CONTROL TEST CARD

Use in conjunction with:

DOSAGE REQUIREMENTS PAGE
ONBOARD LOG

COOLING WATER TREATMENT – MAXIGARD® HIGH-RANGE

Read SDSs before running these tests. Before testing, samples should be cooled to 25°C (77°F).

CWT TITRETS PROCEDURE WEEKLY TEST – SYSTEM WATER

Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.
1. Fill the Sample Cup (included) to the 25 ml mark with treated cooling water sample (Fig. 1).
2. Slide the flexible rubber end of the Valve Assembly over the tapered tip of the Titret to the white Reference Line for a snug fit (Fig. 2). 1 2 Slide Over 3 Snap
Valve
Valve
3. Snap the tip of the Titret (ampoule) at the Score Mark (Fig. 3). ml
25 Score Assembly Score Assembly

4. Lift the control bar and insert the Titret assembly into the body of the Titrettor (Fig. 4). 20 Mark Mark

5. With the tip of the Valve Assembly immersed in the sample, press the control bar firmly, but briefly, to pull in a small amount of 15 3
10 Reference
sample (Fig. 5). The contents will turn a GREEN color. CAUTION: Do not press the control bar unless the tip of the Valve Assembly is 5 Line
Titret Titret
immersed below the surface of the liquid.
6. Press the control bar again briefly to allow another small amount of sample to be drawn into the Titret (Fig. 5).
7. After each addition, rock the entire assembly to mix the contents of the Titret. Watch for color to change from GREEN to BRIGHT 4 Titrettor 5 6
Watch for
ORANGE. NOTE: Immediately before the contents turn BRIGHT ORANGE, they will briefly turn BLUE. Make further additions with care. Lift
Color Change 1.4
Insert Here Value
8. Repeat steps 5 through 7 until a permanent color change occurs. Control
Here Read
1.5
= 1.5
Bar 1.6
9. When the color of the liquid in the Titret remains BRIGHT ORANGE, remove the Titret from the Titrettor. Hold in a vertical position and Press
Control Bar
Here

carefully read the depth scale on the Titret that corresponds to the liquid level at the bottom of the concave meniscus (Fig. 6). Refer to Sample
the chart below for dosage adjustments.
6
TEST RESULTS AND CONTROL DOSAGE REQUIREMENTS CONVERSION CHART
DEPTH SCALE UNITS 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.8 2.0 2.5 3.0 3.5 4.0 5.0 7.0 10.0
MAXIGARD (PCN 0034405)
as ppm product
12,000* 13,000 14,000 16,000 17,000 18,000 19,000 22,000 24,000 30,000 36,000 **42,000 48,000 60,000 84,000 120,000
DOSAGE in liters/ton OK OK HIGH HIGH
23 23 22 22 22 22 19 16 13 8 3 HIGH
Initial = 33.0 liters/ton No Dosing No Dosing HIGH HIGH
*If readings are below 12,000 (scale unit 1.0), add 25.0 ltr/ton and retest. If system has been partially drained and refilled, use initial dosage. As long as the system is not foaming and is at or under
* * Minimum requirements for High-Range Engine Program. There is no need to go significantly above these requirements.
Within Control Range a product ppm of 84,000, the high levels can be
reduced by the normal makeup process if that will
occur within a month, otherwise, partially drain and
freshen the system.

COOLING WATER CHLORIDE TEST PROCEDURE WEEKLY TEST – SYSTEM WATER

Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.
1. Add one scoop (0.5 g) of Sample Pretreatment (available individually, not part of Chloride LMP Test Kit) to approximately 70 ml of
cooling water, collected in Beaker 100 ml - Clear Plastic, and stir until granules dissolve into solution (Fig. 1). 1 2 3
2
2. WAIT 2 MINUTES to allow precipitates to settle .
3. Filter the sample by folding Filter Paper in quarters and overlapping three sections to form a funnel. Pour water through the Filter
OR
Paper and Funnel - Plastic (Fig. 2). Proceed with the chloride determination using the Chloride LMP Test Kit. Sample
~70 ml WAIT 2 MINUTES 10 ml
4. For samples < 100 ppm chlorides: Rinse the Plastic Vial and fill to the mark (10 ml) with the sample to be tested (Fig. 3). Pretreatment
then
2
ml

For samples > 100 ppm chloride: Rinse the tall Glass Vial (test tube) and fill to the mark (2 ml) with the sample to be tested (Fig. 3). Filter Sample

5. Neutralize the sample by adding 3 drops of Phenolphthalein Indicator to the sample. Swirl to mix. If the sample turns PINK add
Sulfuric Acid N/10 drop by drop while swirling until the sample turns CLEAR. Afterwards, add one more drop (Fig. 4).
6. Adjust the color of the sample by adding 6 drops of Potassium Chromate. The sample will be YELLOW (Fig. 5). 4 5 6
4
7. Counting the drops, add Silver Nitrate N/10 drop by drop. Swirl between drops until the sample turns ORANGE (Fig. 6). OR &
8. Calculate the chloride concentration:
If plastic vial (< 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 10 = ppm chloride
# #
If glass test tube (> 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 50 = ppm chloride 10 ml 10 ml 10 ml 10 ml 10 ml

TEST RESULTS
Chloride 50 ppm (See Note 1) Maximum Limit
Note 1: If manufacturer’s recommendations are more stringent, take those limits into account.

CW_MAXIGARD HIGH-RANGE-CONTROL TEST CARD_R203

 MAKEUP WATER CONTAMINANTS WEEKLY TEST –MAKEUP WATER CONTAMINANTS
NOTE: The use of high quality, distilled makeup water is recommended as the best means to control scale. Makeup tanks
should be tested every week or more often if there is a change in the source or mixture of the water or any upset is suspected. PARAMETER MAXIMUM LIMIT
If at all possible, do not introduce makeup water with Chlorides above 50 ppm or Hardness over 170 ppm, especially if system Chloride 50 ppm Maximum Limit
water is not sufficiently below these limits to dilute the intended makeup water. Hardness 170 ppm Maximum Limit

MAKEUP WATER CHLORIDE TEST PROCEDURE WEEKLY TEST – MAKEUP WATER CHLORIDE
Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.
1a. For samples < 100 ppm chlorides: Rinse the Plastic Vial and fill to the mark (10 ml) with the sample to be tested (Fig. 1).
1b. For samples > 100 ppm chloride: Rinse the tall Glass Vial (test tube) and fill to the mark (2 ml) with the sample to be tested (Fig. 1). 1 2
2. Neutralize the sample by adding 3 drops of Phenolphthalein Indicator to the sample. Swirl to mix. If the sample turns PINK add
Sulfuric Acid N/10 drop by drop while swirling until the sample turns CLEAR. Afterwards, add one more drop (Fig. 2). OR
OR &

3. Adjust the color of the sample by adding 6 drops of Potassium Chromate. The sample will be YELLOW (Fig. 3).
10 ml
4. Counting the drops, add Silver Nitrate N/10 drop by drop. Swirl between drops until the sample turns ORANGE (Fig. 4). 2
ml
10 #
10 ml 10 ml 10 ml
5. Calculate the chloride concentration:
If plastic vial (< 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 10 = ppm chloride
If glass test tube (> 100 ppm) was used in Step 4: - Number of drops of Silver Nitrate N/10 * 50 = ppm chloride 3 4

TEST RESULTS
#
Chloride 50 ppm (See Note 1) Maximum Limit 10 ml 10 ml

Note 1: If manufacturer’s recommendations are more stringent, take those limits into account.

MAKEUP WATER HARDNESS TEST PROCEDURE WEEKLY TEST – MAKEUP WATER CHLORIDE
Note: If the sample is colored or turbid, filter before running the test. If the sample remains cloudy after the first filtering, the sample should again be filtered through the same paper since the filter becomes more retentive on the second filtration.

1. Rinse and fill the Sample Cup to the 25 ml mark with makeup water sample (Fig. 1).
2. Slide the flexible rubber end of the Valve Assembly over the tapered tip of the Titret to the white Reference Line for a snug fit (Fig. 2). 1 2 Slide Over 3 Snap
Valve
3. Snap the tip of the Titret (ampoule) at the Score Mark (Fig. 3). ml
Score
Valve
Assembly Score Assembly
25
4. With the tip of the valve assembly immersed in the sample, squeeze the bead valve briefly to add a small amount of sample to the 20 Mark Mark
15
Titret (Fig. 4). The red indicator in the Valve Assembly will also be added to the Titret. 10 Reference
NOTE: Do not squeeze the bead value unless the tip of the Valve Assembly is immersed below the surface of the liquid. 5 Line
Titret Titret
5. Rock the Titret to mix the contents. The contents of the Titret will turn a BLUE color.
6. Continue to add small amounts of sample until the liquid in the Titret turns from BLUE to PINK. Be sure to rock the Titret to mix the
contents after each addition of sample. When the color of the liquid in the Titret changes to PINK, the end point has been reached. 4 55
Stop the test, hold the Titret in a vertical position and carefully read the depth scale on the Titret that corresponds to the liquid level at Squeeze 26
Value
the bottom of the concave meniscus (Fig. 5). Results are in ppm total hardness as calcium carbonate CaCO3. Bead
Valve Read
28
= 28
Here 30

TEST RESULTS
Hardness 170 ppm Maximum Limit

APPARATUS AND REAGENTS

CWT Titrets: CWT Titrets (PCN 0367012) Beaker 100 ml Plastic: Beaker 100 ml - Clear Plastic (PCN 0247016)
Chlorides: Chloride LMP Test Kit (PCN 0373019) Filter Paper: Filter Paper - 100/BX (PCN 0225012)
Pretreatment: Sample Pretreatment (PCN 0374025) (for SYSTEM Water Chloride Test) Funnel: Funnel - Plastic (PCN 0221010)
Hardness: Total Hardness Titrets (PCN 0378019) Stirring Rod: Stirring Rod - 150 mm Plastic (PCN 0417015)

CW_MAXIGARD HIGH-RANGE-CONTROL TEST CARD_R203