4ol.

aed. apporatao )dhe

AUT1un YREC
egzixeal filtiatk paper.
the FilHer
ten and mànatea 3-4 contentE
ahing cenotant itod
a gaso caita tiing alnd
beaken a emtok
Yo eaute thin
mke to late `lled dis h
tHa olable atarch 14 about
TRocEDREGind
ater disilled ADluble Staxch
MATERTALS
et. atandodtpod glad
pestile pohes, kilter Calpacitaa
funne Morton
beake cao
APPARATUS
Adazch eparecolloidal
solution
aolutin
of Collbidal To
ATM
Dated
 Dated

2)Dis t4llea coat Lalasald oluaygs be

ied hile prebanieg tle in Lsat,
Londent
Conatant ig
 Dated

ATM

ppure
ARARATus
Conical Soo mL
boiling fube, tipod atard ,nnel
ire
gaugeYon otand cellopkane
Aeot tbe ating e.
MATERTALS
chlorde
Ferns
ol Disaolue dg
chlonde in

feznc hycide aol i hydophebic in

mature here here ut does not pen a
LAst 7eadily like Dr star choeYer
nder auitable Con di tion henc clalaride
hydrolysed aoita disled oote
to obtain hed dish
hydro ide.
CHEMLCAL REALTLon
Fe.Cl t 3 hon
Ferrie de)
chlsi
As
(wate)
koduteds re moked
Feowon)
(Reddis h

lwi th th
34CL

dialysis procea.
 PRECAVTLoN OMPORTANT PRocE
DaRE
3)
0thercaise oh preacre Fetla
evaforakanat
interval.
cqular IS a aCly Fe about csnilalthe 1ake
keantig
HCL
by
a tae
Fell3 he obtaied, de
dta
fell apfaratua ep abod
boikantkinintoge abparatas NpTE pper.
Ao. Yed
Aol.
imay is ianie Con 200
ahould Yeoved thalld ul Reblace knue
Ce
pr
mo . t bailig
utarts t vl
as emhlayaduhucen ed broln
a infun in
destablis be
be sealt be the
y througly de disklled
added called hcA of
clecmedl
dialyaie 7horoyaly Csaky Ad Dated
oolio
For prefamion
e
dohydralytis
aol ateaMing ntil taiater
acair
protees clecaig Cleangd st(on) Fe
by by
of
 Dated

bheximend3
M Ozalieatich

CooM

By the debonihon of lar val.

loo0 ml st1M ohalie acid =
Tequires oralic add Cyptals
20
reaui reA onalic aid ctalo
sh onalie a.cid ohold be
Menle l.sts

ARPARASMS coeighing tube, anyhcal balance

hiatch pas or
rnd, oaah bottlé
hunnel glas
CHEMQ LALS Ona aidcayatala Caon.hod dis6ed
AR
 Dated

DRoCEDURE

nqalred and the disoluing cohole h it

defnite VElyolurae
)aeihacLurately lss h oalic aud
cxyatah in aclean dig alteadg egted
Caatch
ga taking all the þecantian calkile
analytal balance
2)ran hex the coeigl ed onalic acid Cyyatalo
racaseiin
a lingle crya tal hall aucade.
Wash tha Laite
dishlled boatey laing c. aah bottle
Lâo that all te Cryatala o,alic acid balla
nto the heakey îake caze that the olene
distled ioter hoed
is apfpanmately 50-60 L ad not hore
Suoirl the shlast Carehuly th dientlue all the

)Enally cona
consh cae thehunnel oita cithlle d
Laater Misg a Coadh botfle to make aol ahching
to the Utte fLe
Ymeao aling plaok Add mose dithled taake, dn haf

tem oy the mt aahing hlaak ..

 Dated

and Ppehe add

As kled caateY dnp by dnh to ynake the loboey
mhris Cuo
mnjs of ae aol. in level oi th te ark

S) Snsert ah ai tight atojpbe ito the month

) Weigain the oh alic oid tryatals athould be

accurcte
2)ranagarrtate tae weigard unbtan te into.
a dean beakey houd be done veny Lar hely

be done thorli caita dai tled áuater

4) loat hes nd disklled coakr ekold be adde

5)'Look at the Men's cud o6 Lwat level arord

pavallan
6) 1he loLIer me hi sCus whould be
 Duted

Experiet- 4
ATM
JMoby's

Molar Masd Mohy's vhat

FeSog .(Nna) So4.6H0
foy thi oefivitian
looonl mlay vtot.
Teqire
RS0nl Mao Mohy's salt
Memce 4.2
veqied 392-X5e4.9
prepore
AreARATUs
Watch glais, hnalytial balance kolgot ber,
mesruug
botffe
flask , beakes fumnt glan
CMEM2CALS
AR Mohy's
Aaltdistlled hattr d cont.
 PRocEDvRE
tasate
Smeatang
caatchthe thatnetlaska Cyatalà
4) 3)
caredpuy R)
Goighetpr
farsus
wtickig waterdydende.
pxevt oAdd ml
Finaly
1yaafr Catio,
amdnot
abo eflyad ca in
ash ie ac the leat
caigle chilë
he Sml dimelue
the htighed glas
of Cyyt caash sig
cnyital
bottle
anhel all talo
dil tot
iatotealytaking
the tabo
Hy ballo ataand dy
coell offtonitaately
q
SocHyetala, fall
all Mohr's Dated
to in
taake orsilled
bak to out. galt hcal
fumet oite wi ta tae cale
Taka ta
lagh tigatala balarCe satt
pAolutih.
distihed ael neaaiy
S0-bo
 Dated

dickled oadey wailg

add disi Wed GahbottHe to

paake tt tieiing to 483 daopsise to maRe

in lekel cait
Ahe moe Dn the easahn9 lask
tae measang
nto the
6)Dhsert
mouth acaaun'ug lasa ad thaka
it to mako tte
thrngh ot Label the flask
M/Ro Mehr'c

be clear dcalarles
sehedd not be tusbid ad vehold rot Contal
aay diyht green or yelas paeapifate
PRccAU1ToN
Dponot oget to add 3-Sml
bsfene making up
Lulphake into fexes ycdreoide
 Dated

Fxpeninet-§
this wol.. find oud
the holarity
gtuen Potooniusn fe tnaganak

Votaaik permagaale oxidigeo ens kerrga o

into hernc in acd medi in celd aud
is uta elh edLced to alorles marganau
Mole cular egaton)
FeSo4.NH4), s04.6 M, o fe So4 t Wng), fog
+6 Ma0

tSo

&FesD44 ny So4 t0 Fe,cog)3 tnyoxs

Ks04 t 2Mh so4 t SfeSo),

RKMna t lo fesD4 t&h,s04 +&n,o

(Pink) Colouslem)

egui re d= 332 X2so 4.9

Moleda Maad
Aoks'c alt regired
A&lA
bol,
20

2 So ml
392
Mohrs wal
aly Yequired 20
b Mao Gol.
loom I
preparng
AerARA TVs Dated
tabe

buettePipette,Coniu
dtand.

MAIERIALS
tlask hi le
burette
Mohr'sal! chyatalo, dl. H, Sa, di
stlled aoter
NDTCAioR
KMnlg94 to ao Meh indica tor
END PoNT
Colausr les to Pinkixh

RRoEDURE
)Weigh accurotely e required ant Mokrs sct
Cnyotado n acdean dy,and
alxeady atigtedhile
al ta hrecahian
sing te analy tial balomee
Jiohr's calt yptala gey
int a clear me aannigak
Case that not
bing eunne, Take
Cgatal halle outide.hlaah the coa
ajth dis hlled yate h¡iig
all the Salt
bote
fall into tthe
hme sauig plask. Taka care Hat
per tic
more

3) Add abot S ml
n dil Ma soa to tae oe.

4 Finally coah ciell a bunnel wite_ diehlle d

a co ash bottle to moke voot

cinto
to t intenoy o funnel fall
easwhng gloak. Dheh add nmore
distlled aatey to tat the level
2embelo te mark

s) Renmoke the funnel

fannel onud ig a pipe te add
distilled oater 'obsh
olizp by drop tomaké He loLJe
haeniSCAs ln level coith he mank
flask
tgt atopper into the met
plask andl hake it
the
to naake
hesytod
vahould be
dol.
Coloileno.91 hold hot le turbid amd
hot contain o diyt gtan hold
AJ1ilahon sh
tandard
PodtiMka
Moh' Salt peLtran ganat ve
(ROCEDURE

Corkal lask -5 Mokr'ç salt sal

aanrinae
itoith

bearte toad
)Eill the burete laita knos ot note don
menisus

alr bbble ig otoþ- Cock

3)Risc cean lo kilte oi ta standord

Mohs cadt ao 3tmeo

usto a deaa oni Lal flask

teot tube bull ofdil.

tte conical blak j t beka Ha noygle

5) Place each
the buteHe Sati Ha aol entty abthr
KMalg solhion
oddifan. Contine additon f
uhl Lalour juet changs to
 Dated
Reheal he
Leading enpeniobtammedet All 4bree
OBSERVA 1TON
A) Trearahanogatandord Makys
Concordont
salt aolution
Man of coshh

Molar moA sh Mah's Salt Votume

392

892
b) tration oh Atandar ohr's lat soatio ve Sus
KMnog so
Volune ss ohr's sal! sa. taken in each titruhon - lon)

Saho nital Reodiu

ReodiugFinad
Final reading
reading olune KMng cael. waed
V,-V V ml

Mohr's bali kol. Vml kKMnlg uAÐl.

 Dated

CAL CULA1TON)

Coith (o moeo
MaMog X Mohrls calt.
Mmsr cale Vmehr-t

SMMno4

MkMnog M Xio
6V lo V

XMolar

Sne

ORECAUTTON
)he balonee ohould be in level.

Centse
3) h tndow enes yahoudd be kelpt clased cale
 Dated

haviaed oith
bo.

Check it by addina abous So. pnl tap

canter an te meaalaihg hlash ,atper it
held ts otupfer hiay
Chack tHot atey doe
odoe not leok . 2f it leaks

6) A the volumetic abparatus ahold be booahed

) Rns tthe buIette Li th the aot. to he taken

in the burette