Professional Documents
Culture Documents
NERMAS FIX (1) - 20221222 - 214531-WPS Office
NERMAS FIX (1) - 20221222 - 214531-WPS Office
KONVERSI SATUAN
1 tahun = 330 hari
1 hari = 24 jam
1 jam = 60 menit
1 ton = 1000 kg
1 Kg = 2.20462 lb
1 lb = 0.45359291 kg
1 Liter = 0.26417 gallon
1 gallon = 3.78544 liter
1 cm = 0.3937 in
1 in = 2.54000508 cm
1 m = 3.28084 ft
1 ft = 0.30479999 m
1 in = 0.0833333 ft
1 ft = 12.0000048 in
1 atm = 101325 Pa
1 Pa = 9.8692E-06 Atm
1 mmHg = 133.3224 Pa
1 Pa = 0.00750062 mmHg
1 Kgf/cm2 = 98066.5 Pa
1 Pa = 1.0197E-05 Kgf/cm2
1 Lbf/in2 = 6.89476 Kpa
1 Kpa = 0.14504 Lbf/in2
1 oC = 33.8 oF
1 oF = -17.222222 oC
1 J = 0.2389 cal
1 cal = 4.1858 J
APPENDIX A REAKTOR
Kapasitas = 55,000 ton/tahun
= 6944.4444 kg/jam
= 51.0058 kmol/jam
Komponen R.Kimia BM
Formaldehida CH2O 30.03
Asetaldehida C2H4O 44.05
Natrium Hidroksida NaOH 40
Natrium Format HCOONa 68.01
Pentaeritritol C5H12O4 136.15
Asam Format CH2O2 46.03
Air H2O 18.0160
Metanol CH3OH 32.04
1. Reaktor
C5H12O4
CH2O HCOONa
CH2O
C2H4O REAKTOR C2H4O
NaOH
NaOH H2O
Reaksi :
4 HCHO + CH3CHO + NaOH C(CH2OH)4 + HCOONa
KONVERSI 90%
WAKTU TINGGAL 30 MENIT keyes
Komponen Koef kmol/jam
Pentaeritritol 1 C5H12O4 51.0058
Produk
Natrium Format 1 HCOONa 51.0058
Komposisi Berat
Bahan masuk
(%) kg/jam
CH2O 37% 2518.8042
Formaldehida CH3OH 3% 204.2274
H2O 60% 4084.5473
Asetaldehida C2H4O 99% 2471.4877
H2O 1% 24.9645
Natrium NaOH 50% 1133.4630
hidroksida H2O 50% 1133.4630
Netralizer
kg/jam
6,944.4444
3,468.9068
6,126.8209
2,246.8070
2,040.2334
6,807.5788
2,496.4523
2,266.9260
APPENDIX A REAKTOR
2473.0102
kmol/jam
226.6926
56.6732
56.6732
75.4886
5.7367
204.0460
50.4958
1.2471
25.5029
56.6228
8.3876
0.6374
12.7483
5.6106
0.0779
2.8337
6.2914
Fraksi (X)
2.18%
APPENDIX A REAKTOR
0.18%
2.14%
0.98%
4.53%
60.02%
29.98%
1.000
NETRALIZER
Dari Reaktor :
Komponen keluar (kg/jam)
Produk Ke Netralizer
Formaldehid = 251.8804
Metanol = 20.4227
Asetaldehida = 247.1488
Natrium Hid = 113.3463
Air = 524.2975
Pentaeritrito = 6944.4444
Natrium For = 3468.9068
Total = 11571.0000
2. Netralizer
CH2O2
CH2O
Keluaran dari Reaktor NETRALIZER HCOONa
C2H4O vaporizer
C5H12O4
H2O
3. Vaporizer CH2O
CH2O (V2) Uap C2H4O
(V1) Uap C2H4O H2O
H2O
Dari C5H12O4
Netralizer VAPORIZER I VAPORIZER II HCOONa Kristalizer
H2O
A. Vaporizer I
Neraca Massa Total
VAPORIZER
F = V1 + L1
11713.912 = 2275.0175 + L1
L1 = 9438.8947
Aliran Vaporizer I
VAPOR LIQUID
Komponen F1 XF1 V1 L1
CH2O 251.8804 0.2274 57.2678 194.6127
CH4O 20.4227 0.0184 0.3765 20.0462
C2H4O 247.1488 0.2231 55.1364 192.0124
H2O 588.3920 0.5311 312.5035 275.8885
HCOONa 3661.6239
C5H12O4 6944.4444
TOTAL 1107.8439 1.0000 425.2842 11288.628
Neraca Massa Vaporizer I
Aliran
Komponen Masuk (Kg/jam) Komponen Keluar (Kg/jam)
Produk
Dari Netralizer
Vapor Liquid
Formaldehida 251.8804 Formaldehida 57.2678 Formaldehida 194.6127
Metanol 20.4227 Metanol 0.3765 Metanol 20.0462
Asetaldehida 247.1488 Asetaldehida 55.1364 Asetaldehida 192.0124
Air 588.3920 Air 312.5035 Natrium Format 3661.6239
Pentaeritritol 6944.4444 Pentaeritritol 6944.4444
Natrium Format 3661.6239 air 275.8885
TOTAL 425.2842 TOTAL 11288.628
TOTAL 11713.9122 TOTAL 11713.9122
B. Vaporizer II
Neraca Massa Total
L1 = V2 + L2
9438.895 = 758.3391707 + L2
L2 = 8680.5556
Neraca Massa Komponen
F = V2 + L2
F.XF = V2.XV2 + L2.XL2
6944.44444 = 0 + 8680.5556 x XL2
XL2 = 0.8000
VAPORIZER
Aliran Vaporizer II
VAPOR LIQUID
Komponen F2 XF2 V2 L2
CH2O 194.6127 0.2851 194.6127 0.0000
CH4O 20.0462 0.0294 20.0462 0.0000
C2H4O 192.0124 0.2813 192.0124 0.0000
H2O 275.8885 0.4042 55.1777 220.7108
HCOONa 3661.6239
C5H12O4 6944.4444
TOTAL 682.5597 1.0000 461.8490 10826.779
4. Kristalizer
HCOONa
Dari Vaporizer KRISTALIZER C5H1204(aq) Centrifuge
C5H1204(s)
Perhitungan :
Penguapan H2O : Asumsi
Tidak terjadi penguapan H2O = 0%
H2O yang menguap = 0 kg
Perhitungan R :
BM
C(CH2OH)4 = 136.15
C(CH2OH)4.7H2O = 126.00
R = 0.93
Evaporation ( E )
E = 0
P = R x 100.Wo - S x (Ho-E)
100 - S x (R-1)
P = 0.93 x 694444.44 - 0.056 x 220.71
100 - 0.056 x -0.07
P = 642661.16
100.00417
P = 6426.3433
Fresh Feed
Komponen kg/jam
Natrium Format 183.0812
Pentaritritol (s) 6452.2484
Air 11.0355
Total 6646.3651
5.Centrifuge
H2O
Dari Kristalizer CENTRIFUGE C5H12O4 (aq) Rotary Dryer
C5H12O4 (s)
Mother Liquor
HCOONa
H2O
C5H12O4
KOMPONEN LIQUID KELUAR
Liquid terikut dalam soli = 5% (Perry 6th ed:19-87)
Liquid Keluar = 95%
Komponen kg/jam 5% Liq terikut solid kg/jam Liquid Keluar Fraksi (X)
HCOONa 3661.6239 183.0812 3478.5427 0.83
C5H12O4(aq) 518.1011 25.9051 492.1961 0.12
H2O 220.7108 11.0355 209.6752 0.05
Total 4400.4358 220.0218 4180.4140 1.00
Air 11.0355
6. Rotary Dryer
Udara Panas
Dari Centrifuge ROTARY DRYER
C5H12O4
H2O
7. Cyclone
Udara Bersih Keluar
Ke Belt Conveyor
C5H12O4(S)
8. Cooling Conveyor
Dari Cyclone
8. Belt Conveyor
Dari Cyclone
Total 6635.9864
9. Ballmill
P = F + R
= 6635.9864 + 331.799321
= 6967.7857
Total 7128.2131
P = F + R
= 7128.2131 + 356.410653
= 7484.6237
10. Screen
F = R + P
6967.7857 = 331.799321 + P
P = 6635.9864
Total 7484.6237
F = R + P
7484.6237 = 356.41065 + P
P = 7128.2131
Fraksi (X)
0.03
0.97
0.00