Format MEGHNA PVC LTD(PET DIVISION) Document:MPL/PET/QAC/F/5001

MPL/PET-QC QUALITY CONTROL DEPARTMENT Effective Date:01/01/2022

Title: Normal Operating Limits

Frequency of
Sr. No. SAMPLE DETAILS Parameter Unit Aim Value Operating Limit Remarks
Analysis
AREA : CP

1 Catalyst(Pre.TK) Sb203(Concentration) %W/W 2 0.95-2.05 Once/Batch

2 P.Additive preparation Tank H3PO4(Concentration) %W/W 1 0.95-1.05 Once/Batch

Tonner Preparation Tank

3 Concentration %
Red Tonner 0.01 0.008-0.012 Once/Batch
Blue Tonner 0.02 0.018-0.022 Once/Batch
4 EG-PTA paste Mole ratio N/A 1.18 1.15-1.22 once/Shift

5 ES1 Acid No mg KOH/g 67 60-74 Twice / day

6 ES2 Acid No mg KOH/g 27 21-33 Twice / day
COOH meq/kg 65 60-70 Twice / day
7 Prepolymer From P2
IV dl/g 0.29 0.260-0.32 Twice / day
IV dl/g ±0.03 Once/Shift Presently 0.630
COOH meq/kg 33 30-36 Once/Shift
Moist % ≤ 0.1 ≤ 0.15 Onece/Day
8 Base chips From Dryer L* Hunter ≥ 80 Twice / Shift
b* Hunter -5 ­4.0 to ­6.0 Twice / Shift
Melting point °C 248 247-249 Onece/Day
Chips No/gm No 60 55-65 Twice / Shift
≤
9 Split off EG immersion vessel(PP1) Moist % 30
To monitor once / day
≤
10 Split off EG immersion vessel(PP2) Moist % 5
To monitor once / day
≤ 1
11 Split off EG immersion vessel finisher Moist %
To monitor once / day
≤ 1
12 Split off EG Eg jet after heat exchanger Moist %
To monitor once / day
13 RECOVERY EG Moist % ≤ 1 To monitor once / day
14 RECOVERY EG Moist % ≤ 3 To monitor once / day

Issue No:01
PREP. BY APPROVED BY
Revision No:00
Issued by: QMR
 Issued by: QMR
Page No: 1 of 1
Asst. Manager(QC) HOD (QC)
Format MEGHNA PVC LTD(PET DIVISION) Document:MPL/QAC/F/5001

MPL/PET-QC QUALITY CONTROL DEPARTMENT Effective Date:01/01/2022

Title: Normal Operating Limits

Frequency of
Sr. No. SAMPLE DETAILS Parameter Unit Aim Value Operating Limit Remarks
Analysis
AREA : SSP

15 Precrystallizer O/L

16 Crystallizer O/L

IV dl/g ±0.015 Twice/Shift

COOH meq/kg 25 Max 30 Max Onece/Day
17 Chips From Cooler-Deduster Moist PPM ≤ 500 600 Onece/Day
L* Hunter ≥ 85 To monitor
b* Hunter ≤ -0.1 ≤ 1.2 & -0.5 Twice / Shift

Issue No:01
PREP. BY APPROVED BY
Revision No:00
Issued by: QMR
Page No: 1 of 1
Asst. Manager(QC) HOD (QC)