Professional Documents
Culture Documents
Courier 6HX Sampling Data Sheet
Courier 6HX Sampling Data Sheet
Figure 1 shows a number of typical sampling Samples from locations near to the analyzer can
setups which can be applied in processes such as be taken through a Controlled Direct Sample
copper heap-leach, solvent extraction and Connection CDS configured to operate safely at
electrowinning, copper electrorefining and impurity the actual process pressure.
removal, nickel/cobalt acid leach, solvent
PROCESS PROCESS
GRAVITY FLOW
IN PIPE
WATER
WATER
RETURN
RETURN
P
WATER
TANK OR CCS TANK OR
LAUNDER CLOSED CIRCUIT SET LAUNDER
WITH PUMPED CIRCULATION
(FAST LOOP) CDS CCS RETURN
TO ANALYZER CONNECTION DIRECT
GRAVITY FLOW CLOSED CIRCUIT SET
SET FROM SAMPLE WITH PUMPED CIRCULATION
IN PIPE
POINT TO ANALYZER (FAST LOOP)
TO SFS NEAR ANALYZER
WATER
AIR PUMPED CIRCULATION TO
SAMPLE FILTER SET
SDS NEAR ANALYZER
SAMPLE DISPATCH STATION
RETURN PNEUMATIC BATCH
TRANSPORT TO ANALYZER P
SFS
SAMPLE FILTER SET
SFS
SAMPLE FILTER SET
FREE FLOW TO
SAMPLE FILTER SET
AND PNEUMATIC
PUMPED WATER BATCH TRANSPORT PUMPED
FLOW TO ANALYZER FLOW
SAMPLE INLET
WATER
AIR RETURN
SFS
RETURN
FLS SDS
FAST LOOP SET SAMPLE DISPATCH STATION
FREE-FLOWING PNEUMATIC BATCH
OTI 16 OTI 16
CIRCULATION TRANSPORT TO ANALYZER
TITRATORS
(FAST LOOP)
TO ANALYZER WATER HSA
HYDROMETAL-
RETURN
LURGICAL
ELECTRICITY
SAMPLER
PROCESS PRIMARY SECONDARY SAMPLING / HXM 4540 Courier 6 HX PCS 4000 PRIMARY PROCESS
SAMPLING ANALYZER SHELTER SOLUTION ANALYZER PROBE SAMPLING
MULTIPLEXER PROBE CONTROL SET
A process pressure or gravity driven free-flowing operation at up to 1000 kPa (10 bar), 150 psi
Controlled Fast Loops Set FLS brings a process pressure.
continuous or semi-continuous flow of sample
2.2. HSA 2570 Hydrometallurgical Sampler
close to the analyzer, from which it takes a small
sample. HSA 2570 poppet type valve for sampling from
process pipe, diameter 63 mm and greater.
Controlled Circulation Pump Set CCS circulates • spring loaded, normally closed valve. The
the sample from the process sample point close effect of the process pressure is also to close
by the analyzer and back to the process. An SFS the valve, thus ensuring safe operation.
Filter Set may be integrated in the loop. • operated by a pneumatic actuator, which is
connected through a remote VBS solenoid
The discharge from a low pressure sample point box to the Courier 6 HX.
(a gravity pipeline or low pressure pump outlet) or • all AISI 316 construction, with TEFLON (R)
from an SFS filter set can be transported by a actuator rod seals.
pneumatic Sample Dispatch Station SDS. This • two sample ports: One connects the sampler
transfers a small quantity of clear solution, and to the Courier 6 HX sampling system, the
minimizes the amount of process solution that other is available for flushing the sample line
leaves the immediate process area. through the valve body.
Sample preparation The HSA 2570 is inserted through a flange into
The Sample Filtering Set SFS which is dedicated the pipeline
to one sample produces a small quantity of filtered
sample, returning the bulk of the sample intake to
the process.
Sample multiplexing
All samples are taken into the Courier 6 HX
analyzer through a Hydrometallurgical
Multiplexer HXM, located in the analyzer room or
shelter. This is described more closely in the
Courier 6 HX Analyzer System Datasheet.
The CDS Controlled Direct Sample Connection is • the sample will flow by gravity or by process
a compact unit which can be installed in an pressure to the analyzer location, and
industrial environment close to the sample point. • the distance from the sample point to the
analyzer is very long and flushing the pipe up
It includes - to the analyzer location would use a large
• necessary valves for volume of process solution or take an
− sample intake and supply of washing unacceptably long time.
water and transport of the sample along a
pipe to the analyzer location The FLS Controlled Fast Loop Set is a compact
• a pressure sensor and manual pressure unit which can be installed in an industrial
regulators to ensure a suitable environment close to the sample point.
− Instrument air (dry, oil-free compressed standard routines for taking and transporting
air) pressure 600 - 1000 kPa (90 - 150 samples, and for washing the flow system after
psig) if required sample transport, can be chosen in the
• Water supply configuration of the analyzer.
− Potable, sand-filtered water, pressure 5.1. CCS 4590 for clear samples only
300 - 600 kPa, 45 - 90 psig Pump type
Materials • Diaphragm pump, electrically driven
Wetted parts • Capacity, max. 5.8 l/min, 1.67 US gpm,
• Module blocks, valve bellows and pistons, manually variable
piping, fittings: PVDF Pipe Connections - Sample Circulation
• Valve seals, O-rings: Viton • Maximum inlet pressure : 500 kPa 75
Structural parts psi
• Frame: Acid resistant steel AISI 316 • Maximum back pressure: 1000 kPa 150
psi
5. CCS Controlled Circulation • Maximum temperature: 97 degrees C
• Pipe size
Pump Set − OD: 8 mm, (5/16 or 0.394 inch)
The CCS Controlled Circulation Pump Set is used − ID: 6 mm, (15/64 or 0.236 inch)
to deliver small quantities of clear sample from a
sample point to a filtering device close to the 5.2. CCS 4591 for samples with solids, to feed
analyzer or to the HXM multiplexer for the SFS Sample Filter Set
Pump type
COURIER 6 HX system.
• Peristaltic (hose) pump, electrically driven
It is applied in the following circumstances - • Capacity 10 l/min, 2.88 US gpm, fixed
• the sampling point is below the level of the capacity
analyzer location, or the sample will not flow • Solids content: maximum 100 g/l (10%)
by gravity or by process pressure to the • Hose size 32 mm 1 1/4”
analyzer location, or Pipe Connections - Sample Circulation
• the distance from the sample point to the • Maximum inlet pressure : 500 kPa 75
analyzer is very long and flushing the pipe up psi
to the analyzer location would use a large • Maximum back pressure: 1000 kPa 150
volume of process solution or take an psi
unacceptably long time, or • Maximum temperature: 97 degrees C
• the sample contains solids and must be • Intake - Hose or AISI 316 pipe, nominal
filtered before analysis diameter
− 16 mm, 5/8”, or
The CCS Controlled Circulation Pump Set is a − 19 mm, 3/4”, or
compact unit which can be installed in an − 25 mm, 1”
industrial environment close to the sample point. • Outlet - Hose, Nominal diameter
− 16 mm, 5/8”, or
It includes -
− 19 mm, 3/4”
• a small peristaltic pump or diaphragm pump,
designed maintain a suitable circulation of 5.3. CCS 4592 Heavy Duty Set for samples with
sample solution solids, to feed SFS Sample Filter Set
• necessary valves for Pump type
− sample intake and supply of washing • Peristaltic (hose) pump, electrically driven
water and transport of the sample along a • Capacity 20 l/min, 5.76 US gpm, fixed
pipe to the analyzer location capacity
• a pressure sensor and manual pressure • Solids content: maximum 250 g/l (25%)
regulators to ensure a suitable • Hose size 40 mm 1 9/16”
Pipe Connections - Sample Circulation
The CCS Controlled Circulation Pump Set is • Maximum inlet pressure : 500 kPa 75
controlled by the COURIER 6 HX analyzer and psi
6(13)
• Maximum back pressure: 1000 kPa 150 to the analyzer location would use a large
psi volume of process solution or take an
• Maximum temperature: 97 degrees C unacceptably long time.
• Intake - AISI 316 pipe nominal diameter 50
mm, 2” The Sample Dispatch Station SDS is a compact
• Outlet - Hose, Nominal diameter unit which can be installed in an industrial
− 25 mm, 1”, or environment close to the sample point.
− 32 mm, 1 1/4”
It includes -
Common Data • a collection vessel, designed to be easy to
Outlet to HXM wash clean after sample dispatch
• Maximum back pressure: 1000 kPa 150 • necessary valves for
psi − sample intake form the process or filtering
• Pipe size device
− OD: 8 mm, (5/16 or 0.394 inch) − sample reject to drain
− ID: 6 mm, (15/64 or 0.236 inch) − supply of washing water and or air or inert
gas for propelling the sample
• Air supply − transport of the sample along a pipe to
− Instrument air (dry, oil-free compressed the analyzer location
air), pressure 600 - 1000 kPa (90 - 150 • a sensor to detect the presence of solution
psig) if required • the necessary pressure regulators and filters
• Water supply for air and water supply
− Potable, sand-filtered water, pressure 300 • a sturdy frame and drip shield
- 600 kPa, 45 - 90 psig
Materials
Wetted parts
• Pumping head: AISI 316, PVDF, PP, PVC,
depending on sample
• Module blocks, valve bellows and pistons,
piping, fittings: PVDF
• Hoses of peristaltic pumps, NBR, for high
temperatures EPDM, other hoses available
on case by case basis
• Valve seals, O-rings: EPDM, VITON
Structural parts
• Frame: Acid resistant steel AISI 316
− 19.8” (w) x 18.4” (d) x 19.7” (h) Washing the flow system is performed
− Weight: 24.9 kg, 54.8 lbs automatically at suitable intervals.
Intake It includes -
• Minimum pressure: 25 kPa 4 psi • a bypass filter with an exchangeable filter
• Maximum pressure : 500 kPa 75 psi cartridge using commercially available filter
• Maximum temperature: 97 degrees C cloth
• Solids content: solids free • manual valves for
• Pipe size − shut off of the sample inlet from the
− OD: 8 mm, (5/16 or 0.394 inch) process or circulating flow
− ID: 6 mm, (15/64 or 0.236 inch) − shut of the sample exit to the process or
circulating flow
Outlet
− regulation of inlet pressure
• Maximum back pressure: 200 kPa 30 − adjustment of short circuit to reduce flow
psi through the filter, if the available flow
• Pipe size exceeds the filter capacity
− OD: 8 mm, (5/16 or 0.394 inch) • a pressure sensor
− ID: 6 mm, (15/64 or 0.236 inch) • a sturdy frame and drip shield
Air supply 7.1. Sample Filter Set SFS 4520
• Dry, oil-free instrument air • Overall:
(Inert gas e.g. nitrogen may also be used if − 459 mm (w) x 200 mm (d) x 1151 mm (h)
required) − 18.1” (w) x 7.9” (d) x 45.3” (h)
• Pressure − weight 18.5 kg 40.8 lbs
− max. 600 kPa, 90 psi
− min. 300 kPa, 45 psi
Water supply
• Potable, sand-filtered water,
− max. pressure 600 kPa, 90 psi
− min. pressure 300 kPa, 45 psi
Materials
Wetted parts
• Module blocks, valve bellows and pistons,
piping, fittings: PVDF
• Valve seals, O-rings: Viton
Structural parts
• Frame and drip shield: Acid resistant steel
AISI 316
• Support for vessel: HDPE Figure 5. SFS 4520 Sample Filter Set Dimensions
PRESSURE
FLOW IN PIPE
HSA
SAMPLER
WATER
MAX. 15 m
CDS WATER
DIRECT
CONNECTION
TO ANALYZER
MAX. 15 m
CDS
DIRECT
CONNECTION
TO ANALYZER
SAMPLE INLET
SAMPLE INLET
8.2. Free-flowing Controlled Fast Loop to the If the pump pressure is sufficient to maintain a
Analyzer flow of about 6 l/min, 1.5 US gpm a 13 mm, 1/2’
This connection shown in Figure 8 is suitable if pipe the pressure at the analyzer location will be
the pressure or static head at the sample points is usually be within the limits for the HXM inlet.
sufficient to transport the sample to the analyzer,
so that the pressure at the analyzer location is It may be convenient to return the solution to a
within the limits for the HXM inlet. The bulk of the common point close to the analyzer, in which case
fast loop flow is returned to the process, e.g. to the connection is as shown in Figure 9. below
the pump feed tank or the another suitable return
point. The same connection can be used with an HSA
Sampler if the sample point is close to the
analyzer but the pressure is too high for the HXM
inlet, see Figure 10.
15 - 200 m
PUMPED WATER
FLOW
SAMPLE INLET
FLS
FAST LOOP SET
FREE-FLOWING
CIRCULATION
(FAST LOOP)
TO ANALYZER
RETURN
Figure 8. Controlled Fast Loop Set sampling form a remote pump pressure line
15 - 200 m
PUMPED WATER
FLOW
SAMPLE INLET
FLS
FAST LOOP SET
FREE-FLOWING
CIRCULATION
(FAST LOOP)
TO ANALYZER
RETURN
Figure 9. Fast loop from remote pump pressure line terminating at analyzer location
11(13)
PROCESS
WATER
RETURN
P
TANK OR
CCS
LAUNDER
PUMPED CIRCULATION
(FAST LOOP)
TO ANALYZER
SAMPLE INLET
WATER
RETURN
TANK OR
LAUNDER
SAMPLE INLET
CCS
CLOSED CIRCUIT SET
WITH PUMPED CIRCULATION
(FAST LOOP)
TO SFS NEAR ANALYZER
PUMPED CIRCULATION TO
SAMPLE FILTER SET
NEAR ANALYZER
SFS RETURN
SAMPLE FILTER SET
Figure 12. Filtering a sample from a point where pressure is low, using a Controlled
Pumped Circulation Set and Sample Filter Set
SFS
SAMPLE FILTER SET
FREE FLOW TO
SAMPLE FILTER SET
AND PNEUMATIC
BATCH TRANSPORT PUMPED
TO ANALYZER FLOW
SAMPLE INLET
WATER
AIR RETURN
SFS
RETURN
SDS
SAMPLE DISPATCH STATION
PNEUMATIC BATCH
TRANSPORT TO ANALYZER
HSA
HYDROMETAL-
LURGICAL
SAMPLER
Figure 13. Filtering a sample from a point under pressure in an SFS Sample Filter Set, and
transporting the clear filtrate using an SDS Sample Dispatch Station
13(13)