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Tempcal
Tempcal
Dr.K.Sulochana
Temperature
• Temperature is an intensive parameter : the temperature of 2 different bodies which
are put together is not the sum of the two temperatures of the different bodies.
Temperature is also not directly measurable.
• The primary thermometer is a sensor that links temperature to others physical
parameters with a law like the ideal gases law (PV=nRT), it is a thermodynamical
temperature of which unit is Kelvin (K).
• But such primary thermometers are quite difficult to use and expensive.
• Even, they cannot cover all the different experimental cases. But we need sensitive,
reproductible, consistent and easy to use, sensors.
• To link physical laws with reality, an international scale of temperature has been
defined.
• A scale of temperature is made up of:
• a thermometer, a sensor with an output depending on temperature;
• an interpolation function that links the sensor’s output with temperature;
• fixed points of temperature to define the interpolation function.
• The International Temperature Scale, first defined in 1927, has been reviewed to
reduce the difference between absolute temperature and temperature in the scale. The
last scale was defined in 1990 hence ITS 90. The triple point of water is the major
point of definition (t=0.01 °C).
• Temperature is the most commonly measured parameter in commercial and
industrial settings.
• Industries as diverse as food processing, pharmaceuticals, cold storage,
paper manufacturing, and others absolutely rely on process temperatures
being within a certain range.
• Measuring temperature involves a wide range of specialty sensors such as
– thermocouples
– thermistors
– resistive temperature detectors (RTDs)
– infrared (IR) sensors
– bimetal thermometers, etc.
• These sensors produces an electrical output such as resistance, millivolts or
milliamps which correspond to the temperature.
• These output signals are sent to a readout or controller where they are
displayed or used to control a process function.
SI Unit of Temperature
• The Kelvin (K) is the fraction 1/273.16 of the thermodynamic
temperature of the triple point of water.
• The temperature 0 K is commonly referred to as "absolute zero."
• On the widely used Celsius temperature scale, water freezes at 0°C and
boils at about 100°C.
• One Celsius degree is an interval of 1 K, and zero degrees Celsius is
273.15 K.
• An interval of one Celsius degree corresponds to an interval of 1.8
Fahrenheit degrees on the Fahrenheit temperature scale.
• The standard temperature at the triple point of water is provided by a
special cell, an evacuated glass cylinder containing pure water.
• When the cell is cooled enough so that a mantle of ice forms around
the reentrant well, the temperature at the interface of solid, liquid, and
vapor is 273.16 K.
• Thermometers to be calibrated are placed in the reentrant well.
Temperature Units
• The three units used to specify the temperature in general are
• Kelvin
• Celcius
• Fahrenheit
Disadvantages:
1. Low sensitivity.
2. Higher cost than many other temperature transducers.
3. Requires no point sensing.
4. Can be affected by contact resistance, shock, and acceleration.
5. Requires three or four wire operations.
Thermistors
• A thermistor is a type of resistor used to measure temperature changes, relying on
the change in its resistance with changing temperature.
• Thermistor is composed of sintered semiconductor material, which exhibits a
large change in resistance proportional to a small change in temperature.
• If the relationship between resistance and temperature is assumed to be linear,
then the change in resistance is given by:
ΔR = k.ΔT
where
ΔR = change in resistance
ΔT = change in temperature
k = first-order temperature coefficient of resistance
Stability:
• Finished thermistors are chemically stable and not
significantly affected by aging.
Advantages of Thermistors
• A main advantage of thermistors for temperature measurement is their
extremely high sensitivity. For example, a 2252 thermistor has a sensitivity
of -100 /°C at room temperature.
• Higher resistance thermistors can exhibit temperature coefficients of -10
k/°C or more, in comparison, a 100 platinum RTD has a sensitivity of
only 0.4 /°C.
• The physically small size of the thermistor bead also yields a very fast
response to temperature changes.
• Another advantage of the thermistor is its relatively high resistance.
Thermistors are available with base resistances (at 25°C) ranging from
hundreds to millions of ohms.
– This high resistance diminishes the effect of inherent resistances in the lead wires,
which can cause significant errors with low resistance devices such as RTDs.
– For example, while RTD measurements typically require 3-wire or 4-wire
connections to reduce errors caused by leadwire resistances, 2-wire connections to
thermistors are usually enough.
Disadvantages of Thermistors
• The major tradeoff for the high resistance and sensitivity of the
thermistor is its highly nonlinear output and relatively limited
operating range. Depending on the type of thermistors, upper ranges
are typically limited to around 300°C.
• The curve shows the resistance-temperature curve for a 2252
thermistor. The curve of a 100 RTD is also shown for comparison.
• The thermistor has been used primarily for high-
resolution measurements over limited temperature
ranges. The classic example of this type of
application is medical thermometry.
350°C
• Unfortunately it is not possible to simply connect a voltmeter to the
thermocouple to measure this voltage, because the connection of the
voltmeter leads will make a second, undesired thermocouple junction.
• To make accurate measurements, this must be compensated for by using a
technique known as Cold Junction Compensation (CJC).
• The law of intermediate metals states that a third metal, inserted between the
two dissimilar metals of a thermocouple junction will have no effect
provided that the two junctions are at the same temperature.
• This law is also important in the construction of thermocouple junctions.
• It is acceptable to make a thermocouple junction by soldering the two metals
together as the solder will not affect the reading.
• In practice, however, thermocouples junctions are made by welding the two
metals together (usually by capacitive discharge) as this ensures that the
performance is not limited by the melting point of solder.
• All standard thermocouple tables allow for this second thermocouple junction
by assuming that it is kept at exactly zero degrees centigrade.
• Traditionally this was done with a carefully constructed ice bath (hence the
term 'cold' junction compensation).
• Maintaining a ice bath is not practical for most measurement applications, so
instead the actual temperature at the point of connection of the thermocouple
wires to the measuring instrument is recorded.
• Typically cold junction temperature is sensed by a precision thermistor in
good thermal contact with the input connectors of the measuring instrument.
• This second temperature reading, along with the reading from the
thermocouple itself is used by the measuring instrument to calculate the true
temperature at the thermocouple tip.
• For less critical applications, the CJC is performed by a semiconductor
temperature sensor. By combining the signal from this semiconductor with the
signal from the thermocouple, the correct reading can be obtained without the
need or expense to record two temperatures.
• Understanding of cold junction compensation is important; any error in the
measurement of cold junction temperature will lead to the same error in the
measured temperature from the thermocouple tip.
Thermocouple – Merits and demerits
Merits:
• They have rugged construction
• Thermocouple are inexpensive
• Thermocouples are simpler to use than resistance thermometers
• There is no need of a bridge circuit and an excitation source
Demerits:
• Thermocouples have limited use in temperature spans of less than about
33°C because of the relatively small change in junction voltages with
temperature.
• Thermocouples require an amplifier for many applications.
• Thermocouples need expensive accessories for control applications.
Thermocouples - Material
S.No Type Material Colour (+/-)
1 Type T Copper / Constantan Blue/Red
2 Type J Iron / Constantan White/Red
3 Type E Chromel / Constantan Purple/Red
4 Type K Chromel / Alumel Yellow/Red
5 Type S Platinum 10% Rhodium/ Black/Red
Pure Platinum
6 Type R Platinum 13% Black/Red
Rhodium/Pure Platinum
7 Type B Platinum 30% Rhodium/ Gray/Red
Platinum 6% Rhodium
8 Type N Nicrosil / Nisil Orange/Red
Thermocouples - characteristics
Thermocouples - Tolerence
Thermocouples –Scale Factor
K Type Thermocouple Chart
Temperature Conversion Equation
T = a0 + a1V + a2V2 + …. + anVn
Precautions
Connection problems:
• Many measurement errors are caused by unintentional
thermocouple junctions.
• Remember that any junction of two different metals will
cause a junction.
• If you need to increase the length of the leads from your
thermocouple, you must use the correct type of thermocouple
extension wire (eg type K for type K thermocouples).
• Using any other type of wire will introduce a thermocouple
junction.
• Any connectors used must be made of the correct
thermocouple material and correct polarity must be observed.
Lead Resistance:
• To minimise thermal shunting and improve response times,
thermocouples are made of thin wire (in the case of platinum types
cost is also a consideration).
• This can cause the thermocouple to have a high resistance which can
make it sensitive to noise and can also cause errors due to the input
impedance of the measuring instrument.
• A typical exposed junction thermocouple with 32 AWG wire (0.25
mm diameter) will have a resistance of about 15 Ohms / meter.
• The Pico TC-08 has an input impedance of 2 MΩ so will have an
error of less than 0.01% for 12 meters of such cable.
• If thermocouples with thin leads or long cables are needed, it is worth
keeping the thermocouple leads short and then using thermocouple
extension wire (which is much thicker, so has a lower resistance) to
run between the thermocouple and measuring instrument.
• It is always a good precaution to measure the resistance of your
thermocouple before use.
Common Mode Voltage:
• Although thermocouple signal are very small, much larger voltages often
exist at the input to the measuring instrument.
• These voltages can be caused either by inductive pick up (a problem when
testing the temperature of motor windings and transformers) or by 'earthed'
junctions.
• A typical example of an 'earthed' junction would be measuring the
temperature of a hot water pipe with a non insulated thermocouple.
• If there are any poor earth connections a few volts may exist between the
pipe and the earth of the measuring instrument.
• These signals are again common mode (the same in both thermocouple
wires) so will not cause a problem with most instruments provided they are
not too large.
• For example, the TC-08 has a common mode input range of -4 V to +4 V.
• If the common mode voltage is greater than this then measurement errors
will result.
• Common mode voltages can be minimised using the same cabling
precautions outlined for noise, and also by using insulated thermocouples.
Thermal Shunting:
• All thermocouples have some mass. Heating this mass takes energy so will
affect the temperature you are trying to measure.
• Consider for example measuring the temperature of liquid in a test tube:
there are two potential problems.
• The first is that heat energy will travel up the thermocouple wire and
dissipate to the atmosphere so reducing the temperature of the liquid around
the wires.
• A similar problem can occur if the thermocouple is not sufficiently immersed
in the liquid, due to the cooler ambient air temperature on the wires, thermal
conduction may cause the thermocouple junction to be a different
temperature to the liquid itself.
• In the above example a thermocouple with thinner wires may help, as it will
cause a steeper gradient of temperature along the thermocouple wire at the
junction between the liquid and ambient air.
• If thermocouples with thin wires are used, consideration must be paid to lead
resistance.
• The use of a thermocouple with thin wires connected to much thicker
thermocouple extension wire often offers the best compromise.
Temperature Calibration
• When discussing temperature calibration it is important to note that
output of the temperature sensors cannot be adjusted.
• Instead, the controller or readout is adjusted to account for the
inaccuracy of the sensor.
• Calibration is a comparison between two devices. The first device is
the unit to be calibrated, often called the device under calibration
(DUC). The second device is the standard, which has a known
accuracy.
• Using the standard as a guide, the DUC is adjusted until both units
display the same results while exposed to the same temperature.
• Typically, calibration of an instrument is checked at several points
throughout the calibration range of the instrument.
• Not all standards are created equally. While all standards have a known
accuracy, there are some—known as primary standards— that are the
highest level of accuracy for a specific parameter.
• Primary standards achieve their high accuracy by relying upon
measurement technologies using fundamental physical constants that
do not drift such as the triple point of water.
• These fixed values minimize uncertainty, making primary standards
the most accurate calibration tools.
International Temperature Scale 90
Typically the standard is four times more accurate than the thermometer under test.
Any sensor can be calibrated by comparison, and comparison calibrations can take
place either in a laboratory or on-site.
Temperature Calibrator Specifications
Temperature range: The temperature limits of the dry-well must meet your minimum test requirements
for the sensors being calibrated.
Accuracy: It specifies close the unit’s well temperature is to the programmed set point.
Stability: Stability is the temperature fluctuation of the instrument around the desired set-point over
time. It is also defined as the tendency of an attribute to remain within tolerance. When a calibrator
reaches its set-point, there is some fluctuation in temperature as the unit tries to maintain that
temperature. Stability adds to accuracy in determining overall system uncertainty.
Uniformity: It is the temperature homogeneity of the heat source throughout the test zone. All
calibrators have slight temperature differences from the bottom of the of the test well to the top (axial)
as well as from the middle of the test well outward (radial). A few simple strategies allow users to place
probes in such a way as to minimize uniformity errors.
Well Flexibility: When purchasing a dry-well, make certain that the probes you need to test will fit in the
unit’s heated block. Most dry-wells use removable sleeves to size the main temperature well. This gives
you the flexibility to calibrate a wider variety of probes with one instrument.
Sensor Immersion: Sensor immersion is a recurring topic when considering a dry-well for calibration of
temperature probes. Immersion can be the single largest contributor to error in dry-well calibrations.
Throughput: If you’re like the rest of the world, trying to calibrate as many sensors as possible in a limited
time period, get a block calibrator that allows you to insert more than one probe at a time.
Reference Sensor (SPRT) Specification
Accuracy of the Sensor: It usually refers to the temperature deviation or tolerance grade at some reference
temperature of the sensor, as its “real” tolerance is temperature dependent.
Repeatability: The degree to which two successive readings of a temperature sensor agree refer to its
“repeatability”. That is, a sensors ability to repeat the same behavior under the same conditions for any
given temperature, even though it has been used and exposed to different temperatures, refers to its
repeatability (e.g. its ability to remain stable over many heating and cooling cycles). Repeatability is often
lumped together with the measure of stability and ordinary industrial platinum RTD sensors will specify
repeatability less than ±0.1°C per year of normal use and measured at 0°C. High precision RTD sensors can
be obtained with repeatability as low as 0.0025°C per year.
Stability/Drift: The stability of an RTD sensor refers to its ability to maintain the same resistance versus
temperature relationship for the same conditions over time. Stability and drift are often used
interchangeably and sometimes lumped together with repeatability measurements. Similar to repeatability,
a typical stability specification will limit drift to less than 0.1°C per year for rated operation.
Self Heating: Heat energy is generated while applying current to excite the RTD element in order to measure
its signal. The self-heating that occurs will drive error in temperature measurement. The self-heating of an
RTD sensor is most often expressed in mW/°C, which refers to the power required to raise the internal
element temperature by 1°C.
Response Time/Time Constant: The time constant of an RTD refers to the speed with which its element
changes resistance in response to a change in contact temperature. A rapid time constant helps to reduce
error in a measurement system that encounters rapid changes in temperature.
Example – RTD Calibration
Mathematical model:
T T
C r
T bath T ref T readout