Professional Documents
Culture Documents
Food Pacakging Lesson Plan Detailed-1
Food Pacakging Lesson Plan Detailed-1
LESSON PLAN
COURSE NO: ELE PFE-483
2021
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 1
Course No : ELE PFE 483 Course Title : Food Packaging
Teaching Schedule
a) Lesson Plan- Theory
1. Introduction, 7 1 5-6
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 2
Lect. Title Book Chapter Page Weightage
(%)
No. No. /ArticleNo. No.
21 - MAP, 7 7 22-24
22
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 3
Lect. Title Book Chapter Page Weightage
(%)
No. No. /ArticleNo. No.
3 9.1 282-
284
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 4
b) Practical Exercises
No. Title
Identification of different types of packaging materials
1
Determination of tensile/ compressive strength of given material/package
2
To perform different destructive and non-destructive tests for glass containers
3
Vacuum packaging of agricultural produces
4
Determination of tearing strength of paper board
5
Measurement of thickness of packaging materials
6
14 Aseptic packaging
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 5
Suggested readings
Text Books
Book Title Author Publisher Year
No.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 6
LECTURE NO. 1
1.Metal cans and glass bottles have lost large markets to rigid and flexible plastics and
printed monocartons.
2.Flexible packaging has replaced all forms of rigid packaging. The flexible packaging
segment has seen many new innovations. The concept of the single use unit pack is now
globally acknowledged as a marketing first.
3.Laminate tube has almost entirely replaced the aluminium collapsible tube for
toothpaste packaging, now making inroads into the pharmaceutical sector.
4.PET bottles & Jars have made a spectacular entry into the Indian market, recording
annual growth rates in excess of 20% per annum; in its wake, the demand for a whole
new range of plastic closures has also emerged replacing metal closures.
5.PET bottles are used for mineral water, edible oil, carbonated soft drinks and ahost of
other products.
DEFINITION OF PACKAGING:
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 7
Packaging has been defined as a socio scientific discipline which operates in
society to ensure delivery of goods to the ultimate consumer of those goods in the
best condition intended for their use.
The verb "packing" can be defined as the enclosing of an individual item (or
several items) in a package or container.
For example:
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 8
However, the basic functions of packaging are more specifically stated:
Containment: depends on the product’s physical form and nature. For example, a
hygroscopic free-flowing powder or a viscous and acidic tomato concentrate
Information about the product: legal requirements, product ingredients, use etc.
Convenience: for the pack handlers and user(s) throughout the packaging chain
Presentation: material type, shape, size, colour, merchandising display units etc.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 9
Brand communication: e.g. pack persona by the use of typography, symbols,
illustrations, advertising and colour, thereby creating visual impact
Promotion (Selling): free extra product, new product, money off etc.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 10
LECTURE NO. 2-4
TOPICS: Factors affecting shelf life of food material during storage, Interactions of
spoilage agents with environmental factors as water, oxygen, light, pH, etc. and
general principles of control of the spoilage agents.
Shelf life is the length of time that foods, beverages, and many other perishable
items are given before they are considered unsuitable for sale, use, or
consumption.
It is the time between the production and packaging of a product and the point at
which the product first becomes unacceptable under defined environmental
conditions.
It is a function of the product, package and the environment through which the
product is transported, stored and sold.
The main factors that cause deterioration of foods during storage are:
It controls light transmission, the rate of transfer of heat, moisture and gases, and
movement of micro organisms or insects.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 11
Interactions of spoilage agents with environmental factors as water, oxygen, light,
pH, etc. and general principles of control of the spoilage agents:
1. Light
2. Heat
However, control over the temperature of storage is more important than reliance
on the packaging to protect foods from heat.
Moisture loss or uptake is one of the most important factors that controls the
shelf life of foods.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 12
packages and resulting mould growth (for example in fresh vegetables and bread),
or to prevent freezer burn in frozen foods.
Foods that have a low equilibrium relative humidity, such as dehydrated foods,
biscuits and snackfoods, require packaging that has a low permeability to
moisture or they will gain moisture from the atmosphere and lose their crispness.
If the water activity rises above a level that permits microbial growth they will
spoil.
Conversely, fresh foods that are respiring and have a high equilibrium relative
humidity, require a high degree of permeability to allow exchange of oxygen and
carbon dioxide with the atmosphere, without excessive loss of moisture that
would cause a loss of weight and shrivelling.
Chilled foods require controlled movement of water vapour out of the pack to
prevent fogging in display packs when the storage temperature changes, and foods
packaged in modified atmospheres require careful control over both the gas
composition and water vapour movement to achieve the expected shelf life.
Micro-organisms, insects, animals and soils Metal, glass and polymer packaging
materials are barriers to micro-organisms, but their seals are a potential source of
contamination.
Packs that are folded, stapled or twist wrapped are not truly sealed.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 13
• contaminated air or water drawn through pinholes in hermetically sealed
containers as the head space vacuum forms
5. Mechanical strength
Some foods (for example fresh fruits, eggs, biscuits, etc.) are easily damaged and
require a higher level of protection from a package, including cushioning using
tissue paper, foamed polymer sheets, or from paperpulp that is formed into shaped
containers for individual pieces (e.g. egg cartons, fruit trays).
Wooden crates and barrels or metal drums have a long history of use as shipping
containers as they provide good mechanical protection.
These are now being replaced by cheaper composite intermediate bulk containers
(IBCs) made from fibreboard and polypropylene.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 14
• Young's modulus
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 15
LECTURE NO. 5-6
technological
political/legal
socio-cultural
demographic
ecological
raw material availability
economic.
The world’s total food production has more than doubled over the past fifty years
due to improved methods in animal husbandry, the use of advanced seed varieties and
crop protection products that boost crop yields and quality. Mass production of
packaged food has been enabled by technological innovations in food production,
processing and logistics with packaging playing a key role.The economies of scale
involved and the intense industrial competition have made many products more
affordable.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 16
Packaging combined with developments in food science, processing and
preservation techniques, has been applied in a variety of ways to ensure the safety of the
consumer and integrity of the product. The success of both pack- aging and food
technology in this regard is reflected by the fact that the contents of billions of packs are
being safely consumed every day. In order to help minimise food waste throughout the
supply chain and save cost, an optimum level of packaging is required. Significant food
wastage occurs in many less developed countries – between 30% and 50% of food
produced iswasted due to inadequate means of preservation, protection, storage and
transportation (World Health Organisation). In developed countries, where modern
processing, packaging and distribution systems are commonplace, food wastage before it
reaches the consumer is only 2–3%.
The value of food packaging to society has never been greater nor, paradoxically, has
packaging attracted so much adverse media publicity and political attention. In response,
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 17
stakeholders in the food industries need to fully appreciate and actively promote the
positive contributions that their packaging makes to the quality of life. Food packaging is
governed by a mass of laws, regulations, codes of practice and guidelines.
prevents or reduces product damage and food spoilage, thereby saving energy and
vital nutrients, and protecting the health of the consumer
requires less municipal solid waste disposal since it promotes processed food
residue recycling for use as animal feed or compost. For example, from 454 g (1
lb) of fresh corn-on-the-cob purchased at the supermarket, the customer eats
approximately only 170 g (six ounces), and the rest ends
up in the trash can and, ultimately, in the local landfill (Institute of Pack- aging
Professionals, IOPP, USA). This same amount of edible frozen corn can be
packed in a polyethylene bag weighing less than 5 g (less than 0.18 ounce)
lowers the cost of many foods through economies of scale in mass pro- duction
and efficiency in bulk distribution. Savings are also derived from reduced product
damage
reduces or eliminates the risk of tampering and adulteration
presents food in an hygienic and often aesthetically attractive way
communicates important information about the food and helps consumers make
informed purchases
provides functional convenience in use or preparation, freeing up more time
promotes goods in a competitive marketplace and increases consumer choice
facilitates the development of modern retail formats that offer consumers the
convenience of the one-stop shop and the availability of food from around the
world throughout the year
extends the shelf life with the benefit of prolonged product use, thereby reducing
wastage
saves energy through the use of ambient packs that do not require refrigeration or
frozen distribution and storage.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 18
The food industry is aware of current public concerns related to packaging which include:
Packaging may also be defined as: a means of safely and cost effectively
delivering products to the consumer in accordance with the marketing strategy of the
organisation.
A packaging strategy is a plan that addresses all aspectsand all activities involved
in delivering the packaged product to the consumer. Packaging strategy should be allied
to clearly defined marketing and manufacturing strategies that are consistent with the
corporate strategy or mission of the business. Key stakeholders in the strategic
development process include management from technical/quality, manufacturing,
procurement, marketing,supply chain, legal and finance functions. Packaging is both
strategically and tactically important in the exercise of themarketing function.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 19
Environmental considerations:
In industrialised countries, 67% of all packaging is used by the food industry and
an average household uses around 200 different packaged items (INCPEN, undated).
There have been a number of developments in both the types of materials used for
packaging and themethods of handling and distribution of packaged foods that have
affected the environmental impact of food packaging.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 20
LECTURE NO. 7-8
TOPICS: Packaging systems, types: flexible and rigid; retail and bulk; Levels of
packaging
The most recent EU Directive relating to ‘plastic materials and articles intended to
come into contact with foodstuffs’ defines plastics as being: ‘organic macromolecular
compounds obtained by polymerisation, polycondensation, polyaddition or any
similar process from molecules with a lower molecular weight or by chemical
alteration of natural macromolecular compounds’. Plastics are widely used for
packaging materials and in the construction of food processing plant and equipment,
because:
they are flowable and mouldable under certain conditions, to make sheets, shapes
and structures
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 21
The most widely used plastic today, polyethylene, was invented in 1933 –
it was used in packaging from the late 1940s onwards in the form of squeeze
bottles, crates for fish replacing wooden boxes and film and extrusion coatings on
paper-board for milk cartons. In Europe, nearly 40% of all plastics is used in the
packaging sector, and packaging is the largest sector of plastics usage
(Association of Plastics Manufacturers in Europe, APME). About 50% of
Europe’s food is packed in plastic packaging (British Plastics Federation, BPF).
Most packaging plastics are thermoplastic, which means that they can be
repeatedly softened and melted when heated. This feature has several important
implications for the use and performance of plastics, as in the forming of
containers, film manufacture and heat sealability. Thermosetting plastics are
materials which can be moulded once by heat and pressure. They cannot be
resoftened, as reheating causes the material to degrade.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 22
Plastics do not support the growth of microorganisms. Some plastics may
absorb some food constituents, such as oils and fats, and hence it is important that
a thorough testing is conducted to check all food applications for absorption and
migration. Gases such as oxygen, carbon dioxide and nitrogen together with water
vapour and organic solvents permeate through plastics. The rate of permeation
depends on:
• type of plastic
• method of processing
• storage temperature.
Plastics are chosen for specific technical applications taking the specific
needs, in packing, distribution and storage, and use of the product into
consideration, as well as for marketing reasons, which can include considerations
of environmental perception.
• rigid plastic containers such as bottles, jars, pots, tubs and trays
• flexible plastic films in the form of bags, sachets, pouches and heat-sealable
flexible lidding materials
• plastics combined with paperboard in liquid packaging cartons
• expanded or foamed plastic for uses where some form of insulation, rigidity and
the ability to withstand compression is required
• plastic lids and caps and the wadding used in such closures
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 23
• diaphragms on plastic and glass jars to provide product protection and tamper
evidence
• plastic bands to provide external tamper evidence
• pouring and dispensing devices
• to collate and group individual packs in multipacks, e.g. Hi-cone rings for cans
of beer, trays for jars of sugar preserves etc.
• plastic films used in cling, stretch and shrink wrapping
• films used as labels for bottles and jars, as flat glued labels or heat-shrinkable
sleeves
• components of coatings, adhesives and inks.
Plastic films may be combined with other plastics by coextrusion, blending,
lamination and coating to achieve properties which the components could not provide
alone. Coextrusion is a process which combines layers of two or more plastics together at
the point of extrusion. Lamination is a process which combines two or more layers of
plastics together with the use of adhesives. Different plastic granules can be blended
together prior to extrusion. Several types of coating process are available to apply plastic
coatings by extrusion, deposition from either solvent or aqueous mixtures or by vacuum
deposition.
• polyethylene (PE)
• polypropylene (PP)
• ionomers
• polyamides (PA)
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 24
• polyvinyl chloride (PVC)
• polystyrene (PS)
• fluoropolymers (PCTFE/PTFE)
• cellulose-based materials
Many plastics are better known by their trade names and abbreviations. In the
European packaging market, PE constitutes the highest proportion of consumption, with
about 56% of the market by weight, and four others, PP, PET, PS (including expanded
polystyrene or EPS) and PVC, comprise most of the remaining 46% (source BPF). The
percentages may vary in other markets, but the ranking is similar. The other plastics listed
meet particular niche needs, such as improved barrier, heat sealability, adhesion, strength
or heat resistance. These materials are all thermoplastic polymers.
It is also important to appreciate the fact that plastics are continually being developed,
i.e. modified in the polymerisation process, to enhance specific properties to meet the
needs of the:
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 25
In the case of food packaging, end use properties relate to performance properties,
such as strength, permeability to gases and water vapour, heat sealability and heat
resistance, and optical properties, such as clarity.
Additionally, the way the plastic is subsequently processed and converted in the
manufacture of the packaging film, sheet, container etc., will also have an effect
on the properties of that packaging item.
Levels of Packaging:
A primary package is the one which is in direct contact with the contained
product. It provides the initial, and usually the major protective barrier. Example:
Metal cans, paperboard cartons, glass bottles and plastic pouches, aerosal spray
can, Beverage can, cushioning envelopes, plastic bottles, skin pack.
A secondary package contains a number of primary packages. It is outside the
primary packaging perhaps used to group primary packages together. It is the
physical distribution carrier and is sometimes designed so that it can be used in
retail
outlets for the display of primary packages. Ex. Corrugated case, Boxes
A tertiary package is made up of a number of secondary packages. It is used for
bulk handling. Example being a stretch-wrapped pallet of corrugated cases. A
quaternary package is frequently used to facilitate the handling of tertiary
packages. This is generally a metal container up to 40 m in length which can be
transferred to or from ships, trains, and flatbed trucks by giant cranes. Certain
containers are also able to have their temperature, humidity and gas atmosphere
controlled. This is necessary in particular situations such as the transportation of
frozen foods, chilled meats and fresh fruits and vegetables.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 26
LECTURE NO. 9-20
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 27
Three-piece cans
Three-piece ‘sanitary’ cans, consisting of a can body and two end pieces, are used
to hermetically seal heat-sterilised foods and also to package powders, syrups and
cooking oils.
They are made from mild steel that is rolled to a strip 1.8 mm thick, and then
dipped into hot dilute sulphuric acid, cold-rolled to 0.15–0.50 mm thick, and then
temper-rolled to give required hardness and surface finish.
Further cold reduction produces steel with greater stiffness and so thinner sheet
can be used (known as ‘double cold-reduction’ steel).
Tin is applied by electroplating to a different thickness of tin coatings on each
side of the steel (e.g. 2.8–1.2 g m2 or 0.1–0.3 mm thick).
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 28
However, this produces a dull surface, due to the porous finish and it is heated
quickly in a bath of hot oil or by electric induction (known as ‘flow brightening’)
to slightly melt the tin and improve surface brightness and resistance to corrosion.
It is then treated with chromate solution to stabilise the finish.
The tin may be coated with the following lacquers toprevent interactions with
foods
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 29
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 30
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 31
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 32
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 33
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 34
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 35
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 36
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 37
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 38
Single films
Most polymer films are made by extrusion, in which pellets of the polymer are
meltedand extruded under pressure as a sheet or tube.
Other methods are callandering, where the polymer is passed through heated
rollers until the required thickness is achieved, and casting, in which the extruded
polymer is cooled on chilled rollers.
The most important types of film for food packaging are described below and a
selection of their properties is shown in Table 24.2.
Cellulose films are produced by mixing sulphite paper pulp with caustic soda to
dissolve it and it is allowed to ‘ripen’ for 2–3 days to reduce the length of polymer
chains and form sodium cellulose.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 39
This is then converted to cellulose xanthate by treatment with carbon disulphide,
ripened for 4–5 days to form ‘viscose’, and then cellulose is regenerated by
extrusion or casting into an acid–salt bath to form cellulose hydrate.
Glycerol is added as a softener and the film is then dried on heated rollers.
Higher quantities of softener and longer residence times in the acid–salt bath
produce more flexible and more permeable films.
Plain cellulose is a glossy transparent film which is odourless, tasteless and
biodegradable within approximately 100 days.
It is tough and puncture resistant, although it tears easily.
It has low-slip and dead-folding properties and is unaffected by static buildup,
which make it suitable for twist-wrapping.
However, it is not heat sealable, and the dimensions and permeability of the film
vary with changes in humidity.
It is used for foods that do not require a complete moisture or gas barrier,
including fresh bread and some types of confectionery (Table 24.2).
An international code is used to identify the various types of cellulose film (Table
24.5).
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 40
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 41
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 42
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 43
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 44
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 45
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 46
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 47
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 48
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 49
High impact polystyrene (HIPS) and acrylonitrile butadiene styrene (ABS) are
widely used for thermoformed trays, tubs and cups to contain yoghurt, margarine,
cheeses, spreads, ice cream and desserts.
In its natural state it is translucent but it can easily be
coloured.
Polyvinyl chloride (PVC) trays, tubs and bottles are made by extrusion- or
injection-stretch blow moulding.
Food-grade PVC is tough, clear and easy to colour. It
has good oil resistance and low gas permeability and is therefore used in trays for
meat products and chocolates, in tubs for margarine or jams, and in bottles for
edible oils, fruit juices, squashes and concentrates.
However, it has lower strength than PET and is not used for carbonated beverages
as it cannot withstand the pressure of carbonation.
It also has a relatively low temperature resistance (65–70ºC). Polypropylene is
currently more expensive than HIPS or PVC and is less widely used for
rigid/semi-rigid containers.
However, it is resistant to a wider temperature range (deep-freeze temperatures to
120–140ºC) and also provides a good barrier to water vapour and oxygen.
High-density polyethylene is at present the most common material used for
bottles and jars.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 50
It is used for vinegar, milk, syrups and as drums for salt and bulk fruit juices
(Briston, 1987).
Polypropylene coextrusions, in which ethylene–vinyl alcohol copolymer is a
central barrier material, are used for mustard, mayonnaise, jams, tomato ketchup
and other sauces to give a shelf life of 18 months.
They are shatterproof, oxygen and moisture resistant, squeezable and suitable for
hot filling
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 51
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 52
Coated papers-
Many papers are treated with wax by coating, dry waxing (in which wax
penetrates the paper while hot) or wax sizing (in which the wax is added during
the preparation of the pulp).
Wax provides a moisture barrier and allows the paper to be heat sealed.
However, a simple wax coating is easily damaged by folding or by abrasive
foods, but this is overcome by laminating the wax between layers of paper and/or
polyethylene.
Waxed papers are used for bread wrappers and inner liners for cereal cartons.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 53
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 54
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 55
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 56
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 57
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 58
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 59
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 60
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 61
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 62
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 63
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 64
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 65
LECTURE 21-22
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 66
4. Special equipment and training required.
5. Increased pack volume adversely affects transport costs and retail display
space.
6. Loss benefits once the pack is opened or leaks.
7.CO2 dissolving into the food could lead to pack collapse and increased drip.
Gases used in MAP:
The three main gases used in MAP are CO2,, O2, and N2, either singly or in
combination.
Carbon dioxide: Carbon dioxide is the most important gas in the MAP of foods
because of its bacteriostatic and fungistatic properties. It inhibits the growth of
many spoilage bacteria, the degree of inhibition increasing with increasing
concentration. It is particularly effective against aerobic spoilage bacteria such as
Pseudomonas species.
The solubility of CO2 increases with decreasing temperature and therefore
the antimicrobial activity of CO2 is markedly greater at lower temperatures. This
has significant implications for MAP of foods. The high solubility of CO2 in high
moisture/high fat foods such as meat, poultry and seafood can result in package
collapse owing to the reduction of heads pace volume. High levels of CO2 can
also result in increased drip or exudate from flesh foods, and the addition of
absorbent pads in the base of the package is used to compensate for this.
Oxygen: Oxygen promotes several types of deteriorative reactions in foods
including fat oxidation, browning reactions and pigment oxidation. Most of the
common spoilage bacteria and fungi require O2 for growth. For these reasons, O2
is either excluded or the level set as low as possible. Exceptions occur where O2
is needed for fruit and vegetable respiration or the retention of color in red meat.
Nitrogen: Nitrogen is an inert gas with no odor or taste. It has a lower density
than air and a low solubility in water and other food constituents, making it a
useful filler gas in MAP to counteract package collapse caused by CO2 dissolving
in the food. Nitrogen indirectly influences the micro-organisms in perishable
foods by retarding the growth of aerobic spoilage microbes but it does not prevent
the growth of anaerobic bacteria.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 67
LECTURE NO. 23
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 68
have blends of LLDPE as well. Sometimes a little quantity of HDPE material is
also added.
For selection of plastic material, besides type of plastics, the yield of the
film is also important to be considered from theeconomy point of view. The yield
means the area obtained or number of square meters of filmconverted from a
kilogram of material of a given thickness or gauge.
Shrink wrapping is covered loosely around a product andit shrinks tightly
when heat is applied This type of wrapping is employed to protect a product from
dust or weather Heating machine is essential when using any type of shrink wrap.
Shrink wrap machine available for heating arrangement are Heat gun
which releases a stream of hot air Shrink tunnel which are mounted over a
conveyor systemfor the product to flow through along with oven
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 69
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 70
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 71
LECTURE NO. 24
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 72
b) Its principal purpose is to remove oxygen by pulling the packaging material into intimate
contact with the product.
Factors affecting vacuum packaging :
a) Characteristics of food products to be packaged.
b) Reliability of packaging machine and packaging material.
Vacuum packaging for agricultural products :
The agricultural produce may be fresh fruit or fresh vegetables.
• The agricultural produce may be high acid food products such as fruit or acidified
vegetables.
• The vacuum may extract residual entrained or dissolved gasses present within the
agricultural produce.
Vacuum Packaging Machinery :
Packaging machine is used for vacuum packing with packaging materials having an extremely
high gas barrier for the persistence of food preservation. The four types of machines are
classified by mechanical faculty: nozzle, chamber, skin and deep-draw type.
Procedure :
1. Nozzle-Type Vacuum Packaging Machine :
Air in the bag is evacuated through a nozzle; a mouthpart of the bag is sealed by heater
or impulse system. The two processes o vacuuming and sealing on most of this type of
machines are automatically done, initiated by stepping on a foot switch. Accordingly,
although the operation is easier than those of other types of vacuum packaging
machines, the degree of vacuum of bags packaged by this type of machine is lower than
for others.
2.Chamber-Type
Vacuum Packaging Machine: The bag containing food placed in the chamber then
vacuum is created after that packet is sealed by an impulse system in a vacuum-seal
chamber. The appearance of food vacuum-packaged by this type machine increases
food value and display effect.
3.Skin-Type Vacuum Packaging Machine :
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 73
it can be done by loading food in pack and applying a lid over it. In this vacuum packaging
machine, heated and softened upper film is applied skin-tight over food and a lower film in the
vacuum chamber. The appearance of food vacuum-packaged by this type machine
increases food value and display effect.
4.Deep-Draw Type Vacuum Packaging Machine :
The lower film is warmed by a hot plate and then deep drawn by vacuuming
through a pump. After food loaded in the bag is covered by the upper film, both films are
sealed in the vacuum chamber. The newest machine of this type is controlled by computer,
and deep drawing, loading, vacuuming, sealing, trimming, etc. are set going automatically.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 74
LECTURE NO.25
The rapid growth of chilled, MAP/CAP, and minimally processed foods during
the 1990s has been accompanied by a number of developments in packaging
technologies, which may be grouped under the term ‘active’ packaging. Active packaging
has been described by Labuza (1996), Plaut (1995) and Rooney (1995) and includes:
• oxygen scavenging
• CO2 production
• antimicrobial action
• aroma release
• moisture removal
• time–temperature indicators
• gas indicators
• films to slow moisture transfer between ingredients that have different water activities
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 75
It is used in packs for popcorn, French fries, pizzas, pies, baked goods, etc. De-
metallised susceptors have areas in which the metallisation is etched off during
production. This enables heat to be directed to specific areas of a pack and also
prevents carton glues from melting or producing volatiles that could contaminate the
product (Woods, 1993)
• infrared films that radiate energy to inactivate micro-organisms
• steam release films
• time–temperature indicators to display loss of shelf life and extreme-temperature
indicators to display temperature abuse conditions
• indicator labels that change colour when a specified level of CO2 is attained in a
modified atmosphere package
• tamper-evident labels that change colour when they are removed and leave
behind a message on the pack that cannot be hidden.
Possible future developments in active packaging include self-venting microwave
packs in which a vent opens at a pre-set temperature and closes on cooling, respiring
trays that respond to changing atmospheric conditions to optimise respiration, materials
that generate electrical impulses when moved; their electrical conductivity may change
when exposed to light and their opacity may change or they become softer or harder
when subjected to small electrical charges (Louis, 1998).
Active packaging refers to the incorporation of certain additives into packaging
film or within packaging containers with the aim of maintaining and extending
product shelf life (Day, 1989). Packaging may be termed active when it performs some
desired role in food preservation other than providing an inert barrier to external
conditions (Rooney, 1995; Hotchkiss, 1994). Active pack- aging includes additives or
freshness enhancers that are capable of scavenging oxygen; adsorbing carbon dioxide,
moisture, ethylene and/or flavour/odour taints; releasing ethanol, sorbates, antioxidants
and/or other preservatives; and/or maintaining temperature control. Table 9.1 lists
examples of active packaging systems, some of which may offer extended shelf life
opportunities for new categories of food products (Day, 1989, 2001; Rooney, 1995).
Active packaging has been used with many food products and is being tested with
numerous others. Table 9.1 lists some of the food applications that have benefited from
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 76
active packaging technology. It should be noted that all food products have a unique
deterioration mechanism that must be understood before applying this technology.
The shelf life of packaged food is dependent on numerous factors such as the
intrinsic nature of the food, e.g. acidity (pH), water activity (aw), nutrient content,
occurrence of antimicrobial compounds, redox potential, respiration rate and biological
structure, and extrinsic factors, e.g. temperature, relative humidity (RH) and the
surrounding gaseous composition. These factors will directly influence the chemical,
biochemical, physical and microbiological spoilage mechanisms of individual food
products and their achievable shelf lives. By carefully considering all of
these factors, it is possible to evaluate existing and developing active packaging
technologies and apply them for maintaining the quality and extending the shelf life of
different food products (Day, 1989). Active packaging is not synonymous with intelligent
or smart packaging, which refers to packaging that senses and informs (Summers, 1992;
Day, 2001).
Intelligent packaging devices are capable of sensing and providing information
about the function and properties of packaged food and can provide assurances of pack
integrity, tamper evidence, product safety and quality, and are being utilised in
applications such as product authenticity, anti-theft and product traceability (Summers,
1992; Day, 2001).
Intelligent packaging devices include time-temperature indicators, gas sensing
dyes, microbial growth indicators, physical shock indicators, and numerous examples of
tamper proof, anti-counterfeiting and anti-theft technologies. Information on intelligent
packaging technology can be obtained from other reference sources (Summers, 1992;
Day, 1994, 2001). It is not the intention of this chapter to extensively review all active-
packaging technologies but rather to describe the different types of devices, the scientific
principles behind them, the principal food applications and the food safety and regulatory
issues that need to be considered by potential users. The major focus of this chapter is on
oxygen scavengers but other active packaging techno- logies are also discussed and some
recent developments highlighted. More detailed information on active packaging can be
obtained from the numerous references listed.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 77
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 78
LECTURE NO. 26
TOPICS: Packaging requirement for raw and processed foods, and their selection of
packaging materials.
The technical factors that should be taken into account when selecting a
packaging material for a particular product are described by Briston (1988). The
requirements of packaging to protect foods for their expected shelf life are discussed in
more detail in Section 24.1. The shelf life of packaged foods is controlled by the
properties of the food (including water activity, pH, susceptibility to enzymic or
microbiological deterioration and the requirement for, or sensitivity to, oxygen, light,
carbon dioxide and moisture) and the barrier properties of the package.
1. Shipping containers which contain and protect the contents during transport and
distribution, but have no marketing function. Corrugated fibreboard cases are the most
widely used shipping container for 5–20 kg loads, although they are steadily
being replaced by shrink wrapped or stretch wrapped corrugated trays. Other types of
shipping containers include wooden or metal cases, crates, barrels, drums and sacks.
More recently, intermediate bulk containers (IBCs), including combi-bins, large
boxes made from metal, plastic or corrugated fibreboard, and large bags made from
woven plastic fabric, have been introduced to increase handling efficiencies and have
largely displaced wooden crates and cases (see also Section 24.1.5 and Chapter 26).
IBCs have a capacity between that of a bulk road tanker and 220 l drums (e.g. 1000 l
containers with integral pallet and bottom discharge valve), and are mainly used for
powders and liquids. Many shipping containers are expensive and therefore made to
be returnable (e.g. plastic crates for milk, beer and soft drink bottles). Others (for
example expanded polystyrene shipping containers) provide insulation and mechanical
protection for tomatoes and grapes or cured and wet fish and are used
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 79
• protect against the climate and contamination
• be compatible with the product
• be easily and efficiently filled and sealed
• be easily handled
• remain securely closed in transit, open easily when required (e.g. customs inspection)
and reclose securely
• carry information for carriers, wholesalers, and manufacturers about contents,
destination, and how to handle and open the pack.
• have minimum cost
• be readily disposable, re-usable or have another use.
2. Retail containers (or consumer units) which protect and advertise the food in
convenient quantities for retail sale and home storage (for example metal cans, glass
bottles, jars, rigid and semi-rigid plastic tubs, collapsible tubes, paperboard cartons,
and flexible plastic bags, sachets and overwraps).For convenience, this section describes
both shipping and retail containers in categories that reflect their material of construction.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 80
LECTURE NO. 27
The key to successful food packaging is to identify the packaging needs of the
product. These relate to the nature of the product, the intended market, shelf life,
distribution and storage, point of sale to the ultimate consumer and the use and eventual
disposal of the packaging. The choice should take account of environmental and waste
management issues. Ensuring food safety with respect to biological risks and needs
relating to flavour, colour and texture is essential. Packaging needs can be considered in
terms of:
• protection of the product – quality, safety etc.
• appearance – sales promotion, pack design etc.
• production – extrusion, forming, printing, packing etc.
Having decided that a type of plastic pack selected from the range of pos- sible
choices, such as a film sachet, lidded tray, bottle etc., the next decision concerns the type
of plastic or combination of plastics necessary to meet the functional needs. Performance
is related to the structural design of the pack and whether it is made from film, sheet,
moulding or expanded plastic. As we have seen, there are many plastics, each offering a
range of properties, and within each packaging type there are differences.
All plastics provide barriers to the ingress of gaseous and volatile materials from the
external environment into a hermetically sealed pack and from the food product both into
and through the pack into the external environment. The extent to which these effects
occur will depend on the food product and on the type of plastic(s), its thickness and on
the temperature and RH ranges to be experienced during the life of the product.
Some plastics are heat sealable so that packs can be sealed; some are also heat
resistant to meet defined needs, e.g. reheating by microwave, radiant heat and retort
sterilization. Some are suitable for storage in deep freeze. Many specific needs can be
met within the defined conditions of use. In a chapter of this type, we can make readers
aware of the choices and provide a basis for meaningful discussions between
technologists whether they be suppliers or users of plastic packaging. The following
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 81
Tables 7.1 to 7.3 give some guidance in terms of ranking for moisture vapour
permeability, gas permeability, optical properties, packing machine performance and heat
sealability.
The commercial consideration of cost must also be considered. Run lengths and
lead times are also important. It is not unknown for there to be run length cost
differences, where at one point a particular solution is cost effective rela- tive to an
alternative solution and for the position to be reversed at a different run length.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 82
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 83
LECTURE NO. 28
An important strategic issue facing the food industry is the political and public
pressure over the environment, particularly in relation to concerns over the amount of
packaging and packaging waste. For over a decade, packaging and packaging waste have
been the focus of attention from politicians as a result of pressure from the public, media
and environmental pressure groups. The industry’s options to improve the environmental
performance of packaging are summarised in Table 1.18.
Packaging forms only a small part of the total solid waste (TSW) stream. In the
UK, packaging waste represents approximately 6% of non-agricultural land-filled TSW
which amounts to 120 million tonnes per year. This packaging waste comprises 3% of
packaging from the household waste stream and 3% of packaging from
commercial/industrial waste streams (INCPEN). For many years, the packaging sectors
of the food industry have made signifi- cant efforts, for both commercial and
environmental reasons, to reduce the
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 84
amount of packaging and its environmental impact through light-weighting and
packaging redesign. Examples of light-weighting are given below:
•Food cans – 50% lighter than 50 years ago
•Yoghurt pots – 60% lighter than 30 years ago
•PET bottles for carbonated drinks – 33% lighter than almost 30 years ago
•Drinks cartons – 16% lighter than 10 years ago
Source: INCPEN Environmental policy on packaging should focus on resource-
efficiency and not just waste and recycling. A full strategic response to the environmental
issue would include:
•minimising energy and raw material use
•minimising the impact on the waste stream
•not causing environmental damage.
There are many alternative routes to achieve these objectives but the key
possibility for gaining a competitive edge for a retailer or manufacturer is repositioning
all products to satisfy a comprehensive environmental audit. The risk and uncertainty
involves the relative strength of environmental concerns and other key consumer
attributes.
There are management tools to reduce or compare the environmental impacts of
industrial systems and these include life-cycle inventory analysis (LCI) and life-cycle
assessment (LCA). The International Organization for Standardization (ISO) has
responded to the need for an internationally recognised methodology for LCI and LCA.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 85
LECTURE NO. 29
TOPICS: Package testing: Testing methods for flexible materials, rigid materials
and semi rigid materials
Package Testing:
Package testing must be performed under standard conditions (see ISO 2206 or
BS 4826 pt.2). All packages should be tested in a controlled atmosphere, generally 23°C,
50% rh.
Thickness:
Thickness of a material is the perpendicular distance between the two outer
surfaces of the material. Many physical properties of packaging materials are dependent
upon the thickness e.g. Water Vapour Transmission Rate (WVTR) and Gas transmission
Rate (GTR) of a film is inversely proportional to thickness and decrease with increase in
thickness.
Dial gauge, micrometer, screw gauge, vernier calipers are used for the
measurement of thickness. For paper boards, thickness is reported in points or in mm (1
point = 1/1000 of an inch); for papers it is in mm or inches. For films, thickness is
reported in micron, mils or in gauge (25 micron = 1mil = 1/1000 of an inch = 100 gauge
= 0.25 mm).
Paper density:
Paper density (also known as basis weight and grammage) is a term used in the
pulp and paper industry to denote a measure of mass of the product per unit of area for a
type of paper or paperboard.
The term "density" is not used in its traditional sense of mass per unit volume.
"Paper density", rather, is a measure of the area density. Paper density can also be used to
distinguish paper from paperboard as the latter usually has a grammage
greater than 224 g/m².
Two ways of expressing paper density are commonly used:
• Expressed in grams per square meter (g/m²), paper density is also known as grammage.
This is the measure used in most parts of the world.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 86
• Expressed in terms of the mass (expressed as weight) per number of sheets, it is known
as basis weight.
The convention used in the United States and a few other countries using US
paper sizes is pounds of a ream of 500 (or in
some cases 1000) sheets of a given (raw, still uncut) basis size. Japanese paper is
expressed as the weight in kg of 1000 sheets.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 87
LECTURE NO. 30-31
TOPICS: Tests for paper (thickness, bursting strength, breaking length, stiffness,
tear resistance, folding endurance, ply bond test, surface oil absorption test, etc.),
Tests for Plastic film and laminates (thickness, tensile strength, gloss, haze, burning
test to identify polymer, etc.), Tests for aluminium foil (thickness, pin holes, etc.),
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 88
Impact Strength — Impact strength is the energy required to puncture a flexible
structure to shock loading. This gives a measure of the toughness. The test is described in
the ASTM D 3420 and ASTM D1709.
Tear Strength — The measurement of tear strength takes into account the energy
absorbed by the film sample in propagating a tear. Two standard methods are available:
ASTM standard D 1004 describes the measurement for initial tear resistance, and ASTM
D 1922 refers to the energy absorbed by a test specimen in propagating the tear that has
already been initiated by cutting a small hole in the sample. The value of tear strength in
one film may vary widely depending on the degree of orientation such as oriented PP,
and whether the measurement is performed in the machine direction or cross machine
direction. This is described by ASTM D 1938.
Pinhole Flex Test — Pinhole flex resistance is the ability of a film to avoid the formation
of pinholes during repeated folding. A film that has a low value of pinhole flex resistance
will generate pinholes, at the folding line, following repeated flexing (ASTM F 456). A
related test is the folding endurance.
Folding Endurance — This test measures the resistance of the material to flexure or
creasing. The ASTM recommended procedure is described in the standard D 2176 which
is used to determine the number of folds necessary to break a sample film.
Heat sealing Temperature — Important properties for wrapping,bag making, or sealing
a flexible structure is the heat sealability characteristic of the material. To evaluate the
seal, two values are normally measured: the peel strength (ASTM F 88), and the hot tack
strength. As previously indicated, the absolute temperature and range of temperature
must be considered. The polymer’s average molecular weight determines the temperature
level and the MWD determines its range.
Coefficient of Friction — The coefficient of friction (COF) is a measurement of the
friction force between two surfaces. Cases in which friction is important include films
passing overfree-running rolls, bag forming, wrapping film around a product, and bag
stacking. Speed, temperature, static, humidity, blocking, and surface smoothness affect
the COF (TAPPI T 503 and ASTM D 1894).
Blocking — This is the tendency of two films to stick together when they are contacting
each other. This effect is enhanced by a smooth surface and when the films are left under
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 89
pressure, as is the case of stacked sheets or compacted rolls of film. Blocking can be
measured by the force needed to separate two sheets when force is applied perpendicular
to them, (ASTM D 1893 and D 3354, or Packaging Institute Procedure T 3629).
Haze — Haze is the percentage of transmitted light that, in passing through the sample,
deviates by more than 2.5° from an incident parallel beam. The appearance of haze is
caused by light being scattered by surface imperfections and non-homogenous materials,
Gloss — Gloss is the percentage of incident light that is reflected at an angle equal to the
angle of incidence (normally 45°). It is a measure of the ability of a surface to reflect the
incident light. High gloss produces a sharp image of any light source and gives a pleasing
sparkle, (ASTM D 2457).
Transparency and Opacity — A transparent material has a transmittance above 90%.
Transmittance is the percent of incident light that passes through a material sample and is
determined by the effectiveness of the absorption and scattering of light by the material.
In most polymers light absorption is insignificant, therefore, scattering controls the light
trans-mission. The scattering of power of a polymer results from morphological in
homogeneities and/or the presence of crystal and fillers. The less crystalline a polymer is,
the more transparent it is. Amorphous homogeneous polymer, such as “crystal”
polystyrene, showing little or no scattering power, is transparent. A highly crystalline
polymer as HDPE will be mostly opaque.
Transmittance is measured according to ASTM D 1003.
Dimensional Stability — Dimensional stability refers to the capability of a structure to
maintain its dimensions under changing conditions of temperature and humidity.
Machine and transverse directions may produce different changes in dimensional
stability. Dimensional stability is important in any flexible material converting process
particularly in printing, since even small changes in dimensions during printing may lead
to serious problems in holding a print pattern (ASTM D 1204).
Permeability — The barrier properties of a plastic material is commonly expressed by its
permeability coefficient value P. As the permeability increases, the barrier value
decreases. But the permeability coefficient actually depends on the combined effect of
the diffusion and solubility process. The well known relationship P = DS where D is the
diffusion coefficient and S is the Henry’s law solubility applies well to relatively low
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 90
concentration values of permeant, which is the case found in many food systems. Several
factors affect D, S, and P of polymers: (1) chemical composition of polymer and
permeant; (2) polymer crystallinity; the diffusion and sorption occur mainly through the
polymer’s amorphous phase; (3) temperature, as temperature increases permeation
increases; and (4) presence of plasticizers andfillers in the polymer. In food systems, the
values of permeability of water, gases as well as aromas and flavor components. ASTM
1434 describes the standard method for measuring gas permeability of plastic film and
sheeting. The oxygen permeability of films using a coulometric sensor is described in
ASTM D 3985, and for packages in ASTM F 1307. Water vapor permeability method for
flexible barrier materials is describe in ASTM 372, for film/sheeting using infrared
sensor in F 1249, and for packages in ASTM D 895, D 1251, and D 3079.
Water vapor transmission rate (WVTR) for pressure sensitive tapes is in ASMT D
3833. Permeability of organic compounds, flavors, and aroma are described by
Hernandez et al. (1986).
Chemical Resistance — The evaluation of plastics resistance to chemicals is as follows:
acids, ASTM D 543; for alkalis, ASTM D 543; greases and oils, ASTM D 722; solvents,
ASTM D 543; and sunlight, ASTM D 1435.
Wettability — Adhesion and printing operations to a plastic surface depend on the value
of the plastic surface tension. A measure of a material’s surface tension is given by the
wettability(ASTM D2578).
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 91
LECTURE NO. 32
TOPICS: Tests for Glass containers (visual defects, colour, dimensions, impact
strength, etc.), Tests for metal containers (pressure test, product compatibility, etc.)
Burst Strength: The test measures the ability of a paper or paper board to withstand
pneumatic or hydraulic pressure built up. For films, foils, laminates and papers, the
pneumatic test is used. Heavy papers and paper boards are tested on hydraulic type of
testers (lbs/sq. inch or kg/sq. cm).
The test gives a sort of combined tear and tensile properties. In many cases it
serves as good index of the quality of fabrication of packaging materials.
Tear Resistance:
The papers are tested for their tearing resistance properties in two ways:
Internal tearing: The energy required to propagate an internal tear is measured.
Edge tearing: The energy required to initiate a tear is measured.
The test is done on both directions of the paper. The work done in tearing is measured by
the loss in potential energy of the pendulum of the instrument.
Tensile Strength:
The tensile strength of a paper is defined as the force applied parallel to the plane
of the specimen of specified width and length under specified condition of loading. The
test indicates the durability and serviceability of papers in many packaging operations
such as wrapping, bagging, printing etc.
Plastic films are normally tested at higher speeds because of higher extensibility.
The stress strain curve helps in locating the yield point and knowing the yield strength
Grease Resistance:
Grease resistance is measured by exposing one of the test specimen creased to
grease containing red dye. The time required for the red stain to show on the unexposed
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 92
side is taken as a measure of this property. For plastic films, the test can be performed
directly in pouches using groundnut oil coloured with red Sudan dye.
Gas Transmission Rate (GTR):
The gas transmission rate is normally determined by measuring the change in
pressure at constant volume. The quantity of gas flowing across the film is compiled
as volume at NTP (Normal Temperature and pressure). GTR is an important property to
estimate the efficiency of the packaging material or a package resistance to the flow of
gases and helps in selection of barrier materials for oxygen sensitive foods.
Water Vapour Transmission Rate (WVTR):
The WVTR is measured as the quantity of water vapour in grams that will
permeate from one side to other side of the film of an area of one square meter in 24
hours, when the relative humidity difference between the two sides is maintained at
90 per cent gradient at 37.8°C. The property is important to estimate the efficiency of the
packaging material or a package for resistance to the flow of water vapour and is
helpful in considering the selection of barrier materials for hygroscopic foods.
Impact Strength:
These tests are designed to measure the ability of the films to withstand fracture
by shock the test is a measure of toughness of the material. It is a combination of
deformation and breaking properties.
Abrasion Resistance:
This test is designed to measure the ability to withstand surface wear and rubbing.
It is a measure of some mechanical properties like hard resilience. The procedure consists
of abrading the sample with a wheel of standard abrade for a definite number of
revolutions and finding the weight loss of the sample.
Prof. P. K. Ambre (Assistant Professor), Deptt. of Process and Food Engineering/APE, SCAET, Maldad
Page 93