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Original Brabender® Instruments

for Material Research and Quality Control

… where quality is measured.


Company

Brabender® GmbH & Co. KG, Brabender Messtechnik® C. W. Brabender® Instruments Inc.
GmbH & Co. KG and Brabender Technologie KG

The Brabender® The Brabender®


group support
Founded in 1923, Brabender® A modern application laboratory
belongs to the leading manufac- is at the disposal of all customers
turers of instruments and systems and interested parties for trials with
for testing physical properties in their own material. All measuring
all fields of research, development, systems of Brabender® can be
and industrial production. tested under practice-oriented
Today, the Brabender® group conditions.
comprises four companies, each of An experienced expert team will
which is responsible for its special assist the tests and will stay at your
range of development, production, disposal at any time for further
and service. This allows versatility questions.
in each of the special lines. To the Apart from that, numerous articles
benefit of our customers. dealing with the application of the Brabender® Applicational Laboratory
Brabender® instrument systems for
manifold tests have been published
all over the world during the past
decades. We shall be pleased to
send you a bibliography comprising
about 1500 articles at present.
Together, we will find the optimum
solutions for your special problems
and prove their suitability.

2
Table of contents

Company 2
- The Brabender® group
- The Brabender® support
Table of contents 3
Torque rheometers 4-5
- Plasti-Corder® Lab-Station / Lab-Station EC
- Plastograph® EC plus / Plastograph® EC
Mixers 6-8
- Measuring mixers
- Mixer type 30 / 50 & type 30 EHT / 50 EHT
- Thermoplastics: PVC, PE, PP...
- Mixer type 350 / 350 E
- Special Mixer type 350 S
- Step-controlled Measuring Mixer
Single screw extruders 9-11
- Measuring Extruders and Extrusiograph®
Measuring heads
- Extrusiograph® 19 / 25 D
- Measuring extruder 19 / 10 DW
- Grooved extruder 19 / 20 DN
Stand-alone
- Stand-alone extruder KE 19 / KE 30
Twin screw extruders 12-14
Docking stations
- Twin screw extruderTSE 20 / 40 D
- Twin screw extruder TSE 25
- Twin screw extruder TSE 35 / 17 D
- Twin screw extruder CTSE
Stand-alone
- Mini-Compounder KETSE 12 / 36 D
- Lab-Compounder KETSE 20 / 40 D and 20 / 40 D EC
Software 15
Processing / measuring die heads 16
Downstream equipment 17
- Pelletizer
- Film Blowing Unit
- Univex
- FSR
On-line production control 18
- Auto-Grader®: MFR, MVR
- Film Quality Analyzer
- Film Testing Line
Carbon black and rubber testing 19
- Absorptometer ”C”
- Elatest®

… where quality is measured.


3
Torque rheometers

Plasti-Corder® Lab-Station / Lab-Station EC

The heart of a flexible testing and The Plasti-Corder® Lab-Station / and computer, easy wiring of the
Lab-Station EC are torque system components, manifold
simulation unit rheometers for applicational expansion facilities - just plug
investigations or processing tasks and play.
in laboratories and for simulation. All control modules and sensors
t Modular configuration The heart of the Lab-Station is the required for additional equipment
t Multi-master system with self-intelligence modules fully digital 16 kW motor which are allocated to the docking
ensures fulltorque of 400 Nm over stations and are recognized auto-
t Self-validation the entire speedrange of 0.2 min-1 matically after coupling.
t Real-time transmission of events and actual values to 350 min-1. The inverter drive Integration of the performance
provides for precise and constant electronics in the individual docking
t State of the art software for all current speed even under this load. Further
Windows® versions stations allows preheating of the
more, a torque measurement is measuring head even without the
t Real multitasking integrated. basic unit or cleaning of the extru-
t Raw material and recipe development The movable and self-centering der or mixer under temperature.
docking stations like mixers and For manual operation, all important
t Quality control parallel to production extruders are just coupled to this control data can be read on a con-
t Laboratory-scale production basic unit. trol panel at the Lab-Station.
of samples for further investigations The integration of a modern Profit from state of the art soft-
field-bus system into the new ware packages for recording,
Plasti-Corder® Lab-Station / Lab- representing, and evaluating your
Station EC makes working a real measuring data and documenting
breeze: permanent communication your tests.
between control modules, sensors,

Plasti-Corder® Lab-Station

Plasti-Corder® Lab-Station EC
Single Screw
Extruder
Type 30
Mixer
Type 30 / 50
P 600

Mixer
Type 350
TSE 20 / 40

Single Screw
CTSE Extruder Type 19
Twin Screw
Extruder TSE 25

4
Plastograph® EC plus / Plastograph® EC

The economical torque rheometer The Brabender® Plastograph® EC fiable materials under practice-
and EC plus are the economical oriented conditions, cost-effectively,
for mixers and extruders table-top versions of the reliably, with little expenditure of
Brabender® torque rheometer time and material.
applied all over the world for inves- The Plastograph® EC plus is the
t Quick and cost-effective setup tigation and simulation in labora- advanced version for measuring
tories. The Plastograph® EC and mixers and extruders.
t Easy connection of additional equipment EC plus are the perfect measuring
such as mixers and extruders drives for practice-oriented mea- With its digital 3.8 kW motor, a
surements with the Brabender® torque measuring range of 200 Nm,
t Automatic recognition of additional equipment and a speed range from 0.2 to
measuring heads.
t State of the art software under all current 150 min-1, the Plastograph® EC
Brabender® Plastograph® EC plus is the perfect measuring drive
Windows® versions for reliable recording and EC plus serve for testing the for practice-oriented measurements
and evaluation of measuring data processibility of thermoplastics, with the Brabender® series of 30
thermosets, elastomers, ceramic and 50 mixers, measuring extruder
molding materials, fillers, pigments, type 19, and the conical twin screw
and many other plastic and plasti- extruder.

Plastograph® EC plus

Plastograph® EC

Conical Twin
Screw Extruder
Mixer
Type 30 / 50

Planetary Mixer P 600


Single Screw
Extruder Type 19

… where quality is measured.


5
Mixers

Brabender® measuring mixers

The efficient machines for quality control Principle Application


and recipe development The measuring principle is based on With Brabender® measuring
making visible the resistance the mixers, you can simulate on a
sample material opposes to the ro- laboratory scale all processes like
tating blades. The corresponding compounding, mixing, masticating,
t Raw material and recipe development
torque moves a dynamometer out etc. that are relevant for production
t Material testing of its zero position. and processing of polymers and
t Quality control parallel to production In compliance with the existing other plastic and plastifiable mate-
standards and test specifications, a rials. Or use them for producing
t Optimization of the production process typical ”Plastogram®” (torque and your sample material or for reactive
t Laboratory-scale production of samples stock temperature vs. time) is processing.
for further investigations recorded for each sample material. Brabender® measuring mixers
This diagram shows the relation- test the processibility of thermo-
ship between torque (viscosity) and plastics, thermosets, elastomers,
temperature/time in consideration ceramic molding materials,
of structural changes of the mate- pigments, and many other plastic
rial. and plastifiable substances.
Blade geometries
The measured data are displayed
numerically as a table and/or Select the optimum blade geometry
graphically as a diagram during the for your special application from a
measurement on the monitor and large program of different blades.
can be printed and stored. These comprise Banbury, cam, and
roller blades which have proven
successful in industrial application
C.W. Brabender said for many decades, but also specially
optimized blade geometries for cer-
“It is only testing, measuring, and tain measuring tasks as e.g. delta
recording as a function of time blades for thermosetting materials.
which efficiently helps to rise
production quality; only this way,
certain processes can be recognized
which cannot be grasped with Evaluation
static measurements.” t Fusion behavior of PVC
t Heat and shear stability of
polymers
t Flow and cure behavior of
crosslinking polymers acc. to
DIN 53 764
t Automatic evaluation of the black
incorporation time (BIT) with
selectable zero point
t Flow and cure behavior of
elastomers
t Plasticizer absorption of PVC
dry blends
t Liquid absorption of powders
t Semi-automatic universal
evaluation

6
Mixer type 30 / 50 & type 30 EHT / 50 EHT

Measuring mixer type 30 / 50 The series type 30 / type 50 and These measuring heads are per-
type 30 EHT / 50 EHT measuring fectly suited for materials like PAEK
mixers can be equipped with differ- and PEEK with melting temperatu-
ent blades. Within a series, the free res of more than 300 °C.
t Easy handling and cleaning
mixer volume varies depending on This makes these mixer types par-
t Interchangeable blades the blades mounted. Due to ticularly interesting for research
liquid temperature conditioning,
t Liquid or electric heating and development applications with
these measuring heads stand out steadily changing test materials.
t Precise and constant temperature for particularly precise and uniform
heating/cooling. The EHT version is available for the
t Conditioning up to 500 °C series 30 and 50 mixers.
Mixers with the extension EHT
(electric, high temperature) distin- The rotor speed ratio of 2 : 3
guish by their electric temperature (driven to non driven) results in a
conditioning in three control zones high torque resolution which allows
with compressed air cooling. As a better differentiation, especially
compared to liquid heated mixers, when testing low viscosity
this extends the operating range to polymers.
a maximum temperature of 500 °C.

Thermoplastics: PVC, PE, PP...

Use this evaluation method for others, the extreme values in the
testing the fusion behavior of torque curve (as a measure for vis-
thermoplastic polymers. Measure cosity), fusion time, gelation speed,
material-specific Plastograms® and the mechanical energy input.
which also permit to draw conclu- These material characteristics are
sions as to the history of the material. valuable data for incoming and
The WINMix software analyzes final inspection or for the configu-
the curve and determines, among ration of production processes.

Fusion behavior

… where quality is measured.


7
Mixers

Mixer type 350 / 350 E

t Large mixer volumes volumes of 370 to 440 cm3, these


mixer heads are frequently used for
t Liquid or electric producing sample compounds for
heating subsequent tests. The material can
t Precise and constant easily be taken out and rolled out
temperature to sheets or pressed to plates. Con-
trol and document the entire
t Conditioning compounding process from your
up to 300 °C computer. Or implement and profit
from an optional step-control of
Mixer heads of the 350 series are each individual mixing step.
available with liquid heating/coo- Of course, these mixers can also be
ling and with electric heating and applied for material testing (e.g. of
air cooling. Due to the large mixer rubber compounds).

Special Mixer type 350 S

t Accurate feeding recipe components. Taking out of


the mixing good is facilitated by the
t Quick emptying horizontal division of the middle
t Easy cleaning part of this mixer. Just tilt the upper
and lower halves open for remo-
ving the material and use it for
The special mixer type 350 S is
subsequent tests.
mainly used in the rubber and
caoutchouc industry for mixing and Extensive software packages are
compounding tasks or for material available for material tests like e.g.
testing. The large free mixer volume the determination of the black in-
of 370 to 440 cm3 has proven fa- corporation time (BIT).
vorable for proportioning of the

Step-controlled Measuring Mixer

The series 50 and 350 measuring in AND / OR functions. Additionally,


mixers can be equipped with a tep- several optional sensors e.g. for
control which offers special advan- measuring the electric conductivity
tages for recipe development. of the sample material can be
Define a sequencer control with up connected.
to 20 mixing steps from your com- This makes step-controlled mixers
puter keyboard. The individual mix- the optimum tools for the pro-
ing steps can be switched as a duction of elastomer compounds.
function of registered units like
t Time
t Stock temperature
t Energy input

8
Single screw extruders

Measuring Extruders and Extrusiograph®

The multipurpose machines for testing Application Heating/cooling


and processing In the measuring extruder / All Brabender® measuring extru-
Extrusiograph®, the sample ma- ders and Extrusiograph® consist
terial is plastified under practice- of an extruder barrel with honed
t Applications in laboratories and oriented conditions and extruded and nitrided bore, water-cooled
through the die head. All measuring feed zone, and various heating or
small scale production values such as torque, melt tempe- heating/cooling zones with electric
t The development of new products rature, melt pressure are recorded heating and air cooling. The measu-
continuously and represented in ring extruders and Extrusiograph®
t Testing the processing behavior for recipe develop- the form of tables and diagrams have additional solenoid valves for
ment or incoming and final material inspection parallel to the current test. controlled cooling air supply to the
t Quality control during production in combination The extrudate is tested for various individual heating/cooling zones.
with measuring heads criteria: The temperature of the individual
t Uniform plastification, gloss, gels extruder zone is controlled and
t Production of small tubes and profiles displayed by self-optimizing elec-
t Production of blown and flat films t Color dispersion and color tronic temperature controllers.
matching
t Transparency and formation of
streaks, e.g. with transparent Temperature and
materials pressure sensors
t Swelling and contraction Two threaded bores (1/2“ x 20
behaviour UNF) opposite each other are
t Segregation of individual recipe provided at the end of the barrel of
components of a compound at each measuring extruder for taking
the die and/or at the screw`s tip a thermocouple and a pressure
(e.g. titanium dioxide) transducer for measuring the tem-
perature and the pressure of the
t Output per unit of time, etc.
melt in front of the die channel.
Besides, subsequent mechanical
All Extrusiograph® have six threa-
material tests can be run with the
ded bores (1/2“ x 20 UNF) opposite
extruded specimens.
each other along the barrel for
The Brabender® measuring extru- taking thermocouples and pressure
ders and Extrusiograph® can be transducers.
Principle Screws mounted very quickly and easily to
Simulate Production Realisti- For each measuring extruder/ the drive unit. The torque is trans-
cally on a Laboratory Scale Extrusiograph®, different screws mitted electronically which protects
are available. The screws are made both the drive unit and the measu-
Brabender® single screw measu- ring extruders and Extrusiograph®
ring extruders and Extrusiograph® of special steel, the flight basis and
the lands are chromium-plated. from damage due to overload.
are interchangeable measuring-
heads which, in connection with Single- and multi-stage screws with
a Brabender® Plasti-Corder® various compression ratios and
Lab-Station or Plastograph® EC different lengths are available for
plus, serve for testing the extruda- testing a large range of materials.
bility of polymers and for studying
thesis occurring in research and
E = feed opening L1 = feed section L3 = metering section
development as well as in practical of the extruder L2 = compression section L4 = mixing section
application. The Brabender®
modular system allows a complete
instrumentation of the extruders
for the control and development of
raw material. Different screws, die
heads, and downstream equipment
fulfill all kinds of extrusion tasks.

… where quality is measured.


9
Single screw extruders
Measuring heads

Extrusiograph® 19 / 25 D

t Variable feed units The Brabender® Extrusiograph®


19 / 25 D has a barrel diameter of
t Interchangeable 19 mm and a processing length of
feed zone 25 D.
t Measuring ports along The Extrusiograph® is equipped
the barrel with vibrating feed hopper in
the standard version. Vibrating
feed chutes and feed screws are
available.
The feed zone of the 19 mm
Extrusiograph® is interchange-
able and can be designed either
conically grooved or as a smooth
cylinder.
All Extrusiograph® have six threa-
ded bores (1/2“ x 20 UNF) opposite
each other along the barrel for
taking thermocouples and pressure
transducers.

Measuring extruder 19 / 10 DW Grooved extruder 19 / 20 DN

t Feed roll The extruder 19 / 10 DW with its t Liquid heated The liquid heated extruder
feed roll and its short length of 10 D 19 / 20 DN has a grooved barrel
t Short processing length is specially used for elastomers. t Grooved barrel over the entire length. Together
t Expandable with Frequently, it is used in combination t Pneumatic feed unit with the pneumatic feed unit, it is
pin barrel with a pin barrel supplement and a perfectly suited for pasty materials
Garvey die head. which have a strong tendency to
heat formation due to internal
friction. Therefore, this extruder is
frequently applied with ceramic
materials.

10
Single screw extruders
Stand-alone extruders

Stand-alone extruder KE 19 / KE 30

t Compact design Brabender® stand-alone extru-


ders are multi-purpose machines
t High perfomance for testing and processing a large
extrusion variety of materials. Their compact
design makes these machines the
t Cost-effective setup ideal solution for applications
in laboratories and smallscale
production.
Equipped with a grooved feed zone,
and a barrier screw, throughputs
comparable to high-performance
extrusion can be reached. A large
program of downstream equipment
is available to build up complete
processing lines.

Stand-alone extruder KE 30

… where quality is measured.


11
Twin screw extruders

Twin screw extruders and compounders

Ideal companion for compounding Principle


continiously The basic steps of compounding Brabender® twin screw extruder
can perfectly be realized with co- as a modern in-line compounder.
rotating twin screw extruders. Depending on the extruder size, on
t Development of new material This makes modular co-rotating the material to be tested, and on
twin screw extruders the ideal the processing task, throughputs
t Recipe development companion for plastics from synthe- up to 60 kg/h can be reached. This
t Production simulation sis up to recycling. Profit from the opens up the entire application
harmonized, modular conception range to these extruders - from
t Applications in laboratories of screws and barrels for optimally material development up to small-
and small scale production realizing all processing steps scale production of sheets and
(feeding, conveying, plasticizing, films.
dispersing, reacting, venting,
Of course, the necessary additional
pressure build-up).
Advantages equipment like measuring and
The system configuration of each control units or metering systems
Intermeshing co-rotating twin t Well-defined plastification model can easily be adapted to the (gravimetric, volumetric, liquid) as
screw extruders stand out for time and purposive shearing individual processing task - anytime well as down-stream equipment is
decisive processing features: t Gentle mixing at low energy and at low cost. available, too, allowing for modular
t Good feeding characteristics, input and highquality homogeni- Or combine several processing setup of complete extrusion lines.
even with materials with poor zation steps within a continuously Expansion is possible whenever
flow properties t Gentle material treatment working extruder and use your needed.
t High conveying constancy without temperature peaks
without pulsation or irregular even at high speed
thermal loads t Variable shearing by using
t Narrow residence time mixing and kneading
spectrum of the melt within the elements
screw area t Kneading blocks with different
t Constantly high quality of the disk widths and offset angles
extrudate t Good control of the pressure in
t High output at long energy the melt for optimum venting
transfer t Self-cleaning of the screws by
t High energy input as compared intermeshing flights
to the free screw volume

12
Twin screw extruders
Docking stations

Twin screw extruder TSE 20 / 40 D Twin screw extruder TSE 25

t Clamshell barrel The TSE 20 is available with barrel t Interchangeable The corotating twin screw
length of 40 D. The barrel length barrel segments extruder TSE 25 with a barrel
t Variable processing can be reduced to 30 or 20 D by diameter of 25 mm is a true all-
length means of a distance sleeve in the t Variable processing rounder among the extruders. With
t Vertical- and screw configuration to easily adapt length its variable processing length of 22
your extruder to the individual to 48 D, the TSE 25 can be used for
sidefeeding processing task. Metering and/or
t Interchangeable multistage compounding tasks, as
t Interchangeable vent ports can be installed every screw elements pilot plant, for reactive extrusion,
screw elements 10 D. For this purpose, the barrel is t Through put range and for recipe development.
equipped with 4 ports which can
t Electric heating / for laboratory and A special software helps to build up
be closed. the screws from a construction kit
water cooling pilot plant
Furthermore, side feeding is so as to perfectly suit the respec-
t Conditioning possible. The barrel of the TSE 20 tive application. Depending on
up to 400 °C is divided horizontally and can be the material, this extruder reaches
tilted open on both sides. throughputs of 0.6 to 50 kgs/h.
This allows visual assessment of Feed units and a large program of
individual processing steps and die heads and downstream equip-
makes this extruder particularly sui- ment are available as additional
ted for application in research and equipment.
development. This extruder is also
available as stand-alone version.

Twin screw extruder TSE 35 / 17 D Twin screw extruder CTSE

t Counter-rotating The counter-rotating TSE 35 was t Counter-rotating Conical twin screw extruder,
conceived for processing tasks counterrotating for laboratory scale
t Implying high torque implying a high torque. t Conical screw design production. Including venting zone
t Screws with closed loop Different screw geometries are t Constant material and measurement of pressure /
heat exchanger available, according to the pro- transport temperature inside the cylinder and
cessing task. at the screw tip. There are various
t Degassing screw geometries available.
Its fixed processing lengths of 17 D opening
and the available torque of 200 Nm
per screw make this extruder parti-
cularly suited for one- or two-step
processing of difficult material.
This extruder is supplied as
counterrotating version.

… where quality is measured.


13
Twin screw extruders
Stand-alone extruders

Mini-Compounder KETSE 12 / 36 D

t Extremly small material The Brabender® Mini-Compound-


amount processing er KETSE 12 / 36 D is a co-rotating
twin screw extruder miniature with
t Clamshell barrel application to the chemical as well
t Vertical- and as to the pharmaceutical industry to
develop new products.
sidefeeding
Almost each processing task and
t Interchangeable the easy handling of the system,
screw elements distinguish the Mini-Compounder
as an excellent laboratory
apparatus.
The Brabender® Mini-Com-
pounder KETSE 12 / 36 D has an
integrated drive with an output of
2.4 kW and reaches speeds up
to max. 600 U/min-1. The modular
screw conception offers all indivi-
dual processing possibilities with
minimum material requirements.

Miniature screws compared with a


paper clip

Lab-Compounder KETSE 20 / 40 D

t Clamshell barrel With the new Stand-Alone KETSE


20 / 40 D, Brabender® offers a
t Variable processing twin screw extruder as miniature
length scale with application to the che-
t Vertical- and mical industry for material research
and process simulation.
sidefeeding
The scale-down of the machine
t Interchangeable in combination with the compre-
screw elements hensive adaptability to almost
t Electric heating / water each processing task, and the
easy handling of the system,
cooling explain the distinction of the
t Conditioning KETSE 20 / 40 D as an excellent
up to 400 °C laboratory apparatus.

t Compact design The clam shell barrel (length: 40 D)


is divided horizontally, can be tilted
t Cost-effectiv setup open, and allows visual assessment
of individual processing steps. Fur-
thermore, a comfortable mounting
of the screws and a quick cleaning
of the cylinder is possible.
In addition to the main metering,
metering or venting ports at a bar-
rel length of 10 D, 20 D and 30 D
are available. Side feeding can be
installed at 12 D and 22 D length.

14
Software

User-optimized software

The user-optimized Windows® Special data correlation programs


With program modules like software allows recording of permit a direct comparison of the
process data and evaluation of result of different test series with
tWINMIX the test results according to the each other.
(mixer applications) state of the art. Memorization of the measuring
tWINEXT On-line diagrams give a quick values in MS Access® database
(extruder applications incl. capillary rheometry) survey of the test data and format and a real 32-bit software
evaluation results already during ensure quickness, safety, and a
tWINAG
the running test. high flexibility combined with easy
(on-line testing of melt index and film purity),
The users of Brabender® handling of the system.
etc.
instruments have a high degree
of system-technical intelligence
on hand.

Plastogramm®

Correlation of flow curves from round and slot capillary tests


… where quality is measured.
15
Processing / measuring die heads

Processing / measuring die heads

Principle
Mounting and interchanging of the However, if you need a liquid heated
die heads at the extruder or design for a special application, just
Extrusiograph® is very easy: just ask us. All die heads have threaded
fix them with the ring nut at the bores for taking melt temperature
extruder barrel. The die heads are and/or pressure transducers. Most
made of extremely corrosion- of the die heads can be used verti-
resistant steel and are heated elec- cally and horizontally.
trically in the standard version.

Single strand die head Rheometric slot


Round die assembly for extruding capillary die head
a rod or a filament. Capillary viscometer slot die assem-
bly for scientific viscometric tests.

Tubing die head Rheometric round


Tube die assembly for extruding capillary die head
a tube or a hose. Capillary viscometer round die
assembly for scientific viscometric
tests.

Flexlip die head with Garvey die head


coathanger Garvey die assembly for testing
Flat sheet die assembly for extru- special injection properties
ding a sheet or a film. The thickness according to ASTM D 2230.
of the die gap is variable.

Principle of the spiral Swelltest


mandrel die head Optoelectronic thickness measuring
Fim blowing die assembly with device for round strands for testing
cooling ring for testing the pro- the swell behaviour of polymers.
cessibility of thermoplastics.

16
Downstream equipment

Pelletizer Film Blowing Unit

t Adjustable pellet size The pelletizer can handle up to t Realistic production The Film Blowing Unit serves for
4 strands with diameters of 1 to simulation simultaneous blowing, cooling,
t Low-noise operation 4 mm. taking off, and winding up of ext-
t Easy discharge t Expandable with ruded blown films and for exactly
The control of the cutting speed as
well as the take off speed allow to Film Quality Analyzer adjusting the hose diameter and
adjust the pellet size. the film thickness.

Further features are its low-noise Depending on the material,


operation and its perfected design, common blowing ratios are 1 : 2
including e.g. a drawer system for up to 1 : 4.
easy discharge. An additional Film Quality Analy-
Air showers are available for drying zer mounted into the film blowing
the strands after a water bath. tower enables simultaneous purity
tests.

Univex FSR

t Excellent film quality The Univex can take off, cool, and t Film, sheet or ribbon The Take-off Unit with integrated
wind up flat films up to a max. film take off inverter drive can take off film
t High take off speed speed of 30 m/min. Liquid tempe- sheets and ribbons up to a max.
t Accurate temperature rature conditioning of the nip rolls t Accurate temperature film speed of 10 m/min.
conditioning positively influences e.g. crystalliza- conditioning The FSR can be controlled manually
tion processes. The Univex can be or through the PC (via CAN bus).
controlled manually or through PC It is adjustable for height on a
(via Canbus). movable base frame including
safety device. The Liquid Tempera-
ture conditioning is intended for a
regulation between 10 - 180° C.

… where quality is measured.


17
On-line production control

Auto-Grader®: MFR, MVR Film Quality Analyzer

tObjective The Auto-Grader® continuously t Objective The Film Quality Analyzer tests
determines the melt index, film the purity of transparent films.
tContinuous purity, and transparency - within t Continuous Apart from transparency, the
tReal-time testing seconds online with polymer t Detection of black content of gels, impurities, black
production. spots, gels and fisheyes specks, and fisheyes is tested.
tIntegration into process Self-optimizing and automatic ope- All particles detected are sized
control system t Evaluation of film and allocated to size classes. As a
ration ensures optimum adaptation
to the polymer to be tested. All rele- quality note result, you get the size distribution
vant data are stored in a database and the impurity development
and can be transmitted to a process over time. Extrapolations to the
control system. material area, weight, and volume
are possible as well.
When production changes over to
a new charge, the Auto-Grader® The standard version permits to
allows to exactly determine the determine particles with a mini-
time when the product meets the mum diameter of 19 μm. In special
specification. This minimizes the cases, resolutions down to 5 μm
portion of “out-of specification” have been realized. The minimum
material. film transparency may go down
to 20 %.
The system is open to expansion
for running further on-line measu-
rements, e.g. of color, haze, etc.

Film Testing Line

tModular built The flat film from the measuring


extrusion line extruder is led through inbetween
a light source and a high-resolution
tSingle screw extruder electronic camera where it is mea-
sured. The pictures are analyzed
tIntegrated film quality by an intelligent data transfer
analyzer FQA CCD interface. The picture signals and
camera 4096 pixel the processed measuring values
are transferred to the computer.
tFSR take off for film The test and evaluation results are
sheet ribbon shown on the monitor and printed.
tDetection of black spots,
gels and fisheyes
tEvaluation of film
quality note

18
Carbon black and rubber testing

Absorptometer ”C”

Precise and reproducible absorption test The established Brabender During the free flowing phase,
Absorptometer ”C” for running liquid is absorbed into the structure
precise and reproducible absorption of the carbon black. Upon absorpti-
tests fully meets ASTM D 2414 on of sufficient liquid, the particles
tFrequency inverter drive unit including new procedures B and C begin to adhere to each other and
with precise torque measurement as well as ASTM D 3493. form agglomerates. Resistance to
mixing rises, indicated by a sharp
tHigh-precision measuring mixer with special blades The principle consists in measuring
the resistance which the carbon increase in torque.
tCooling jacket with temperature indication black puts up against the rotating A maximum torque (saturation) is
for mixer (option) blades during oil addition and in reached, follwed by a state change
determining the absorption. The from liquid into solid to solid into
tHigh-precision burette,
high-presision burette adds liquid liquid.
sequencer controlled as a titrant to the powder sample in The oil absorption number of
titration rate for optimum the mixing chamber. carbon black is directly related to
test procedure As the liquid wets the sample, three the processing and vulcanization
distinct phases can be observed in properties of the rubber compounds
the torque curve: prepared with these carbon blacks.
t Free flowing phase
t Agglomeration phase
t End phase

Elatest®

Compact density measurement The Elatest® determines the


density of polymers, in particular
of rubber and unvulcanized rubber
compounds - a dimension which is
tFully automatically of decisive importance for rubber
tWith minimum processing, both during recipe
development and for continuous
time requirement
production control.
tWith a reproducible The sample material is compressed
accuracy of 0.03 % within the measuring cylinder.
(0.0008 g/cm3 absolute) Any gas contained in the sample
escapes during this compression Elatest® with touch screen
process. Under a preset pressure,
the moving piston reaches a
From the sample weight and
position which is specific for each
volume, the computer automati-
individual sample, i.e. the sample is
cally calculates the density. Use
compressed to its specific volume.
the software easily with the touch
The stroke of the piston is measu-
screen. Excellent reproducibility of
red by a displacement transducer
the measured values, the ease of
and transmitted to the computer.
handling, and the reliability make
the Elatest® best suited for produc-
tion control as well as for research
and development.

… where quality is measured.


19
Made
in
Germany

Brabender® agencies all over the world.


© 2010 Brabender® GmbH & Co. KG
All trademarks are registered.
Subject to change of design and technical
modification without notice.
Brabender / C / Übersicht / GB / 10 / 2010

Brabender® GmbH & Co. KG


Kulturstr. 51-55 · 47055 Duisburg · Germany
Phone: +49 203 7788-0 · Fax: +49 203 7788-101
E-Mail: plastics-sales@brabender.com
www.brabender.com … where quality is measured.

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