 1 OK 1.1748 1.7500 0.6713
Acrolein 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetaldehyde 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetone 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isopropanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetic acid 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
n-Propanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetal 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Diacetyl 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Ethyl acetate 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isobutanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
n-Butanol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Acetoin 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isoamyl alcohol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
n-Amyl alcohol 0.0000 0.0000 0.0000 0.0000 #DIV/0! #DIV/0! 0.0000 0.0000 #DIV/0!
Isopropanol 1.0000 1.0000 1.0000 0.0000 0 OFF SPEC 1.0000 1.0000 1.0000